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Jutharat Intapun
Consequences on
dry rubber properties?
Po, PRI and
mesostructure
Objective
1. Characterization of industrial maturation conditions
7m
3m
Cup coagula pile
20m
depth
0cm
RH %
Temp °C
50cm
3m 100cm Digicon HT765232
Humidity/temperature
20cm 150cm meter
200cm
probe
Figure1. Coagula maturation pile equipped with two drilled stainless steel tube
10kg
Delivery day 10 kg
baskets
0 cm
10kg Creping of 10 kg Drying of crepe
50 cm 10kg sample
100 cm 10kg
150 cm 10kg
Po,
Po PRI and
200 cm 10kg mesostructure
Drying in Factory
129°C, 3h
21 passes
Figure 3. Cup coagula Processing
2.2 Maturation device at labscale
factory pile maturation
-conditions
-rubber properties
Factory to laboratory
laboratory maturation
- Monoclonal coagula
-T°, RH, O2 controlled and
recorded
3. The effect of micro-organisms on cup
coagula properties
Clean Latex
- Microorganisms controlled
by antibiotic adding or
various inoculum added
Maturation boxes
At 40C for 34
days
40
70
35 60 10
50
30
40 5
25 (b)
30
20 20 0
0 50 100 150 200 0 50 100 150 200 0 50 100 150 200
Depth of coagula pile (cm)
Depth of coagula pile (cm) Depth of coagula pile (cm)
Figure 4. Temperature, Relative humidity and oxygen content with depth of the pile
Measurements were performed at 8 AM ( ), 12 AM ( ) and 4 PM ( )
1.2 Properties of cup coagula from maturation pile
Po (Po Unit)
PRI (%)
0 5 10 15 20 25 30 35 40 45
0 5 10 15 20 25 30 35 40 45 50
0 25.9
0 25.9
31.3
Depth of pile (cm)
-50 21.1
0 41.0 0 869.7
Depth of pile (cm)
42.5 1038.2
Figure 5. Po, PRI, Gel content and Molar mass of cup coagula with depth of the pile
Results and discussion
in laboratory
Results and discussion
6 passes 1616passes
+7,11, and 18 passes
Drying in Factory
129°C for 3hr
21 passes
50
45
40
Po (median)
35
30
25
20
Drying conditions
30
25
PRI
20
15
10
120-2 120-2.5 120-3 125-2 125-3 control
125-2.5
Drying conditions
2.2 Scaling down : Maturation boxes
Maturation box
P0 / P30
20
20 20
10
10 P30 10
0 0 0
0 4 15 28 34 0 4 15 28 34 0 4 15 28 34
75 75 75
PRI
PRI
PRI
50 50 50
PRI 25 25 25
0 0 0
0 4 15 28 34 0 4 15 28 34 0 4 15 28 34
50
40
30 PRI
20
10
With micro-organism
0
N+F+M+ N+F+M- N-F+M+ N-F-M+ Each Pair
Student's t
code 0.05
120.0
3x104 CFU/ml
The drop of PRI is 100.0
proportional to the
initial quantity of 5x105 CFU/ml
80.0
PRI
0.0
0 1 2 3 4 5 6
Maturation time (days)
• Drying : 2 hr at 125°C
Conclusions (3)