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NEELACHAL ISPAT NIGAM LIMITED

TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


03. LABORATORY FACILITIES (IMPORTED) List of equipme t fo! "#$o!#to!% f#&i"ities (P'ASE(II) S". )o. 03.01. 03.02. 03.03. 03.0 . 03.0#. 03.0&. 03.0(. Des&!iptio X-ray fluorescence spectrometer (sequential type) Optical emission spectrometer Simultaneous carbon-sulphur analyzer Simultaneous o!y"en-nitro"en analyser $utomate% hy%ro"en %eterminator S'in" "rin%in" mill )riquettin" press *t%.+ )o. 1 2 1 1 1 1 1

Laboratory Facilities (Imported)


2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

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NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT

03. List of equipme t # , $!o#, spe&ifi&#tio fo! "#$o!#to!% f#&i"ities ( P-#se ( II ) S". )o. 03.0 . Des&!iptio /0!#% f"uo!es&e &e spe&t!omete! (seque ti#" t%pe) *he equipment shall be use% for sequential analysis of chemical constituents in the samples of hot metal+ burnt lime+ calcine% %olomite+ iron ore lump+ spon"e iron+ )O, sla" + Si--n+ ,e-Si+ ,e--n+ ,e . *i+ ,e-/+ ,e-0b+ ,e-) an% other ferro-alloys in the steel ma1in" unit of an inte"rate% steel plant. ,or analysis of hot metal samples+ typical precision of analysis of the offere% equipment shall be in line 'ith the stipulations of $S*- 2-322+ (latest e%ition). *he X-ray fluorescence spectrometer
shall be pro3i%e% 'ith facilities for analysis of C#!$o # , Bo!o + hi"h alumina bric1s+ lo' alumina bric1s+ silica bric1s+ la%le sla"+ sli%e "ate san%+ continuous castin" po'%er+ petroleum co1e ash+ fly ash+ S-S slu%"e+ lime stone+ %olomite either by pro3i%in" t'o number of fi!e% channels for %etermination of 4arbon an% )oron + hi"h alumina bric1s+ lo' alumina bric1s+ silica bric1s+ la%le sla"+ sli%e "ate san%+ continuous castin" po'%er+ petroleum co1e ash+ fly ash+ S-S slu%"e+ lime stone+ %olomite or throu"h pro3ision of separate crystals for analysis of 4arbon an% )oron + hi"h alumina bric1s+ lo' alumina bric1s+ silica bric1s+ la%le sla"+ sli%e "ate san%+ continuous castin" po'%er+ petroleum co1e ash+ fly ash+ S-S slu%"e+ lime stone+ %olomite. 2lement-'ise 5o'er 5imit of 6etection (5.5.6.) fi"ures

*t%.+ )o. .

an% accuracy fi"ures for X-ray ,luorescence Spectrometer at Laboratory Facilities (Imported)
2009 MEC ! Limite"# $ll %ig&ts %eser'e"( Page 2 of 40

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio %ifferent concentration le3els shall be furnishe% by the ten%erer. $ typical analytical pro"ram for the equipment is in%icate% in table-7 an% table 77 of this specification. *he X-ray fluorescence spectrometer shall be of 'a3elen"th %ispersi3e type an% shall consist of hi"h 3olta"e X-ray "enerator+ spectrometer 'ith mounte% optics+ countin" an% control electronics+ computer+ laser printer+ colour "raphic monitor+ multime%ia 1eyboar%+ 'ater chiller+ etc. as a composite unit. *he hi"h 3olta"e "enerator shall supply stabilise% po'er supply to X-ray tube. -ain components of the hi"h 3olta"e X-ray "enerator shall be hi"h 3olta"e stabilise% po'er supply system+ filament po'er supply system+ safety circuits+ X-ray tube 'ith coolin" arran"ement+ etc. *he selection of parameters shall be automatic throu"h computer. *he X-ray tube shall be 8h tar"et 'ith )eryllium 'in%o' of (# micron or less thic1ness 'ith hi"h purity 8ho%ium tar"et an% pro3i%e% 'ith requisite 0os. of filters for remo3al of interferin" lines an% for impro3ement in lo'er limit of %etection. *ube life+ to be "uarantee%+ shall be specifie%. 7t shall be possible to store X-ray tube un%er normal laboratory con%ition. 9ser:s certificate re"ar%in" tube life shall be furnishe%. *he %esi"n of the spectrometer shall pro3i%e 3ery close couplin" bet'een the X-ray tube ano%e an% sample. *he Spectrometer chamber shall be maintaine% at a hi"h le3el of 3acuum Laboratory Facilities (Imported)
2009 MEC ! Limite"# $ll %ig&ts %eser'e"( Page ) of 40

*t%.+ )o.

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio an% shall house collimator+ "oniometer mounte% 'ith crystals an% %etectors+ multi position area limitin" %iaphra"m e!chan"er (mas1)+ crystal chan"er 'ith crystals fitte%. *he equipment shall ha3e automatic 10 (minimum) sample chan"er an% sample chamber un%er 3acuum. *he spee% of rotation of the sample shall be sufficient to suppress the effect of non- homo"enities in the specimen. 7t shall ha3e facility for quic1 chan"eo3er of samples. *he "oniometer shall be fully automatic an% microprocessor controlle%. *he equipment shall be capable of analysin" 2# mm to #0 mm %iameter samples. *t%.+ )o.

0ecessary har%'are an% soft'are for remote %ia"nostic facility shall be pro3i%e%. *he combination of 1/ an% m$ 3alues for ;* "enerator shall be selecte% by the equipment supplier < manufacturer+ 1eepin" in 3ie' the analytical pro"ram+ the precision an% accuracy of analysis. Selection of slit 'i%th+ crystal+ %etector+ collimator+ primary beam filter (*i)+ flo' counter+ 'in%o' (of minimum thic1ness)+ etc. shall be optimum to pro3i%e ma!imum intensity an% spectral resolution. *he repro%ucibility+ precision an% accuracy of analysis for each element shall be finishe% in tabular form. *he e!citation con%itions+ the "eometry an% X-ray optics of the spectrometer shall pro3i%e for lar"e si"nal to bac1"roun% ratio+ stable an% repro%ucible results an% lo' %etection limits

Laboratory Facilities (Imported)


2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

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NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio 'ith shortest measurin" time. *he equipment shall be pro3i%e% 'ith electronic %e3ices li1e pulse hei"ht analyser+ scalar 'ith hi"h countin" capacity+ timer+ etc. *he spectrometer shall ha3e built-in computer 'ith 'in%o's base% soft'are to control instrument parameters+ e3aluate an% correct the analysis results+ select pre-set analytical pro"ramme an% print out analytical results+ soft'are shall also ha3e capability for transmission of results to an upper computer. It s-#"" $e p!o2i,e, 3itBOF "e2e"0II #utom#tio s%stem. $ suitable 'ater chiller for coolin" of the X-ray tube shall be pro3i%e% an% shall 'or1 at #0=4. *he chiller 'ater pump must be sin"le phase an% separate 'irin" to be pro3i%e% from the 1# >/$ 9?S. *he instrument shall be calibrate% at the users plant 'ith samples pro3i%e% by the user. ;o'e3er+ # sets of international 48- stan%ar%s to be supplie% alon" 'ith the equipment for each of the matri!+ in%icate% in *able-7 an% also for calibration at user site. Sample hol%er+ mas1s+ etc. shall be inclu%e% in the scope of supply. Supply of the spectrometer shall be complete in e3ery respect inclu%in" 2 0os. of ?-10 "as shall be pro3i%e% 'ith its purity certificate @ e!plosi3e certificate+ fille% - in cylin%er 'ith re"ulators+ 3olta"e stabiliser of Laboratory Facilities (Imported)
2009 MEC ! Limite"# $ll %ig&ts %eser'e"( Page * of 40

*t%.+ )o.

e&ess#!% f#&i"ities (&ompute!

i te!f#&i 4) so t-#t it is #$"e to t!# smit # #"%ti&#" !esu"ts ,i!e&t"% to

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio require% capacity+ A# >/$ 9?S+ mechanical tool set (1 0o.) for re"ular maintenance an% initial 3 months consumption etc. *hese items shall be supplie% from in%i"enous sources. M#5o! te&- i&#" p#!#mete!s *he equipment shall "enerally conform to the follo'in" technical parameters. X-ray "enerator X-ray tube B )eryllium 'in%o' of (# micron or less thic1ness 'ith hi"h purity 8ho%ium tar"et preferably 'ith ceramic insulation an% tapere% nose+ output 6.0 78 (mi .). 4ombination of e!citation potential up to &0 1/ an% filament current up to 12# (min) m$ but hi"her filament current is preferre%. *he supplier shoul% %emonstrate performance of X8, at %ifferent m$ an% 1/ 1C 'ith settin". *t%.+ )o.

*he ten%erer shall "uarantee for the tube life an% pro3i%e certificate for a minimum perio% of 12 months. *he X-ray tube shall be manufacture% by the supplier of the X-ray spectrometer. X-ray tube coolin" B 4lose% circuit+ usin" %eionise% 'ater ;* "enerator B ,ull 'a3e rectification+ ratin" .0 1C (min.) 120 m$ (min.)+ stability of tube current an% tube 3olta"e shall be D0.0001E for D1E fluctuations in input 3olta"e an% current. 7t shall support iso-'att s'itchin". Laboratory Facilities (Imported)
2009 MEC ! Limite"# $ll %ig&ts %eser'e"( Page + of 40

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio Spectrometer chamber B X-ray beam 23acuation system 4rystal B /acuum path B 8otary 3acuum pump 'ith oil mist filter system B $ combination of minimum ei"ht 0o. of %ifferent crystals (e!cept those use% for fi!e% channels) li1e 5i, (200)+ 5i, 220+ ?2*+ F2+ *$?+ F2 111 etc.+ in line 'ith the requirement of the analytical pro"ram an% other synthetic crystals of latest technolo"y.. Out of the ei"ht crystals t'o or more crystals must be co3ere%. 6etector B $ combination of minimum three %etectors (,lo' proportional counter+ Scintilation counter+ 7nert "as seal% proportional counter) 'ith countin" electronics for optimum co3era"e of all elements in the ran"e of )oron to 9ranium. ,-?4 'ith "as %ensity stabiliser for li"ht elements an% S4 for hea3y element. Foniometer co3era"e *emperature B 0o - 1 G o (2) (min.) B ?76 control to 1eep the temperature of chamber 'ithin D 0.0# o 4 for ambient temperature ran"e of 1G o4 to 2G o4. S#mp"e -# ,"i 4 s%stem Sample type -a!imum sample %imension Laboratory Facilities (Imported)
2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

*t%.+ )o.

9 B B Soli% @ briquette% po'%er #0 mm %ia ! 30 mm hei"ht

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NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio Sample spin B 30 rpm ( typical ) *t%.+ )o.

Cou ti 4 # , &o t!o" e"e&t!o i&s 7tems to be controlle% B$ll mechanical motions+ controls+ linearity of countin" up to 1.# million counts per secon% or better an% %ata transfer. 6ea% time correction ,ast an"ular rotation 7nte"ration time -emory bac1-up Compute! s%stem (-#!,3#!e ) 7t shall be pro3i%e% 'ith 4ore 2 6uo < ?entium processor 'ith latest 3ersion alon" 'ith 1( inch *,* colour monitor+ ;66 of 2#0 F) an% 6/6 Criter < 8ea%er. 7t shall be pro3i%e% 'ith full 1ey boar% 'ith a%%itional function 1eys+ mouse+ 8S 2324 interface+ -icrosoft Cin%o's of latest 3ersion+ etc. Compute! soft3#!e *he soft'are pac1a"e shall be comprehensi3e an% shall inclu%e all pro"rammes 'hich are necessary for control of equipment+ analysis+ online an% off-line %ata processin"+ report ma1in" an% %ata transmission+ etc. 7n "eneral+ it shall inclu%e. - )ac1 "roun% correction @ %rift correction Laboratory Facilities (Imported)
2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

B )etter than 20 nano- secon%s B H20000<minute or better B 0.1 . III sec B *hrou"h stan%-by battery

;i"h repro%ucibility of an"ular position B D0.00020 or better

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NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio - 7nternal stan%ar% correction @ matri! correction ?rocess parameter calculations Stan%ar%isation @ calibration 8e"ression analysis ?reparation of calibration cur3es 8epeat analysis *t%.+ )o.

- 8eportin" - *ransmission to e!ternal 4?9 Stan%ar% less analysis ?ea1 search+ pea1 i%entification+ ?;$ a%Justment+ selection of output for chart+ etc. 6ialo"ue functions 2quipment monitorin" Job *heoretical matri! calculation - $ll mounte% electrics an% instrumentations alon" 'ith computer har%'are /acuum pump 7nterface an% soft'are for %ata transmission up%ate% free of char"e %urin" 'arranty - *he license% copy of the X8, soft'are shall be pro3i%e% in 468O- alon" 'ith the necessary help Spares for t'o years of operation an%

*he equipment shall be quote% alon" 'ith the follo'in" items B

- 46 soft'are for ser3icin" of the equipment+ the soft'are shall be

Laboratory Facilities (Imported)


2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

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NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio maintenance as recommen%e% by the manufacturer the manufacturer samples. Suitable require% stan%ar%s (settin" up type) are to be inclu%e% in the supply. Semi quantitati3e analysis also shoul% co3er the ran"e of elements form ) to 9. 8emote %ia"nostic pac1a"e 'ith suitable soft'are for accessin" the manufacturer for remote ser3icin". *he equipment<computer shoul% be equippe% 'ith suitable soft'are an% har%'are li1e mo%em an% < or internet net'or1 boar% < car%+ etc. %ifferent elements. 8#!!# t% # , suppo!t *he instrument an% its accessories < au!iliaries li1e 4hiller+ ;y%raulic ?ress+ /ibratory %isc mill+ 9?S+ etc. shoul% ha3e minimum fi3e years 'arranty. Laboratory Facilities (Imported)
2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

*t%.+ )o. 4ommissionin" spares as recommen%e% by Stan%ar% accessories. 7nitial fill of oil an% "rease an% consumables

for three months of operation after commissionin" Semi quantitati3e < stan%ar% less soft 'are pac1a"e is to be inclu%e% for analysis of non-routine or un1no'n

,acility for settin" quality control limits for

*he spectrometer an% its all parts shoul%


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NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio ha3e inspection certificate. of the equipment. 4omplete set of %ra'in"s of 3acuum pump+ spectrometer ('ith 3arious O-rin"s mar1e% on it) shoul% be supplie% alon" 'ith the equipments. "i3en. elements in each 6e%icate% 8, earthin" to be pro3i%e%. 7nstallation+ commissionin" an% I st#""#tio : Commissio i 4: Demo st!#tio 9 %emonstration shoul% be %one an% trainin" shoul% be "i3en. $ll "roup mentione% in the table-1 shoul% be ?re-requisites material shoul% be supplie%. *rainin" on operation+ maintenance an% calibration to be pro3i%e% at site. 5ist of users (?referable in steel plant) since year 2000 to be pro3i%e%. C#"i$!#tio : st# ,#!,i;#tio # , Routi e A #"%sis. for installation an% %emonstrate% for as1e% ran"e. commissionin" shoul% "i3en after placement of or%er. ,8 earthin" ?re-installation %etails 'ith necessary instructions to be pro3i%e%. 6etaile% electrical specification to be Supplier shoul% "i3e "uarantee that the spare parts 'ill not be obsolete for ne!t 1# years from the %ate of supply *t%.+ )o.

Laboratory Facilities (Imported)


2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

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NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio 7n%i3i%ual calibration for each element+ co3erin" the entire ran"e for each "roup mentione% in the *able-7 an% *able- 77 ha3e to be pro3i%e%. $t least fi3e stan%ar% samples ha3in" certificate% shoul% be incorporate% for each "roup. Stan%ar% sample use% for calibration shoul% be -); or )$S ma1e certifie% 8eference -aterial. ?referably each "roup shoul% ha3e stan%ar% of same ma1e. plotte% foun% ,in%in" correction coefficient ;ar% copy for each "roup calibrate%+ 'ith abo3e information to be pro3i%e%. $fter stan%ar%ization the instrument shall be han%e% o3er for routine analysis of anlytes. 03.0 Opti&#" emissio spe&t!omete! <
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*t%.+ )o.

Stan%ar% calibration soft'are shoul% capable of %oin" follo'in" Jobs. ?lottin" of calibration cur3es ,in%in" re"ression coefficients -easurin" ra' intensities ?ro3i%in" ori"inal an% calculate% concentration of stan%ar% samples use% for calibration Stan%ar% error of calibration for each "raph Stan%ar% sample ha3in" ma! %e3iation to be

Laboratory Facilities (Imported)


2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. < Des&!iptio *he equipment shall be in a steel plant. 7t computer controlle%+ sin"le < composite *t%.+ )o.

equipment+ floor mounte% type an% suitable for in%ustrial application shall be use% for fast an% accurate analysis of 4u+ 4r+ chemical constituents in steel samples 'ith hi"h accuracy an% precision for simultaneous measurement of elements (4+ -n+ ?+ S+ Si+ $l+ 0i+ -o+ /+ C+ *i+ )+ 0b+ 4o+ $s+ ?b + Sn+ Kn+ Kr+ Sb+ -"+ *e+ 4a+ )i+ 0 + ) from trace le3el to concentration le3el ( in concentration E) in steel lollypop ( %isc-pin type ) samples. *he spectrometer shall be capable of analysin" #&i, so"u$"e an% #&i, i so"u$"e aluminium an% calcium separately. *ypical analytical pro"ram for this spectrometer is in%icate% in *able-777 of this specification. 7t shall also be capable of analysin" small %iameter ro% + 'ire+ scre'+ an% nut + etc. 'ith necessary a%opters. *he spectrometer shall be %esi"ne% to ta1e care of the e!ternal temperature an% humi%ity fluctuations an% shall pro3i%e stable an% accurate analytical results. 7t shall be pro3i%e% 'ith facility for %ata transmission. 7t shall be fully microprocessor ( ?.4. ) controlle%+ %irect rea%in" type an% the entire operation from initiation of spar1 to printin" of analytical results shall be fully automatic. 8ecommen%e% precision requirements of the offere% equipment shall be in line 'ith the stipulations of $S*- . 2 100I (latest re3ision). 7t shall be pre-calibrate%+ co3erin" the entire ran"e from traces to hi"her concentration+ a3ailable in the international stan%ar%s.

Laboratory Facilities (Imported)


2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

Page 1) of 40

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio *he equipment shall consist of the follo'in" maJor components as a combine% unit B Spar1 unit Source unit Optical system $nalytical channels Spectrometer control an% %ata processin" system 4olour monitor >ey boar% an% mouse ?rinter *he spar1 stan% shall consist of a sample hol%in" %e3ice+ a counter electro%e an% mechanism for a%Justin" the analytical "ap. 7t shall be open < close $r"on flushe% 'ith thoriate% *un"sten electro%e to "enerate hi"h 3olta"e spar1 e!citation. shape an% size of samples. *he source unit shall be pro3i%e% 'ith e!citation parameters confi"ure% accor%in" to the analytical pro"ramme. *he optical system of the spectrometer shall consist of entrance slit+ e!it slits+ photomultiplier tubes+ etc. *he optical system shall be stabilise% a"ainst fluctuation in temperature. *he spectrometer shall ha3e hi"h. resolution "ratin" 'ith 3&00 "ro3es<mm or more. *he optical system shall either be a 3acuum optics or inert "as fille% optics an% shall ha3e a focal len"th of (#0 mm ( minimum ) + base% on 8o'lan%:s circle. 7t shall be pro3i%e% 'ith ?hoto -ultiplier *ube ( ?-* ) < 4har"e 4ouple Laboratory Facilities (Imported)
2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

*t%.+ )o.

*he sample stan% shall be flushe% 'ith accommo%ate o%%

an inert "as li1e ar"on. 7t shall be %esi"ne% to

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NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio 6e3ice ( 446 ) base% %etector system or a combination of these t'o %etector system+ 6i"ital 4urrent 4ontrol Source an% facility for *ime 8esol3e% Spectroscopy for better precision+ impro3e% %etection limits+ etc. *he analytical 'a3elen"th ran"e shall be from .<0 m to =00 m o! mo!e: in line 'ith the analytical pro"ram . 6epen%in" on the analytical pro"ramme+ the number of channels shall be %eci%e% by the ten%erer. It s-#"" $e p!o2i,e, 3ite&ess#!% f#&i"ities ( &ompute! s%stem. *t%.+ )o.

i te!f#&i 4) so t-#t it is #$"e to t!# smit # #"%ti&#" !esu"ts ,i!e&t"% to BOF: SR> # , CCP "e2e" II #utom#tio

*he spectrometer shall be pro3i%e% 'ith 1(L colour monitor. *he %ata printer shall be laser type. *he operatin" me%ia shall be Cin%o's X? or latest 3ersion. *he equipment shall be pro3i%e% 'ith facility for %etermination of aci% soluble an% aci% insoluble aluminium an% calcium. *he soft'are pac1a"e shall be Cin%o' base% an% shall inclu%e all pro"rammes 'hich are necessary for control of equipment+ analysis+ %ata processin"+ report ma1in" an% %ata transmission. 7t shall inclu%e B Selection of proper spectrometer parameters an% automatic selection of pro"rams Selection of correct calibration cur3e Selection of stan%ar%isation mo%e+ up%atin" of calibration $utomatic s'itchin" o3er of spectral lines accor%in" to their concentration ran"es

Laboratory Facilities (Imported)


2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

Page 1* of 40

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio -

*t%.+ )o.

6rift correction or a%%iti3e an% multiplicati3e inter elementary correction an% bac1"roun% calculation $nalysis of percenta"e composition an% print out of analytical results 4alculation of stan%ar% %e3iations Stora"e of analytical results $%3ice of incomplete analysis or other errors $3era"e calculation 'ith user control 4alculation for a%%itional statistical %ata ( S6 + 8S6 ) -atrices correction $utomatic chec1in" of repro%ucibility ,la""in" of results beyon% calibration ran"e )a% sample %etection system *ransmission of result to remote printers < terminals $utomatic < user controlle% %ata transmission to e!ternal computers

*he scope of supply shall inclu%e the follo'in" itemsB 7nterface an% soft'are for transmission of analytical results $r"on purifier (sircal) 4onsumables for t'enty four months of operation after commissionin"+ as recommen%e% by manufacturer inclu%in" electro%es+ electro%e cleanin" brush+ 3acuum "rease+ lens+ printer paper+ etc. *ool 1it ( 1 set ) + containin" set of scre' %i3ers+ $llen 1eys+ spanners+ sol%er iron + etc. $r"on cylin%er (2 0os.) purity II.II#E 'ith pipin"s+ re"ulators an% manifol%s ( all 2 0os. ) $r"on purification an% pur"in" system in line 'ith the international < manufacturer stan%ar% Set of international spectro- chemical stan%ar%s ( reference
Page 1+ of 40

Laboratory Facilities (Imported)


2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio sample) ( )$S stan%ar%s)+ co3erin" the analytical pro"ramme+ in%icate% in *able-777. One set of set . up stan%ar% for stan%ar%ization an% re calibration ?ersonal 4omputer ( 4ore 2 6uo < latest processor ) 'ith 1( inch *,* colour monitor + ;66 of 1&0 F) or more an% 6/6 C<8 9?S system for optical emission spectrometer 9?S ( 1.0 1/$ or more ) for ?4+ monitor an% printer 6- printer + $3 size *ool 1it 'ith 6-Stan%ar% samples for calibration for ma!imum an% minimum concentration ran"e as per analytical pro"ramme shall be supplie% in line 'ith the rele3ant $S*-<)S stan%ar%. 4omplete set of electrical %ia"rams (in 2n"lish lan"ua"e) of the instrument+ its accessories an% printe% circuit boar%s shoul% be "i3en alon" 'ith the instrument. 8#!!# tee # , suppo!t *he instrument a% its accessories < au!iliaries shoul% ha3e minimum fi3e years 'arranty. *he spectrometer an% its all parts shoul% ha3e inspection certificate from its principal. Supplier shoul% "i3e "uarantee that the spare parts 'ill not be obsolete for ne!t 1# years operation an% Ser3ice -anuals B full sets in 2n"lish shoul% be "i3en alon" 'ith the instrument. I st#""#tio : Commissio i 4: Demo st!#tio 9 7nstallation+ commissionin" an% %emonstration shoul% be %one an% trainin" shoul% be "i3en. $ll elements in each "roup mentione% in the *able-777 shoul% be %emonstrate% for as1e%
Page 1, of 40

*t%.+ )o.

Laboratory Facilities (Imported)


2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio ran"e. ?re-requisites for installation an% commissionin" shoul% be "i3en after placement of or%er. *rainin" on operation+ maintenance an% calibration to be pro3i%e% at site. 5ist of users (?referably in steel plant) since year 2000 to be pro3i%e%. C#"i$!#tio : St# ,#!,i;#tio # , Routi e A #"%sis 9 7n%i3i%ual calibration for each element+ co3erin" the entire ran"e for each "roup mentione% in the *able-777 has to be pro3i%e%. $t least fi3e stan%ar% samples ha3in" certificate% shoul% be incorporate% for each "roup. Stan%ar% sample use% fro calibration shoul% be -); or )$S ma1e 4ertifie% 8eference -aterial. ?referably each "roup shoul% ha3e stan%ar%s of same ma1e. $fter stan%ar%ization the instrument shall be han%e% o3er for routine analysis of anlytes. 03.0 3 Simu"t# eous &#!$o 0su"p-u! # #"%;e! 7t shall be microprocessor controlle% an% shall be use% for rapi%+ accurate an% simultaneous %etermination of carbon an% sulphur content in blast furnace hot metal+ steel samples+ ferro-alloys+ 4opper-alloys+ $luminium alloy+ 4arbi%es+ ceramics+ san%+ ores+ etc. 7t shall basically consist of hi"h po'er in%uction furnace+ analyser an% control console. $nalytical results shall appear %irectly in 'ei"ht percent of carbon an% sulphur. *he %etection metho% shall be infra-re% absorption for both carbon an% sulphur. B!o#, p#!#mete!s of equipme t Laboratory Facilities (Imported)
2009 MEC ! Limite"# $ll %ig&ts %eser'e"( Page 1- of 40

*t%.+ )o.

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio 8an"e ('ith 1" sample) 4arbon B 0.& ppm to &.00E Sulphur B 0.& ppm to 0. 0E P!e&isio 4arbon Sulphur B 0.3 ppm or 0.#E 8S6+ 'hiche3er is "reater B 0.3 ppm or 0.#E 8S6+ 'hiche3er is "reater *t%.+ )o.

8ea%ability B 0.001 ppm *he equipment shall be quote% alon" 'ith the follo'in" itemsB manufacturer 4onsumables < operatin" supplies require% for 1000 analyses+ as recommen%e% by the manufacturer *'o (2) 0os. of "as cylin%er+ one each for o!y"en (purity II.#E) an% instrument quality compresse% air 'ith pipin"+ re"ulator an% manifol%. 4alibration samples One 0o. sample cuttin" %e3ice for cuttin" of pin portion (1.0" sample) from lollypop sample+ 'ith abrasi3e %isc 1it+ recommen%e% cuttin" 'heel Silicon 4arbi%e to re%uce heat "eneration. 0 Laboratory Facilities (Imported)
2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

7nterface an% soft'are for %ata transmission Spares for 2 years of operation an% maintenance+ as recommen%e% by the manufacturer 4ommissionin" spares+ as recommen%e% by the

Stan%ar% accessories an% items as recommen%e% by the manufacturer

/olta"e stabiliser of require% capacity (in%i"enous


Page 19 of 40

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio ma1e) $ny other item 'hich is not mentione% in this specification but is require% for smooth an% proper functionin" of the equipment for the inten%e% purpose. *he %eterminator must incorporate must incorporate pro"rammable automatic 6ual Kone cleanin" mechanism for both -etal ,ilter an% combustion tube remo3al 3acuum cleaner en3ironment. *he equipment shall be complete in all respects inclu%in" cablin" an% special earthin" if require% It s-#"" $e p!o2i,e, 3it- e&ess#!% f#&i"ities (&ompute! i te!f#&i 4) so t-#t it is #$"e to t!# smit # #"%ti&#" !esu"ts ,i!e&t"% to BOF: SR> # , CCP "e2e" II #utom#tio s%stem. 8#!!# tee # , Suppo!t. *he instrument an% its accessories < au!iliaries shoul% ha3e minimum fi3e years 'arranty. *he spectrometer an% its all parts shoul% ha3e inspection certificate from its principal. Supplier shoul% "i3e "uarantee that the spare parts 'ill not be obsolete for ne!t 1# years from the %ate of supply of the equipment. Operation an% ser3ice -anuals alon" 'ith the instrument. Laboratory Facilities (Imported)
2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

*t%.+ )o.

full sets in 2n"lish shoul% be "i3en

Page 20 of 40

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio *t%.+ )o.

I st#""#tio : Commissio i 4: Demo st!#tio 9 7nstallation+ commissionin" an% %emonstration shoul% be %one an% trainin" shoul% be "i3en. $ll elements in each "roup mentione% in )oar% ?arameters of 7nstrument shoul% be %emonstrate% for as1e% ran"e. ?re-requisites for installation an% commissionin" shoul% be "i3en after placement of or%er. *rainin" on operation+ maintenance an% calibration to be pro3i%e% at site. 5ist of users (?referably in steel plant) since year 2000 to be pro3i%e%. C#"i$!#tio : St# ,#!,i;#tio # , Routi e A #"%sis 9 7n%i3i%ual calibration for each element+ co3erin" the entire ran"e for each "roup mentione% in the )oar% ?arameters of 7nstrument has to be pro3i%e%. $t least fi3e stan%ar% samples ha3in" certificate shoul% be incorporate% for each "roup. Stan%ar% sample use% for calibration shoul% be -); or )$S ma1e 4ertifie% 8eference -aterial. $fter stan%ar%ization the instrument shall be han%e% o3er for routine analysis of anlytes. 03.0 6 Simu"t# eous o?%4e 0 it!o4e # #"%se! *he equipment shall be use% for rapi%+ accurate an% simultaneous Laboratory Facilities (Imported)
2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

Page 21 of 40

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio %etermination of o!y"en an% nitro"en content in steel samples. *he analytical operation of the equipment shall be microprocessor controlle% an% analytical results shall appear %irectly in 'ei"ht percent of o!y"en an% nitro"en. *he equipment shall basically consist of the follo'in" main 2lectro%e furnace $nalytical unit 4ontrol console unitsB *t%.+ )o.

*he electro%e furnace shall be able to "enerate uniform an% controllable temperature up to 3000o4. 7t shall be pro3i%e% 'ith appropriate sensors an% microprocessor electronics 'hich shall ensure repro%ucible fusion con%itions for each sample. *he electro%e system shall be %esi"ne% in such a 'ay that only the electro%e tip assembly nee%s replacement in case of occurrence of 'ear. *he crucible shall be raise% pneumatically to ensure uniform contact pressure 'ith the upper electro%e. *he electro%e furnace shall be pro3i%e% 'ith soli% state in%icators at the front panel for important electrical parameters. 2!ternal chiller for the furnace shall be offere% as an optional item. *he analytical unit shall contain the basic analytical system inclu%in" a thermal con%ucti3ity %etector for nitro"en %etermination an% an infra-re% %etector for o!y"en %etermination+ a "as flo' system 'ith controllers+ an inte"ral balance 'ith automatic 'ei"ht compensation an% all the instrument electronics. *he control console shall control the instrument functions throu"h touch Laboratory Facilities (Imported)
2009 MEC ! Limite"# $ll %ig&ts %eser'e"( Page 22 of 40

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio 1ey boar% an% shall consist of 3isual %isplay unit for %irect %i"ital %isplay of o!y"en an% nitro"en content+ operatin" calibration an% ser3ice information+ automatic printer for permanent recor% of o!y"en an% nitro"en content+ etc. *he equipment shall ha3e automatic-cum-manual calibration facility. *he calibration shall not 3ary more than 1E in a 'ee1. *he equipment shall ha3e an au%io alarm system 'hich shall %isplay the cause of alarm an% the analytical cycle 'oul% not function till the cause of the alarm is rectifie%. M#5o! p#!#mete!s of t-e equipme t R# 4e ('ith 1" sample) O!y"en 0itro"en P!e&isio O!y"en 0itro"en B B B B 0.0# ppm to 1E 0.0# ppm to 0.#E 0.02# ppm or 0.#E 8S6+ 'hiche3er is "reater 0.02# ppm or 0.#E 8S6+ 'hiche3er is "reater *t%.+ )o.

*he equipment shall be quote% alon" 'ith the follo'in" itemsB 7nterface an% soft'are for %ata transmission Spares for 2 years of operation an% maintenance+ as recommen%e% by the manufacturer 4ommissionin" spares+ as recommen%e% by the manufacturer 4onsumables < operatin" supplies + require% for 1000 analyses+ as recommen%e% by the manufacturer Si! numbers of "as cylin%er+ t'o each for nitro"en (purity II.IIE)+ carbon %io!i%e (purity II.II#E) : helium (purity
Page 2) of 40

Laboratory Facilities (Imported)


2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio II.II#E) an% instrument quality compresse% air 'ith pipin"+ re"ulators an% manifol%s. 4alibration samples One 0o. of sample cuttin" %e3ice for cuttin" of pin portion ( 1.0 " sample ) from lollypop sample+ 'ith abrasi3e %isc 1it. 8ecommen%e% cuttin" 'heel is Silicon 4arbi%e to re%uce heat "eneration. *'o 0os. of special type of scissor (for cuttin" of sample 'ithout heat "eneration) shall also be offere%. *'o 0os. of special type of file to remo3e impurities from the sample surface+ for sample preparation Stan%ar% accessories an% items as recommen%e% by the manufacturer /olta"e stabiliser of require% capacity (in%i"enous ma1e) $ny other item 'hich is not mentione% in this specification but is require% for smooth an% proper functionin" of the equipment for the inten%e% purpose. *he supply shoul% inclu%e pro"rammable automation cleaner for cleanin" both 5o'er @ 9pper electro%es simultaneously after each sample analysis. *he equipment as a 'hole an% analysis proce%ure shall conform strictly to latest $S*- specification. *he instrument shall be supplie% 'ith a set of international stan%ar% samples an% a number of settin" up samples (S9S) an% control stan%ar%s. *he instrument shall be factory calibrate% an% the %ata of the calibration shall be submitte% before pac1in" of the instrument of facilitate the user for conformin" the accuracy+ ran"e+ result
Page 24 of 40

*t%.+ )o.

Laboratory Facilities (Imported)


2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio format etc. *he instrument shall ha3e multi-point calibration facility. *he equipment shall be complete in all respects inclu%in" cablin" an% special earthin" if require% an% a set of international stan%ar% samples for calibration. It s-#"" $e p!o2i,e, 3it- e&ess#!% f#&i"ities ( &ompute! i te!f#&i 4) so t-#t it is #$"e to t!# smit # #"%ti&#" !esu"ts ,i!e&t"% to BOF: SR> # , CCP "e2e" 0II #utom#tio 8#!!# tee # , Suppo!t. *he instrument an% its accessories < au!iliaries shoul% ha3e minimum fi3e years 'arranty. *he spectrometer an% its all parts shoul% ha3e inspection certificate from its principal. Supplier shoul% "i3e "uarantee that the spare parts 'ill not be obsolete for ne!t 1# years from the %ate of supply of the equipment. Operation an% ser3ice -anuals alon" 'ith the instrument. I st#""#tio : Commissio i 4: Demo st!#tio 9 7nstallation+ commissionin" an% %emonstration shoul% be %one an% trainin" shoul% be "i3en. $ll elements in each "roup mentione% in )oar% ?arameters of 7nstrument shoul% be %emonstrate% for as1e% ran"e. ?re-requisites for installation an% commissionin" shoul% be "i3en after Laboratory Facilities (Imported)
2009 MEC ! Limite"# $ll %ig&ts %eser'e"( Page 2* of 40

*t%.+ )o.

s%stem.

full sets in 2n"lish shoul% be "i3en

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio placement of or%er. *rainin" on operation+ maintenance an% calibration to be pro3i%e% at site. 5ist of users (?referably in steel plant) since year 2000 to be pro3i%e%. *t%.+ )o.

C#"i$!#tio : St# ,#!,i;#tio # , Routi e A #"%sis 9 7n%i3i%ual calibration for each element+ co3erin" the entire ran"e for each "roup mentione% in the )oar% ?arameters of 7nstrument has to be pro3i%e%. $t least fi3e stan%ar% samples ha3in" certificate shoul% be incorporate% for each "roup. Stan%ar% sample use% for calibration shoul% be -); or )$S ma1e 4ertifie% 8eference -aterial. $fter stan%ar%ization the instrument shall be han%e% o3er for routine analysis of anlytes. 03.0 @ Autom#te, -%,!o4e ,ete!mi #to! *he equipment shall be use% for rapi% an% accurate %etermination of hy%ro"en content in steel samples. *he analytical operation of the equipment shall be microprocessor controlle% an% analytical results shall appear %irectly in ppm of hy%ro"en. 7t shall analyse both %iffusible an% resi%ual hy%ro"en. *he equipment shall basically consist of the follo'in" main units. .

Laboratory Facilities (Imported)


2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

Page 2+ of 40

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio 8esistance furnace $nalyser alon" 'ith *hermal 4on%ucti3ity 6etector 4ontrol console 4omputer an% printer *t%.+ )o.

*he furnace shall be resistance furnace+ current+ po'er an% temperature controlle%. 6etector shall be *hermal 4on%ucti3ity type. B!o#, p#!#mete!s of t-e equipme t 8an"e ('ith 1" sample) B 0.1 ppm to #0 ppm or more ?recision 8ea%ability B 0.02 ppm or 2.0E 8S6+ 'hiche3er is "reater B 0.001 ppm

*he equipment shall be quote% alon" 'ith the follo'in" itemsB 7nterface an% soft'are for %ata transmission Spares for 2 years of operation an% maintenance+ as recommen%e% by the manufacturer 4ommissionin" spares+ as recommen%e% by the manufacturer 4onsumables < operatin" supplies require% for 1000 analyses inclu%in" special e3acuate% quartz probes for sample collection for %etermination of resi%ual an% %iffusible hy%ro"en+ as recommen%e% by the manufacturer 4alibration samples *'o numbers of nitro"en "as cylin%er+ (purity II.IIE) an% instrument quality compresse% air (2 0os. of cylin%er ) 'ith pipin"+ re"ulators an% manifol%s 4alibration samples
Page 2, of 40

Laboratory Facilities (Imported)


2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio Stan%ar% accessories an% items as recommen%e% by the manufacturer /olta"e stabiliser of require% capacity (in%i"enous ma1e) 4omputer 'ith colour monitor+ 1eyboar% an% printer $ny other item 'hich is not mentione% in this specification but is require% for smooth an% proper functionin" of the equipment for the inten%e% purpose. ,acilities shoul% be pro3i%e% to control @ monitor carrier "as flo' alon" 'ith necessary traps for remo3in" moisture+ hy%ro"en+ an% other hy%rocarbons from the carrier "as. *hermal con%ucti3ity %etector 'ith impro3e% si"nal to noise ratio+ lo'er %etection limit+ impro3e% stability an% e!pan%e% %ynamic ran"e shall be use% for %eterminin" hy%ro"en content. 6etector si"nal shall be automatically processe% to percenta"e concentration an% %isplaye% on the instrument panel an% also printe% out simultaneously. 7nstrument shall be capable of stan%ar%+ -ulti-point @ "as %ose% calibration. $utomatic 'ei"ht compensation %urin" instrument calibration as 'ell as for un1no'n sample analysis shall be a stan%ar% feature of the instrument. *he instrument shall be supplie% 'ith a set of international stan%ar% samples an% a number of settin" .up samples (S9S) an% control stan%ar%s. *he equipment as 'hole an% analysis proce%ure shall conform strictly to latest $S*- Specification. Supply shall be complete in all respect an% all optional items necessary to achie3e %esire% instrumental performance shoul% be inclu%e% in the offer. Laboratory Facilities (Imported)
2009 MEC ! Limite"# $ll %ig&ts %eser'e"( Page 2- of 40

*t%.+ )o.

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio It s-#"" $e p!o2i,e, 3ite&ess#!% f#&i"ities ( &ompute! s%stem. *t%.+ )o.

i te!f#&i 4) so t-#t it is #$"e to t!# smit # #"%ti&#" !esu"ts ,i!e&t"% to BOF: SR> # , CCP "e2e" II #utom#tio 8#!!# tee # , Suppo!t. *he instrument an% its accessories < au!iliaries shoul% ha3e minimum fi3e years 'arranty. *he spectrometer an% its all parts shoul% ha3e inspection certificate from its principal. Supplier shoul% "i3e "uarantee that the spare parts 'ill not be obsolete for ne!t 1# years from the %ate of supply of the equipment. Operation an% ser3ice -anuals alon" 'ith the instrument. I st#""#tio : Commissio i 4: Demo st!#tio 9 7nstallation+ commissionin" an% %emonstration shoul% be %one an% trainin" shoul% be "i3en. $ll elements in each "roup mentione% in )oar% ?arameters of 7nstrument shoul% be %emonstrate% for as1e% ran"e. ?re-requisites for installation an% commissionin" shoul% be "i3en after placement of or%er. *rainin" on operation+ maintenance an% calibration to be pro3i%e% at site. full sets in 2n"lish shoul% be "i3en

Laboratory Facilities (Imported)


2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

Page 29 of 40

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio 5ist of users (?referably in steel plant) since year 2000 to be pro3i%e%. C#"i$!#tio : St# ,#!,i;#tio # , Routi e A #"%sis 9 7n%i3i%ual calibration for each element+ co3erin" the entire ran"e for each "roup mentione% in the )oar% ?arameters of 7nstrument has to be pro3i%e%. $t least fi3e stan%ar% samples ha3in" certificate shoul% be incorporate% for each "roup. Stan%ar% sample use% for calibration shoul% be -); or )$S ma1e 4ertifie% 8eference -aterial. $fter stan%ar%ization the instrument shall be han%e% o3er for routine analysis of anlytes. 0A.0 B S3i 4 4!i ,i 4 mi"" *he equipment shall be use% for pul3erisin" materials li1e steelma1in" sla"+ iron ore+ limestone+ calcine% lime+ ra' %olomite+ burnt %olomite+ Si-n+ ,e-Si+ ,e--n+ ,e-/+ ,e-0b + ,e-/ an% other ferro-alloys+ etc.+ for "ettin" uniform composition for X-ray spectrometric analysis. 7t shall consist of a bo'l+ a rin" an% a hammer. *he sample shall be 1ept in the space bet'een the bo'l+ rin" an% hammer. *he top of the bo'l shall be close% an% it shall be clampe% on a 3ibratory platform 'hich shall impart 1inetic ener"y to the rin" an% hammer. *he "rin%in" 3essel shall be of 100 cc 3olume. -aterial of construction of "rin%in" 3essel shall be tun"sten carbi%e (2 for each machine) an% chrome steel (& 0os. for each machine). *he mill an% the %ri3e mechanism shall be house% in a suitable metallic . *t%.+ )o.

Laboratory Facilities (Imported)


2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

Page )0 of 40

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio enclosure so that not much noise is "enerate%. *he sample "rin%in" area shall be co3ere% by a li% 'hich can be lifte% an% close% easily for operatin" safely. One electronic<electromechanical timer shall be pro3i%e% for automatically stoppin" the mill after a preset perio% of operation. *he actual time count%o'n shall also be %isplaye%. *he timer shall ha3e %ust proof co3erin" an% tactile 1eys<1nobs for easy settin" of time. *he transmission of rotational force require% shall be throu"h sprin"s of a%equate stren"th. 7t Shall ha3e auto trippin" on motor o3er loa% for safety of motor. 7t shall ha3e enou"h electrical capacity to 'or1 continuously. 7t shall ha3e enou"h spee% for pul3erizin" the sample to the require% size for the set time. 7t shall also be pro3i%e% start an% stop button. 7t shall be pro3i%e% 'ith safety s'itches to pre3ent start of the operation if li% is open. *he input size shall be (-) # mm an% the output size of the sample shall be less than 200 mesh+ suitable for briquettin". *he scope of supply shall inclu%e spares for t'o years of operation an% maintenance+ commissionin" spares+ stan%ar% accessories+ foun%ation bolts+ initial fill of oil an% "rease+ starter an% s'itch fuse unit+ consumables for three months of operation after commissionin" an% any other item 'hich is not mentione% in this specification but is require% for smooth an% proper functionin" of the equipment for the inten%e% purpose. 8#!!# tee # , Suppo!t. *he instrument an% its accessories < au!iliaries shoul% ha3e minimum fi3e years 'arranty from %ate of supply. 03.0 B!iquetti 4 p!ess .
Page )1 of 40

*t%.+ )o.

Laboratory Facilities (Imported)


2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. A Des&!iptio *he equipment shall be use% for preparin" pellets from po'%ere% samples for X-ray spectrometric analysis. ?ressure shall be applie% to a %ie fi!e% to a cross-arm by means of an electro-hy%raulic system. *here shall be pro3ision for a%Justin" the press force from 0 to 0 tf. $ timer shall be pro3i%e% for applyin" the pre-set pressure for pre-set perio% of time. *hus a time limit relay shall automatically s'itch-off the po'er supply to the hy%raulic pump after the lapse of the pre-set time. *he timer shall also in%icate the countin" of time from start to en%. 7t shall be pro3i%e% 'ith %ust proof co3erin" an% tactile 1eys < 1nobs for easy settin" of time. *he scope of supply shall inclu%e #00 0os. of aluminium cups for initial perio% an% bin%in" material of # 1" for facilitatin" compaction. ;o'e3er+ the bin%er material shall be such that it %oes not interfere 'ith the analytical 'or1. *he hy%raulic oil use% for the pressin" ener"y shall be easily a3ailable an% shall be of correct "ra%e to support pressin" of the concerne% material for the set time in or%er to "enerate a "oo% sample surface for X8, analysis. *he pressin" pressure shall not be affecte% by the temperature of the oil. *he top li% of the press tool shall be capable of bein" fi!e% ti"htly onto the sample 'ith the help of a scre' mechanism. 7t shall be pro3i%e% 'ith facility for remo3al < fittin" of the press tools ha3in" %ifferent %iameters. *he scope of supply shall inclu%e spares for t'o years of operation an% Laboratory Facilities (Imported)
2009 MEC ! Limite"# $ll %ig&ts %eser'e"( Page )2 of 40

*t%.+ )o.

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


S". )o. Des&!iptio maintenance+ commissionin" spares+ stan%ar% accessories+ foun%ation bolts+ initial fill of oil an% "rease+ starter an% s'itch fuse unit+ consumables for three months of operation after commissionin" an% any other item 'hich is not mentione% in this specification but is require% for smooth an% proper functionin" of the equipment for the inten%e% purpose. *he ten%erer shall stan% "uarantee for the o3erall performance of the equipment co3ere% un%er this specification. 8#!!# tee # , Suppo!t. *he instrument an% its accessories < au!iliaries shoul% ha3e minimum fi3e years 'arranty from %ate of supply.
T#$"e0I T%pi&#" # #"%ti&#" p!o4!#m fo! seque ti#" /0!#% f"uo!es&e &e spe&t!omete! Bu! t Stee" m#7i 4 Spo 4e 'ot met#" Bu! t "ime I!o o!e ,o"omite s"#4 i!o 0.20 -#.00 0.10 -2.00 0.10-2.00 0.00# . 1.00 0.0# . 1.00 &#.0 .I0.0 1.0- #.0 0.10-10.0 #.0 . ##.0 30.0- 0.0 0.10 . 10.0 3#.00-&0.00 &.00 . 1#.00 12.00 . 20.00 2.00. .00 0.10-0.# 0.01-0.0# 0.10-1.00 0.01 . 0.0# 0.02 - 0.10 0.#0 . #.00 1.00 . 2.00

*t%.+ )o.

E"eme t 4 Si -n S ? 0i $l 4aO -"O SiO2

Fe!!o0 i&7e" 0.01 . 0.10 0.10 . 0.G0 0.10 . 0.G0 0.01 . 0.0G 0.01 . 0.0G

Laboratory Facilities (Imported)


2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

Page )) of 40

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


E"eme t $l2O3 ,e ,eO ?2O# -nO 0i 'ot met#" Bu! t "ime 2.0 . &.0 Bu! t ,o"omite 1.00 .&.0 Stee" m#7i 4 s"#4 0.# . 3.0 1#.0 .2#.0 0.#0 .3.0 3.00 .(.0 Spo 4e i!o 1.#0. 3.0 G0.00 . I2.00 10.0.13.0 I!o o!e Fe!!o0 i&7e"

1.00 . 2.00 &0.00 . &(.00 0.00 . #0.00 0.00 . #0.00

T#$"e0I ( &o t,. ) E"eme t 4 Fe!!o ( Fe!!o0 tit# ium $o!o 0.10 . 10.00 0.10 . #.00 0.01 -0.G0 0.01 -0.G0 3.00 . (.00 3#.00 . 0.00 0.01 . 0.G0 0.01 . 0.G0 3.00 (.00 0.10 -10.00 0.10 -#.00 Fe!!o0 m# 4# ese 0.10-10.00 Fe!!o0 si"i&o 0.10 . 10.00 &#-(# 0.#0 . #.00 0.010.G0 0.01 . 0.G0 0.#0 3.00 1.00 . #.00 0.10 . 0.G0 Si"i&o0 Fe!!o Fe!!o0 m# 4# ese 0&-!omium 2# #,ium 0.10-3.00 0.0#-(.00 0.10 . #.00 1.00 . #.00 0.10 . 1.00 0.01 . 0.G0 0.01 . 0.G0 0.01 . 0.20 0.10 . 0.#0 0.01 . 0.G0 0.01 . 0.G0 Fe!!o0 )io$ium 1.00. 3.#0 1.00 . #.00 Fe!!o mo"%$,e um 0.10 . 10.00

Si -n S ? 0i $l *i

0.#0-3.00 &#.0-(#.0 0.01-0.G0 0.01-0.G0

12.0-30.0 G.0-(G.0 0.01-0.G0 0.01-0.G0

1.00 . (.00 0.01-0.G0 0.10-0.G0

1.00 . #.00

Laboratory Facilities (Imported)


2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

Page )4 of 40

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


) 4r / 0b -o ,e )alance )alance )alance )alance )alance )alance )alance 1#.00 . 20.00 &0.00 . G0.00 (0.00 . G0.00 #0.00 . (#.00 1.00 . 3.00 )alance ##.00 . (0.00 )alance

T#$"e0II

'i4- A. ( B!i&7s 9 E"eme t + Compou , $l2O3 ,e2O3 *iO2 4aO -"O 0a2O >2O Lo3 A. ( B!i&7s 9 Laboratory Facilities (Imported)
2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

R# 4e C (0 .0 . IG.0 0.0 . 3.# 0.0 . 3.# 0.0 . 3.0 0.0 . 2.0 0.0 . 2.0 0.0 . 2.0

A&&u!#&% 1.00 0.10 0.10 0.10 0.10 0.10 0.10

Page )* of 40

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


E"eme t + Compou , $l2O3 ,e2O3 *iO2 4aO -"O 0a2O >2O Si"i&# B!i&7s 9 E"eme t + Compou , SiO2 ,e2O3 *iO2 4aO -"O 0a2O >2O C! 0 M#4 esi# 9 E"eme t + Compou , 4r ,e2O3 -"O R# 4e C 30 .0 . (0.0 0.0 . 3.0 0.0 . 3.# 0.0 . 3.0 0.0 . 2.0 0.0 . 2.0 0.0 . 2.0 R# 4e C G0 - IG 0.0 . 3.# 0.0 . 3.# 0.0 . 3.0 0.0 . 2.0 0.0 . 2.0 0.0 . 2.0 R# 4e C 10 . 30 0.0 . 1# 0.0 . (0 A&&u!#&% 1.00 0.10 0.10 0.10 0.10 0.10 0.10 A&&u!#&% 1.00 0.10 0.10 0.10 0.10 0.10 0.10 A&&u!#&% 1.00 1.00 1.00

L#,"e s"#4 9 E"eme t + Compou , SiO2 ,e (element) 4aO -nO -"O $l2O3 S"i,e D#te S# , 9 Laboratory Facilities (Imported)
2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

R# 4e C #. # 0 . 20 # . #0 3 . 30 0 . 1# 0- 0

A&&u!#&% 1.00 1.00 1.00 1.00 1.00 1.00

Page )+ of 40

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


E"eme t + Compou , SiO2 4r2O3 $l2O3 ,e2O3 Co ti uous C#sti 4 Po3,e! 9 E"eme t + Compou , SiO2 $l2O3 4aO 4 , Pet!o"eum Co7e As- 9 E"eme t + Compou , $l2O3 ,e2O3 4aO -"O 0a2O >2O SiO2 ? S R# 4e C #0 . G# # . 2# 0 . 10 0.0 . #.0 R# 4e C 1# . 0 0 . 2# 1# . 0 0 . 20 0-# R# 4e C 10 . 0 0.00 . 1# 0.0 . 1# 0.0 . 10 0.0 . 2.0 0.0 -3.0 30 . (0 0.2 0-2 A&&u!#&% 1.00 1.00 0.#0 0.#0 A&&u!#&% 1.00 1.00 1.00 1.00 0.10 A&&u!#&% 1.00 0.#0 0.#0 0.#0 0.10 0.10 1.00 0.1 0.1

F"% As- 9 E"eme t + Compou , $l ,e 4a 0a > S Laboratory Facilities (Imported)


2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

R# 4e C 10 . 1# 0.00 . 1# 0.0 . 10 0.0 . #.0 0.0 . #.0 10 - 30

A&&u!#&% 1.00 1.00 0.#0 0.#0 0.#0 1.00


Page ), of 40

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


SMS S"u,4e 9 E"eme t + Compou , SiO2 $l2O3 4aO -"O ,e2O3 4

R# 4e C #. 0 0 . 2# 1# . 0 # . 10 0.00 - 1# 0 - 20

A&&u!#&% 1.00 1.00 1.00 0.#0 0.#0 1.00

T#$"e 0 III T%pi&#" # #"%ti&#" p!o4!#mme of opti&#" emissio spe&t!omete! S". E"eme t Co &e t!#tio !# 4e (3ei4-t pe!&e t#4e)

Laboratory Facilities (Imported)


2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

Page )- of 40

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


)o. 01. 02. 03. 0 . 0# 0&. 0(. 0G. 0I. 10. 11. 12. 13. 1 . 1#. 1&. 1(. 1G. 1I. 20. 21. 22. 23. 2 . 2#. 23. 2 . 2#. 4arbon -an"anese ?hosphorous Sulphur Silicon $luminium 4hromium 0ic1el /ana%ium -olyb%enum *itanium *un"sten 4obalt 4opper 0iobium 4alcium Kinc Kirconium $ntimony )ismuth $rsenic )oron 0itro"en -a"nesium *in 5ea% *ellurium ,e ( matri! ) Mi 0.001 0.1 0.0003 0.0003 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.0001 0.0001 0.0001 0.0001 0.0001 0.0001 0.0001 0.000# 0.0001 0.0001 0.0001 0.0001 M#?. #.00 2#.00 1.#0 0.#0 G.00 #.00 3#.00 0.00 10.00 10.00 2.00 2#.00 10.00 #.00 3.00 0.10 0.10 0.30 0.#0 0.30 0.30 0.#0 0.#0 0.30 0.30 0.30 0.10

D#t# + i fo!m#tio to $e fu! is-e, $% t-e te ,e!e!

Laboratory Facilities (Imported)


2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

Page )9 of 40

NEELACHAL ISPAT NIGAM LIMITED


TECHNICAL SPECIFICATION FOR LABORATORY EQUIPMENT

(PHASE II) IMPORTED EQUIPMENT


i) 6etails of all the equipment offere%+ printe% catalo"ues+ %escripti3e literature an% Feneral $rran"ement %ra'in" for each equipment in%icatin" ma1e an% mo%el offere%+ list of spares an% essential accessories ii) iii) 5ist of users (preferably in certificate $ny %e3iation from the *S in%icatin" clause number of the *S an% reasons for such %e3iations steel plants) for each equipment alon" 'ith user

Laboratory Facilities (Imported)


2009 MEC ! Limite"# $ll %ig&ts %eser'e"(

Page 40 of 40

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