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  • A Distillation Column With A Partial Reboiler and A Total Condenser Is Being Used To Separate A Mixture of Benzen1

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    José De Jesús Ramírez
    802 vizualizări3 pagini
    The document describes a distillation column used to separate a mixture of benzene, toluene, and cumene. The feed contains 40% benzene, 30% toluene, and 30% cumene at a rate of 100 kg/hr. The problem requires 95% recovery of toluene in the distillate and 95% recovery of cumene in the bottoms. Given relative volatilities, the number of stages for total reflux operation and minimum reflux ratio are calculated. For a reflux ratio of 2, the total number of stages and optimal feed stage location are estimated.

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    A Distillation Column With a Partial Reboiler and a Total Condenser is Being Used to Separate a Mixture of Benzen1

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    The document describes a distillation column used to separate a mixture of benzene, toluene, and cumene. The feed contains 40% benzene, 30% toluene, and 30% cumene at a rate of 100 kg/hr. The problem requires 95% recovery of toluene in the distillate and 95% recovery of cumene in the bottoms. Given relative volatilities, the number of stages for total reflux operation and minimum reflux ratio are calculated. For a reflux ratio of 2, the total number of stages and optimal feed stage location are estimated.

    Drepturi de autor:

    Attribution Non-Commercial (BY-NC)
    Descărcați ca DOCX, PDF, TXT sau citiți online pe Scribd
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    802 vizualizări3 pagini

    A Distillation Column With A Partial Reboiler and A Total Condenser Is Being Used To Separate A Mixture of Benzen1

    Încărcat de

    José De Jesús Ramírez
    The document describes a distillation column used to separate a mixture of benzene, toluene, and cumene. The feed contains 40% benzene, 30% toluene, and 30% cumene at a rate of 100 kg/hr. The problem requires 95% recovery of toluene in the distillate and 95% recovery of cumene in the bottoms. Given relative volatilities, the number of stages for total reflux operation and minimum reflux ratio are calculated. For a reflux ratio of 2, the total number of stages and optimal feed stage location are estimated.

    Drepturi de autor:

    Attribution Non-Commercial (BY-NC)
    Descărcați ca DOCX, PDF, TXT sau citiți online pe Scribd
    Indicator pentru conținut neadecvat
    din 3

    A distillation column with a partial reboiler and a total condenser is being used to separate a mixture of benzene, toluene and

    cumene. The feed ( F = 100 kg moles/h ) is 40 mole % benzene, 30 mole % toluene and 30 mole % cumene and is input as a saturated vapor. We desire 95% recovery of the toluene in the distillate and 95% recovery of the cumene in the bottoms. The reflux is returned as a saturated liquid and a constant molal overflow can be assumed. Pressure is 1 atm. Equilibrium can be represented as constant relative volatilities. Choosing toluene as the reference component, BT=2,25 and CT=0,21. A) 1.- Find the number of equilibrium stages required at total reflux and the recovery fraction of benzene in the distillate. 2.- Find the minimum reflux ratio. Use a basis of 100 kg moles/hour of feed. 3.- Estimate the total number of equilibrium stages and the optimum feed plate location required if the actual reflux ratio is set at L/D = 2. B) Find the optimum feed location and the total number of stages by analytical stage-bystage calculation. External reflux ratio is L/D = 2. Assume that all the benzene is in the distillate. Thus xBenz.,W = 0. If x Benz.,cal. < 5 10-4, do not repeat the calculation.

    A1: 3.77, 99.8%. A2: Lmin=44.48mol-kg/h, Vmin=114.4 mol-kg/h, L/D=0.636 A3: NTotal = 5.53, NF-Dmin = 1.9, NF-D = 2.79

    LK ES EL TOLUENO HK ES EL CUMENO HNK ES EL BENCENO SUPOSICIN INICIAL No aparecen claves pesados en cabezas, slo en colas (xHNK) D= 0 No aparecen claves ligeros en colas, slo en cabezas (xLNK) W= 0

    Balance global a la torre con esta suposicin Comenzar a resolver por un extremo en que todos x 0 Por cabezas porque tengo LNK FONDOS ( ( ( DOMO ( ( ( ) ) ) ) ) )

    NUMERO MINIMO DE ETAPAS ( [ ( ) ) ]

    ( ( (

    ) ) )

    CALCULO DEL NUMERO MINIMO DE ETAPAS BALANCE DE MATERIA DESTILADO

    FONDOS

    DE LA ECUACION DE FENSKE

    *( ( *( ( )( )

    )( )

    )+

    )+

    CALCULO DEL REFLUJO MINIMO

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