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Introduction
positive displacement pumps, where the fluid fills enclosed chambers and is moved
forward by the mechanical movement of the parts of the machine (ram extruder in
processing of thermoplastic)
drag flow pumps, in this case the fluid fills a region between two surfaces, where one
is in motion.
The relative movement of the two surfaces drags the fluid along a channel, gradually
pressurising and forcing it through a die. The second mechanism has some technical
solutions developed along the years, but the simplest machine is the drum flow pump or
drum extruder invented by Gabrielli (1952) apnd White and Potente (2003). In this
machine, the material to be pumped is put on an annular space between the rotating drum
and surrounding barrel. The rotation of the drum carries the liquid to a position where
there is a wiper bar that diverts the liquid into the die. The die pressurises the liquid and a
pressure gradient develops along the length of the channel between the drum and the
barrel. A complete study about behaviour of extrusion processes involve an estimative on
thermo-physical parameters, mainly related to screw, where its geometry, polymer
rheology, and processing conditions must be considered. Breaux et al. (2009), Chung
(2000) and White and Potente (2003) describe the extrusion process to a standard single
screw extruder into three zones related with screw design. The performance of an
extrusion process can be improved substantially by optimisation of the screw design.
Summarising, the screw performs three basic functions:
melting function
In most applications, these three functions occur simultaneously along screw length and
they are strongly interdependent. The size of a screw is described by its diameter and
length or length-to-diameter (L/D) ratio. Chung (2000) used geometrical names to the
three different sections:
Feeding section at the hopper end with a constant, deep channel depth called
feeding depth. In this region conveying of a solid bed from compacted pellets
occurs. Pressure increases steeply along the screw but cannot reach high values in
smooth barrel extruder without the phenomenon of melting of the superficial layer in
contact with the barrel hence releasing any extra pressure.
Metering section or pumping section at the die end with a constant, shallow channel
depth called metering depth. Breaux et al. (2009) define this zone as delay
where the molten film of polymer increases in thickness and possibly permeates the
solid bed itself. This condition occurs at the end of the feed zone of the screw.
A compression section (or transition section or melting section) between the feeding
section and the metering section with a decreasing channel depth.
In this region occurs the melting process, when the melt film has increased up to a point
where it runs through the solid bed of ever decreasing width as presented in Figure 1.
Breaux et al. (2009) identify a forth section in the direction of the end of the
compression zone and in the metering zone the solid bed is completely melted and there
is melt conveying only. Throughput in the conveying zone is the combination of screw
rotation that provides the drag flow and the pressure gradient in the screw channel. When
the pressure gradient is positive it blocks the drag flow, while it promotes the flow when
it is negative. Throughput is constant along the channel, while pressure development start
from atmospheric pressure and ends at back pressure imposed on the screw in the case of
injection moulding, or at atmospheric pressure at the die exit in the case of extrusion. For
the extrusion process, the level of back pressure is the result of the combination of die
and screw.
Figure 1
these, a calculation methodology was made. With this calculation methodology it was
proposed the verification, dimensioning and choosing of the main components as screw
extrusion, stepper motor, worm gear and barrel. The vertical configuration designed to
the screw extrusion head allows better use of space design as well as the arrangement of
the drive system.
Case study
For a desktop 3-D printer an alternative and interchangeable head design the users
requirements and technical characteristics were defined:
Raw material related to the use of different forms (pellets, powder, solids) and
in reduced amount. In bioengineering applications the use of powder material to
generate prototypes is highly indicated due to commercial availability. The use of
powder raw material is common in the polymer industry, especially in injection
and extrusion moulding. In non-commercial AM machines, specifically desktop
3-D printers, the solutions found are: syringe injection (Malone and Lipson, 2007),
thermoplastic filament extruder (Inforatti Neto et al., 2012) and transport extrusion
system for previously melted biopolymer (Almeida et al., 2008); all of them on opensource design.
Figure 2
(a) Fab@CTI desktop 3-D printer and (b) syringe head extruder and fused deposition
modelling head (see online version for colours)
(a)
Source: Inforatti Neto et al. (2012)
(b)
The Fab@CTI 3-D printer platform was designed from of the following demand:
Inforatti Neto (2013) presented a technical design feasibility of the mini screw with
variable section head. The users requirements composed by users researcher were raised
at design phase and obtained from quality function deployment (QFD) analysis described
in Cheng and Melo Filho (2007). The list of users requirements was translated into
technical characteristics which supports the constructive solutions choice to mechanical
design of extrusion mini-head. The most important users requirements identified by
QFD were:
The -PCL was the biomaterial chosen for the device trials and this material is related to
other previous studies (Rezende et al., 2012; Inforatti Neto et al., 2012) in the health
area. The choice of the polyamide is related to the reuse of material discarded
from commercial machines. In this case, the availability of the material in the laboratory
(CTI), in its non-degraded and degraded form, result of previous prototyping processes
by selective laser sintering (SLS) and second, its wide use in industrial parts.
The conceptual design uses the technical requirements which are identified as having
greater importance in the phase before (informational design). There are some which
have the objective to proportion a technical system to be understood as functions of the
design subsequently related to technical items or components, and, on a higher abstract
level, find innovative solutions or just improvements of technical solutions. The outcome
of this step for the preliminary design is one or more sketches of technically viable
solutions. For the development of the mini-head design of extrusion functions of
technical developments of the head and of the structure material functions technical
elements inside the 3-D printer system were extracted, which is presented in Figures 3
and 4, using one of the engineering techniques of systems that relate Energy (E); Material
(M) and Signal (S).
Figure 3
Figure 4
Inside the technical system 3-D printer, the production of the prototype piece is the
principal function of the machines engineering design. In Figure 7(b) the production
process of the piece is detailed, and for each described function, decisions of the design
should be made based on conventional and alternative solutions which contemplate
restrictions of this design, as there is the heads weight in relation to the machine,
reduced spaces, and portability and low costs. Thus, starting from the information
obtained with the QFD, a set of the designs parameters was chosen to find technical
solutions. To organise the choice of solutions a morphologic picture was mounted,
presented in Figure 5.
The first option of technical solutions is presented by the arrows, to attend the
designs restrictions described beforehand as shown by Table 1.
The choice of the deposition material in the form of powder was made in function of
its availability on the market and the possible mixtures with additives and other materials.
The step motor to start the head was chosen for its control facilities and adjustment
beforehand tested with the systems of injecting by syringe and filament.
Morphologic analysis
Table 1
Components
Design functions
Structure
363.10
16.6
Barrel
335.19
15.4
Extrusion screw
837.98
38.5
Stepper motor
90.50
4.14
Gearbox
335.19
15.3
111.73
5.12
Temperature sensor
18.44
0.84
Nozzle
16.75
0.77
Mechanical coupling
33.52
1.54
Thermal blanked
22.35
1.02
Ball bearings
22.35
Total cost
2187.1
1.02
100
The heads structure will be interchangeable to couple with other processes of deposition
(Inforatti Neto, 2007; Inforatti Neto et al., 2012). A big part of the fixation done
together with screws, mainly due to the easiness with which they can be bought,
mounted, and subsystems can be maintained. In this first study, the extrusion will be
made with a simple screw to test the concept of extrusion in the deposition process, so the
polymers thermal effects in the cylinder part of the screw of the materials chosen, the
easiness of assembly and manufacture can be studied. The die of extrusion is
interchangeable to enable diverse diameters of the thread of material when exiting the
machine. So, different resolutions and superficial finishings of the piece are possible.
The feeding of the material is done by gravity using a mixer consisting of a rotating shaft
coupled to the screw during the feeding phase to avoid the compression of the material.
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The raw-material for the extrusion is made of polymers and was chosen because of it is
so easily manipulated in the extrusion process. The mechanism of heating up will be
carried out by electric resistances because they can be wrapped around the external
cylinder in the extrusion process to guarantee controlled heating throughout the whole
process of extrusion. On the basis of the data provided by the suppliers and our own data
on estimates for the Fab@CTI printer an initial estimate for the costs of the extrusion
head was made, presented in Table 1. The analysis of the value has the purpose to
estimate the costs of each one of the components as well as their functions making it
possible to analyse the economic impact of each part of the head more precisely. This is
because of the choice of the material of the screw: titanium alloy (changed by stainless
steel) for the extruder and the difficulty to find a commercially produced screw with the
required dimensions (~150 mm long and 7 mm in diameter). With the procedures
adopted, the conception design and the initial costs (based on Value Analysis Technique)
of the head were estimated and are represented in Table 1, and an outline of the technical
solution for the extrusion head is presented in Figure 6.
Figure 6
Calculation procedures
With the aim to ensure strength and performance required, calculations to define the
geometries of the extrusion screw and barrel were done. Calculation procedure was based
on technical literature of standard industrial extrusion screw. A functional prototype was
fabricated and assembled. From the theory described in item 4, were obtained the main
design parameters of the barrel-screw and actuation system. Usually, the screws are not
subjected to a high bending force because they run inside a strong rigid barrel and the
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clearance between screw and barrel is small, around 0.00050.002 (White and Potente,
2003). The small gap between screw and barrel prevents solidification by cooling of the
melt. Leakage flow caused by the clearance between the inner barrel and screw flight
reduces the melting efficiency also. Then, the manufacturing process of extrusion screw,
in this case, must have high precision. The critical strength requirement is mechanical
resistance to torque that is very dependent of polymerics material type. In this step, a
pre-calculation was made considering some geometric and fluid characteristics to the
mini screw as well as the head extruder. In this step, calculations were made considering
some geometric and fluid characteristics to the extrusion screw as well as the head
extruder in general. The flowchart presented in Figure 7(a) shows a simplified sequence
of calculations applied in a single screw extrusion head to a portable 3-D printer
(Fab@CTI). The procedure of the calculation was based on Rauwendaal (2001) and
Chung (2000).
The transmission system chosen was a gearbox (worm gear). This first choice has
considered the high transmission ratio as well as the space restrictions. The polymers
viscosities were considered to selection of the stepper motor and those are directly related
with power and torque characteristics represented in Figure 7(b).
Figure 7
(a) Flowchart related to calculation procedure and (b) design parameters to choice of the
gearbox (see online version for colours)
(a)
(b)
12
Nylon 12 was the first polymeric material used to obtain some important materials
properties such as the relationship: shear rate and linear velocity. Polyamide (Nylon 12)
is a semi-crystalline polymer which is highly hygroscopic and because of this
characteristic it should be taken to a greenhouse with air ventilation, before being
processed. Its processing temperature is higher than 240C, having a melting temperature
in a narrow range and oxidises easily when exposed to hot air and it presents low
viscosity after being fused. With these properties this material needs a dosage zone with a
constant shallow canal, to avoid fluctuations due to its low viscosity. The control of
polyamide viscosity in different extrusion velocities, rheometry analysis of virgin and
degraded materials were considered and the objective was the determination of
rheological curves of these samples at 225C. From the rheometry analysis it was
possible to observe the shear strength of the non-degraded polyamide is significantly less
than the degraded one, probably due to the thermal and mechanical solicitation, which are
suffered in previous processing, this information are available in Inforatti Neto (2013).
This means when leaking, through the extrusion process the non-degraded polymer offers
less resistance to shearing, and therefore needs less energy in the activation of the
extrusion screw to flow along the extruders body. However, the rheometry analysis
indicated a higher resistance in the case of -PCL shearing and thus, calculation of the
gearbox was based on the torque moment of -PCL. Figure 8 presents the input design
data and calculated design parameters.
Figure 8
(a) Main input and output design parameters and (b) AISI stainless steel 304
for mini-screw (see online version for colours)
(a)
13
(a) Main input and output design parameters and (b) AISI stainless steel 304
for mini-screw (see online version for colours) (continued)
(b)
The screw extrusion design presents three sections and it was developed considering
mechanical strength to the torque caused by the turning into the viscous melted polymer
material. The mixer in the feed section was proposed to avoid the caking of the powder
material which would cause the locking of the screw and bubbles formation in the
polymer material. Figure 9(a) presents a mock-up of the constructive solution for
extrusion head and Figure 9(b) presents the functional head assembly stand alone for
preliminary experimental tests.
Figure 9
(a) Mock-up and (b) functional mini screw head (see online version for colours)
(a)
(b)
From the detailed design, it was generated a mock-up to verify the assembly system
and kinematics aspects. The following step was the manufacturing of a functional
prototype. Machining processes and additive manufacturing were used in the fabrication
of this prototype. Finally, experimental tests were conducted to investigate the capacity
of extrusion head to generate continuous filaments from powder raw material.
The preliminary tests showed the generation of continuous filaments with no large
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This initial test is important to demonstrate the capacity to transform the polymer powder
in a melted polymer. The expected performance for the feed section is carrying the
material to the downstream sections. The continuous filaments obtained reflect an
adequate performance in the compression and metering section. In these sections, the
rising pressure forces the melted polymer through the nozzle tip with the aim to produce
continuous filaments demonstrating the conceptual design of create filaments from
powder using polymers in a screw extruder of small proportions. This concept is based
in an idea of using the known extrusions process in a small scale. In Figure 12, it is
shown the nozzle tip of the extrusion head performing the manufacturing a Polyamide
Nylon 12 15 layers block, without air gap, and 0.8 nozzle tip, showing the capacity of
generating parts extruding layer by layer as it is required in rapid prototype purposes. The
morphological characteristics were analysed with scanning electron microscopy (SEM).
The photomicrographs were obtained in the Instrumental Chemical Analysis Center of
the So Carlos Chemical Institute (CAQI/IQSC/USP) in ZEISS LEO 440 (Cambridge,
England) with detector OXFORD (model 7060) equipment, operating with electron beam
of 15 kV. The samples were covered with 10 nm of gold in a sputter Coating System
BAL-TEC MED 020 (BAL-TEC, Liechtenstein) and it was maintained in desiccators
until the moment of the analysis.
Figure 11 (a) Nylon 12 filaments and (b) photomicrographs
(a)
(b)
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It is possible to observe in Figure 11(a) that the filament generated from Nylon 12
powder is homogeneous. In Figure 11(b), it can be seen that the material has a solid
surface without any pore or surfaces discontinuities.
For the -PCL material, SEM micrographs shows the total transformation of the
grains in feed section to solid homogenous material in compression section, the scheme
in Figure 13(a) and (b) shows the sections where the -PCL was collected and the
micrographs also. Figures 12(a) and (b) present an experimental test generating a scaffold
manufacturing with polyamide.
Figure 12 (a) The extrusion head constructing a Scaffold; (b) detailed view on the nozzle tip and
(c) Scaffold generate (see online version for colours)
Figure 13 (a) SEM for -PCL showing the material state and (b) morphological aspects in feed
and compression sections
(a)
(b)
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Conclusions
The innovative characteristics presented in this work are based on the fact that
the feeding of material is in powder form, its extrusion into filament and transformation
in the form of deposition layers occurs simultaneously. Control of process parameters
such as temperature and extrusion output stream of material contributing to the quality
of the material constituting the 3-D model obtained. The miniaturisation of the subassembly barrel-screw applied to AM machines is other important aspect of this design
development. The preliminary tests of the head showed the capacity of extruding melted
material producing continuous filaments demonstrating the performance of each section
of the screw extrusion. The transmission system, including the stepper motor, presented a
satisfactory performance, mainly related to driving control systems, once it was shown
the screw extrusion head capability to fabricate a block composed by various layers
characterising the application in additive manufacturing. The results present the potential
of this interchangeable screw extrusion head to provide new opportunities for desktop
3-D printers in several applications using powder as feedstock with the aim to generate
3-D models.
The use of QFD support the identification of the more important design
characteristics that lead the choices during design development. The use of mock-up and
additive manufacturing are important to previously identify assembly failures reducing
the design time. The preliminary tests of the head showed the capacity of extruding
melted material (SEM photomicrographs), which showed homogeneous and continuous
filaments, a necessary condition for layer deposition purposes demonstrating the
performance of each section of the screw extrusion. The results present the potential of
this interchangeable screw extrusion head to provide new opportunities for desktop 3-D
printers in several applications using powder as feedstock with the aim to generate 3-D
models. In direction of new additive manufacturing correlated areas as health, tissue
engineering and biomaterial applications, this new device presents results using -PCL as
powder material and has demonstrated its capacity to produce scaffolds. As future works,
it is proposed the optimisation of the extrusion process using design of experiment (DOE)
and RSM looking for the best mechanical settings coupling with material properties. The
use of new materials, in specific thermoplastics, is a promising area towards the material
sciences applications in additive manufacturing, more specifically, in desktop 3-D printer
machines. The blend or mixture of two or more kinds of polymers in feed section and its
respective study is another possibility of research.
Acknowledgements
The authors thank to the CNPq (Brazilian Counsel of Technological and Scientific
Development) for the financial support.
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