ChemiSoft TPx V1.

02

Unit 1 (2720)

Serial # 112

Sample: TPR-Rohit-CuFe2O3 18-06-12

Operator: Tarun
Submitter:
File: D:\ALL\TPX\DATA\SANCHIT\000-275.SMP
Started: 6/18/2012 6:27:04PM
Completed:

Sample Mass: 0.6690 g

Report Time: 6/18/2012 7:52:07PM

Summary Report
Experiment 1: TPR Ce Zr Support Tarun
Analysis Type: Temperature Programmed Reduction
Calibration: (CHM_0005) sushil new caliberation file
Measured Flow Rate: 30.00 mL STP/min
Signal Offset: -0.58381
Signal Inverted: No
Temperature
Volume
at Maximum (mL/g STP)
(C)

Peak
Number
1
2
3
4

360.7
519.1
626.7
640.0

0.55870
1.34454
0.00601
0.00277

Peak Height

0.03254
0.05457
0.00221
0.00152

Page 1

ChemiSoft TPx V1.02

Unit 1 (2720)

Serial # 112

Sample: TPR-Rohit-CuFe2O3 18-06-12

Operator: Tarun
Submitter:
File: D:\ALL\TPX\DATA\SANCHIT\000-275.SMP
Started: 6/18/2012 6:27:04PM
Completed:

Sample Mass: 0.6690 g

Report Time: 6/18/2012 7:52:07PM

Tabular Report
Experiment 1: TPR Ce Zr Support Tarun
Sampling Interval: 1.0 s
Analysis Type: Temperature Programmed Reduction
Time
(minutes)
0.00
0.02
0.03
0.05
0.07
0.08
0.10
0.12
0.13
0.15
0.17
0.18
0.20
0.22
0.23
0.25
0.27
0.28
0.30
0.32
0.33
0.35
0.37
0.38
0.40
0.42
0.43
0.45
0.47
0.48
0.50
0.52
0.53
0.55
0.57
0.58
0.60
0.62
0.63
0.65
0.67
0.68
0.70
0.72
0.73
0.75
0.77
0.78

Temperature
(C)
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.7
31.8
31.7
31.7
31.7
31.8
31.8
31.8
31.8
31.8
31.8
31.9
31.9
31.9
31.8
31.9
31.9
32.0
32.0
32.0
32.1
32.1
32.2
32.2
32.2
32.2
32.3

TCD Signal
0.00000
-0.00003
-0.00001
-0.00002
-0.00003
-0.00002
-0.00001
0.00000
-0.00003
-0.00002
-0.00001
-0.00001
-0.00001
0.00001
-0.00001
0.00001
-0.00001
-0.00002
-0.00001
0.00001
0.00002
0.00000
-0.00002
-0.00002
-0.00001
0.00001
0.00001
-0.00001
0.00000
0.00002
-0.00001
-0.00001
-0.00001
-0.00004
-0.00004
-0.00002
-0.00002
-0.00003
-0.00001
-0.00002
-0.00002
-0.00002
-0.00002
-0.00002
-0.00001
-0.00004
-0.00002
-0.00002

Furnace
Temp. (C)
33.07
32.95
32.82
32.44
32.39
32.50
32.42
32.45
32.38
32.59
32.65
32.56
32.58
32.61
32.57
32.50
32.58
32.52
32.55
32.62
32.62
32.61
32.66
32.71
32.66
32.71
32.77
32.89
32.87
32.88
32.96
33.01
33.08
33.08
33.13
33.17
33.25
33.39
33.50
33.60
33.71
33.81
33.90
33.94
34.06
34.16
34.31
34.40

Auxiliary 2

Page 2

ChemiSoft TPx V1.02

Unit 1 (2720)

Serial # 112

Sample: TPR-Rohit-CuFe2O3 18-06-12

Operator: Tarun
Submitter:
File: D:\ALL\TPX\DATA\SANCHIT\000-275.SMP
Started: 6/18/2012 6:27:04PM
Completed:

Time
(minutes)
0.80
0.82
0.83
0.85
0.87
0.88
0.90
0.92
0.93
0.95
0.97
0.98
1.00
1.02
1.03
1.05
1.07
1.08
1.10
1.12
1.13
1.15
1.17
1.18
1.20
1.22
1.23
1.25
1.27
1.28
1.30
1.32
1.33
1.35
1.37
1.38
1.40
1.42
1.43
1.45
1.47
1.48
1.50
1.52
1.53
1.55
1.57
1.58
1.60
1.62
1.63
1.65
1.67
1.68

Temperature
(C)
32.3
32.4
32.4
32.5
32.6
32.6
32.7
32.7
32.8
32.9
32.9
32.9
33.1
33.1
33.1
33.2
33.3
33.4
33.4
33.5
33.6
33.7
33.8
33.9
34.0
34.0
34.1
34.2
34.3
34.4
34.5
34.5
34.5
34.6
34.6
34.7
34.7
34.8
34.9
35.0
35.1
35.2
35.3
35.4
35.5
35.6
35.7
35.7
35.8
35.9
36.0
36.2
36.3
36.4

Sample Mass: 0.6690 g

Report Time: 6/18/2012 7:52:07PM

TCD Signal
-0.00001
-0.00003
-0.00004
-0.00002
0.00000
-0.00004
-0.00002
-0.00002
-0.00001
-0.00001
-0.00004
-0.00002
-0.00003
-0.00004
-0.00002
-0.00005
-0.00002
-0.00003
-0.00004
-0.00005
-0.00006
-0.00004
-0.00004
-0.00005
-0.00004
-0.00003
-0.00005
-0.00003
-0.00004
-0.00005
-0.00004
-0.00004
-0.00008
-0.00007
-0.00007
-0.00009
-0.00009
-0.00004
-0.00008
-0.00008
-0.00007
-0.00007
-0.00008
-0.00009
-0.00009
-0.00006
-0.00007
-0.00008
-0.00011
-0.00009
-0.00010
-0.00009
-0.00011
-0.00012

Furnace
Temp. (C)
34.47
34.66
34.86
35.04
35.17
35.39
35.57
35.70
35.93
36.09
36.29
36.43
36.63
36.63
36.95
37.20
37.44
37.71
38.09
38.26
38.48
38.74
39.00
39.11
39.38
39.70
39.85
40.02
40.32
40.61
40.78
40.67
40.92
41.11
41.21
41.42
42.06
42.23
42.53
42.73
43.06
43.32
43.50
43.79
43.89
44.01
44.21
44.48
44.75
44.99
45.24
45.61
45.87
46.13

Auxiliary 2

Page 3

ChemiSoft TPx V1.02

Unit 1 (2720)

Serial # 112

Sample: TPR-Rohit-CuFe2O3 18-06-12

Operator: Tarun
Submitter:
File: D:\ALL\TPX\DATA\SANCHIT\000-275.SMP
Started: 6/18/2012 6:27:04PM
Completed:

Time
(minutes)
1.70
1.72
1.73
1.75
1.77
1.78
1.80
1.82
1.83
1.85
1.87
1.88
1.90
1.92
1.93
1.95
1.97
1.98
2.00
2.02
2.03
2.05
2.07
2.08
2.10
2.12
2.13
2.15
2.17
2.18
2.20
2.22
2.23
2.25
2.27
2.28
2.30
2.32
2.33
2.35
2.37
2.38
2.40
2.42
2.43
2.45
2.47
2.48
2.50
2.52
2.53
2.55
2.57
2.58

Temperature
(C)
36.5
36.5
36.6
36.8
36.9
37.0
37.1
37.1
37.2
37.2
37.3
37.5
37.6
37.7
37.9
37.9
38.1
38.2
38.3
38.5
38.6
38.7
38.8
38.9
39.1
39.1
39.3
39.4
39.5
39.6
39.7
39.7
39.8
39.8
40.0
40.1
40.2
40.3
40.4
40.6
40.7
40.9
40.9
41.0
41.2
41.2
41.4
41.5
41.6
41.7
41.8
41.9
42.0
42.1

Sample Mass: 0.6690 g

Report Time: 6/18/2012 7:52:07PM

TCD Signal
-0.00009
-0.00013
-0.00011
-0.00011
-0.00012
-0.00013
-0.00014
-0.00013
-0.00013
-0.00016
-0.00015
-0.00015
-0.00015
-0.00016
-0.00017
-0.00017
-0.00016
-0.00017
-0.00016
-0.00018
-0.00019
-0.00016
-0.00017
-0.00021
-0.00019
-0.00018
-0.00020
-0.00018
-0.00018
-0.00020
-0.00021
-0.00020
-0.00019
-0.00020
-0.00021
-0.00022
-0.00021
-0.00020
-0.00021
-0.00020
-0.00022
-0.00021
-0.00023
-0.00023
-0.00023
-0.00024
-0.00023
-0.00021
-0.00023
-0.00021
-0.00022
-0.00023
-0.00021
-0.00022

Furnace
Temp. (C)
46.38
46.54
46.66
46.69
46.97
47.17
47.35
47.57
47.60
48.10
48.21
48.43
48.70
48.79
49.09
48.99
49.23
49.63
49.64
49.93
50.27
50.48
50.54
50.74
50.93
51.03
50.99
51.35
51.36
51.64
51.75
51.85
52.00
52.13
52.22
52.13
52.38
52.60
52.64
52.87
53.05
53.20
53.28
53.41
53.56
53.58
53.92
54.03
54.16
54.20
54.41
54.59
54.72
54.79

Auxiliary 2

Page 4

ChemiSoft TPx V1.02

Unit 1 (2720)

Serial # 112

Sample: TPR-Rohit-CuFe2O3 18-06-12

Operator: Tarun
Submitter:
File: D:\ALL\TPX\DATA\SANCHIT\000-275.SMP
Started: 6/18/2012 6:27:04PM
Completed:

Time
(minutes)
2.60
2.62
2.63
2.65
2.67
2.68
2.70
2.72
2.73
2.75
2.77
2.78
2.80
2.82
2.83
2.85
2.87
2.88
2.90
2.92
2.93
2.95
2.97
2.98
3.00
3.02
3.03
3.05
3.07
3.08
3.10
3.12
3.13
3.15
3.17
3.18
3.20
3.22
3.23
3.25
3.27
3.28
3.30
3.32
3.33
3.35
3.37
3.38
3.40
3.42
3.43
3.45
3.47
3.48

Temperature
(C)
42.3
42.4
42.4
42.5
42.6
42.7
42.7
42.9
42.9
43.0
43.1
43.2
43.2
43.4
43.5
43.6
43.7
43.9
44.0
44.2
44.3
44.4
44.5
44.7
44.8
44.9
45.0
45.2
45.3
45.4
45.6
45.7
45.8
45.9
46.1
46.2
46.4
46.5
46.6
46.7
46.8
47.0
47.1
47.2
47.3
47.5
47.5
47.6
47.6
47.6
47.6
47.7
47.8
48.0

Sample Mass: 0.6690 g

Report Time: 6/18/2012 7:52:07PM

TCD Signal
-0.00021
-0.00022
-0.00023
-0.00023
-0.00023
-0.00021
-0.00025
-0.00025
-0.00021
-0.00023
-0.00025
-0.00020
-0.00021
-0.00023
-0.00021
-0.00025
-0.00023
-0.00022
-0.00020
-0.00021
-0.00021
-0.00023
-0.00022
-0.00018
-0.00020
-0.00022
-0.00021
-0.00021
-0.00021
-0.00018
-0.00020
-0.00020
-0.00017
-0.00020
-0.00021
-0.00022
-0.00019
-0.00020
-0.00020
-0.00019
-0.00021
-0.00021
-0.00022
-0.00020
-0.00020
-0.00019
-0.00020
-0.00021
-0.00019
-0.00020
-0.00020
-0.00018
-0.00016
-0.00018

Furnace
Temp. (C)
54.98
54.95
55.17
55.22
55.10
55.33
55.32
55.60
55.66
55.83
55.89
55.96
56.07
56.23
56.38
56.60
56.73
56.92
56.96
57.10
57.33
57.36
57.54
57.86
58.03
58.21
58.39
58.65
58.76
58.97
59.14
59.34
59.52
59.65
59.87
60.10
60.31
60.49
60.66
60.75
60.86
60.85
61.12
61.28
61.46
61.64
61.88
62.02
62.13
62.14
62.23
62.36
62.51
62.84

Auxiliary 2

Page 5

ChemiSoft TPx V1.02

Unit 1 (2720)

Serial # 112

Sample: TPR-Rohit-CuFe2O3 18-06-12

Operator: Tarun
Submitter:
File: D:\ALL\TPX\DATA\SANCHIT\000-275.SMP
Started: 6/18/2012 6:27:04PM
Completed:

Time
(minutes)
3.50
3.52
3.53
3.55
3.57
3.58
3.60
3.62
3.63
3.65
3.67
3.68
3.70
3.72
3.73
3.75
3.77
3.78
3.80
3.82
3.83
3.85
3.87
3.88
3.90
3.92
3.93
3.95
3.97
3.98
4.00
4.02
4.03
4.05
4.07
4.08
4.10
4.12
4.13
4.15
4.17
4.18
4.20
4.22
4.23
4.25
4.27
4.28
4.30
4.32
4.33
4.35
4.37
4.38

Temperature
(C)
48.1
48.3
48.5
48.6
48.8
49.0
49.1
49.3
49.4
49.6
49.8
49.9
50.0
50.2
50.3
50.5
50.6
50.8
50.9
50.9
50.8
50.9
51.0
51.1
51.3
51.5
51.6
51.8
51.9
52.0
52.1
52.2
52.3
52.4
52.6
52.8
52.9
53.1
53.3
53.4
53.6
53.8
53.9
54.1
54.2
54.4
54.4
54.6
54.6
54.7
54.8
54.9
55.1
55.3

Sample Mass: 0.6690 g

Report Time: 6/18/2012 7:52:07PM

TCD Signal
-0.00019
-0.00016
-0.00018
-0.00015
-0.00015
-0.00016
-0.00015
-0.00016
-0.00016
-0.00016
-0.00015
-0.00015
-0.00015
-0.00015
-0.00017
-0.00016
-0.00016
-0.00017
-0.00017
-0.00015
-0.00016
-0.00018
-0.00019
-0.00019
-0.00016
-0.00017
-0.00017
-0.00016
-0.00015
-0.00016
-0.00016
-0.00018
-0.00018
-0.00015
-0.00014
-0.00016
-0.00014
-0.00015
-0.00017
-0.00015
-0.00015
-0.00016
-0.00015
-0.00013
-0.00016
-0.00014
-0.00015
-0.00012
-0.00013
-0.00014
-0.00012
-0.00012
-0.00014
-0.00013

Furnace
Temp. (C)
63.00
63.26
63.46
63.63
63.87
64.03
64.22
64.42
64.64
64.93
65.21
65.41
65.56
65.81
65.96
66.17
66.37
66.62
66.55
66.49
66.34
66.48
66.61
66.85
67.03
67.26
67.44
67.53
67.85
68.09
68.27
68.41
68.62
68.75
69.00
69.23
69.51
69.70
69.77
69.90
70.12
70.35
70.53
70.50
70.65
70.75
70.84
71.08
71.04
71.16
71.21
71.68
71.93
72.17

Auxiliary 2

Page 6

ChemiSoft TPx V1.02

Unit 1 (2720)

Serial # 112

Sample: TPR-Rohit-CuFe2O3 18-06-12

Operator: Tarun
Submitter:
File: D:\ALL\TPX\DATA\SANCHIT\000-275.SMP
Started: 6/18/2012 6:27:04PM
Completed:

Time
(minutes)
4.40
4.42
4.43
4.45
4.47
4.48
4.50
4.52
4.53
4.55
4.57
4.58
4.60
4.62
4.63
4.65
4.67
4.68
4.70
4.72
4.73
4.75
4.77
4.78
4.80
4.82
4.83
4.85
4.87
4.88
4.90
4.92
4.93
4.95
4.97
4.98
5.00
5.02
5.03
5.05
5.07
5.08
5.10
5.12
5.13
5.15
5.17
5.18
5.20
5.22
5.23
5.25
5.27
5.28

Temperature
(C)
55.4
55.6
55.8
55.9
56.1
56.3
56.4
56.6
56.8
57.0
57.2
57.4
57.5
57.7
57.9
58.2
58.3
58.5
58.7
58.9
59.1
59.2
59.4
59.5
59.6
59.7
59.8
60.0
60.1
60.3
60.5
60.6
60.8
60.9
61.1
61.3
61.4
61.5
61.7
61.9
62.0
62.2
62.4
62.6
62.6
62.6
62.6
62.6
62.8
63.0
63.1
63.3
63.4
63.6

Sample Mass: 0.6690 g

Report Time: 6/18/2012 7:52:07PM

TCD Signal
-0.00016
-0.00017
-0.00015
-0.00017
-0.00016
-0.00017
-0.00018
-0.00017
-0.00020
-0.00016
-0.00016
-0.00016
-0.00017
-0.00017
-0.00014
-0.00015
-0.00012
-0.00013
-0.00012
-0.00012
-0.00011
-0.00011
-0.00009
-0.00013
-0.00013
-0.00012
-0.00011
-0.00010
-0.00010
-0.00011
-0.00010
-0.00010
-0.00012
-0.00013
-0.00013
-0.00012
-0.00013
-0.00012
-0.00013
-0.00012
-0.00013
-0.00015
-0.00014
-0.00008
-0.00010
-0.00010
-0.00009
-0.00012
-0.00011
-0.00010
-0.00010
-0.00007
-0.00007
-0.00009

Furnace
Temp. (C)
72.37
72.51
72.76
72.97
73.23
73.44
73.63
73.68
73.83
73.92
74.19
74.43
74.71
74.92
75.14
75.56
75.87
76.06
76.22
76.48
76.60
76.54
76.70
76.85
77.05
77.21
77.30
77.62
77.95
78.15
78.27
78.44
78.52
78.65
78.69
78.90
78.99
79.20
79.37
79.61
79.76
80.06
80.19
80.34
80.30
80.21
80.33
80.29
80.46
80.58
80.78
80.76
80.94
81.16

Auxiliary 2

Page 7

ChemiSoft TPx V1.02

Unit 1 (2720)

Serial # 112

Sample: TPR-Rohit-CuFe2O3 18-06-12

Operator: Tarun
Submitter:
File: D:\ALL\TPX\DATA\SANCHIT\000-275.SMP
Started: 6/18/2012 6:27:04PM
Completed:

Time
(minutes)
5.30
5.32
5.33
5.35
5.37
5.38
5.40
5.42
5.43
5.45
5.47
5.48
5.50
5.52
5.53
5.55
5.57
5.58
5.60
5.62
5.63
5.65
5.67
5.68
5.70
5.72
5.73
5.75
5.77
5.78
5.80
5.82
5.83
5.85
5.87
5.88
5.90
5.92
5.93
5.95
5.97
5.98
6.00
6.02
6.03
6.05
6.07
6.08
6.10
6.12
6.13
6.15
6.17
6.18

Temperature
(C)
63.8
63.9
64.1
64.3
64.4
64.5
64.7
64.8
64.9
65.0
65.1
65.3
65.4
65.6
65.8
65.9
66.1
66.3
66.5
66.7
66.9
67.0
67.2
67.4
67.5
67.6
67.8
67.9
68.1
68.2
68.4
68.5
68.7
68.9
69.1
69.2
69.4
69.6
69.8
70.0
70.2
70.3
70.5
70.7
70.9
71.1
71.2
71.4
71.6
71.7
71.9
72.1
72.2
72.4

Sample Mass: 0.6690 g

Report Time: 6/18/2012 7:52:07PM

TCD Signal
-0.00009
-0.00007
-0.00008
-0.00009
-0.00008
-0.00009
-0.00009
-0.00009
-0.00009
-0.00010
-0.00009
-0.00013
-0.00011
-0.00013
-0.00012
-0.00013
-0.00013
-0.00010
-0.00011
-0.00010
-0.00011
-0.00009
-0.00009
-0.00010
-0.00009
-0.00009
-0.00010
-0.00008
-0.00010
-0.00007
-0.00005
-0.00005
-0.00007
-0.00007
-0.00007
-0.00007
-0.00007
-0.00007
-0.00003
-0.00006
-0.00004
-0.00005
-0.00004
-0.00004
-0.00001
-0.00002
0.00000
-0.00001
0.00001
0.00001
0.00000
0.00001
-0.00001
-0.00001

Furnace
Temp. (C)
81.29
81.50
81.58
81.95
82.03
82.15
82.32
82.41
82.55
82.60
82.74
82.87
83.01
83.22
83.45
83.54
83.78
83.95
84.07
84.30
84.50
84.72
84.92
85.08
85.25
85.42
85.57
85.77
85.99
86.17
86.34
86.53
86.66
86.90
87.03
87.22
87.41
87.62
87.82
88.02
88.22
88.37
88.65
88.82
89.03
89.21
89.38
89.57
89.74
89.87
90.05
90.23
90.46
90.65

Auxiliary 2

Page 8

ChemiSoft TPx V1.02

Unit 1 (2720)

Serial # 112

Sample: TPR-Rohit-CuFe2O3 18-06-12

Operator: Tarun
Submitter:
File: D:\ALL\TPX\DATA\SANCHIT\000-275.SMP
Started: 6/18/2012 6:27:04PM
Completed:

Time
(minutes)
6.20
6.22
6.23
6.25
6.27
6.28
6.30
6.32
6.33
6.35
6.37
6.38
6.40
6.42
6.43
6.45
6.47
6.48
6.50
6.52
6.53
6.55
6.57
6.58
6.60
6.62
6.63
6.65
6.67
6.68
6.70
6.72
6.73
6.75
6.77
6.78
6.80
6.82
6.83
6.85
6.87
6.88
6.90
6.92
6.93
6.95
6.97
6.98
7.00
7.02
7.03
7.05
7.07
7.08

Temperature
(C)
72.6
72.8
73.0
73.2
73.3
73.5
73.7
73.9
74.1
74.2
74.5
74.6
74.7
74.8
75.0
75.2
75.4
75.5
75.7
75.9
76.1
76.2
76.4
76.6
76.8
76.9
77.1
77.2
77.4
77.6
77.8
77.9
78.0
78.2
78.4
78.5
78.6
78.7
78.9
79.1
79.2
79.4
79.6
79.8
79.9
80.1
80.3
80.4
80.6
80.8
81.0
81.1
81.3
81.5

Sample Mass: 0.6690 g

Report Time: 6/18/2012 7:52:07PM

TCD Signal
0.00000
0.00001
0.00001
-0.00001
0.00000
0.00001
-0.00001
0.00003
0.00002
0.00003
0.00002
0.00002
0.00002
0.00001
0.00001
0.00001
0.00002
0.00001
0.00002
0.00004
0.00004
0.00003
0.00005
0.00004
0.00005
0.00005
0.00005
0.00005
0.00004
0.00004
0.00007
0.00005
0.00003
0.00005
0.00005
0.00005
0.00002
0.00003
0.00004
0.00003
0.00005
0.00003
0.00004
0.00004
0.00004
0.00005
0.00005
0.00004
0.00005
0.00007
0.00007
0.00004
0.00005
0.00005

Furnace
Temp. (C)
90.77
90.95
91.12
91.28
91.46
91.67
91.97
92.16
92.36
92.51
92.75
92.82
93.03
93.13
93.26
93.45
93.66
93.81
93.96
94.12
94.24
94.41
94.54
94.77
94.99
95.18
95.37
95.57
95.68
95.84
95.99
96.11
96.30
96.43
96.58
96.60
96.73
96.79
96.97
97.12
97.33
97.47
97.63
97.82
97.98
98.19
98.32
98.49
98.67
98.83
99.01
99.13
99.30
99.43

Auxiliary 2

Page 9

ChemiSoft TPx V1.02

Unit 1 (2720)

Serial # 112

Sample: TPR-Rohit-CuFe2O3 18-06-12

Operator: Tarun
Submitter:
File: D:\ALL\TPX\DATA\SANCHIT\000-275.SMP
Started: 6/18/2012 6:27:04PM
Completed:

Time
(minutes)
7.10
7.12
7.13
7.15
7.17
7.18
7.20
7.22
7.23
7.25
7.27
7.28
7.30
7.32
7.33
7.35
7.37
7.38
7.40
7.42
7.43
7.45
7.47
7.48
7.50
7.52
7.53
7.55
7.57
7.58
7.60
7.62
7.63
7.65
7.67
7.68
7.70
7.72
7.73
7.75
7.77
7.78
7.80
7.82
7.83
7.85
7.87
7.88
7.90
7.92
7.93
7.95
7.97
7.98

Temperature
(C)
81.6
81.8
81.9
82.1
82.3
82.4
82.6
82.7
82.9
83.1
83.2
83.5
83.6
83.8
83.9
84.1
84.2
84.4
84.5
84.7
84.9
85.0
85.2
85.4
85.6
85.7
85.8
86.0
86.0
86.2
86.2
86.3
86.5
86.7
86.8
87.0
87.3
87.4
87.6
87.7
87.9
88.1
88.3
88.5
88.7
88.9
89.0
89.2
89.4
89.6
89.9
90.0
90.2
90.4

Sample Mass: 0.6690 g

Report Time: 6/18/2012 7:52:07PM

TCD Signal
0.00002
0.00002
0.00002
0.00002
0.00002
0.00002
0.00003
0.00005
0.00007
0.00006
0.00005
0.00007
0.00009
0.00009
0.00008
0.00005
0.00009
0.00007
0.00007
0.00006
0.00007
0.00005
0.00006
0.00005
0.00006
0.00007
0.00005
0.00007
0.00008
0.00008
0.00009
0.00010
0.00011
0.00013
0.00011
0.00013
0.00013
0.00012
0.00014
0.00012
0.00012
0.00011
0.00010
0.00010
0.00011
0.00011
0.00012
0.00013
0.00012
0.00013
0.00015
0.00012
0.00012
0.00015

Furnace
Temp. (C)
99.54
99.65
99.93
100.01
100.18
100.33
100.44
100.68
100.84
100.94
101.07
101.28
101.46
101.60
101.76
102.00
102.14
102.26
102.40
102.60
102.70
102.90
103.00
103.16
103.38
103.39
103.61
103.76
103.83
104.05
104.15
104.24
104.41
104.61
104.80
105.05
105.18
105.31
105.45
105.60
105.75
105.88
106.14
106.33
106.51
106.70
106.90
107.06
107.37
107.55
107.75
107.94
108.14
108.33

Auxiliary 2

Page 10

ChemiSoft TPx V1.02

Unit 1 (2720)

Serial # 112

Sample: TPR-Rohit-CuFe2O3 18-06-12

Operator: Tarun
Submitter:
File: D:\ALL\TPX\DATA\SANCHIT\000-275.SMP
Started: 6/18/2012 6:27:04PM
Completed:

Time
(minutes)
8.00
8.02
8.03
8.05
8.07
8.08
8.10
8.12
8.13
8.15
8.17
8.18
8.20
8.22
8.23
8.25
8.27
8.28
8.30
8.32

Temperature
(C)
90.5
90.7
90.9
91.1
91.3
91.4
91.6
91.8
92.0
92.2
92.4
92.6
92.8
92.9
93.1
93.3
93.5
93.6
93.8
94.0

Sample Mass: 0.6690 g

Report Time: 6/18/2012 7:52:07PM

TCD Signal
0.00015
0.00016
0.00016
0.00017
0.00018
0.00018
0.00016
0.00018
0.00019
0.00017
0.00020
0.00020
0.00017
0.00018
0.00019
0.00020
0.00019
0.00020
0.00019
0.00020

Furnace
Temp. (C)
108.44
108.67
108.82
109.06
108.94
109.21
109.39
109.62
109.91
110.08
110.32
110.52
110.83
110.99
111.22
111.40
111.15
111.71
111.83
111.96

The table has been truncated to 500 entries. Consider using a larger sampling interval.

Auxiliary 2

Page 11

ChemiSoft TPx V1.02

Unit 1 (2720)

Serial # 112

Page 12

Sample: TPR-Rohit-CuFe2O3 18-06-12

Operator: Tarun
Submitter:
File: D:\ALL\TPX\DATA\SANCHIT\000-275.SMP
Started: 6/18/2012 6:27:04PM
Completed:

Sample Mass: 0.6690 g

Report Time: 6/18/2012 7:52:08PM

TCD Signal (a.u.) vs. Temperature

TCD Signal (a.u.) - TPR Ce Zr Support Tarun
0.06

0.05

TCD Signal (a.u.)

0.04

0.03

0.02

0.01

0.00
50

100

150

200

250

300

350

400

Temperature (C)

450

500

550

600

650

700

ChemiSoft TPx V1.02

Unit 1 (2720)

Serial # 112

Sample: TPR-Rohit-CuFe2O3 18-06-12

Operator: Tarun
Submitter:
File: D:\ALL\TPX\DATA\SANCHIT\000-275.SMP
Started: 6/18/2012 6:27:04PM
Completed:

4227- The data requested on this report are not available.

Sample Mass: 0.6690 g

Report Time: 6/18/2012 7:52:08PM

Page 13