Caculo Incertidumbre de Equipos - Materiales

6/6/2002
DETERMINACION DE INCERTIDUMBRE
REFRACTMETRO RX-500
N
PATRON
1
2
3
4
5
6
7
8
9
10
7.00
7.00
7.00
7.00
7.00
7.00
7.00
7.00
7.00
7.00
Xprom.
u1 =
N
PATRON
1
2
3
4
5
6
7
8
9
10
11.00
11.00
11.00
11.00
11.00
11.00
11.00
11.00
11.00
11.00
Xprom.
u2 =
N
PATRON
1
2
3
4
5
6
7
8
9
10
40.00
40.00
40.00
40.00
40.00
40.00
40.00
40.00
40.00
40.00
Xprom.
u3 =
BRIX
LECTURA (Xi)
6.99
7.00
6.99
6.99
6.99
6.99
7.00
6.98
6.99
6.98
6.99
Xi-Xprom.
(Xi-Xprom.)*2
0.00
0.01
0.00
0.00
0.00
0.00
0.01
-0.01
0.00
-0.01
0.0000
0.0001
0.0000
0.0000
0.0000
0.0000
0.0001
0.0001
0.0000
0.0001
0.0004
0.002108185
BRIX
LECTURA (Xi)
10.99
10.99
10.99
10.99
11.00
11.00
10.99
10.99
10.99
11.00
10.99
Xi-Xprom.
(Xi-Xprom.)*2
0.00
0.00
0.00
0.00
0.01
0.01
0.00
0.00
0.00
0.01
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0002
Xi-Xprom.
(Xi-Xprom.)*2
-0.02
0.02
0.01
-0.02
-0.01
0.01
0.00
0.00
-0.01
-0.02
0.0003
0.0006
0.0002
0.0003
0.0000
0.0002
0.0000
0.0000
0.0000
0.0003
0.0018
0.001527525
BRIX
LECTURA (Xi)
39.98
40.02
40.01
39.98
39.99
40.01
40.00
40.00
39.99
39.98
40.00
0.004521553
N
PATRON
1
2
3
4
5
6
7
8
9
10
50.00
50.00
50.00
50.00
50.00
50.00
50.00
50.00
50.00
50.00
Xprom.
u4 =
N
PATRON
1
2
3
4
5
6
7
8
9
10
60.00
60.00
60.00
60.00
60.00
60.00
60.00
60.00
60.00
60.00
Xprom.
u5 =
BRIX
LECTURA (Xi)
49.99
50.00
49.99
50.00
50.01
50.01
50.00
49.99
49.99
50.01
50.00
Xi-Xprom.
(Xi-Xprom.)*2
-0.01
0.00
-0.01
0.00
0.01
0.01
0.00
-0.01
-0.01
0.01
0.0001
0.0000
0.0001
0.0000
0.0001
0.0001
0.0000
0.0001
0.0001
0.0001
0.0007
Xi-Xprom.
(Xi-Xprom.)*2
0.02
0.00
-0.01
0.00
-0.01
-0.02
-0.02
0.02
0.00
-0.01
0.0005
0.0000
0.0000
0.0000
0.0000
0.0003
0.0003
0.0005
0.0000
0.0000
0.0018
0.002768875
BRIX
LECTURA (Xi)
60.02
60.00
59.99
60.00
59.99
59.98
59.98
60.02
60.00
59.99
60.00
0.004484541
Incertidumbre de Refractmetro RX-500:

Uy =
0.007416198
Al 75%
Uy =
0.014832397
Al 95%
6/6/2002
HIDROMETRO HI01CC (985237)
N
PATRON
1
2
3
4
5
6
7
8
9
10
10.00
10.00
10.00
10.00
10.00
10.00
10.00
10.00
10.00
10.00
Xprom.
u1 =
N
PATRON
1
2
3
4
5
6
7
8
9
10
11.00
11.00
11.00
11.00
11.00
11.00
11.00
11.00
11.00
11.00
Xprom.
u2 =
BRIX
LECTURA (Xi)
10.10
10.05
10.10
10.00
9.95
9.95
9.95
9.95
9.95
9.95
10.00
Xi-Xprom.
(Xi-Xprom.)*2
0.10
0.05
0.10
0.00
-0.05
-0.05
-0.05
-0.05
-0.05
-0.05
0.0110
0.0030
0.0110
0.0000
0.0020
0.0020
0.0020
0.0020
0.0020
0.0020
0.0373
Xi-Xprom.
(Xi-Xprom.)*2
0.02
0.02
0.02
0.02
-0.03
0.02
0.02
0.02
-0.03
-0.08
0.0004
0.0004
0.0004
0.0004
0.0009
0.0004
0.0004
0.0004
0.0009
0.0064
0.0110
0.020344259
BRIX
LECTURA (Xi)
11.05
11.05
11.05
11.05
11.00
11.05
11.05
11.05
11.00
10.95
11.03
0.011055416
Incertidumbre del Hidrmetro HI01CC ( 985237):

Uy =
0.023154073
Al 75%
Uy =
0.046308147
Al 95%
6/6/2002
N
PATRON
1
2
3
4
5
6
7
8
9
10
10.00
10.00
10.00
10.00
10.00
10.00
10.00
10.00
10.00
10.00
Xprom.
BRIX
LECTURA (Xi)
10.10
10.10
10.10
10.15
10.15
10.10
10.10
10.05
10.10
10.15
10.11
u1 =
N
PATRON
1
2
3
4
5
6
7
8
9
10
11.00
11.00
11.00
11.00
11.00
11.00
11.00
11.00
11.00
11.00
Xprom.
u2 =
Xi-Xprom.
(Xi-Xprom.)*2
-0.01
-0.01
-0.01
0.04
0.04
-0.01
-0.01
-0.06
-0.01
0.04
0.0001
0.0001
0.0001
0.0016
0.0016
0.0001
0.0001
0.0036
0.0001
0.0016
0.0090
Xi-Xprom.
(Xi-Xprom.)*2
-0.07
-0.02
0.03
-0.02
0.03
-0.02
0.03
0.03
0.03
-0.02
0.0049
0.0004
0.0009
0.0004
0.0009
0.0004
0.0009
0.0009
0.0009
0.0004
0.0110
0.01
BRIX
LECTURA (Xi)
11.00
11.05
11.10
11.05
11.10
11.05
11.10
11.10
11.10
11.05
11.07
0.011055416

Uy =
0.01490712
Al 75%
Uy =
0.02981424
Al 95%
6/8/2002
N
PATRON
1
2
3
4
5
6
7
8
9
10
10.00
10.00
10.00
10.00
10.00
10.00
10.00
10.00
10.00
10.00
Xprom.
u1 =
N
PATRON
1
2
3
4
5
6
7
8
9
10
11.00
11.00
11.00
11.00
11.00
11.00
11.00
11.00
11.00
11.00
Xprom.
u2 =
BRIX
LECTURA (Xi)
10.20
10.10
10.10
10.05
10.05
10.05
10.15
10.10
10.05
10.05
10.09
Xi-Xprom.
(Xi-Xprom.)*2
0.11
0.01
0.01
-0.04
-0.04
-0.04
0.06
0.01
-0.04
-0.04
0.0121
0.0001
0.0001
0.0016
0.0016
0.0016
0.0036
0.0001
0.0016
0.0016
0.0240
Xi-Xprom.
(Xi-Xprom.)*2
0.02
-0.03
0.02
0.02
0.02
-0.03
0.02
-0.03
0.02
0.02
0.0002
0.0012
0.0002
0.0002
0.0002
0.0012
0.0002
0.0012
0.0002
0.0002
0.0052
0.016329932
BRIX
LECTURA (Xi)
11.10
11.05
11.10
11.10
11.10
11.05
11.10
11.05
11.10
11.10
11.09
0.007637626

Uy =
0.018027756
Al 75%
Uy =
0.036055513
Al 95%
6/8/2002
N
PATRON
1
2
3
4
5
6
7
8
9
10
7.00
7.00
7.00
7.00
7.00
7.00
7.00
7.00
7.00
7.00
Xprom.
u1 =
N
PATRON
1
2
3
4
5
6
7
8
9
10
8.00
8.00
8.00
8.00
8.00
8.00
8.00
8.00
8.00
8.00
Xprom.
u2 =
BRIX
LECTURA (Xi)
7.10
7.15
7.10
7.10
7.10
7.15
7.15
7.15
7.15
7.15
7.13
Xi-Xprom.
(Xi-Xprom.)*2
-0.03
0.02
-0.03
-0.03
-0.03
0.02
0.02
0.02
0.02
0.02
0.0009
0.0004
0.0009
0.0009
0.0009
0.0004
0.0004
0.0004
0.0004
0.0004
0.0060
Xi-Xprom.
(Xi-Xprom.)*2
-0.08
-0.03
0.02
0.02
0.02
0.02
-0.03
0.02
0.02
0.02
0.0064
0.0009
0.0004
0.0004
0.0004
0.0004
0.0009
0.0004
0.0004
0.0004
0.0110
0.008164966
BRIX
LECTURA (Xi)
8.00
8.05
8.10
8.10
8.10
8.10
8.05
8.10
8.10
8.10
8.08
0.011055416

Uy =
0.013743685
Al 70%
Uy =
0.027487371
Al 95%
DETERMINACION DE LA INCERTIDUMBRE DE LOS EQUIPOS DEL LABORATORIO

Material / Equipo involucrado:
Operador:Miguel Luna G.
Fecha:
Hora:
Prueba
Peso fiola +
100 ml Patrn
159.674
159.628
159.85
Fiola / Bureta / pH-metro
Lectura
bureta
Gotas NaOH
Lectura del
pH-metro
11.7
11.7
11.8
11.8
11.9
11.9
12.0
12.1
12.1
12.2
12.2
12.3
12.3
12.4
0
1
2
3
4
5
6
7
8
9
10
11
12
13
8.00
8.04
8.08
8.13
8.18
8.24
8.28
8.35
8.42
8.47
8.54
8.63
8.70
8.78
11.7
11.7
11.8
11.8
11.9
11.9
12.0
12.1
12.1
12.2
12.2
12.3
12.4
12.4
0
1
2
3
4
5
6
7
8
9
10
11
12
13
8.00
8.04
8.07
8.12
8.17
8.22
8.28
8.35
8.41
8.49
8.56
8.64
8.70
8.78
11.6
11.6
11.7
11.7
11.8
11.8
11.9
12.0
12.0
12.1
12.1
12.2
12.2
12.3
0
1
2
3
4
5
6
7
8
9
10
11
12
13
8.00
8.02
8.05
8.09
8.14
8.19
8.25
8.31
8.35
8.42
8.49
8.56
8.63
8.70

Operador: Edward Quezada
Fecha:
Hora:
Prueba
Peso fiola +
100 ml Patrn
159.64
159.566
159.622
Lectura
bureta
11.8
11.8
11.9
11.9
12
12
12.1
12.1
12.2
12.2
12.3
12.4
12.4
12.5
12.5
12
12
12.1
12.2
12.2
12.3
12.3
12.4
12.4
12.5
12.5
12
12.1
12.1
12.2
12.2
12.3
12.3
12.4
12.4
12.5
12.5
159.85
159.816
159.68
159.825
159.827
159.622
12.4
14
8.77
11.6
11.7
11.7
11.8
11.9
11.9
12.0
12.0
12.1
12.1
12.2
12.2
12.3
12.3
12.4
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
8.01
8.03
8.06
8.10
8.15
8.19
8.25
8.35
8.37
8.43
8.49
8.57
8.63
8.71
8.77
11.7
11.7
11.8
11.9
11.9
12.0
12.0
12.1
12.1
12.2
12.3
12.3
12.4
0
1
2
3
4
5
6
7
8
9
10
11
12
8.03
8.07
8.12
8.17
8.22
8.28
8.35
8.42
8.48
8.56
8.63
8.71
8.78
11.6
11.6
11.7
11.7
11.8
11.8
11.9
11.9
12.0
12.1
12.1
12.2
12.3
12.3
12.4
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
8.01
8.03
8.07
8.12
8.16
8.21
8.27
8.33
8.39
8.45
8.52
8.58
8.66
8.73
8.80
11.6
11.6
11.7
11.7
11.8
11.9
0
1
2
3
4
5
8.00
8.03
8.06
8.11
8.16
8.21
159.63
159.599
159.622
12.1
12.2
12.2
12.3
12.3
12.4
12.4
12.5
12.5
12
12.1
12.1
12.2
12.2
12.3
12.3
12.4
12.4
12.5
12
12.1
12.1
12.2
12.2
12.3
12.3
12.4
12.4
12.5
12.5
12
12.1
12.1
12.1
12.2
12.3
159.621
159.827
PARA pH-METRO
Prueba
Promedio
1
0.060
2
0.060
3
0.055
4
0.054
5
0.063
6
0.056
7
0.058
Desviacion: +/- 0.058
11.9
12.0
12.0
12.1
12.2
12.2
12.3
12.4
12.4
6
7
8
9
10
11
12
13
14
8.27
8.33
8.38
8.44
8.51
8.59
8.66
8.74
8.81
159.621
12.3
12.4
12.4
12.5
12.5
12.6
PARA pH-METRO
Prueba
0.002
0.002
-0.003
-0.004
0.004
-0.002
0.000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0001
W - W prom.
1
2
3
4
5
6
7
0.056
0.053
0.052
0.055
0.060
0.058
0.057
0.056
Promedio
-0.002
-0.005
-0.006
-0.003
0.002
0.000
-0.001
U +/-
0.001
AL 75%
U +/- =
0.0014
AL 75%
U +/-
0.002
AL 95%
U +/- =
0.003
AL 95%
Para la Bureta:
Prueba
1
0.054
2
0.054
3
0.057
4
0.057
5
0.058
6
0.057
7
0.057
PARA BURETA:
Prueba
0.054
0.054
0.057
0.057
0.058
0.057
0.057
0.00290
0.00290
0.00327
0.00327
0.00340
0.00327
0.00327
peso fiola
1 159.674
2 159.628
3 159.850
4 159.816
5 159.680
6 159.825
7 159.827
W promedio 159.757
0.035
-0.006
-0.006
-0.006
-0.006
-0.001
-0.006
-0.002
u = +/-
0.003
AL 75%
u = +/-
0.005
AL 95%
PARA FIOLA:
2
W - W prom. (W - W prom.)
-0.083
-0.129
0.093
0.059
-0.077
0.068
0.070
Sumatoria
Desviacion: +/-
0.050
0.050
0.050
0.050
0.056
0.050
0.055
0.051
Desviacion: +/-
Para la fiola:
Prueba
W - W prom.
1
2
3
4
5
6
7
0.00691
0.01668
0.00862
0.00346
0.00595
0.00460
0.00488
Prueba
1
2
3
4
5
6
7
W promedio
peso fiola
W - W prom.
159.640
159.566
159.622
159.630
159.599
159.622
159.621
159.614
0.026
-0.048
0.008
0.016
-0.015
0.008
0.007
0.05111
Sumatoria
u = +/-
0.009
AL 75%
u = +/-
0.019
AL 95%
UIPOS DEL LABORATORIO

Gotas NaOH
Lectura del
pH-metro
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
8.01
8.05
8.09
8.14
8.18
8.23
8.29
8.34
8.4
8.47
8.53
8.59
8.67
8.73
8.79
0
1
2
3
4
5
6
7
8
9
10
8.25
8.27
8.31
8.37
8.42
8.48
8.54
8.6
8.66
8.72
8.78
0
1
2
3
4
5
6
7
8
9
10
8.28
8.31
8.36
8.41
8.46
8.46
8.52
8.6
8.66
8.73
8.8

Operador: William Moran
Fecha:
2/1/2002
Pepsi Cola TQ N 04 (31/01/02)
Prueba
Peso fiola + 100

ml Patrn
159.817
159.769
159.817
Lectura
bureta
Gotas NaOH
Lectura del
pH-metro
11.6
11.6
11.7
11.7
11.8
11.8
11.9
11.9
12
12
12.1
12.1
12.2
12.3
12.3
12.4
11.6
11.7
11.7
11.8
11.8
11.9
11.9
12
12.1
12.1
12.2
12.2
12.3
12.3
12.4
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
8
8.03
8.07
8.11
8.16
8.21
8.25
8.3
8.36
8.41
8.48
8.55
8.62
8.68
8.74
8.81
8.01
8.05
8.09
8.14
8.19
8.24
8.29
8.34
8.41
8.48
8.55
8.61
8.68
8.74
8.81
11.6
11.6
11.7
11.7
11.8
11.9
11.9
12
12
12.1
12.1
12.2
12.2
12.3
0
1
2
3
4
5
6
7
8
9
10
11
12
13
8.03
8.06
8.1
8.14
8.2
8.25
8.31
8.37
8.43
8.49
8.56
8.63
8.7
8.76
159.817
0
1
2
3
4
5
6
7
8
8.37
8.42
8.47
8.52
8.56
8.62
8.69
8.75
8.81
0
1
2
3
4
5
6
7
8
9
8.26
8.31
8.36
8.42
8.48
8.54
8.6
8.67
8.73
8.8
0
1
2
3
4
5
6
7
8
9
10
8.22
8.26
8.31
8.37
8.43
8.49
8.55
8.62
8.68
8.74
8.8
0
1
2
3
4
5
8.2
8.25
8.29
8.34
8.39
8.45
159.843
159.836
159.785
159.828
11.6
11.6
11.7
11.8
11.8
11.9
11.9
12
12
12.1
12.2
12.2
12.3
12.4
0
1
2
3
4
5
6
7
8
9
10
11
12
13
8.01
8.04
8.08
8.12
8.16
8.21
8.29
8.36
8.43
8.49
8.59
8.66
8.74
8.8
11.6
11.6
11.7
11.7
11.8
11.8
11.9
11.9
12
12.1
12.1
12.2
12.2
12.3
0
1
2
3
4
5
6
7
8
9
10
11
12
13
8.01
8.03
8.1
8.15
8.2
8.26
8.32
8.38
8.45
8.51
8.58
8.64
8.72
8.78
11.6
11.6
11.7
11.7
11.8
11.8
11.9
11.9
12
12
12.1
12.2
12.2
12.3
12.3
12.4
11.6
11.6
11.7
11.7
11.8
11.8
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
0
1
2
3
4
5
8
8.03
8.06
8.11
8.15
8.2
8.26
8.32
8.37
8.43
8.49
8.56
8.62
8.68
8.74
8.81
8.01
8.04
8.08
8.13
8.17
8.22
6
7
8
9
10
11
(W - W prom.)2
0.000005
0.000025
0.000036
0.000009
0.000004
0.000000
0.000001
0.000081
(W - W prom.)2
0.000041
0.000041
0.000041
0.000041
0.000001
0.000041
0.000003
0.000207
8.51
8.58
8.64
8.71
8.77
8.83
159.828
PARA pH-METRO
Prueba
Promedio
1
0.054
2
0.057
3
0.056
4
0.061
5
0.059
6
0.054
7
0.056
11.9
11.9
12
12
12.1
12.1
12.2
12.3
12.3
-0.004
-0.001
-0.002
0.003
0.001
-0.004
-0.002
U +/-
0.001
AL 75%
U +/-
0.002
AL 95%
6
7
8
9
10
11
12
13
14
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0001
Para la Bureta:
Prueba
1
0.053
2
0.057
3
0.054
4
0.062
5
0.054
6
0.053
7
0.050
Para la fiola:
(W - W prom.)2
0.00066
0.00233
0.00006
0.00025
0.00023
0.00006
0.00005
Prueba
peso fiola
1
2
3
4
5
6
7
W promedio
159.817
159.769
159.817
159.843
159.836
159.785
159.828
159.814
0.00364
W - W prom. (W - W prom.)2
0.003
-0.045
0.003
0.029
0.022
-0.029
0.014
Sumatoria
Desviacion: +/-
0.010
0.00001
0.00199
0.00001
0.00087
0.00050
0.00082
0.00021
0.00440
8.28
8.33
8.39
8.45
8.51
8.58
8.65
8.72
8.79

Operador: Isaias Granados
Fecha:
2/1/2002
Factor NaOH: 0.9852
Prueba
Peso fiola +
100 ml Patrn
159.489
159.479
159.472
Lectura
bureta
Gotas NaOH
Lectura del pHmetro
11.5
11.6
11.7
11.8
11.9
12
12
12.1
12.1
12.2
12.3
12.3
12.4
15.4
12.5
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
8.00
8.40
8.07
8.12
8.17
8.22
8.28
8.34
8.40
8.46
8.53
8.60
8.67
8.74
8.80
11.6
11.7
11.75
11.8
11.8
11.9
12
12
12.1
12.1
12.2
12.3
12.3
12.4
12.4
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
8.03
8.07
8.11
8.17
8.22
8.28
8.33
8.39
8.45
8.52
8.58
8.64
8.70
8.76
8.82
11.6
11.6
11.7
11.8
11.8
11.9
11.9
12
12.1
12.1
12.2
12.2
12.3
12.4
0
1
2
3
4
5
6
7
8
9
10
11
12
13
8.10
8.04
8.08
8.13
8.18
8.23
8.29
8.38
8.45
8.52
8.60
8.67
8.75
8.83

Operador:
Luis Bazalar
Fecha:
Hora:
Prueba
Peso fiola + 100

ml Patrn
159.731
159.714
159.735
159.472
159.578
159.56
159.55
159.572
159.735
11.6
11.6
11.7
11.7
11.8
11.8
11.9
12
12
12.1
12.1
12.2
12.3
12.3
12.4
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
8.03
8.07
8.11
8.16
8.21
8.25
8.31
8.36
8.42
8.48
8.55
8.62
8.69
8.76
8.83
11.6
11.6
11.7
11.7
11.8
11.9
11.9
12
12
12.1
12.2
12.2
12.3
12.3
12.4
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
8.03
8.06
8.11
8.15
8.19
8.25
8.30
8.36
8.42
8.49
8.56
8.63
8.70
8.77
8.83
11.6
11.6
11.7
11.7
11.8
11.8
11.9
11.9
12
12
12.1
12.2
12.2
12.3
12.3
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
8.01
8.04
8.08
8.12
8.17
8.22
8.27
8.33
8.39
8.45
8.52
8.59
8.66
8.74
8.81
11.5
11.6
11.6
11.7
11.7
11.8
0
1
2
3
4
5
8.02
8.04
8.08
8.12
8.17
8.21
159.722
159.711
159.728
159.719
159.572
11.8
11.9
11.9
12
12.1
12.1
12.2
12.2
12.3
6
7
8
9
10
11
12
13
14
PARA pH-METRO
Prueba Promedio
1
0.057
2
0.056
3
0.056
4
0.057
5
0.057
6
0.057
7
0.056
Para la Bureta:
Prueba
1
0.071
2
0.057
3
0.062
4
0.057
5
0.057
6
0.050
7
0.057
Para la fiola:
Prueba
peso fiola
1 159.489
2 159.479
3 159.472
4 159.578
5 159.560
6 159.550
7 159.572
W promedio 159.529
-0.040
-0.050
-0.057
0.049
0.031
0.021
0.043
Sumatoria
Desviacion: +/-
0.018
0.00157
0.00246
0.00320
0.00244
0.00099
0.00046
0.00189
0.01300
8.27
8.33
8.38
8.45
8.52
8.59
8.67
8.73
8.80
159.719
al / Equipo involucrado:
Lectura bureta
11.5
11.6
11.7
11.8
11.9
12
12.1
12.2
12.3
Gotas NaOH
Lectura del pHmetro

Operador:
Andres Trinidad
Fecha:
2/2/2002
Hora:
Prueba
Peso fiola + 100

ml Patrn
159.419
159.361
159.374
Lectura
bureta
Gotas NaOH
11.6
11.7
11.8
11.8
11.9
11.9
12.0
12.0
12.1
12.1
12.2
12.3
12.3
12.4
12.4
12.5
11.6
11.7
11.7
11.8
11.8
11.9
11.9
12.0
12.0
12.1
12.2
12.2
12.3
12.3
12.4
12.4
11.6
11.7
11.7
11.8
11.8
11.9
11.9
12.0
12.0
12.1
12.2
12.2
12.3
12.3
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
1
2
3
4
5
6
7
8
9
10
11
12
13
14
159.374
159.371
159.390
159.426
159.420
12.4
12.4
11.6
11.7
11.7
11.8
11.8
11.9
11.9
12.0
12.0
12.1
12.1
12.2
12.2
12.3
12.3
12.4
11.6
11.7
11.7
11.8
11.8
11.9
11.9
12.0
12.0
12.1
12.1
12.2
12.2
12.3
12.4
12.4
11.5
11.6
11.6
11.7
11.8
11.8
11.9
11.9
12.0
12.0
12.1
12.1
12.2
12.3
12.3
12.4
11.5
11.5
11.6
11.6
11.7
11.7
15
16
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
1
2
3
4
5
6
159.420
11.8
11.8
11.9
12.0
12.0
12.1
12.1
12.2
12.3
12.3
7
8
9
10
11
12
13
14
15
16
PARA pH-METRO
Prueba
Promedio
1
0.052
2
0.050
3
0.051
4
0.052
5
0.051
6
0.051
7
0.049
Desviacion: +/0.051
Para la Bureta:
Prueba
1
0.056
2
0.050
3
0.050
4
0.050
5
0.050
6
0.056
7
0.050
Desviacion: +/0.052
Para la fiola:
Prueba
1
2
3
4
5
6
7
W promedio
peso fiola
159.419
159.361
159.374
159.371
159.390
159.426
159.420
159.394
0.025
-0.033
-0.020
-0.023
-0.004
0.032
0.026
Sumatoria
Desviacion: +/-
0.010
0.00060
0.00112
0.00042
0.00055
0.00002
0.00100
0.00065
0.00436
Lectura del
pH-metro
8.00
8.04
8.08
8.12
8.17
8.22
8.27
8.32
8.38
8.44
8.51
8.58
8.64
8.70
8.77
8.83
8.00
8.04
8.08
8.12
8.16
8.21
8.26
8.31
8.37
8.43
8.49
8.55
8.61
8.68
8.74
8.80
8.00
8.04
8.07
8.12
8.16
8.21
8.26
8.32
8.37
8.44
8.50
8.56
8.63
8.69

Operador: Luis Marcenaro
Fecha:
Hora:
Prueba
Peso fiola +
100 ml
Patrn
159.477
159.498
159.446
Lectura
bureta
Gotas
NaOH
Lectura del
pH-metro
11.7
11.8
11.8
11.9
11.9
12
12
12.1
12.1
0
1
2
3
4
5
6
7
8
8.3
8.33
8.4
8.49
8.55
8.62
8.72
8.76
8.81
11.7
11.8
11.9
11.9
12
12.1
12.1
12.2
12.2
0
1
2
3
4
5
6
7
8
8.3
8.37
8.43
8.49
8.55
8.61
8.68
8.75
8.82
11.8
11.9
11.9
12
12
12.1
12.1
12.2
12.2
0
1
2
3
4
5
6
7
8
8.3
8.36
8.42
8.49
8.56
8.63
8.69
8.75
8.83
159.446
8.76
8.82
8.01
8.04
8.09
8.13
8.18
8.23
8.28
8.34
8.40
8.46
8.51
8.58
8.65
8.71
8.77
8.84
8.00
8.04
8.08
8.12
8.17
8.22
8.27
8.32
8.38
8.44
8.50
8.56
8.63
8.70
8.76
8.82
8.02
8.05
8.09
8.13
8.18
8.23
8.28
8.33
8.39
8.45
8.50
8.57
8.65
8.71
8.78
8.84
8.01
8.04
8.06
8.10
8.14
8.19
159.531
159.493
159.378
159.562
11.7
11.8
11.8
11.9
12
12
12.1
12.1
12.2
0
1
2
3
4
5
6
7
8
8.29
8.33
8.39
8.46
8.52
8.59
8.65
8.72
8.79
11.8
11.8
11.9
11.9
12
12
12.1
12.1
12.2
0
1
2
3
4
5
6
7
8
8.29
8.35
8.39
8.45
8.52
8.59
8.66
8.73
8.78
11.7
11.8
11.8
11.9
11.9
12
12
12.1
12.1
0
1
2
3
4
5
6
7
8
8.29
8.34
8.4
8.46
8.52
8.59
8.66
8.73
8.79
11.8
11.8
11.9
11.9
12
12
0
1
2
3
4
5
8.29
8.35
8.4
8.44
8.5
8.57
8.24
8.29
8.35
8.41
8.46
8.54
8.60
8.67
8.73
8.80
159.562
12.1
12.1
12.2
6
7
8
PARA pH-METRO
Prueba
Promedio
1
-0.064
2
0.065
3
0.066
4
0.063
5
0.061
6
0.063
7
0.060
Desviacion: +/0.045
Para la Bureta:
Prueba
1
0.050
2
0.063
3
0.050
4
0.063
5
0.050
6
0.050
7
0.050
Desviacion: +/0.054
Para la fiola:
(W - W prom.)2
Prueba
peso fiola
1
2
3
4
5
6
7
W promedio
159.477
159.498
159.446
159.531
159.493
159.378
159.562
159.484
-0.007
0.014
-0.038
0.047
0.009
-0.106
0.078
Sumatoria
Desviacion: +/-
0.023
0.00004
0.00021
0.00141
0.00225
0.00009
0.01115
0.00615
0.02130
8.63
8.7
8.77
PARA pH-METRO
Prueba
1
2
3
4
5
6
7
Promedio =
w
0.058
0.053
0.052
0.055
0.060
0.058
0.057
0.056
W - W prom.
(W - W prom.)2
0.002
-0.003
-0.004
-0.001
0.004
0.002
0.001
0.000003
0.000010
0.000017
0.000001
0.000015
0.000003
0.000001
0.000051
U = +/- 0.0011
AL 75%
U = +/- 0.0022
AL 95%
PARA BURETA:
Prueba
1
2
3
4
5
6
7
Promedio =
W - W prom.
(W - W prom.)2
0.050
0.050
0.050
0.050
0.056
0.050
0.055
0.052
-0.002
-0.002
-0.002
-0.002
0.004
-0.002
0.003
0.000002
0.000002
0.000002
0.000002
0.000020
0.000002
0.000012
0.000044
U +/- =
0.0010
AL 75%
U +/- =
0.0020
AL 95%
PARA FIOLA:
Prueba
1
2
3
4
5
6
7
Promedio =
W - W prom.
(W - W prom.)2
159.640
159.566
159.622
159.630
159.599
159.622
159.621
159.614
0.026
-0.048
0.008
0.016
-0.015
0.008
0.007
0.000661
0.002332
0.000060
0.000247
0.000234
0.000060
0.000045
0.003637
U +/- =
0.0093
AL 75%
U +/- =
0.0186
AL 95%
Pesa de 1g
t = 22.5 C
w
1.0005
1.0006
1.0004
1.0005
1.0005
1.0005
1.0005
1.0005
1.0004
1.0005
1.0005
1
2
3
4
5
6
7
8
9
10
Promedio =
W - W prom.
(W - W prom.)2
0.0000100
0.0001100
-0.0000900
0.0000100
0.0000100
0.0000100
0.0000100
0.0000100
-0.0000900
0.0000100
0.00000000010
0.00000001210
0.00000000810
0.00000000010
0.00000000010
0.00000000010
0.00000000010
0.00000000010
0.00000000810
0.00000000010
0.00000002900
U +/- =
0.0000180
AL 75%
U +/- =
0.0000359
AL 95%
Pesa de 2g "A"
t = 22.5 C
W
1.9994
1.9994
1.9993
1.9994
1.9992
1.9993
1.9994
1.9994
1.9993
1.9994
1.9994
1
2
3
4
5
6
7
8
9
10
Promedio =
W - W prom.
(W - W prom.)2
0.0000500
0.0000500
-0.0000500
0.0000500
-0.0001500
-0.0000500
0.0000500
0.0000500
-0.0000500
0.0000500
0.00000000250
0.00000000250
0.00000000250
0.00000000250
0.00000002250
0.00000000250
0.00000000250
0.00000000250
0.00000000250
0.00000000250
0.00000004500
U +/- =
0.0000224
AL 75%
U +/- =
0.0000447
AL 95%
Pesa de 2g "B"
1
2
3
4
5
6
7
8
9
10
Promedio =
U = +/-
t = 22.4 C
W
1.9984
1.9984
1.9984
1.9984
1.9984
1.9984
1.9984
1.9984
1.9985
1.9984
1.9984
0.0003
W - W prom.
(W - W prom.)2
-0.0000100
-0.0009500
-0.0009500
-0.0009500
-0.0009500
-0.0009500
-0.0009500
-0.0009500
-0.0008500
-0.0009500
0.00000000010
0.00000090250
0.00000090250
0.00000090250
0.00000090250
0.00000090250
0.00000090250
0.00000090250
0.00000072250
0.00000090250
0.00000794260
AL 75%
U = +/-
0.0006
AL 95%
Pesa de 5g
t = 22.4 C
W
4.9973
4.9971
4.9969
4.9970
4.9969
4.9970
4.9970
4.9971
4.9971
4.9967
4.9970
1
2
3
4
5
6
7
8
9
10
Promedio =
W - W prom.
(W - W prom.)2
0.0002900
0.0000900
-0.0001100
-0.0000100
-0.0001100
-0.0000100
-0.0000100
0.0000900
0.0000900
-0.0003100
0.00000008410
0.00000000810
0.00000001210
0.00000000010
0.00000001210
0.00000000010
0.00000000010
0.00000000810
0.00000000810
0.00000009610
0.00000022900
U = +/-
0.00005
AL 75%
U = +/-
0.00010
AL 95%
Pesa de 10g
1
2
3
4
5
6
7
8
9
10
Promedio =
t = 22.4 C
W
9.9970
9.9973
9.9969
9.9971
9.9971
9.9970
9.9970
9.9971
9.9969
9.9970
9.99704
W - W prom.
(W - W prom.)2
-0.0000400
0.0002600
-0.0001400
0.0000600
0.0000600
-0.0000400
-0.0000400
0.0000600
-0.0001400
-0.0000400
0.00000000160
0.00000006760
0.00000001960
0.00000000360
0.00000000360
0.00000000160
0.00000000160
0.00000000360
0.00000001960
0.00000000160
0.00000012400
U = +/- 0.000037
AL 75%
U = +/- 0.000074
AL 95%
Pesa de 20g "A"

1
2
3
4
5
6
7
8
9
10
Promedio =
t = 22.3 C
W
20.0007
20.0008
20.0007
20.0007
20.0006
20.0006
20.0005
20.0007
20.0005
20.0007
20.00065
U = +/- 0.000031
W - W prom.
(W - W prom.)2
0.0000500
0.0001500
0.0000500
0.0000500
-0.0000500
-0.0000500
-0.0001500
0.0000500
-0.0001500
0.0000500
0.00000000250
0.00000002250
0.00000000250
0.00000000250
0.00000000250
0.00000000250
0.00000002250
0.00000000250
0.00000002250
0.00000000250
0.00000008500
AL 75%
U = +/- 0.000061
AL 95%
Pesa de 20g "B"

1
2
3
4
5
6
7
8
9
10
Promedio =
t = 22.3 C
W
20.0001
20.0001
20.0001
20.0001
20.0001
20.0001
20.0001
20.0002
20.0002
20.0001
20.00012
W - W prom.
(W - W prom.)2
-0.0000200
-0.0000200
-0.0000200
-0.0000200
-0.0000200
-0.0000200
-0.0000200
0.0000800
0.0000800
-0.0000200
0.00000000040
0.00000000040
0.00000000040
0.00000000040
0.00000000040
0.00000000040
0.00000000040
0.00000000640
0.00000000640
0.00000000040
0.00000001600
U = +/- 0.000013
AL 75%
U = +/- 0.000027
AL 95%
U +/- =
0.00061357

Caculo Incertidumbre de Equipos - Materiales

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Drepturi de autor:

Formate disponibile

Caculo Incertidumbre de Equipos - Materiales

Încărcat de

Drepturi de autor:

Formate disponibile

6/6/2002

Incertidumbre de Refractmetro RX-500:

Incertidumbre del Hidrmetro HI01CC ( 985237):

Incertidumbre del Hidrmetro HI01CC ( 985217):

Incertidumbre del Hidrmetro HI31CC ( 985247):

Incertidumbre del Hidrmetro HI04CC ( 2006410):

DETERMINACION DE LA INCERTIDUMBRE DE LOS EQUIPOS DEL LABORATORIO

Fiola / Bureta / pH-metro

Material / Equipo involucrado:

UIPOS DEL LABORATORIO

Material / Equipo involucrado:

Peso fiola + 100

Fiola / Bureta / pH-metro

Material / Equipo involucrado:

Fiola / Bureta / pH-metro

Lectura del pHmetro

Material / Equipo involucrado:

Peso fiola + 100

Fiola / Bureta / pH-metro

Lectura del pHmetro

Material / Equipo involucrado:

Peso fiola + 100

Fiola / Bureta / pH-metro

Fiola / Bureta / pH-metro

Material / Equipo involucrado:

Fiola / Bureta / pH-metro

Pesa de 20g "A"

Pesa de 20g "B"

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