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03. List of equipme t # , $!o#, spe&ifi&#tio fo! "#$o!#to!% f#&i"ities ( P-#se ( II ) S". )o. 03.0 . Des&!iptio /0!#% f"uo!es&e &e spe&t!omete! (seque ti#" t%pe) *he equipment shall be use% for sequential analysis of chemical constituents in the samples of hot metal+ burnt lime+ calcine% %olomite+ iron ore lump+ spon"e iron+ )O, sla" + Si--n+ ,e-Si+ ,e--n+ ,e . *i+ ,e-/+ ,e-0b+ ,e-) an% other ferro-alloys in the steel ma1in" unit of an inte"rate% steel plant. ,or analysis of hot metal samples+ typical precision of analysis of the offere% equipment shall be in line 'ith the stipulations of $S*- 2-322+ (latest e%ition). *he X-ray fluorescence spectrometer
shall be pro3i%e% 'ith facilities for analysis of C#!$o # , Bo!o + hi"h alumina bric1s+ lo' alumina bric1s+ silica bric1s+ la%le sla"+ sli%e "ate san%+ continuous castin" po'%er+ petroleum co1e ash+ fly ash+ S-S slu%"e+ lime stone+ %olomite either by pro3i%in" t'o number of fi!e% channels for %etermination of 4arbon an% )oron + hi"h alumina bric1s+ lo' alumina bric1s+ silica bric1s+ la%le sla"+ sli%e "ate san%+ continuous castin" po'%er+ petroleum co1e ash+ fly ash+ S-S slu%"e+ lime stone+ %olomite or throu"h pro3ision of separate crystals for analysis of 4arbon an% )oron + hi"h alumina bric1s+ lo' alumina bric1s+ silica bric1s+ la%le sla"+ sli%e "ate san%+ continuous castin" po'%er+ petroleum co1e ash+ fly ash+ S-S slu%"e+ lime stone+ %olomite. 2lement-'ise 5o'er 5imit of 6etection (5.5.6.) fi"ures
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an% accuracy fi"ures for X-ray ,luorescence Spectrometer at Laboratory Facilities (Imported)
2009 MEC ! Limite"# $ll %ig&ts %eser'e"( Page 2 of 40
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0ecessary har%'are an% soft'are for remote %ia"nostic facility shall be pro3i%e%. *he combination of 1/ an% m$ 3alues for ;* "enerator shall be selecte% by the equipment supplier < manufacturer+ 1eepin" in 3ie' the analytical pro"ram+ the precision an% accuracy of analysis. Selection of slit 'i%th+ crystal+ %etector+ collimator+ primary beam filter (*i)+ flo' counter+ 'in%o' (of minimum thic1ness)+ etc. shall be optimum to pro3i%e ma!imum intensity an% spectral resolution. *he repro%ucibility+ precision an% accuracy of analysis for each element shall be finishe% in tabular form. *he e!citation con%itions+ the "eometry an% X-ray optics of the spectrometer shall pro3i%e for lar"e si"nal to bac1"roun% ratio+ stable an% repro%ucible results an% lo' %etection limits
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*he ten%erer shall "uarantee for the tube life an% pro3i%e certificate for a minimum perio% of 12 months. *he X-ray tube shall be manufacture% by the supplier of the X-ray spectrometer. X-ray tube coolin" B 4lose% circuit+ usin" %eionise% 'ater ;* "enerator B ,ull 'a3e rectification+ ratin" .0 1C (min.) 120 m$ (min.)+ stability of tube current an% tube 3olta"e shall be D0.0001E for D1E fluctuations in input 3olta"e an% current. 7t shall support iso-'att s'itchin". Laboratory Facilities (Imported)
2009 MEC ! Limite"# $ll %ig&ts %eser'e"( Page + of 40
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Cou ti 4 # , &o t!o" e"e&t!o i&s 7tems to be controlle% B$ll mechanical motions+ controls+ linearity of countin" up to 1.# million counts per secon% or better an% %ata transfer. 6ea% time correction ,ast an"ular rotation 7nte"ration time -emory bac1-up Compute! s%stem (-#!,3#!e ) 7t shall be pro3i%e% 'ith 4ore 2 6uo < ?entium processor 'ith latest 3ersion alon" 'ith 1( inch *,* colour monitor+ ;66 of 2#0 F) an% 6/6 Criter < 8ea%er. 7t shall be pro3i%e% 'ith full 1ey boar% 'ith a%%itional function 1eys+ mouse+ 8S 2324 interface+ -icrosoft Cin%o's of latest 3ersion+ etc. Compute! soft3#!e *he soft'are pac1a"e shall be comprehensi3e an% shall inclu%e all pro"rammes 'hich are necessary for control of equipment+ analysis+ online an% off-line %ata processin"+ report ma1in" an% %ata transmission+ etc. 7n "eneral+ it shall inclu%e. - )ac1 "roun% correction @ %rift correction Laboratory Facilities (Imported)
2009 MEC ! Limite"# $ll %ig&ts %eser'e"(
B )etter than 20 nano- secon%s B H20000<minute or better B 0.1 . III sec B *hrou"h stan%-by battery
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- 8eportin" - *ransmission to e!ternal 4?9 Stan%ar% less analysis ?ea1 search+ pea1 i%entification+ ?;$ a%Justment+ selection of output for chart+ etc. 6ialo"ue functions 2quipment monitorin" Job *heoretical matri! calculation - $ll mounte% electrics an% instrumentations alon" 'ith computer har%'are /acuum pump 7nterface an% soft'are for %ata transmission up%ate% free of char"e %urin" 'arranty - *he license% copy of the X8, soft'are shall be pro3i%e% in 468O- alon" 'ith the necessary help Spares for t'o years of operation an%
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*t%.+ )o. 4ommissionin" spares as recommen%e% by Stan%ar% accessories. 7nitial fill of oil an% "rease an% consumables
for three months of operation after commissionin" Semi quantitati3e < stan%ar% less soft 'are pac1a"e is to be inclu%e% for analysis of non-routine or un1no'n
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Stan%ar% calibration soft'are shoul% capable of %oin" follo'in" Jobs. ?lottin" of calibration cur3es ,in%in" re"ression coefficients -easurin" ra' intensities ?ro3i%in" ori"inal an% calculate% concentration of stan%ar% samples use% for calibration Stan%ar% error of calibration for each "raph Stan%ar% sample ha3in" ma! %e3iation to be
equipment+ floor mounte% type an% suitable for in%ustrial application shall be use% for fast an% accurate analysis of 4u+ 4r+ chemical constituents in steel samples 'ith hi"h accuracy an% precision for simultaneous measurement of elements (4+ -n+ ?+ S+ Si+ $l+ 0i+ -o+ /+ C+ *i+ )+ 0b+ 4o+ $s+ ?b + Sn+ Kn+ Kr+ Sb+ -"+ *e+ 4a+ )i+ 0 + ) from trace le3el to concentration le3el ( in concentration E) in steel lollypop ( %isc-pin type ) samples. *he spectrometer shall be capable of analysin" #&i, so"u$"e an% #&i, i so"u$"e aluminium an% calcium separately. *ypical analytical pro"ram for this spectrometer is in%icate% in *able-777 of this specification. 7t shall also be capable of analysin" small %iameter ro% + 'ire+ scre'+ an% nut + etc. 'ith necessary a%opters. *he spectrometer shall be %esi"ne% to ta1e care of the e!ternal temperature an% humi%ity fluctuations an% shall pro3i%e stable an% accurate analytical results. 7t shall be pro3i%e% 'ith facility for %ata transmission. 7t shall be fully microprocessor ( ?.4. ) controlle%+ %irect rea%in" type an% the entire operation from initiation of spar1 to printin" of analytical results shall be fully automatic. 8ecommen%e% precision requirements of the offere% equipment shall be in line 'ith the stipulations of $S*- . 2 100I (latest re3ision). 7t shall be pre-calibrate%+ co3erin" the entire ran"e from traces to hi"her concentration+ a3ailable in the international stan%ar%s.
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i te!f#&i 4) so t-#t it is #$"e to t!# smit # #"%ti&#" !esu"ts ,i!e&t"% to BOF: SR> # , CCP "e2e" II #utom#tio
*he spectrometer shall be pro3i%e% 'ith 1(L colour monitor. *he %ata printer shall be laser type. *he operatin" me%ia shall be Cin%o's X? or latest 3ersion. *he equipment shall be pro3i%e% 'ith facility for %etermination of aci% soluble an% aci% insoluble aluminium an% calcium. *he soft'are pac1a"e shall be Cin%o' base% an% shall inclu%e all pro"rammes 'hich are necessary for control of equipment+ analysis+ %ata processin"+ report ma1in" an% %ata transmission. 7t shall inclu%e B Selection of proper spectrometer parameters an% automatic selection of pro"rams Selection of correct calibration cur3e Selection of stan%ar%isation mo%e+ up%atin" of calibration $utomatic s'itchin" o3er of spectral lines accor%in" to their concentration ran"es
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6rift correction or a%%iti3e an% multiplicati3e inter elementary correction an% bac1"roun% calculation $nalysis of percenta"e composition an% print out of analytical results 4alculation of stan%ar% %e3iations Stora"e of analytical results $%3ice of incomplete analysis or other errors $3era"e calculation 'ith user control 4alculation for a%%itional statistical %ata ( S6 + 8S6 ) -atrices correction $utomatic chec1in" of repro%ucibility ,la""in" of results beyon% calibration ran"e )a% sample %etection system *ransmission of result to remote printers < terminals $utomatic < user controlle% %ata transmission to e!ternal computers
*he scope of supply shall inclu%e the follo'in" itemsB 7nterface an% soft'are for transmission of analytical results $r"on purifier (sircal) 4onsumables for t'enty four months of operation after commissionin"+ as recommen%e% by manufacturer inclu%in" electro%es+ electro%e cleanin" brush+ 3acuum "rease+ lens+ printer paper+ etc. *ool 1it ( 1 set ) + containin" set of scre' %i3ers+ $llen 1eys+ spanners+ sol%er iron + etc. $r"on cylin%er (2 0os.) purity II.II#E 'ith pipin"s+ re"ulators an% manifol%s ( all 2 0os. ) $r"on purification an% pur"in" system in line 'ith the international < manufacturer stan%ar% Set of international spectro- chemical stan%ar%s ( reference
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8ea%ability B 0.001 ppm *he equipment shall be quote% alon" 'ith the follo'in" itemsB manufacturer 4onsumables < operatin" supplies require% for 1000 analyses+ as recommen%e% by the manufacturer *'o (2) 0os. of "as cylin%er+ one each for o!y"en (purity II.#E) an% instrument quality compresse% air 'ith pipin"+ re"ulator an% manifol%. 4alibration samples One 0o. sample cuttin" %e3ice for cuttin" of pin portion (1.0" sample) from lollypop sample+ 'ith abrasi3e %isc 1it+ recommen%e% cuttin" 'heel Silicon 4arbi%e to re%uce heat "eneration. 0 Laboratory Facilities (Imported)
2009 MEC ! Limite"# $ll %ig&ts %eser'e"(
7nterface an% soft'are for %ata transmission Spares for 2 years of operation an% maintenance+ as recommen%e% by the manufacturer 4ommissionin" spares+ as recommen%e% by the
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I st#""#tio : Commissio i 4: Demo st!#tio 9 7nstallation+ commissionin" an% %emonstration shoul% be %one an% trainin" shoul% be "i3en. $ll elements in each "roup mentione% in )oar% ?arameters of 7nstrument shoul% be %emonstrate% for as1e% ran"e. ?re-requisites for installation an% commissionin" shoul% be "i3en after placement of or%er. *rainin" on operation+ maintenance an% calibration to be pro3i%e% at site. 5ist of users (?referably in steel plant) since year 2000 to be pro3i%e%. C#"i$!#tio : St# ,#!,i;#tio # , Routi e A #"%sis 9 7n%i3i%ual calibration for each element+ co3erin" the entire ran"e for each "roup mentione% in the )oar% ?arameters of 7nstrument has to be pro3i%e%. $t least fi3e stan%ar% samples ha3in" certificate shoul% be incorporate% for each "roup. Stan%ar% sample use% for calibration shoul% be -); or )$S ma1e 4ertifie% 8eference -aterial. $fter stan%ar%ization the instrument shall be han%e% o3er for routine analysis of anlytes. 03.0 6 Simu"t# eous o?%4e 0 it!o4e # #"%se! *he equipment shall be use% for rapi%+ accurate an% simultaneous Laboratory Facilities (Imported)
2009 MEC ! Limite"# $ll %ig&ts %eser'e"(
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*he electro%e furnace shall be able to "enerate uniform an% controllable temperature up to 3000o4. 7t shall be pro3i%e% 'ith appropriate sensors an% microprocessor electronics 'hich shall ensure repro%ucible fusion con%itions for each sample. *he electro%e system shall be %esi"ne% in such a 'ay that only the electro%e tip assembly nee%s replacement in case of occurrence of 'ear. *he crucible shall be raise% pneumatically to ensure uniform contact pressure 'ith the upper electro%e. *he electro%e furnace shall be pro3i%e% 'ith soli% state in%icators at the front panel for important electrical parameters. 2!ternal chiller for the furnace shall be offere% as an optional item. *he analytical unit shall contain the basic analytical system inclu%in" a thermal con%ucti3ity %etector for nitro"en %etermination an% an infra-re% %etector for o!y"en %etermination+ a "as flo' system 'ith controllers+ an inte"ral balance 'ith automatic 'ei"ht compensation an% all the instrument electronics. *he control console shall control the instrument functions throu"h touch Laboratory Facilities (Imported)
2009 MEC ! Limite"# $ll %ig&ts %eser'e"( Page 22 of 40
*he equipment shall be quote% alon" 'ith the follo'in" itemsB 7nterface an% soft'are for %ata transmission Spares for 2 years of operation an% maintenance+ as recommen%e% by the manufacturer 4ommissionin" spares+ as recommen%e% by the manufacturer 4onsumables < operatin" supplies + require% for 1000 analyses+ as recommen%e% by the manufacturer Si! numbers of "as cylin%er+ t'o each for nitro"en (purity II.IIE)+ carbon %io!i%e (purity II.II#E) : helium (purity
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s%stem.
C#"i$!#tio : St# ,#!,i;#tio # , Routi e A #"%sis 9 7n%i3i%ual calibration for each element+ co3erin" the entire ran"e for each "roup mentione% in the )oar% ?arameters of 7nstrument has to be pro3i%e%. $t least fi3e stan%ar% samples ha3in" certificate shoul% be incorporate% for each "roup. Stan%ar% sample use% for calibration shoul% be -); or )$S ma1e 4ertifie% 8eference -aterial. $fter stan%ar%ization the instrument shall be han%e% o3er for routine analysis of anlytes. 03.0 @ Autom#te, -%,!o4e ,ete!mi #to! *he equipment shall be use% for rapi% an% accurate %etermination of hy%ro"en content in steel samples. *he analytical operation of the equipment shall be microprocessor controlle% an% analytical results shall appear %irectly in ppm of hy%ro"en. 7t shall analyse both %iffusible an% resi%ual hy%ro"en. *he equipment shall basically consist of the follo'in" main units. .
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*he furnace shall be resistance furnace+ current+ po'er an% temperature controlle%. 6etector shall be *hermal 4on%ucti3ity type. B!o#, p#!#mete!s of t-e equipme t 8an"e ('ith 1" sample) B 0.1 ppm to #0 ppm or more ?recision 8ea%ability B 0.02 ppm or 2.0E 8S6+ 'hiche3er is "reater B 0.001 ppm
*he equipment shall be quote% alon" 'ith the follo'in" itemsB 7nterface an% soft'are for %ata transmission Spares for 2 years of operation an% maintenance+ as recommen%e% by the manufacturer 4ommissionin" spares+ as recommen%e% by the manufacturer 4onsumables < operatin" supplies require% for 1000 analyses inclu%in" special e3acuate% quartz probes for sample collection for %etermination of resi%ual an% %iffusible hy%ro"en+ as recommen%e% by the manufacturer 4alibration samples *'o numbers of nitro"en "as cylin%er+ (purity II.IIE) an% instrument quality compresse% air (2 0os. of cylin%er ) 'ith pipin"+ re"ulators an% manifol%s 4alibration samples
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i te!f#&i 4) so t-#t it is #$"e to t!# smit # #"%ti&#" !esu"ts ,i!e&t"% to BOF: SR> # , CCP "e2e" II #utom#tio 8#!!# tee # , Suppo!t. *he instrument an% its accessories < au!iliaries shoul% ha3e minimum fi3e years 'arranty. *he spectrometer an% its all parts shoul% ha3e inspection certificate from its principal. Supplier shoul% "i3e "uarantee that the spare parts 'ill not be obsolete for ne!t 1# years from the %ate of supply of the equipment. Operation an% ser3ice -anuals alon" 'ith the instrument. I st#""#tio : Commissio i 4: Demo st!#tio 9 7nstallation+ commissionin" an% %emonstration shoul% be %one an% trainin" shoul% be "i3en. $ll elements in each "roup mentione% in )oar% ?arameters of 7nstrument shoul% be %emonstrate% for as1e% ran"e. ?re-requisites for installation an% commissionin" shoul% be "i3en after placement of or%er. *rainin" on operation+ maintenance an% calibration to be pro3i%e% at site. full sets in 2n"lish shoul% be "i3en
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Fe!!o0 i&7e" 0.01 . 0.10 0.10 . 0.G0 0.10 . 0.G0 0.01 . 0.0G 0.01 . 0.0G
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T#$"e0I ( &o t,. ) E"eme t 4 Fe!!o ( Fe!!o0 tit# ium $o!o 0.10 . 10.00 0.10 . #.00 0.01 -0.G0 0.01 -0.G0 3.00 . (.00 3#.00 . 0.00 0.01 . 0.G0 0.01 . 0.G0 3.00 (.00 0.10 -10.00 0.10 -#.00 Fe!!o0 m# 4# ese 0.10-10.00 Fe!!o0 si"i&o 0.10 . 10.00 &#-(# 0.#0 . #.00 0.010.G0 0.01 . 0.G0 0.#0 3.00 1.00 . #.00 0.10 . 0.G0 Si"i&o0 Fe!!o Fe!!o0 m# 4# ese 0&-!omium 2# #,ium 0.10-3.00 0.0#-(.00 0.10 . #.00 1.00 . #.00 0.10 . 1.00 0.01 . 0.G0 0.01 . 0.G0 0.01 . 0.20 0.10 . 0.#0 0.01 . 0.G0 0.01 . 0.G0 Fe!!o0 )io$ium 1.00. 3.#0 1.00 . #.00 Fe!!o mo"%$,e um 0.10 . 10.00
Si -n S ? 0i $l *i
1.00 . #.00
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'i4- A. ( B!i&7s 9 E"eme t + Compou , $l2O3 ,e2O3 *iO2 4aO -"O 0a2O >2O Lo3 A. ( B!i&7s 9 Laboratory Facilities (Imported)
2009 MEC ! Limite"# $ll %ig&ts %eser'e"(
R# 4e C (0 .0 . IG.0 0.0 . 3.# 0.0 . 3.# 0.0 . 3.0 0.0 . 2.0 0.0 . 2.0 0.0 . 2.0
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L#,"e s"#4 9 E"eme t + Compou , SiO2 ,e (element) 4aO -nO -"O $l2O3 S"i,e D#te S# , 9 Laboratory Facilities (Imported)
2009 MEC ! Limite"# $ll %ig&ts %eser'e"(
R# 4e C #. # 0 . 20 # . #0 3 . 30 0 . 1# 0- 0
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R# 4e C #. 0 0 . 2# 1# . 0 # . 10 0.00 - 1# 0 - 20
T#$"e 0 III T%pi&#" # #"%ti&#" p!o4!#mme of opti&#" emissio spe&t!omete! S". E"eme t Co &e t!#tio !# 4e (3ei4-t pe!&e t#4e)
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