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  • Piperazine GC

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    netelsrt1298
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    This document describes the separation of an ethyleneamine industrial sample using gas chromatography. It shows the chromatogram with peaks representing 7 different ethyleneamines separated on a Rtx®-5 Amine column under temperature program conditions from 40°C to 315°C. The sample contained isopropanol, monoethanolamine, ethylenediamine, piperazine, diethylenetriamine, aminoethylethanolamine, and aminoethylpiperazine.

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    Piperazine

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    This document describes the separation of an ethyleneamine industrial sample using gas chromatography. It shows the chromatogram with peaks representing 7 different ethyleneamines separated on a Rtx®-5 Amine column under temperature program conditions from 40°C to 315°C. The sample contained isopropanol, monoethanolamine, ethylenediamine, piperazine, diethylenetriamine, aminoethylethanolamine, and aminoethylpiperazine.

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    © All Rights Reserved
    Descărcați ca PDF, TXT sau citiți online pe Scribd
    Indicator pentru conținut neadecvat
    51 vizualizări1 pagină

    Piperazine GC

    Încărcat de

    netelsrt1298
    This document describes the separation of an ethyleneamine industrial sample using gas chromatography. It shows the chromatogram with peaks representing 7 different ethyleneamines separated on a Rtx®-5 Amine column under temperature program conditions from 40°C to 315°C. The sample contained isopropanol, monoethanolamine, ethylenediamine, piperazine, diethylenetriamine, aminoethylethanolamine, and aminoethylpiperazine.

    Drepturi de autor:

    © All Rights Reserved
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    din 1

    Restek Corporation 110 Benner Circle Bellefonte, PA 16823

    814-353-1300 800-356-1688 Fax: 814-353-1309 www.restek.com


    Ethyleneamines
    Rtx-5 Amine
    1 2
    3
    4
    5
    6
    7
    min. 5 10 15 20 25
    GC_CH00298
    30m, 0.25mm ID, 0.50m Rtx

    -5 Amine (cat.# 12338)


    3.0L split injection of ethyleneamine industrial sample
    On-column conc.: ~5-80ng
    Oven temp.: 40C (hold 4 min.) to 315C
    @10C/min. (hold 5 min.)
    Inj. & det. temp.: 315C
    Carrier gas: hydrogen
    Linear velocity: 43cm/sec. set @40C
    FID sensitivity: 6.4 x 10
    -11
    AFS
    Split ratio: 20:1
    1. isopropanol
    2. monoethanolamine
    3. ethylenediamine
    4. piperazine
    5. diethylenetriamine
    6. aminoethylethanolamine
    7. aminoethylpiperazine
    remaining impurities consist of
    ethyleneamine and piperazine
    derivatives

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