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Castasus C/Y/S: HUB21 Experiment Number 1 (SOLUBILITY OF ORGANIC COMPOUNDS) Objectives: 1. To determine the solubility of various organic compounds in different solvents. 2. To classify various organic compounds into different functional groups Reagents IUPAC name Structure Melting pt. Boiling pt. Specific Gravity Solubility Safety Data Sodium hydroxide 318 C 1,388 C Group number: 1 Date: April 15, 2013
Sodium bicarbonate Hydrochloric acid Materials and Glasswares: 5 small test tubes (5) Stirring rod
Distilled water
Schematic Diagram: 1. Obtain 2-3 drops or 5 mg compound 1 and 2 mL distilled water. Shake vigorously and observe, 2. If compound 1 doesnt dissolve completely. Add another 1.5 mL of distilled water and stir 3. If the compound dissolves completely in water, It is classified to Group A. After, check the pH. 4. If compound 1 is insoluble in water, obtain a new sample ot compound 1 and add 3 Ml of 5% NaOH. If it dissolves determine further its solubility with 3 mL 4$ NaHCO3 . 5. If it both dissolces it is classified to Group B1 but if it is soluble in NaOH but not in NaHCO3 it beongs to group B2. 6. If compound 1 is insoluble in NaOh Obtain a new sample and add 3 mL 5% HCl. It soluble in HCl it belongs to Group C and if insoluble it belongs to Group D 7. Do procedure 1-3, to compounds 2, 3, 4, and 5. Classify compounds 1, 2, 3, 4, and 5.