5-6 Sem Subjects

BMS College of Engineering, Bangalore -19
(Autonomous College under VTU) Department of Chemical Engineering

1 2 3 4 Name of Course Course Code Designation of the course Rationale for the inclusion of the course/module in the programme CHEMICAL REACTION ENGINEERING - I 10CH5DCCR1 Departmental core The course emphasis on chemical reaction kinetics for ideal reactor systems along with homogeneous and heterogeneous reactions. The performance of different reactors and combination of reactors for different types of reaction are studied. Semester V / Year III Face to Face Total Credits
5 6
7 8 9
10
Semester and year offered Total Student Learning Time(SLT) L = Lecture L T P T = Tutorial Total = 5 credits P = Practical 4 0 1 O = Others Credit Value 5 Prerequisite (if any) Process Engineering thermodynamics Objectives: 1. Course will introduce the concepts of elementary and non - elementary reactions. 2. Analyze the experimental kinetic data to determine performance of the ideal systems. 3. Concept of combinations of reactions, performance and their optimal behavior under non-isothermal conditions. Course outcomes:
By the end of the course, students are able to: CO 1. Develop rate equations for different reactions using suitable mechanism. CO 2. Fit the experimental data to obtain the rate equation and also to find the performance equation of ideal systems. CO 3. Determine optimal ideal reactor design for multiple reactions & predict reactor performance for non-isothermal conditions.
11
12
Transferable Skills: Knowledge of reactor design for different reactions Independent study and self-learning skills Analysis and decision making skills Problem solving skills Academic / Technical writing and presentation skills Oral / Written communication skills Teaching-learning and assessment strategy: Teaching-learning Methods Classroom lectures and power point presentations Lecturer-led problem-solving sessions Assessment strategies include the following: Direct Assessment Strategies Continuous Internal Evaluation (CIE) by Test 1, Test 2 & Test 3. Best two tests are considered for the CIE Quiz 1 Laboratory examination (CIE) Semester End Examination (SEE)

Indirect Assessment Strategies Assignments Lecturer observation during class 13
Synopsis:
Chemical reaction engineering course provides broad coverage on chemical reactors, rate equations, concentration and temperature dependence of rate for different reactions, development of rate equations for different homogeneous reactions are studied. Industrial scale reactor and isothermal batch, flow, semi-batch reactors, performance equations for single reactors, multiple reactor systems and multiple reactions are deliberated.
14
Mode of Delivery:

15
Classroom lectures and Presentations Laboratory practice
Assessment Methods and Types: The assessment for this course will be based on the following: Coursework 10 % Test 1 05% Quiz 10% Test 2 25% Laboratory CIE 50% Final Examination (SEE) Assessment 100% Content outline of the course/module and the SLT per-topic SLT L T P Total 09 09 13 Details
16
Unit 1
Unit 2
Introduction: Scope of Chemical Reaction Engineering, Classification of reactions, Rate equation and rate of reaction. Factors affecting rate of reaction. Chemical kinetics and Thermodynamics Equilibrium. Temperature- 09 dependency of rate constant from Arrhenius, Collision and Transition state theories. Molecularity and order of reaction. Non-elementary reactions: Difference between elementary and non- 09 elementary reactions. Kinetic models and mechanisms for non-elementary reactions. Types of reactors. Homogeneous reactions: Interpretation of batch reactor data. Constant & 13 Variable Volume batch reactor. Analysis: Differential method, Integral method, half-life method. Method of excess and method of isolation (For Reversible and Irreversible reactions up to second order). Autocatalytic reactions. Design of ideal reactors: Concept of ideality. Development of design equations for batch, tubular and stirred tank reactors for both constant and variable volume reactions. Evaluation of rate equations from data obtained in these reactors.
Unit 3

Multiple reactor systems: Plug flow and/or Mixed flow reactors in Series, 13 parallel and series parallel. Reactors of different types and sizes in series. Comparison Of Ideal Reactors, General graphical comparison. Design of reactors for multiple reactions: Design of Batch reactor, Plug and Mixed flow reactors for Parallel, Series and Series-Parallel reactions (Only irreversible reactions must be considered). Non-isothermal reactors: Introduction, Material, Energy balances and 08 conversions. Analysis of non isothermal reactor: Design procedure (For single/simple reactions only). Optimum temperature Progression. 1. 2. 3. 4. 5. 6. 7. 8. 9. 10. LABORATORY COMPONENT Batch Reactor Isothermal plug flow reactor Mixed flow reactor Semi batch reactor Packed bed Reactor RTD Studies in Tubular Reactor Effect of temperature on Rate of reaction Bio Chemical Reaction (Batch) Enzyme catalyzed reactions in batch reactor RTD Studies in mixed flow reactor Adiabatic reactor 13
Unit 4
08
Unit 5
3 hours/week
LABORATORY
Total SLT
17 Main references supporting the Course: 1. Octave Levenspiel, Chemical Reaction Engineering, 3rd edition, John Wiley & Sons - 2001. Additional references supporting the course: 1. J.M. Smith, Chemical Engineering Kinetics, 3rd edition, McGraw Hill, 1984. 2. James J. Carberry, Chemical & Catalytic Reaction Engineering , McGraw Hill - 1976.
52 hours
2. H. Scott Fogler, Elements of Chemical Reaction Engineering, 3 rd edition Prentice Hall 2001
B.M.S. COLLEGE OF ENGINEERING, BANGALORE-19

(Autonomous College Under VTU) Department of Chemical Engineering
1 2 3 4 Name of Course Course Code Designation of the course Rationale for the inclusion of the course/module in the programme Semester and year offered Total Student Learning Time(SLT) L = Lecture T = Tutorial P = Practical Credit Value Prerequisite (if any) CHEMCIAL EQUIPMENT DESIGN 11CH5DCCED Departmental Core Course emphasizes fundaments of mechanical and structural stability required for chemical equipments in process industries. The components and accessories necessary to complete the design and fabrication requirement dealt with economic considerations. Semester V / Year III Face to Face L 4 4 T 0 P 0 Total Guided and Independent Learning Total = 4 credits
5 6
7 8 9
Objectives: 1. Understand the process flow diagrams (PFD) and Process instrument diagrams (P&ID) for processes. 2. Parameters consideration in the design of equipments using different pressure vessel codes, material selection based on the process conditions, economic consideration and feasible operations. 3. Design the pressure vessel, tall vertical vessel, storage vessels, reaction vessel, distillation, absorption tower or silo type vessels and allied parts. 10 Course outcomes: By the end of the course, students are able to: CO 1. Realize the practical applications of basic engineering design principles. CO 2. Select the suitable materials based on the process, environmental, economic & safety. CO 3. Solve the numerical problems of various reaction/pressure vessel components. CO 4. Estimation of sizing of pipes, pumps & storage vessel with its accessories. 11 Transferable Skills: Knowledge of basic concepts of Chemical Equipment Design considerations and its importance Knowledge of various process parameters required to be considered apart from the material selection to the system design Time and self management skills Literature and data searching skills Independent study with problem solving ability 12 Teaching-learning and assessment strategy: Teaching-learning Methods Classroom lectures and power point presentations Direct Assessment Strategies Continuous Internal Evaluation (CIE) Test 1, Test 2 & Test 3. (Two best performance) Quiz 1 & 2 Semester End Examination (SEE)

Indirect Assessment Strategies Assignments Brainstorming Lecturer observation during class Synopsis: The course would be to enhance the knowledge of those who have a basic understanding of process equipment drawing techniques and to build a foundation to those who are new to the design. Mechanical and structural designs are studied with concept of safety, economics and feasible operation in order to get the desired products. The design emphasizes the material selection based on process conditions with reliable fabrications. The course also deals with concepts of P & I diagrams for simple processes and Optimum size of delivery line in pumping operations. Mode of Delivery: Classroom lectures and power point presentations Assessment Methods and Types: Coursework (CIE) Continuous internal assessment 20% Test 1 20% Test 2 10% Quiz 1 & 2 50 % Semester End Examination (SEE) Assessment 16 100% Content outline of the course/module and the SLT per-topic SLT L T P Total 07 13 Details
13
14 15
Unit 1
07 Introduction Basic considerations in design. General design procedure. Equipment classification. Various components of process equipment. Design parameters. Pressure vessel codes. 13 Design considerations Material selection. Factors affecting design. Stresses due to static and dynamic loads (Internal & External). Temperature effects. Economic considerations. Design of pressure vessels Design parameters, conditions & stresses. Design of shell and other vessel components. Vessel at low & high operating temperatures. Numerical design problems using given process parameters.
Unit 2

Vessel component design Design of supports for vessels - Bracket, Lug, Leg, Saddle and Skirt supports. Design of flanges & nozzles Classification of flanges. Flange thickness calculation, Gasket selection and design, Bolt selection and calculation. Nozzle design. Design of vessel closures Flat plates, Formed heads, Elliptical & Hemispherical heads. Reaction vessels Design of reaction tanks with agitation and jacket. Types of agitators, baffles. Power requirement calculations. Design of tank dimensions and agitation system components. Numerical problems Storage vessels Process conditions and design parameters for storage of volatile, nonvolatile fluids & gases. Design of cylindrical tanks with fixed roofs. Design of components, supports and selection of vessels accessories & mountings. Numerical problems Pipe line design Pipe line sizing, Condensate and steam pipe design and Optimum size of delivery line in pumping operations. Concepts of P & I Diagrams, P & I Diagram for simple processes. Total SLT
14 14
Unit 3
09
09
Unit 4
08
08
Unit 5
52 hours
17
Main references supporting the Course: 1. M. V. Joshi, Process Equipment Design , Macmillan & Co. India, Delhi, 3rd edn. reprint 1998. 2. Brownell & Young, Process Equipment Design Vessel Design , John Willey, 1951 3. S. D. Dawande , Process Design of Equipment , Vol 1, Central Techno Publications. 3rd eEdn, 2003. Additional references supporting the course: 1. Perry & Green, Chemical Engineers Handbook, 7th edn, McGraw Hill, 1997. 2. Pressure Vessel Code IS 2825 - IS Code, B.I.S., New Delhi, 1969.

1 2 3 4 Name of Course Course Code Designation of the course Rationale for the inclusion of the course/module in the programme Semester and year offered Total Student Learning Time(SLT) L = Lecture T = Tutorial P = Practical Credit Value Prerequisite (if any) FOOD TECHNOLOGY 10CH5DELA1 Department Elective To impart knowledgeabout advanced food science and technology. Food science is concerned with the basic scientific facts about foods where as food technology is concerned with the processing of raw materials into foods that meet the human needs and works. Semester V / Year III Face to Face L 4 4 T 0 P 0 Total Guided and Independent Learning Total = 4 credits
5 6
7 8 9
Objectives: 1. Acquire the knowledge about quality attributes of food. 2. Familiarize with deterioration of stored food and its processing as well as prevention. 3. Learn about various food additives, food contamination/adulteration, packaging, and advances in processed foods. 10 Course outcomes: By the end of the course, students are able to: CO 1. Comprehend the quality attributes of food involved in food technology. CO 2. Identify sources of contaminants, adulterants with its prevention for safe and healthy food. CO 3. Select biocompatible packaging and additives for food products. CO 4. Discern different technologies involved in food processing. 11 Transferable Skills: Fundamental knowledge of food technology Analysis and decision-making skills Self-learning skill Presentation skills Critical thinking skills 12 Teaching-learning and assessment strategy: Teaching-learning Methods Classroom lectures and power point presentations Direct Assessment Strategies Continuous Internal Evaluation (CIE) Test 1, Test 2 & Test 3. (Two best performance) Quiz 1 & 2 Semester End Examination (SEE) Indirect Assessment Strategies Assignments Brainstorming Lecturer observation during class

13 Synopsis: Food technology refers to knowledge and activities that relate to meeting food needs and wants. The provision and consumption of food are significant activities of human endeavor, with vast resources being expended across domestic, commercial and industrial settings. Developments in food manufacture have an impact on society and the environment. The course deals with food additives and preservations, food laws governing for abatement of food adulteration and modern food processing. Mode of Delivery: Classroom lectures and power point presentations Assessment Methods and Types: Coursework (CIE) Continuous internal assessment 20% Test 1 20% Test 2 10% Quiz 1 & 2 50 % Semester End Examination (SEE) Assessment 16 100% Content outline of the course/module and the SLT per-topic SLT L T P Total 08 13 09 Details
14 15
Unit 1
INTRODUCTION AND QUALITY ATTRIBUTES OF FOOD: Aim of 08 food science and technology, function of foods, food in relation to health. Quality attributes Appearance factors, Textural factors, Flavour factors. Visual and objectively measurable attributes. Additional quality; quality standards, quality control. Introduction to sensory evaluation of foods. Formation And Chemistry Of Food: Carbohydrates, Proteins, Lipids, Vitamins, Minerals, Water and Phytochemical methods. FOOD PROCESSING AND PRESERVATION: Causes for food 13 deterioration. Aims and objectives of preservation and processing. Unit operations in processing.Different methods of food preservation low temperature, high temperature, preservatives, osmotic pressure, dehydrations, food irradiation. PROCESSING AND PRESERVATIONS: Milk and dairy products, vegetables and fruits, cereals, meat and meat products, fats and oils, beverages, sweeteners. ENZYMATIC AND NON-ENZYMATIC REACTIONS DURING 09 STORAGE: Introduction to enzymes. Nature and function of enzymes. Classification of enzymes. Hydrolases Esterase, amylases,pectic enzymes. Proteases. Oxidoreductases phenolases, glucose oxidase, catalose, peroxidase, lipoxygenase, oxidase. Immobilized enzymes. Uses of enzyme in food processing. Non-enzymatic reactions.
Unit 2
Unit 3

FOOD ADDITIVES: Introduction and need for food additives. 13 Types of additives antioxidants,chelating agents, coloring agents, curing agents, emulsions, flavors and flavor enhancers, flavor improvers, humecants and anti caking agents, leavening agents, nutrient supplements, non-nutritive sweeteners, pH control agents. Preservatives types and applications. Stabilizers and thickeners, otheradditives. Additives and food safety. FOOD CONTAMINATION AND ADULTERATION: Types of adulterants and contaminants. Intentional adulterants. Incidental adulterants and its effects. Food laws and standards. ENVIRONMENTAL CONCERNS AND FOOD SAFETY: Water in food 09 production. Properties and requirements of processing water. Environmental concerns solid waste disposal, wastewater properties,wastewater treatment. Safety hazards and risks. Food related hazards. Processing and handling. Cleaning and sanitizing. Modern trends in food science: Biotechnology in food, Biofortification, Nutraceuticals, Organic foods, Low cost nutrient supplements, Packaging of foods and nutrition labeling, Careers in food science and food industries. Total SLT 52 hours 13
Unit 4
09
Unit 5
17
Main references supporting the Course: 1. Norman N. Potter and Joseph H.,Food Science,HotchkinAvi Publishing Co., 1968. 2. N. ShakuntalaManay and M. Shadaksharamurthy,Foods, Facts and Principles, New Age Publishers, 2005. Additional references supporting the course:

1 2 3 4 Name of Course Course Code Designation of the course Rationale for the inclusion of the course/module in the programme Semester and year offered Total Student Learning Time(SLT) L = Lecture T = Tutorial P = Practical MASS TRANSFER -I 10CH5DCMT1 Departmental Core This course introduces the phenomena of diffusion and convective mass transfer which enable quantitative treatment of concentration profile, design of process equipments such as cooling tower, crystallizer and drier. Semester V/ III Year Face to Face L 4 T 0 P 1 Total Guided and Independent Learning Total = 5 credits
5 6
7 8 9
Credit Value 05 Prerequisite (if any) Engineering Mathematics Objectives: 1. The mass transfer analysis in laminar and turbulent flow conditions to transform dimensional expression into dimensionless groups in simulating chemical engineering problems. 2. To make use of the conceptual correlations related to heat transfer and mass transfer in problems related to separation processes. 3. To carry out calculations on humidification, cooling towers, novel separation techniques, drying, crystallization, and adsorption using graphical and theoretical approaches. 10 Course outcomes: By the end of the subject, students should be able to: CO 1. Determination of diffusivities in fluids & solids and analogies amongst the transport processes. CO 2. Apply mass transfer fundamentals to calculate rates of mass transfer for various operations. CO 3. Get the knowledge of the principles of novel separation process. 11 Transferable Skills: Critical thinking skills Problem solving skills Analysis and decision making skills Literature and data searching skills 12 Teaching-learning and assessment strategy: Teaching-learning Methods Classroom lectures Lecturer-led problem-solving sessions Co-operative learning Assessment strategies include the following: Direct Assessment Strategies Continuous Internal Evaluation (CIE) by Test 1, Test 2 & Test 3. Best two tests are considered for the CIE Quiz 1 Laboratory examination (CIE) Semester End Examination (SEE) Indirect Assessment Strategies

Assignments Lecturer observation during classroom sessions Synopsis: The mass transfer analysis in laminar and turbulent flow conditions allows to transform dimensional expression into dimensionless groups. The dimensionless groups enable analysis of chemical engineering problems related to mass transfer operations and use conceptual correlations amongst heat, momentum and mass transfer in numerical problems. Calculations of humidification, novel separation techniques, drying, crystallization, and adsorption using graphical and theoretical approaches are emphasized. This provides a good exposure to the learner about theory of humidification and separation processes. Mode of Delivery: Classroom lectures Classroom interactive sessions Laboratory practice sessions Assessment Methods and Types: The assessment for this course will be based on the following: Coursework (CIE) 10 % Test 1 05% Quiz 10% Test 2 25% Laboratory CIE 50% Final Examination (SEE) Assessment 100%
13
14
15
16
Content outline of the course/module and the SLT per-topic SLT L T P Total 14 14 09 Details INTRODUCTION: Diffusion in fluids, Diffusion in solids, 14 measurement and calculations of diffusivities. Eddy diffusion: MT coefficients and their correlations. Theories of MT. Interphase MT, J D factor, Analogies in Mass Transfer, Heat Transfer and Momentum transfer processes. HUMIDIFICATION: General theory, Psychrometric chart. 14 Concepts in humidification, dehumidification. Equipmentcooling towers, spray chamber. DRYING: Introduction, Equilibria, Drying rate curves, Mechanism of drying, types of dryers, Design of batch and continuous dryers. CRYSTALLIZATION: Factors governing nucleation and 09 crystal growth rates, Controlled growth of crystals, Incorporation of principles into design of equipment, Crystallizer equipments: SwensonWalker and Continuous crystallizers.
Unit-1
Unit-2
Unit- 3

ADSORPTION: Theories of adsorption, Isotherms, Industrial 09 adsorbents. Material balance for co-current, cross current and counter current operations, concept of stages, cascades and equipments. INTRODUCTION TO NOVEL SEPARATIONS: Ion exchange, 06 membrane processes- Reverse osmosis, dialysis, ultra and micro filtrations, super-critical fluid extraction. Laboratory components 1. Diffusion co-efficient of organic vapor into air 2. Surface evaporation 3. Drying characteristics 4. Single stage adsorption 5. Solid dissolution 6. Multistage adsorption 7. 7. Wetted wall column Total SLT 09
Unit- 4
06
Unit- 5
Laboratory
3 hrs /week
52 hours
17
Main references supporting the Course: 1. Mass transfer operations- Robert E. Treybal , McGraw Hill publications, 3rd edition. 2. Unit operations in chemical engineering- McCabe & Smith, McGraw Hill publications, 6th edition. Additional references supporting the course: 1. Transport processes and unit operations-Geankoplis C. J , prentice Hall(I) . 2. Chemical Engineering Vol I, II , IV & V- Coulson and Richardson, 4th edition, Pergamon press. 3. Introduction to Chemical Engineering III Edn., Badger, W.L. and Banchero J.T. McGrawHill International Edition, Singapore 1999.

1 2 3 4 Name of Course Course Code Designation of the course Rationale for the inclusion of the course/module in the programme Semester and year offered Total Student Learning Time(SLT) L = Lecture T = Tutorial P = Practical Credit Value Prerequisite (if any) NANOTECHNOLOGY 11CH5DELB1 Departmental Elective Course introduces the basics of nanotechnology and methods to prepare nano-materials. Knowledge of Instruments required for characterization of nano-materials and its surface morphology. Nanotechnology have the potential to solve difficult and currently unsolvable problems with the most simplified way. Semester V / Year III Face to Face L 4 4 Material science and bio materials Instrumental methods of analysis T 0 P 0 Total Guided and Independent Learning Total = 4 credits
5 6
7 8 9
Objectives: 1. Gain the knowledge to synthesis nano-materials from the bulk component which in turn known as top-down approach and also few methods of bottom-up approach using basic raw materials. 2. The instrumental methods used to measure the change in properties of the materials when reduced to nano-scale and there suitable applications. 3. Application of nano materials in MEMS, NEMS, catalyst and bio sensors. 10 Course outcomes: By the end of the course, students are able to: CO 1. Learn different instrumentations techniques, morphology and dynamic structure of nanomaterials CO 2. Select suitable fabrication techniques for quantum dots and quantum wells and its applications. CO 3. Comprehend the working principles of MEMS, NEMS and bio sensors. 11 Transferable Skills: Knowledge of fabrication techniques and material properties Knowledge of the instrumentation for characterizing the nano materials and its application Independent study and self-learning skills Academic / Technical writing and presentation skills Oral / Written communication skills 12 Teaching-learning and assessment strategy: Teaching-learning Methods Classroom lectures and power point presentations Direct Assessment Strategies Continuous Internal Evaluation (CIE) Test 1, Test 2 & Test 3. (Two best performance) Quiz 1 & 2 Semester End Examination (SEE)

13
14 15
Indirect Assessment Strategies Assignments Brainstorming Lecturer observation during class Synopsis: Present developments in world markets on the use of nano-materials in the modern era mainly focuses on improving the properties of materials by reducing them to nano-scale or synthesizing the nanomaterial from raw materials. Nano-materials in the field of environment, catalysis, automobiles, drug discovery and delivery and electrical engineering are mainly due to the change in properties of these materials like increase in the surface area, mechanical strength and electrical properties when reduced to nano-scale from bulk materials. Mode of Delivery: Classroom lectures and power point presentations Assessment Methods and Types: Coursework (CIE) Continuous internal assessment 20% Test 1 20% Test 2 10% Quiz 1 & 2 50 % Semester End Examination (SEE) Assessment 100% Content outline of the course/module and the SLT per-topic SLT L T P Total 08 14 08 Details
16
Unit 1
Unit 2
Unit 3
Introduction to Physics of the Solid State: Structure, Energy 08 Bands, Localized Particles. Methods of Measuring Properties: Atomic size, crystallography, Particle size determination, Surface structure, Microscopy- Transmission Electron Microscopy, Field Ion Microscopy, Scanning Microscopy;Spectroscopy- Infrared and Raman Spectroscopy, Photoemission and X-ray Spectroscopy, Magnetic resonance. Properties of Individual Nanoparticles: Metal nanoclusters, 14 Semiconducting nanoparticles, rare gas and molecular clusters, methods of synthesis- RF Plasma, Chemical Methods, Thermolysis, Pulsed Laser methods. Carbon nanostructures: Carbon molecule, Clusters, Carbon nanotubes, Applications Bulk nanostructured materials: Solid disordered nanostructures, nanostructure crystals. Nanostructured Ferromagnetism: Basics of ferromagnetism, 08 Effect of bulk nanostructuring of magnetic properties, dynamics of nanomagnets. Optical and vibrational spectroscopy: Infrared frequency range, luminescence, nanostructures in zeolite cage.

Quantum wells, wires and dots: Preparation of quantum 14 nanostructures, Size & dimensionality effects, Excitons, Single electron tunneling, Applications, superconductivity.Catalysis: Nature of catalysis, Surface area of nanoparticles, porous materials, pillered clays, Colloids. Biological materials: Biological building blocks, biological 08 nanostructures. Nanomachines and nanodevices: Microelectromechanical systems (MEMSs), Nanoelectro-mechanical Systems (NEMSs) - Fabrication, Devices. Molecular and Supramolecular Switches. Total SLT 52 hours 14
Unit 4
08
Unit 5
17
Main references supporting the Course: Charles P. Poole, Jr., Frank J. Owens,Introduction to Nanotechnology, John Wiley and Sons, 2009. Additional references supporting the course: Handbook of Nano-structured materials and nanotechnology, Vol. 1-5, Academic press, Boston, 2000.

1 2 3 4 Name of Course Course Code Designation of the course Rationale for the inclusion of the course/module in the programme Semester and year offered Total Student Learning Time(SLT) L = Lecture T = Tutorial P = Practical Credit Value Prerequisite (if any) POLLUTION CONTROL ENGINEERING 09CH5DCPCL Departmental Core Course emphasizes the basic environmental phenomena in which pollution awareness, effects, mitigations, and control measures are discussed in order to meet the environmental regulations. Semester V / Year III Face to Face L 3 3 T 0 P 0 Total Guided and Independent Learning Total = 3 credits
5 6
7 8 9
Objectives: 1. To understand the fundamentals of environmental atmospheric components with its governing legislations. 2. Familiarize with various sources, characteristics, treatment methods of water and wastewater, solid waste with their issues and management. 3. Infer the working principles of the air & noise pollution control equipments for various process industries. 10 Course outcomes:
By the end of the course, students are able to:
CO 1. Identify the components of environmental eco systems and effect of pollutant on environment. CO 2. Characterize the various parameters for treatment of water, waste water as well as solid waste from their sources. CO 3. Recover and recycle the useful resources from the wastes by adopting advanced techniques. CO 4. Appropriate equipments for abatement and control of air and noise pollution. 11 Transferable Skills: Fundamental knowledge of environmental impacts Analysis and decision-making skills Self-learning skill Presentation skills Critical thinking skills 12 Teaching-learning and assessment strategy: Teaching-learning Methods Classroom lectures and power point presentations Direct Assessment Strategies Continuous Internal Evaluation (CIE) Test 1, Test 2 & Test 3. (Two best performance) Quiz 1 & 2 Semester End Examination (SEE) Indirect Assessment Strategies

Assignments Brainstorming Lecturer observation during class Synopsis: The importance of environment for community and effects of environmental pollution are covered. The guidelines for abatement of pollution along with the minimization at source and treatment methods are emphasized. The effects of water, air and noise pollution on the eco system from both anthropogenic and industrial sources are deliberated. This course also explores the methods available for solid waste treatment, disposal methods, recovery and recycle of useful materials. Mode of Delivery: Classroom lectures and power point presentations Assessment Methods and Types: Coursework (CIE) Continuous internal assessment 20% Test 1 20% Test 2 10% Quiz 1 & 2 50 % Semester End Examination (SEE) Assessment 16 100% Content outline of the course/module and the SLT per-topic SLT L T P Total 06 12 Details
13
14 15
Unit 1
INTRODUCTION: Importance of Environment for Mankind. 06 Biosphere and Layers of Atmosphere. Hydrological Cycle and Nutrient Cycles. Types of Pollution. Damages from Environmental Pollution. Environmental Legislations and Environmental Acts in India. WATER POLLUTION: Water Resources. Wastewater 12 Classification. Types of Water Pollutants. Waste Water Sampling, Methods of Analysis: DO, BOD, COD, TOC, Nitrogen, Phosphorus, Trace Elements and Alkalinity. Wastewater Treatment: Preliminary, Primary,Secondary and Tertiary. Advanced wastewater Treatment: Microstraining, Adsorption on Activated Carbon, Ion Exchange,Reverse Osmosis, Electrodialysis cell. Applications to Industries: Petroleum refinery, distillery, Fertilizer and Textile processing.
Unit 2

AIR POLLUTION: Definition, Sources, Classification, Properties of 11 air pollutants, Effects of air pollution on health vegetation and materials. Air pollution sampling: Ambient sampling and Stack sampling. Analysis of air pollutants. Control methods and Equipments for particulates and gaseous pollutants. Applications to Industries: Thermal power plants, Metallurgical and Cement industries. SOLID WASTE TREATEMENT: Sources and Classification, Effect 05 on public health,Methods of Collection, Disposal Methods, Recovery and Recycling of Solid Waste. NOISE POLLUTION: Definition, Sources, Effects of Noise, 05 Equipments Used for Noise Measurement, Approaches for Noise Control. 11
Unit 3
05
Unit 4
05
Unit 5
17
Total SLT 52 hours Main references supporting the Course: 1. Environmental Pollution Control Engg, C.S Rao, New Age International Reprint, 2002. 2. Pollution Control In Industries, S.P. Mahajan,TMH, 1999. Additional references supporting the course: 1. Environmental Chemistry and Pollution Control, S.S. Dara 2. Environmental Engineering, G.N.Pandey and G.C. Carney, Tata McGraw Hill 2002.

1 2 3 4 Name of Course Course Code Designation of the course Rationale for the inclusion of the course/module in the programme Semester and year offered Total Student Learning Time(SLT) L = Lecture T = Tutorial P = Practical Credit Value Prerequisite (if any) Petroleum Refining 10CH5DELA2 Departmental Elective The most prolific and dynamic industries of this century are the petroleum and petrochemical industries. Chemical engineers have a vital role in these industries in upstream as well as downstream processing. Semester V / Year III Face to Face L 4 4 Technical Chemistry T 0 P 0 Total Guided and Independent Learning Total = 4 credits
5 6
7 8 9
Objectives: 1. Concise overview of petroleum and its refinery processes. 2. Understanding of the origin and sources of petroleum, constituents of petroleum, treatment of crude, various fractions obtained in petroleum refining, their assessment and treatment.
10 Course outcomes:
By the end of the course, students are able to:
CO 1. Relate to Indian petroleum industry and world scenario. CO 2. Infer & identify data of composition and thermal properties in refining and treatment of petroleum. CO 3. Familiarise with the different reforming techniques used for petroleum. 11 Transferable Skills: Fundamental knowledge of Refining and treatment. Analysis and decision-making skills. Self-learning skill Presentation skills Critical thinking skills 12 Teaching-learning and assessment strategy: Teaching-learning Methods Classroom lectures and power point presentations Direct Assessment Strategies Continuous Internal Evaluation (CIE) Test 1, Test 2 & Test 3. (Two best performance) Quiz 1 & 2 Semester End Examination (SEE) Indirect Assessment Strategies Assignments Brainstorming

13 Lecturer observation during class Synopsis: The importance of petroleum lies in its unmatched contribution to our present day energy needs. Petroleum and its auxiliary petrochemical industry are the major industries around the world. Chemical engineers play a vital role in these industries. This course gives a concise overview of origin and sources of petroleum, constituents of petroleum, treatment of crude, various fractions obtained in petroleum refining, and their assessment and treatment. Mode of Delivery: Classroom lectures and power point presentations Assessment Methods and Types: Coursework (CIE) Continuous internal assessment 50% 20% Test 1 20% Test 2 10% Quiz/Assignment 50 % Semester End Examination (SEE) Assessment 16 100% Content outline of the course/module and the SLT per-topic SLT L T P Total 6 9 Details Indian Petroleum Industry: 6 Prospects & Future. Major companies. World production, Markets, Offshore and onshore, Oil well technology. Unit 1 Composition of crude: Classification. Evaluation of petroleum. UOP-k factor. TBP analysis. EFV analysis. Average boiling point. ASTM curves. Thermal properties of petroleum fractions. Product properties and test methods: 9 Gas: Various types of gas and LPG. Reid vapor pressure analysis. Gasoline and Naptha. Octane No. Oxidation stability. Additives for gasoline. Kerosene. Characterization for flash point or fire point, volatility, burning qualities etc., Diesel, octane testing, viscosity etc. Grades of diesels e.g. HSD, LDO. Diesel additives. Lube oils: Types, tests-carbon residue and viscosity index.
14 15
Unit 2

Crude pretreatment: 15 Pumping of crude oils. Dehydration of crude by chemical, gravity, centrifugal, electrical de-salter and comparison of each. Heating of crude- heater, different types of pipe still heaters. Crude distillation, arrangement of towers for various types of reflux. Treatment techniques: Types of impurities present and various desulfurization processes. Production and treatment of LPG. LNG technology. Sweetening operations for gases. Catalytic desulfurization. Treatment of kerosene. Treatment of diesel and Treatment of lubes. Catalytic Cracking: 15 Comparison of thermal and catalytic cracking and Cracking conditions. Various catalytic cracking processes: Fluid catalytic cracking-flexi cracking. Theory of coking: various types of coking processes. Naptha cracking. Hydro cracking. Theory of hydro cracking. Catalysts for hydro cracking. Catalytic Reforming: Theory. Factors influencing reforming, catalysts, feedstock requirements. Thermal Processes: 7 Reactions- theory of thermal cracking. Properties of cracked materials and factors influencing the properties of cracked materials. Total SLT 17 52 hours 7 15
Unit 3
15
Unit 4
Unit 5
Main references supporting the Course: 1. Bhaskara Rao, Modern Petroleum Refining Processes, 3rd edition, Oxford & IBH publication, 1999. 2. Nelson, Petroleum Refinery Engineering, 4th Edition, McGraw Hill, 1982. Additional references supporting the course: 1. Ram Prasad, Petroleum Refining Technology, 1st edition, Khanna Publishers, 2000. 2. Sland W.F. and Davidson R.L., Petroleum Processing, 1967, McGraw Hill.

1 2 3 4 Name of Course Course Code Designation of the course Rationale for the inclusion of the course/module in the programme Semester and year offered Total Student Learning Time(SLT) L = Lecture T = Tutorial P = Practical POLYMER PROCESSING 10CH5DELB2 Departmental Elective Polymers are of principal importance in the world of engineering. Chemical engineering has numerous applications of polymers and hence the processing technique of these polymers is an area very important and central to chemical engineering. Semester V / Year III Face to Face L 4 T 0 P 0 Total Guided and Independent Learning Total = 04 credits
5 6
7 8 9
Credit Value 4 Prerequisite (if any) Objectives: 1. To familiarize the basic polymer chemistry 2. To understand how polymers are processed in industry. 10 Course outcomes: By the end of the course, students will be able to: CO 1. Apprehend molten flow behavior of polymer. CO 2. Familiarise with various processing techniques. CO 3. Select suitable techniques based on applications. 11 Transferable Skills: Knowledge of basic polymer chemistry. Understanding of key concepts of polymer processing. Problem solving techniques in design maintenance and operation of machines. 12 Teaching-learning and assessment strategy: Teaching-learning Methods Classroom lectures and power point presentations Lecturer-led problem-solving sessions Direct Assessment Strategies Continuous internal evaluation (CIE) Test 1, Test 2 & Test 3. Best of average Quiz 1 & 2 Semester End Examination (SEE) Indirect Assessment Strategies Assignments Lecturer Observation through presentations Synopsis: This course aims to provide step by step assistance in learning polymer processing principles and equipment required for processing. Polymers in solution and in the liquid, liquid-crystalline, crystalline, and glassy states, theory of polymer processing, non-Newtonian flow, extrusion, injection-molding, fiber, film processing are studied. Physical characterization of microstructure and macroscopic properties, compounding and blending are emphasized. Mode of Delivery:
13
14

15 Classroom lectures and presentations Assessment Methods and Types: Coursework Continuous internal assessment Test 1 Test 2 Quiz 1 &2 Semester End Exam Assessment 16
20% 20% 10% 50 % 100%
Content outline of the course/module and the SLT per-topic SLT L 10 T P Total 10 10 10 12 10 Details Melt behavior of thermoplastics-Compounding for engineering application-Stress-strain behavior-Long term behaviorprocessing of thermoplastics-Classification of processesCrystallization orientation and shrinkage Single screw and double screw extruders-Extruder zones, screws and power calculation-Die and calibration equipment-C0extrusion, extrusion blow moulding for PET bottles-Wire drawingPVC spinning-Rheological applications of extrusion and defectsOperation and maintenance of extrusion equipments. Injection moulding-Reciprocating screw injection moulding-Single impression mould-multi impression moulds-Hot runner moulds, gate and runner calculations-Control of time pressure and temperature of injection-Fibre reinforced polymer injection moulding-Sandwich and injection blow moulding-Reaction injection moulding-Operation and maintenance of injection moulding equipments. Compression molding and applications-Derivation of compression mold thickness and compaction force-Transfer molding and Calendering-Derivation of film thickness and pressure for rollersGauge control-Application of PVC calendered products.
Unit 1
10
Unit 2
10
Unit 3
12
Unit 4
17
Principles of thermoforming-Vacuum and pressure formingUnit 5 Rotational molding-Applications and thickness and cooling calculations. Total SLT Main references supporting the Course: 1. Principles of polymer Processing, Morton Jones 2. Plastics Engineering, R.J.Crawford Additional references supporting the course 1. Principles of polymer engineering, N.G.McCrum, C.P. Buckley
10
52 hours (Theory)

1 2 3 4 Name of Course Course Code Designation of the course Rationale for the inclusion of the course/module in the programme APPLIED MATHEMATICS IN CHEMICAL ENGINEERING. 10CH6DELC2 Departmental Elective Numerous chemical engineering problems can be solved using mathematical tools to obtain first level solutions for analyses. Hence knowledge of these tools and their applications is absolutely necessary to understand the concepts and as a basis for advanced research. Semester VI / Year III Face to Face L 3 T 0 P 0 Total Guided and Independent Learning Total = 03 credits
5 6
Semester and year offered Total Student Learning Time(SLT) L = Lecture T = Tutorial P = Practical
7 8 9
Credit Value 3 Prerequisite (if any) First and Second year engineering mathematics concepts. Objectives: 1. Understand and apply concepts of shell material balance to solve obtained ordinary or partial differential equations. 2. Analyze the solutions obtained of these problems by analytical and numerical methods. 10 Course outcomes: By the end of the course, students will be able to: CO 1. Develop ordinary and partial differential equations to solve Chemical engineering problems. CO 2. Use suitable numerical methods to solve the developed differential equations. CO 3. Apply finite difference method to solve unit operations and processes. 11 Transferable Skills: Knowledge of basic mathematical tools Understanding of key mathematical concepts Problem solving skills using applied math in the field of chemical engineering Develop a strong foundation in conceptualization and solution of problems in chemical engineering 12 Teaching-learning and assessment strategy: Teaching-learning Methods Classroom lectures Lecturer-led problem-solving sessions Solving assigned problems individually and in team Direct Assessment Strategies Continuous internal evaluation (CIE) Test 1, Test 2 & Test 3. Best of average Quiz 1 & 2 Semester End Examination (SEE) Indirect Assessment Strategies Assignments Lecturer Observation through presentations

13 Synopsis: This course aims to provide step by step assistance in using mathematical principle for solving Chemical engineering problem in the area like momentum, heat, mass transfer and reaction engineering. Mathematical methods to solve ordinary, partial differential equations, and Laplace transforms are emphasized. Mode of Delivery: Classroom Lectures and Presentations. Assessment Methods and Types: Coursework Continuous internal assessment Test 1 Test 2 Quiz 1 & 2 Semester End Examination Assessment 16
14 15
20% 20% 10% 50% 100%
Content outline of the course/module and the SLT per-topic SLT L T P Total 06 11 Details
UNIT I
Mathematical Formulation of The Physical Problems: 06 Applications of law of conservation of mass in: mixing tank system, equilibrium batch still and single stage extraction. Applications of law of conservation of energy in: gas compression system and Flow of heat from a fin. Related numerical problems for all above physical systems. Mathematical Formulation of Complex Problems 11 Plug flow model to obtain fluid flow velocity, mass transfer with reaction for gas-liquid contact, heat transfer through multiwall cylinders and spheres, heat transfer in a jacketed vessel, rate expression for series and parallel homogenous reactions.
UNIT II Solving related numerical problems using solutions for ordinary differential equations of first order and first degree, solutions for linear differential equations and solutions for simultaneous linear differential equations

Partial Differential Equations Differentiation formulas for different partial derivates with examples and Differentiation of implicit functions. Formulations of partial differential equations: Formulations of partial differential equations for the continuity equation, Ficks second law of diffusion and heat conduction in rectangular coordinates. Finite Differences method for stage processes Analysis of stage-wise Processes like multistage counter-current extraction, stirred-tank reactor system, Distillation in a plate column and Absorption column. Solutions Of Ordinary Differential Equations: Picards 06 methods, Taylor series method, Eulers method, modified Eulers method, Range-kutta method, Adam bashforth method and problems. Solutions For Partial Differential Equations: Matrix method; Diagonal method. Applications of Laplace Transforms 06 Inverse Laplace transforms, initial and final value theorems. Applications to chemical engineering like level/ temperature in a single tank system, mixing tank, CSTR with first order reaction, interacting system and non-interacting system. 39 hours (Theory) Total SLT 17 Main references supporting the Course: 1. Harold Mickley, Sherwood and Reid, Applied Mathematics in Chemical Engineering, McGraw Hill 2. Jenson and Jeffreys, Mathematical methods in Chemical Engineering, Additional references supporting the course 1. Bronson, Differential Equations, Schaum Series 06 06 10 10
UNIT III
UNIT IV
UNIT V

1 2 3 4 Name of Course Course Code Designation of the course Rationale for the inclusion of the course/module in the programme INTERFACIAL PHENOMENA AND RELATED SEPARATION TECHNIQUES 11CH6DELD2 Departmental Elective
Interfaces play an important role in our daily life, and in the world around us. Surface tension is a fundamental and important property by which the gasliquid interfaces are characterized. Interfacial engineering is a cross-disciplinary subject in which the scientists and engineers from several disciplines work. Separation processes are vital and inevitable in chemical engineering. One of the economical methods of separation is based on utilizing the properties like surface tension.
Semester VI / Year III Face to Face L 3 3 Engineering physics and Basic electrical engineering T 0 P 0 Total Guided and Independent Learning Total = 3 credits
5 6
Semester and year offered Total Student Learning Time(SLT) L = Lecture T = Tutorial P = Practical Credit Value Prerequisite (if any)
7 8 9
Objectives: 1. Importance of various components of interfacial science in different chemical engineering industries viz. food, paint and pharmaceutical industries are emphasized. 2. The properties and functioning of surfactants and detergency are made familiarized. 10 Course outcomes: By the end of the course, students are able to: CO 1. Realize the factors influencing stability of dispersions & emulsions. CO 2. Get the knowledge to measure surface tension & contact angle and apply them for practical problems. CO 3. Comprehend about detergency, surfactants and their applications. 11 Transferable Skills: Knowledge of Interfacial phenomena. Knowledge of emulsion, micro-emulsion and foams. Knowledge of measurement of contact angle and surface tension Literature and data searching skills. Independent study and self-learning skills. Academic / Technical writing and presentation skills. Oral / Written communication skills. 12 Teaching-learning and assessment strategy: Teaching-learning Methods Classroom lectures and power point presentations Direct Assessment Strategies Continuous Internal Evaluation (CIE) Test 1, Test 2 & Test 3. (Two best performance) Quiz 1 & 2 Semester End Examination (SEE) Indirect Assessment Strategies

Assignments Brainstorming Lecturer observation during class Synopsis: The subject provides a general introduction to the field of interfacial phenomena and related separation techniques, introducing students to a variety of interfaces a chemical engineer will come across in industries and day to day life. The significance of surface tension, contact angle, wetting, spreading of a fluid. The formation of capillary condensation, super saturation, nucleation and measurement of Interfacial tension. Application on interfacial science in various chemical industries. The conditions required to form emulsions and microemulsions, charged colloids, emulsions in food science, photographic emulsions, and electrical aspects of surfaces like DLVO theory. The subject will give insight of surfactants, common properties of surfactant solution, thermodynamics of surfactant self assembly, self assembled surfactant structures, surfactants and detergency. The surfactant based separation like foam separations and micellar separations are studied. Mode of Delivery: Classroom lectures and power point presentations Assessment Methods and Types: Coursework (CIE) Continuous internal assessment 20% Test 1 20% Test 2 10% Quiz 1 & 2 50 % Semester End Examination (SEE) Assessment 16 100% Content outline of the course/module and the SLT per-topic SLT L T P Total 08 06 Details
13
14 15
Unit 1
Unit 2
Introduction: Concept of Interface. Surface Tension, 08 Equivalence in the concepts of surface energy and surface tension. Application on interfacial science in industries. Excess Pressure: Generalized equation for excess pressure across a curved surface- the equation of Young and Laplace and its application. Kelvins equation and its application, Capillary condensation, Super Saturation, Nucleation. Measurement of Interfacial tension: Capillary rise 06 method. Drop weight method, Wilhelmy plate method, Du Nuoy method. Methods based on shape of static drops or bubbles.

Wetting fundamentals and contact angles: Work of 10 adhesion, cohesion. Criteria for spreading of liquids. Kinetics of spreading. Lens formation- three phase systems. Youngs equation. Contact angle hysteresis. Emulsions and Microemulsions: The conditions required to form emulsions and microemulsions, charged colloids, emulsions in food science, photographic emulsions. 07 Electrical aspects of surfaces: The electrical double layer. Stern treatment of electrical double layer. Free energy of a diffused double layer. Repulsion between two plane double layers. Colloidal dispersions. Combined attractive and electrical interaction-DLVO theory. Surfactants: Introduction to surfactants, common properties 08 of surfactant solution, Thermodynamics of surfactant self assembly, self assembled surfactant structures, surfactants and detergency Surfactant Based Separations: Fundamentals. Surfactants at inter phases and in bulk. Liquid membrane permeation. Foam separations. Micellar separations
Total SLT 17 Main references supporting the Course: 39 hours 10
Unit 3
07
Unit 4
08
Unit 5
1. Pallab Ghosh, Colloids and Interface Science, Prantice Hall Publications, New Delhi, 2006.
Additional references supporting the course:
1. A. W. Adamson, Physical chemistry of surfaces, John Wiley, 5th edition, 1997. 2. Duncan J. Shaw, Introduction to colloid and surface chemistry, Butterworth Heinemann, 4th Edition. 2000. 3. Milton J. Rosen, Surfactants and Interfacial Phenomena, Wiely publisher, 2012.

1 2 3 4 Name of Course Course Code Designation of the course Rationale for the inclusion of the course/module in the programme Semester and year offered Total Student Learning Time(SLT) L = Lecture T = Tutorial P = Practical MASS TRANSFER II 10CH6DCMT2 Departmental Core All the chemical engineering operation requires either preliminary purification or final separation of products from by-products. For these processes mass transfer operations are used. Semester VI/ III Year Face to Face L 4 T 0 P 1 Total Guided and Independent Learning Total = 5 credits
5 6
7 8 9
Credit Value 05 Prerequisite (if any) Engineering Mathematics and Mass Transfer 1 Objectives: Familiarize with basic concepts of gas-liquid and liquid-liquid contact operations. Process design of particular equipments like distillation column, absorption tower, liquid-liquid extraction and leaching.
10 Course outcomes: By the end of the subject, students should be able to: CO 1. Apply mass balance and composition balance in interfacial mass transfer CO 2. Apply the concept of interfacial mass transfer in multiphase contact processes. CO 3. Design and working of various mass transfer equipments. 11 Transferable Skills: Knowledge of mass transfer operation Knowledge of interfacial mass transfer Knowledge of chemical process design Literature and data searching skills Independent study and self-learning skills Academic / Technical writing and presentation skills Oral / Written communication skills 12 Teaching-learning and assessment strategy: Teaching-learning Methods Classroom lectures Lecturer-led problem-solving sessions Direct Assessment Strategies Continuous Internal Evaluation (CIE) by Test 1, Test 2 & Test 3. Best two tests are considered for the CIE Quiz 1 Laboratory examination (CIE) Semester End Examination (SEE) Indirect Assessment Strategies Assignments Lecturer observation during classroom sessions

13 Synopsis: Mass transfer II covers the concept of material balance in various mass transfer phenomena. This mass transfer processes are those that require either application of heat or a solvent. In the case of distillation where the mixture of the components varies largely in their boiling point components can be separated by application of heat. For liquid with inflammable characteristics liquid-liquid extraction is used where introduction of an immiscible liquid which acts as a solvent for one of the liquid. The liquid mixture then can be separated by simple separating funnels. In case of any toxic gas mixture the toxic component is separated with the help of gas absorbers where the solvent liquid is sprayed in a countercurrent fashion. The effective contact between various phases like gas liquid in particular is ensured by application of either solid packing or by introduction of trays. Mode of Delivery: Classroom lectures Classroom interactive sessions Laboratory practice sessions Assessment Methods and Types: The assessment for this course will be based on the following: Coursework (CIE) 10 % Test 1 05% Quiz 10% Test 2 25% Laboratory CIE 50% Semester End Examination (SEE) Assessment 100%
14
15
16
Content outline of the course/module and the SLT per-topic SLT L T P Total 12 14 Details Gas-Liquid contacting systems: Liquid and gas dispersion: 12 Types, construction and working of tray and packed columns, types and properties of packing, tray efficiencies, HETP and HTU concepts, Concept of flooding , weeping, and entrainment. Comparison of tray and packed columns. Absorption: Equilibrium solubility of gases in liquids. One component transferred: Material balances. Counter current multistage operations: Isothermal only. Continuos contact equipment: Absorption of one component, overall coefficients and transfer units, dilute solutions, Overall heights of transfer units. Design of packed towers from the data of NTU. Absorption with chemical reaction. Distillation: Introduction, Vapour liquid equilibriums. 14 Estimation of VLE data, VLE for multi-component systems. Flash vaporization, Simple or differential distillation, Steam distillation, Continuous rectification, Design using McCabe Thiele method for binary mixtures.
Unit-1
Unit-2

Unit- 3 Design of distillation column:PonchonSavarit method. 08 Efficiencies overall, local, and Murphree plate efficiencies: Reboiler, Use of open steam, Vacuum, molecular, extractive and azeotrope distillations. Liquid-Liquid extraction: Introduction, Ternary equilibrium. 10 Solvent selection. Equipment and flow sheets: Single stage. Multi-stage cross-current. Insoluble systems, Continuous counter current multistage extraction, Equipments: Stage efficiency, stage type extractors (no design aspects): Mixer settler cascades, Continuous contact equipments: packed towers, Rotating disc contactor, Pulsed column, Sheibel extractor, centrifugalextractor. Leaching operation: Introduction, Preparation of solid, 08 equipment for unsteady state operation and steady state operation. Methods of calculation: Equilibrium diagrams, Single stage and multi-stage cross and counter current operations, Counter current constant underflow case, leaching operation Laboratory components 1. Simple distillation 2. Steam distillation 3. Single stage leaching 3 hrs /week 4. Packed column distillation 5. Single stage extraction 6. Multi stage extraction 7. Multi stage leaching Total SLT 52 hours 08
10
Unit- 4
08
Unit- 5
17
Laboratory
Main references supporting the Course: 1. Robert E Treybal,Mass Transfer Operations, 3rdedition, McGraw Hill, 1981. 2. McCabe & Smith,Unit Operations in Chemical Engineering, 6thedition, McGraw Hall, 2001. Additional references supporting the course: 1. Coulson and Richardson,Chemical Engineering,Vol II and V, 4th Edition, Pergamon Press, 1998. 2. Badger &Banchero, Introduction to Chemical Engineering, TMH, 1998.

1 2 3 4 Name of Course Course Code Designation of the course Rationale for the inclusion of the course/module in the programme
Operations Research
10CH6DELC2 Departmental Elective Optimization has played a key role in the design, planning and operation of chemical and related processes, for several decades. Process optimization is one of the main goals of any chemical engineer, operations research (OR) models have attracted decision makers spurred by the new and effective techniques for multiobjective optimization. In order to understand and implement this renewed interest, this course presents various optimization models and their applications in chemical engineering. Semester VI / Year III Face to Face L 3 T 0 P 0 Total Guided and Independent Learning Total = 03 credits
5 6
7 8 9
Credit Value 3 Prerequisite (if any) None Objectives: 1. Familiarise with basics, Phases, approached and limitations of OR with various formulations. 2. Understanding the resource allocations and transportation of various assignments and commodities. 3. Understand the optimal sequencing, planning, scheduling, networking and crashing to maximize the profit for routine logistics. 10 Course outcomes: By the end of the course, students will be able to: CO 1. Get acquainted to find optimum solutions for numerical problems using LPP. CO 2. Solve assignment, transportation and sequencing problems for its optimal solutions. CO 3. Illustrate network constructions and find its feasible solutions for optimization of societal problems. 11 Transferable Skills: Independent study and self-learning skills Academic / Technical writing and presentation skills Oral / Written communication skills Critical thinking and problem solving skills Time and Self-management skills Teamwork skills Analysis and decision-making skills 12 Teaching-learning and assessment strategy: Teaching-learning Methods Classroom lectures Lecturer-led problem-solving sessions Solving assigned problems individually and in team Direct Assessment Strategies Continuous internal evaluation (CIE) Test 1, Test 2 & Test 3. Best of average

Quiz 1 & 2 Semester End Examination (SEE)
Indirect Assessment Strategies Assignments Lecturer Observation through presentations 13 Synopsis: This course aims in understanding the basics of operations research for solving problems on LPP models, assignments, finding feasible solution for optimal transportation of commodities, and sequencing algorithms using various OR techniques. Networking the critical path and project evaluation review techniques for project scheduling to optimize the time and cost. Mode of Delivery: Classroom lectures and presentations. Assessment Methods and Types: Coursework Continuous internal assessment 20% Test 1 20% Test 2 10% Quiz 1 & 2 50% Semester End Examination Assessment 16 100% Content outline of the course/module and the SLT per-topic SLT L 11 T P Total 11 06 06 06 Details
14 15
Introduction: Definition. Scope of Operations Research. Approach and limitations of O.R. Models.
UNIT I
Characteristics and phases of O.R. Linear Programming Problems: Mathematical formulation of L.P. Problems. Graphical solution method. The simplex method: Slack, surplus and artificial variables. Simplex, Dual simplex method, Big-M method.
UNIT II
Assignment problems: Balanced and Unbalanced assignment problems. Maximization assignment problems. Travelling salesman problems. Transportation problem: Basic feasible solutions by different methods. Finding optimal solution using MODI method Degeneracy, Unbalanced transportation problems, Maximization problems. Sequencing: Johnsons algorithm - n jobs - 2 machines, n jobs 3machines and n jobs-n machines without passing sequence. 2 jobs-n, machines (graphical solution).
06
06
UNIT III
06
UNIT IV

UNIT V
PERT-CPM Techniques: Network construction. Determining time estimates and critical path. In network analysis. Variance and probability of completing the project. Calculation of different floats. Project duration. Crashing of simple networks.
10
10
Total SLT 17
39 hours
Main references supporting the Course: th 1. S. D. Sharma, Operation Research, 8 edition, Kedarnath & Co, 2003. th 2. Kantiswaroop, P. K. Gupta and Manmohan, Operation Research, 9 edition, S Chand & Co. 1999. Additional references supporting the course: rd 1. L. S. Srinath, Introduction to Pert and CPM, 3 edition, East west, 1998 2. Hospach Buchan and Earnest Koenigberg, Scientific Inventory Management - 1989

1 2 3 4 Name of Course Course Code Designation of the course Rationale for the inclusion of the course/module in the programme Semester and year offered Total Student Learning Time(SLT) L = Lecture T = Tutorial P = Practical CHEMICAL REACTION ENGINEERING - II 10CH6DCCR2 Departmental Core The knowledge of reactor design considering the non ideal behavior for different types of systems including different types of catalytic reaction & non catalytic reaction (fluid-fluid and fluid-solid reactions) are emphasized. Semester VI / Year III Face to Face L 4 T 0 P 0 Total Guided and Independent Learning Total = 4credits
5 6
7 8 9
Credit Value 4 Prerequisite (if any) Chemical Reaction Engineering -1 Objectives: 1. Chemical reactor design for non-ideal conditions and interrelationship between transport, thermodynamics, and chemical reaction in open and closed systems. 2. Understand the reaction mechanism and design a suitable reactor for catalytic and non catalytic reactions. 3. Suitable design equation for reactor systems like fluidized bed or packed bed or mixed flow. 10 Course outcomes: By the end of the course, students will be able to: CO 1.Distinguish the performance of non ideal with ideal systems. CO 2.Determine rate expression using reaction mechanisms of suitable model for catalytic & non catalytic reactions. CO 3 Develop design equation using models for heterogeneous reaction systems. 11 Transferable Skills: Knowledge of reactor design for non-ideal conditions Knowledge of kinetic models for fluid-fluid and fluid- solid reactions Knowledge of determining reaction rate experimentally for catalytic reactions Independent study and self-learning skills Analysis and decision making skills Academic / Technical writing and presentation skills 12 Teaching-learning and assessment strategy: Teaching-learning Methods Classroom lectures Lecturer-led problem solving sessions Individual and team work Independent study to get acquainted with recent technologies Direct Assessment Strategies Continuous internal evaluation (CIE) Test 1, Test 2 & Test 3. Best of two test average Quiz 1 & 2 Semester End Examination (SEE) Indirect Assessment Strategies

Assignments Lecturer observation during presentations Participation of students during interactive discussion Synopsis:
This course deals with the principles of reaction kinetics for different types of reactions and reactor design considering the non-ideal behavior. Design of various types of chemical reactors is discussed, including continuous stirred-tank reactor (CSTR), plug-flow reactor (PFR), and continuous-operation and batch-operation reactors for various heterogeneous reactions. Types of catalytic reactions, catalyst characterization and catalyst reaction kinetics are emphasized to model a suitable design equation for a given reactor system.
13
14 15
Mode of Delivery: Classroom lectures, Overhead presentations Assessment Methods and Types: Coursework Continuous internal assessment Test 1 Test 2 Quiz 1 & 2 Semester End Examination Assessment
20% 20% 10% 50% 100%
16
Content outline of the course/module and the SLT per-topic SLT L T P Total 08 14 08 14 Details
UNIT I
UNIT II
UNIT III
Basics Of Non Ideal Flow: Introduction on ideal flow reactors 08 and non-ideal reactors. Importance & interpretation of RTD and pulse experiment to determine C and E curve. Step experiment for C & F curve Conversion in non- ideal flow reactors for simple systems. Statistical interpretation and Problems Dispersion model and Tanks in series model. Fluid-fluid reactions: Introduction for fluid-fluid reactions, 14 derivation of rate equation for straight mass transfer and combination of mass transfer and chemical reaction, and Problems. Fluid- particle reactions: Introduction, Progressive conversion model and Shrinking core model, Derivation for different rate controlling for cylindrical particle and problems. Catalysis: Introduction to catalysis and Estimation methods for 08 catalytic properties, Promoters& inhibitors. Mechanism of catalysis and rate equations for different rate controlling steps. Deactivation: Deactivating catalyst and Mechanism and Rate & 14 performance Solid Catalyzed Reactions: Heterogeneous reactionsIntroduction, Kinetic regimes. Rate equation for surface kinetics. Pore diffusion resistance combined with surface kinetics. Thiele modulus and enhancement factor, Porous catalyst particles. Heat effects during reaction
UNIT IV

UNIT V Solid Catalyzed Reactions: Performance equations for reactors 08 containing porous catalyst particles. Experimental methods for finding rates. Packed bed catalytic reactor & reactors with suspended solid catalyst, Fluidized reactors of various types. Gas-Liquid Reactors: Trickle bed, slurry reactors. Three phase fluidized bed. 52 hours Total SLT 08
17
Main references supporting the Course: 1. Octave Levenspiel, Chemical Reaction Engineering, 3rd Edition, John Wiley & Sons, New Delhi 2001. Additional references supporting the course: 1. H. Scott Foggler , Elements of Chemical Reaction Engineering, 3rd Edition, Prentice Hall 2001. 2. James J. Carberry, Chemical & Catalytic Reaction Engineering , McGraw Hill - 1976.

1 2 3 4 Name of Course Course Code Designation of the course Rationale for the inclusion of the course/module in the programme Instrumentation and Process Control 10CH6DCIPC Departmental Core The whole foundation of Industrial Processing and Manufacturing lies in measurement and control of Materials and Products, Operating Conditions like Temperature, Pressure And Vacuum, Flowratesetc right from the stage of Raw Materials to the Finished Products. This requires thorough Instrumentation and Process control. Thus, it is integral and vital to any industry including the Chemical and Allied industries. Semester VI/ III Year Face to Face L 4 T 0 P 1 Total Guided and Independent Learning Total = 5 credits
5 6
7 8 9
Credit Value 5 Prerequisite (if any) Engineering Mathematics Objectives: Provides fundamental concepts of instrumentation and process control with an emphasis to the Chemical Industry. Concepts of the functions and characteristics of instrumentation commonly employed for the measurement of temperature and pressure. Formulation of first order and second order systems from the basics and the analysis of their responses to standard inputs. Evaluation of behavior of P, PI, PD and PID controllers, control systems stability using tools like root locus and frequency response methods. 10 Course outcomes: By the end of the subject, students should be able to: CO 1. Identify the appropriate instruments for a application and evaluate its performance. CO 2. Formulate transfer functions and predict responses to various forcing functions. CO 3. Evaluate the response behaviour of P, PI, PD and PID controllers. CO 4. Verify the stability of control systems. 11 Transferable Skills: Fundamental knowledge of unit operations, calculus, complex numbers and Laplace transforms. Problem solving skills Analysis and decision-making skills 12 Teaching-learning and assessment strategy: Teaching-learning Methods Classroom lectures Lecturer-led problem-solving sessions Student-led problem-solving sessions Co-operative learning Laboratory Interaction Direct Assessment Strategies Continuous internal evaluation (CIE) done by Test 1, Test 2 & Test 3. Best two tests are

considered for the CIE Quiz 1 Lab examination Viva voce Semester End Examination (SEE) Indirect Assessment Strategies Assignments Lecturer observation during the class room sessions Lab practice Synopsis: Instrumentation and process control technology is the tool that enables manufacturers to produce a desired product with a minimum of raw materials and energy. Hence, it is integral to any industry. This course aims to provide the fundamental concepts of Instrumentation and process control with emphasis on first and second order Systems. Mode of Delivery: Classroom lectures Classroom interactive sessions Laboratory practice sessions Assessment Methods and Types: The assessment for this course will be based on the following: Coursework (CIE) 10 % Test 1 05% Quiz 10% Test 2 25% Laboratory CIE 50% Semester End Examination (SEE) Assessment 100%
13
14
15
16
Content outline of the course/module and the SLT per-topic SLT L T P Total 10 10 Details Instrumentation: 10 Fundamentals static and dynamic characteristics.Indicators and recorders. Pressure measurement-Bourdon, diaphragm and bellow type gages. Vacuum measurements, temperature measurement-Bimetal and resistance thermometers, thermocouples and pyrometers. First order systems: 10 The thermometer, level, mixing tank,STR; Linearization; 1storder systems in series. Response for various inputforcing functions.
Unit-1
Unit-2

Unit- 3 Second order systems: 10 Characteristics of manometer and dampedvibrator. Transfer functions, response for various input forcing functions, response for step input for under damped case Terms associated with it, transportation lag. Closed loop system: 10 Basic components, servo and regulator control.Controllers P, I, D and On Off modes. Controller combinations Finalcontrol elements - Valves, actuators and valve positioners. Closed loop response: Block diagram, closed loop transfer function, transient response of servo and regulator control systems with various controller modes and their characteristics. Stability: 12 Stability of linear control systems, Routhtest, frequency response Bode diagrams. Control system design by frequency response: Bode criterion,gain and phase margins, ZieglerNichols controller tuning, Cohen-Coon controller tuning. Root locus: Rules for plotting and problems. 1. Thermometer 3 hours/week 2. Single tank - Step Response 3. Non Interacting Tanks - Step Response 4. Interacting Tanks - Step Response 5. Pressure Tank 6. U Tube Manometer 7. Single tank - Impulse Response 8. Non Interacting Tanks - Impulse Response 9. Interacting Tanks - Impulse Response 10. Level control P controller, PI controller, PD controller, PID controller 11. Valve characteristics. Total SLT 52 hours 10
10
Unit- 4
12
Unit- 5
17
Laboratory
Main references supporting the Course: 1. Coughanowr& Koppel, Process System Analysis and Control, McGraw Hill, New Delhi, 2nd edition, 1991. Additional references supporting the course: 1. Coulson & Richardson, Chemical Engineering, Vol. III, 3rd edition, Pergamon press, 1998. 2. George Stephanopoules, Chemical Process ControlAn Introduction to Theory & Practical, Prentice Hall, New Delhi, 1998.

1 2 3 4 Name of Course Course Code Designation of the course Rationale for the inclusion of the course/module in the programme NON CONVENTIONAL ENERGY TECHNOLOGY 11CH6DCNET Departmental Core The conventional energy sources are not proportionally distributed among countries. Further with the new wave of environmentalism running, the emphasis on fossil fuels as the source of energy has shifted to explore the possibility of non-conventional sources of energy harvesting which are clean and renewable. Energy Security, sustainability and environmental concerns in the World and in particular India are the major factors behind inclusion of this course to educate future engineers to renewable and non-conventional sources of energy. Semester VI / Year III Face to Face L 3 T 0 P 0 Total Guided and Independent Learning Total = 03 credits
5 6
7 8 9
Credit Value 3 Prerequisite (if any) Material science, Pollution control. Objectives: 1. To understand World and Indian scenario with respect to conventional and non-conventional energy situation. 2. To learn the principles and important design aspects behind various renewable nonconventional energy sources like Solar, Wind, Geothermal, fuel cell, hydro energy etc. 10 Course outcomes: By the end of the course, students will be able to: CO 1. Familiarize with the various forms of energy resources and its global distribution with its environmental impacts. CO 2. Familiarize the various non-conventional energy resources and design requirements for its economical utilization. CO 3. Design basic aspects to establish non-conventional energy harvesting units. 11 Transferable Skills: Knowledge of current energy distribution (local and world scenario) Distinction between conventional and non-conventional energy resources Distinction between Renewable and non-renewable energy resources Knowledge to estimate non-conventional energy resource and knowledge of harvesting device Literature and data searching skills Independent study and self-learning skills 12 Teaching-learning and assessment strategy: Teaching-learning Methods Classroom lectures and Power point presentations Lecturer-led case-study sessions Individual and team work to innovate the design of energy capture and conversion Independent study to get acquainted with recent technologies Direct Assessment Strategies

Continuous internal evaluation (CIE) Test 1, Test 2 & Test 3. Best of average Quiz 1 & 2 Brainstorming sessions Semester End Examination (SEE)
13
14 15
Indirect Assessment Strategies Assignments Lecturer observation during presentations Participation of students during interactive discussion Synopsis: The course aims to make a general introduction to the field of alternative energy resources and their potential with their importance towards the ecosystem at local and worldwide aspects. The students will understand the conventional fuel draw backs and their uneven availability in the planet earth. The status of global and regional energy consumption pattern along with environmental impacts. The subject provides the insight in to the non-conventional energy resources such as Solar, Wind, Geothermal, Hydro power and alternative fuel such as Biomass and Fuels cell. Importance is given for economical harvesting methods with respect to transformation to other forms of energy and engineering design aspects. Mode of Delivery: Classroom lectures, Overhead presentations, Case study team discussions Assessment Methods and Types: Coursework Continuous internal assessment 20% Test 1 20% Test 2 10% Quiz 1 & 2 50% Semester End Examination Assessment 100% Content outline of the course/module and the SLT per-topic SLT L T P Total 05 06 Details
16
UNIT I
UNIT II
Introduction 05 Man and Energy. Worlds and Indias production and reserves of energy, present and future power position, Need for alternate energy, Energy alternatives. Solar energy 06 Introduction, Extraterrestrial solar radiation, Radiation at ground level, Solar collectors, Solar cells. Applications of solar energy.

Biomass & Geothermal 12 Introduction to Biomass & it energy, Biomass conversion, Biogas production, Ethanol production, Pyrolysis and gasification, direct combustion, applications of biomass energy. Recovery of thermal conversion products Combustion of waste materials & related calculations, Waste incineration with heat recovery and uses of Refuse Derived Fuels (RDF) Geothermal Energy: Introduction, resource types, resource base applications for heating and electricity generation. Case Study of Biomass & Geothermal Energy. Wind and hydro energy sources 10 Introduction: Basic theory, types of turbines, applications, Hydropower: Introduction to basic concepts, site selection. Types of turbines, small scale hydropower. Case study Hydel power plants Fuel cells 06 Introduction, Principle and operation of fuel cells, Classification and types of fuel cells and applications of fuel cells. 39 hours 12
UNIT III
10
UNIT IV
06
UNIT V Total SLT 17
Main references supporting the Course: 1. G.D.Rai, Non-conventional energy resources, 4th edition, Khanna publications, New Delhi, 2008. 2. B. H Khan, Non-conventional energy resources, Tata McGraw Hill, New Delhi. 3. Fuel Cell Handbook, EG & G Technical Services, 7th edition, Inc. U.S., Department of Energy Office of Fossil Energy, National Energy Technology Laboratory. Additional references supporting the course: 1. Harker and Backhurst, Fuel and energy, Academic press, London, 1981. 2. S. P. Sukhatme and T. K. Nayak, Solar energy-Principle of thermal collections and storage, 3rd edition, Tata McGraw Hill, New Delhi. 3. R. K. Hegde and Niranjan Murthy, Energy engineering, 1st edition, Sapna Book House publications, 2011.

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BMS College of Engineering, Bangalore -19

(Autonomous College under VTU) Department of Chemical Engineering

BMS College of Engineering, Bangalore -19

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BMS College of Engineering, Bangalore -19

B.M.S. COLLEGE OF ENGINEERING, BANGALORE-19

B.M.S. COLLEGE OF ENGINEERING, BANGALORE-19

B.M.S. COLLEGE OF ENGINEERING, BANGALORE-19

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UNIT V Total SLT 17

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