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  • TP ACM 2 Amine Equivalent

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    Meenakshi Shenoy
    120 vizualizări1 pagină
    This method determines amine equivalent of amidoamines using potentiometric titration. Information contained herein is believed to be reliable, but no representations, guarantees or warranties of any kind are made. Information often is based on laboratory work with small-scale equipment and does not necessarily indicate end product performance or reproducibility.

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    This method determines amine equivalent of amidoamines using potentiometric titration. Information contained herein is believed to be reliable, but no representations, guarantees or warranties of any kind are made. Information often is based on laboratory work with small-scale equipment and does not necessarily indicate end product performance or reproducibility.

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    Attribution Non-Commercial (BY-NC)
    Descărcați ca PDF, TXT sau citiți online pe Scribd
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    120 vizualizări1 pagină

    TP ACM 2 Amine Equivalent

    Încărcat de

    Meenakshi Shenoy
    This method determines amine equivalent of amidoamines using potentiometric titration. Information contained herein is believed to be reliable, but no representations, guarantees or warranties of any kind are made. Information often is based on laboratory work with small-scale equipment and does not necessarily indicate end product performance or reproducibility.

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    Attribution Non-Commercial (BY-NC)
    Descărcați ca PDF, TXT sau citiți online pe Scribd
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    din 1

    LUBRIZOL TEST PROCEDURE

    TP-ACM-2 Edition: September 14, 2010 Original Issue: October 8, 2008

    Test Method for the Determination of Amine Equivalent


    Purpose:
    This method determines amine equivalent of amidoamines using potentiometric titration.

    Procedure:
    1. Weigh 1.5 - 2.0 grams to the nearest 0.1 mg into a 250 ml beaker. 2. Add 110 mls of 80/20 IPA/DI Water Solution and 4-6 drops of Bromophenol Blue Indicator. 3. Titrate to the potentiometric or visual (yellow) endpoint with 0.5N HCl.

    Abstract:
    A solution of the surfactant is titrated potentiometrically with HCL to determine the amine equivalent of amidoamines. End point may also be determined visually.

    Calculations:
    Amine equivalent = Sample weight (g) x 103 N x ml

    Safety Precautions:
    1. Proper personal protective equipment should be worn during transfer of materials so that injury due to spillage is avoided. 2. Review MSDS for each material before handling.

    Reagents:
    1. Bromophenol Blue Indicator 2. Isopropanol/DI Water Solution80/20 by volume 3. 0.5N HCl aqueous solution (aqueous)

    Apparatus:
    1. Potentiometric Titrator 2. Combined glass pH electrode (Metrohm # 6.0262.100)

    Lubrizol Advanced Materials, Inc. / 9911 Brecksville Road, Cleveland, Ohio 44141-3247 / TEL: 800.379.5389 or 216.447.5000
    The information contained herein is believed to be reliable, but no representations, guarantees or warranties of any kind are made as to its accuracy, suitability for particular applications or the results to be obtained. The information often is based on laboratory work with small-scale equipment and does not necessarily indicate end product performance or reproducibility. Because of the variations in methods, conditions and equipment used commercially in processing these materials, no warranties or guarantees are made as to the suitability of the products for the applications disclosed. Full-scale testing and end product performance are the responsibility of the user. Lubrizol Advanced Materials, Inc. shall not be liable for and the customer assumes all risk and liability for any use or handling of any material beyond Lubrizol Advanced Materials, Inc.s direct control. The SELLER MAKES NO WARRANTIES, EXPRESS OR IMPLIED, INCLUDING, BUT NOT LIMITED TO, THE IMPLIED WARRANTIES OF MERCHANTABILITY AND FITNESS FOR A PARTICULAR PURPOSE. Nothing contained herein is to be considered as permission, recommendation, nor as an inducement to practice any patented invention without permission of the patent owner.

    For further information, please visit www.personalcare.noveon.com


    Lubrizol Advanced Materials, Inc. is a wholly owned subsidiary of The Lubrizol Corporation * Trademark owned by The Lubrizol Corporation Copyright 2010 / The Lubrizol Corporation

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