Name of Instrument Test Method Standard used Test Stab. Fiber avaiable 7 m appox Carbon.

Fiber avaiable 7 m appox Place

Mechincal test Laser Technique ASTM Tensile test Diameter 1 1 Outside ITA

Gas pycnometery Voulme Density 1 2 ITA

Tensile testing Diameter Voulme density Optical microscope Elementry analysis FR-Infrared spectroscopy SEM Wide angle x ray DSC

how the mechnical properties changes for stabilation to carobination in both sample change in diameter change in density maginfied image of samples H,C,N content from the information of bond vibration so we can define the extend of reaction in bot we can compare the effect of dwell time on fiber surface by using 3D image to observed the crystal struture for both sample after stabilation and carbonization (AI)degree of oxidation by knowing exo heat of oxidized PAN and virgin PAN

Optical Microscope Surface analysis 0.5 0.5 ITA

Elementry analysis H,C,N content 0.5 0.5 Outside (ITA)

FT-IR spectra Extent of reaction 0.2 0.2 Outside

SEM Surface topography 0.5 0.5 ITA

Wide angle X ray Crystral struture 0.2 0.2 ITA

tabilation to carobination in both sample

e can define the extend of reaction in both samples fiber surface by using 3D image mple after stabilation and carbonization of oxidized PAN and virgin PAN

DSC Thermal anaylsis 0.1 0.1 ITA

Samples Density (g/cm3) Aromatization Index (%) Tensile

S1 1.58

C1 1.79

S2 1.48

C2 1.78

S1 - Temp 220,240,260,280 and dwell of 30 min. S2 - Temp 220,240,260,280 and dwell of 15 min C1 & C2 - LT 800, HT 1300 dwell 2 min