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Article history:
Received 17 July 2013
Accepted 5 December 2013
Available online 13 December 2013
Keywords:
Lightweight aggregate concrete
Shrinkage
Fly ash
Silica fume
Nanosilica
a b s t r a c t
A comprehensive experimental study was carried out on the shrinkage behaviour of structural expanded
clay lightweight aggregate concrete (LWC), taking into account different compositions, types and initial
wetting conditions of lightweight aggregates (LWA). The inuence of different compositional parameters
on shrinkage, such as the type and volume of aggregate, the w/c ratio, the binder content and the partial
replacement of normal aggregates by LWA was analysed. The shrinkage of LWC depends on how the volume of LWA varies. The inuence of different pozzolanic materials was also studied, namely, silica fume,
nanosilica and y ash. Depending on the type, content and reactivity of the pozzolanic additions, the
shrinkage was higher or lower than that of LWC without admixtures. The initial wetting condition of
LWA had little inuence on the long-term shrinkage. The LWC with the most porous aggregates is more
affected by the cross-section geometry of concrete in that it is more susceptible to differential shrinkage.
Current standard expressions did not properly predict the shrinkage behaviour of LWC. Multiplier coefcients of about 1.3 for the most common structural LWA and about 1.6 for more porous LWA are suggested, to take into account the higher long-term shrinkage of LWC.
2013 Elsevier Ltd. All rights reserved.
1. Introduction
It is well known that the shrinkage of concrete is essentially
governed by the paste, which is the source of contraction of the
system, and by the aggregates that oppose this contraction. Since
structural lightweight aggregate concrete (LWC) is modied at
these two factors, it is expected that its behaviour differs from that
observed in normal density concrete (NWC).
On the one hand, the use of less rigid porous aggregates decreases the restriction effect on paste deformation [13]. On the
other hand, either for strength purposes or for reasons of workability and stability of the mixes, LWC is usually characterized by larger volumes of better quality paste and lower volumes of coarse
aggregates than NWC [4,5]. Therefore, the long-term shrinkage of
LWC should be higher than that of NWC of the same strength.
However, the paste quality is higher in LWC, which increases the
matrix stiffness. Moreover, the water absorbed by lightweight
aggregates (LWA) is later released into the paste by internal curing,
which compensates for the initial water lost by drying and selfdesiccation.
According to Kayali et al. [2], the improved aggregate-paste
interface in LWC helps to enhance the restriction effect of the
LWA. Moreover, because of the internal curing and the prolonged
Corresponding author. Tel.: +351 218418226; fax: +351 218418380.
E-mail address: abogas@civil.ist.utl.pt (J.A. Bogas).
0261-3069/$ - see front matter 2013 Elsevier Ltd. All rights reserved.
http://dx.doi.org/10.1016/j.matdes.2013.12.013
1040
2. Experimental programme
2.1. Materials
Three Iberian expanded clay lightweight aggregates were used
(Leca and Argex from Portugal and Arlita from Spain). Their total
porosity, PT, particle density, qp, bulk density, qb, and 24 h water
absorption, wabs,24 h, are indicated in Table 2. A more detailed
microstructural characterisation of these aggregates is presented
elsewhere [4,21]. In terms of their specic properties, the selected
LWA are categorized as type A (Arlita), B (Leca) and C (Argex),
which represent LWA of low, moderate and high porosity (Table 2).
Normal density coarse and ne aggregates (NA) were also used. For
the reference normal density concrete, two crushed limestone
aggregates of different sizes were combined so as to have the same
grading curve as Leca (20% ne and 80% coarse gravel). Fine aggregates consisted of 2/3 coarse and 1/3 ne sand. Their main
Table 1
Shrinkage estimation main standard documents.
Standard
Observations
csh Represents the product of several factors that take into account the curing time
EN1992 [19]
(NWC)
Kh, bRH, ads1 e ads2 Are coefcients depending on the notional size (h0), the relative
humidity (RH) and the type of cement (ads1;ads2)
(tc), the relative humidity (RH), the cross-section geometry (vs), the slump (s), the
percentage of ne aggregate (w) and the air content (a)
3=2
(LWC)
MC 2010 [20]
(NWC)
bds t t s t t s =t ts 0:04 h0
eca(t) = [1exp(0.2t0.5)]eca0
eca0 = 2.5(fck10)106
ecs (t, ts) = g3ecd + eca
ecs (t, ts) = ecd + eca
ecd (t) = ecd,0bRHbds (t, ts)
ecd,0 = [(220 + 110ads1)exp(ads2fcm/10)]106
2 0:5
(LWC)
bds t t s t ts =t t s 0:035 h0
eca(t) = [1exp(0.2t0.5)]eca0
eca0 = aas[(fcm/10)/(6+fcm/10)]2.5 106
ecs (t, ts)LWC = gecs (t, ts)NWC
esh,t shrinkage strain after a period of time t; esh,u ultimate shrinkage strain; (v/s) volume/area ratio of the concrete element.
ecs (t, ts) shrinkage strain between the age t and the begining of drying ts; ecs0 ultimate shrinkage strain.
ecs total shrinkage strain; ecd drying shrinkage strain; eca autogenous shrinkage strain.
fcm or fck average or characteristic compressive strength at 28 days.
1041
2620
1416
0.2
0/2
Coarse sand
2610
1530
0.5
0/4
Lightweight aggregates
Fine gravel
Coarse gravel
2631
1343
1.4
4/6.3
33.3
2612
1377
1.1
6.3/12.5
30.5
Type A
Type B
AF7
03
412
24
Type C
38F
1290
738
12.1
52
3/10
1060
562
59
0.5/3
1068
613
12.3
60
4/11.2
865
423
22.9
67
4/8
705
397
23.3
73
6.3/12.5
Table 3
Main characteristics of cement, y ash and silica fume.
Parameter
Standard
Fly ash
Silica fume
Cement I 52.5 R
EN 451-2
EN 196-6
EN 196-1
10.2
83.7b
103.1b
0.5a
6.5
83.0
3.38
0.36
2.33
92.0a
106.7c
3.7
94.0
0.83
not detected
2.25
1.1
5102
40.4
62.7
0.5
1.64
29.1
61.6
1.45
3.11
2 days
28 days
EN
EN
EN
EN
EN
EN
EN
196-1
196-1
196-3
196-7
196-2
451-1
196-6
Table 4
Concrete mix proportions, dry density, compressive strength and total shrinkage.
a
b
Mixes
Coarse
aggreg.
(m3/m3)
Cement
(kg/m3)
Addition
(kg/m3)
wag
(%)a
Sp/c
(%)
Effective
w/b (L/m3)
Oven dry
density, qd
(kg/m3)
fcm,28d
(MPa)
30
90
A350
A450
A450PM
A450PD
A525
VA425
ANS
AFA22
A35 (35%LWA)
A65 (65%LWA)
0.35
0.35
0.35
0.35
0.35
0.425
0.35
0.35
0.35
0.35
350
450
450
450
525
450
414
350
450
450
5.4
100
13.4
13.1
0
0
13.4
13.4
14.0
14.0
16.0
16.0
0.7
0.7
0.7
0.7
0.8
0.7
1.2
0.6
0.7
0.7
0.45
0.35
0.30
0.30
0.30
0.35
0.35
0.35
0.35
0.35
1789
1840
1839
1846
1872
1764
1838
1798
2150
2008
57.6
65.8
63.5
65.1
68.5
57.9
65.5
60.0
72.3
66.5
41
14
34
36
14
31
28
9
36
7
73
36
111
79
10
1
77
50
97
63
231
130
350
278
51
63
176
238
299
245
498
292
502
451
180
258
326
424
389
410
563
490
603
530
360
408
403
510
454
490
640
508
589
509
458
476
408
534
466
502
B350
B450_0.55
B450_0.45
B450
B450PM
B450PD
B525
B450_Wsp0.35
B450_Wsp0.5
VB400
VmB250
VmB425
BSF
BNS
BFA22
BFA40
BS450
B35 (35%LWA)
B65 (65%LWA)
0.35
0.35
0.35
0.35
0.35
0.35
0.35
0.35
0.35
0.4
0.25
0.425
0.35
0.35
0.35
0.35
0.35
0.35
0.35
350
450
450
450
450
450
525
450
450
450
522
414
414
350
270
450
450
450
36
5.4
100
180
23.4
19.5
19.5
24.5
0
0
24.0
20.0
20.0
24.0
23.2
23.9
23.4
24.0
24.0
24.0
24.0
22.2
22.2
0.6
0.0
0.2
0.7
0.7
0.7
0.8
1.0
0.0
0.6
0.6
0.7
0.9
1.0
0.7
0.7
0.6
0.6
0.6
0.45
0.55
0.45
0.35
0.30
0.30
0.30
0.30
0.50
0.30
0.35
0.35
0.35
0.35
0.35
0.35
0.35
0.35
0.35
1712
1540
1676
1740
1744
1753
1770
1678
1876
1675
1741
1754
1703
1668
1435
2112
1950
43.1
36.1
41.9
48.6
46.5
46.5
50.0
43.3
39.0
45.7
43.4
38.6
47.6
46.7
42.4
37.1
37.5
59.8
53.3
15
49
51
18
48
43
38
12
58
18
39
5
8
8
27
24
61
17
59
62
150
87
35
146
136
38
49
138
52
93
41
38
22
66
77
113
67
104
271
583
243
133
369
322
26
128
462
114
322
149
132
86
330
300
374
266
284
531
919
601
333
472
429
49
322
791
303
488
292
381
381
503
421
605
359
441
624
1065
759
493
586
496
184
563
928
511
558
415
537
448
594
468
733
422
529
658
1148
721
591
565
555
369
561
977
596
613
442
587
562
631
462
825
446
569
C450
NWC350
NWC450
0.35
0.35
0.35
450
350
450
19.4
0.3
0.4
0.7
0.8
0.7
0.35
0.45
0.35
1610
2264
2299
31.2
65.8
76.2
37
44
51
91
112
123
190
260
238
470
306
327
616
348
376
638
410
385
180
365
1042
For BS450, coarse sand was replaced by the lightweight sand (LWS)
indicated in Table 2 (type B 0-3). The maximum concrete aggregate
size was 12.5 mm.
LWC with initially dry LWA (PD) or pre-wetted LWA (PW) were
also produced to study their inuence on shrinkage. The PD aggregate was added during mixing after being dried at 200 C and the
PW aggregate was rst wetted for 3 min with 50% of the total
water, before mixing. Based on the method suggested by Bogas
et al. [24], the absorption of LWA in the mix was estimated beforehand to take into account the correction of the total mix water.
Modied normal density concretes (MND) were produced with
partial replacement of NA by 35 and 65 percent of type A LWA
(A35, A65) or type B LWA (B35, B65). The designations SF, NS,
FA22 and FA40 appear when 8% of silica fume, 1.3% of nanosilica
and 22% or 40% of y ash by weight of cement are used. The NS
content was dened based on previous experimental studies with
NWC carried out by the supplier. According to these studies,
about 0.15 kg of NS had the same effect on the compressive
strength of normal weight concrete as about 1 kg of silica fume.
Wsp refers to the mixtures without Sp.
100
0
-100
-200
-300
-400
-500
-600
-700
-800
-900
M (%)
cs (x10-6)
30
60
90
180
365
10
8
6
4
2
0
3
30
60
90
180
365
1043
w/c
0.25
0
cs (x10-6)
When the internal curing becomes less relevant (after about the
rst 730 days) there is a sudden increase in the shrinkage rate of
LWC compared to NWC. After this transition period, the shrinkage
of LWC is proportional to the water lost by evaporation (curve
inection in Fig. 3) and the less rigid type C LWA has the lowest
restriction effect on the paste deformation, which leads to higher
shrinkage rates (more stepped curve).
In the initial ages, the weight loss, DM (water lost by evaporation) in the LWC is not followed by a proportional shrinkage increase, conrming the effectiveness of the internal curing. But
this proportionality is found in the NWC from the rst days of drying. Because of the severe drying and the small equivalent thickness of the specimens, the shrinkage tends to stabilize after
about 912 months. This stabilization is slower in the LWC due
to the drying delay in early ages.
The difference between LWC and NWC stays almost the same,
taking into account the equal strength concrete NWC 350
(Fig. 2). In fact, varying the cement content for the same volume
of water has a small effect on shrinkage when the w/c ratio ranges
between 0.35 and 0.45 [26]. In this case, the reduction of the volume of paste is offset by the increment of the w/c ratio.
0.3
0.35
0.4
0.45
Type B (1 year)
Type A (1 year)
-200
-400
-600
R = 0.81
-800
Fig. 5. One year shrinkage versus w/c ratio.
cst (x10-6)
B450
A450
BS450
C450
NWC450
NWC350
M (%)
-100
-200
A450
ANS
ACZ22
B450
BSF
BNS
BFA22
BFA40
-300
-400
-500
-600
-700
cs (x10-6)
100
0
-100
-200
-300
-400
-500
-600
-700
30
60
90
180
365
M (%)
6
4
2
0
3
30
60
90
180
365
1044
cs (x10-6)
0
-100
-200
-300
-400
-500
-600
-700
-800
-900
-1000
-1100
-1200
30
60
90
180
365
B450
B450_0.45
B450_0.55
B450_Wsp0.35
B450_Wsp0.5
Fig. 6. Inuence of w/c ratio and superplasticizer on the total shrinkage and weight loss up to one year old.
w/c
cs (x10-6)
0.3
0.35
0
-200
-400
-600
-800
-1000
-1200
0.4
0.45
0.5
0.55
Type B (1 year)
R = 0.92
B450Wsp0.5
Fig. 7. One year shrinkage versus w/c ratio, for the same cement content (type B
LWA).
higher the volume of LWA the greater the efciency of the internal
curing.
The increment of the volume of type A aggregate from 350 L/m3
(A450) to 425 L/m3 (VA425) led to a shrinkage reduction at all ages,
although the long-term shrinkage was about the same (Fig. 8).
However, varying the volume of type B aggregate from 350 L/m3
(B450) to 400 L/m3 (VB400) had a small inuence on the shortterm and long-term shrinkage.
Therefore, there is a greater inuence of the volume of aggregate on the shrinkage of LWC with type A aggregate than with type
B LWA. On the one hand, since the stiffness of the type A aggregate
is higher, its replacement by natural sand has less inuence on the
restriction effect on the free deformation of the paste. On the other
hand, the greater amount of particles and the smaller maximum
aggregate size of type A LWA when compared to type B LWA
(Table 2), may have induced more effective internal curing.
Reducing the volume of aggregate without changing the mortar
characteristics implies a proportional increase of the volume of
sand and paste, with a corresponding increase of the shrinkage
(Fig. 9). In fact, the reduction of the LWA volume leads to a simultaneous increase of the paste content and a reduction of the volume of water available for internal curing. The inclusion of
cs (x10-6)
0
-100
-200
-300
-400
-500
-600
-700
M (%)
cs (x10-6)
Considering concrete mixes with different volumes of aggregates but with the same w/c ratio and cement content. On one
hand, since the replacement of sand by lightweight coarse aggregate implies a reduction of the mortar stiffness, increased
shrinkage would be natural. But on the other hand, the
-200
250
300
350
Type A (1 year)
-400
R = 0.78
-600
VB400
-800
Fig. 9. One year shrinkage versus the volume of aggregate.
30
60
90
180
365
6
4
2
0
450
Type B (1 year)
A450
VA425
VB400
B450
VmB425
VmB250
400
30
60
90
180
365
1045
M (%)
cs (x10-6)
3
0
-100
-200
-300
-400
-500
-600
-700
30
60
90
180
365
6
4
2
0
3
30
60
90
180
365
%FA
0
22
40
cs (x10-6)
0
Type B (1 year)
Type A (1 year)
-200
-400
-600
-800
Shrinkage increases at all ages in the LWC with 22% replacement of cement by y ash, regardless the type of LWA. However,
the difference is more relevant in the LWC with more porous
LWA (type B). The shrinkage increase in LWC with y ash is also
reported by Holm [8] and Haque [30], although the opposite was
reported by Malhotra [16]. Since the hydration reactions are slower
in y ash mixtures, their porous structure tends to be coarser, at
least in the early ages. Therefore, the drying rate increases and
the restriction on the paste deformation decreases (Fig. 10). On
the other hand, since the hydration reactions occur later, there is
less compensation for the water stored in the LWA and meanwhile
eliminated by evaporation. The absence of initial water curing and
the increasing volume of paste also affect the results.
Interestingly, although the shrinkage is lower in the LWC with
type A LWA, the water lost is slightly lower in the LWC with type
B LWA. Moreover, the long-term shrinkage of the LWC with 40% of
y ash is lower than that of the LWC produced without it (Fig. 11).
However, the water loss is higher in the LWC with 40% of y ash,
especially in the rst 6 months. This behaviour can be related to
the differences in the level of the paste hydration.
Since the mixes with a higher volume of y ash have a lower degree of hydration, there are more non-hydrated particles that work
as non-shrinkage microaggregates. Therefore, the volume of particles that act as a source of contraction is lower. Termkhajornkit
et al. [31] have conrmed that the shrinkage in NWC is affected
by the extent to which y ash hydrates, which is lower for higher
amounts. In part, this phenomenon may explain the difference observed in how shrinkage evolves in BFA22 and BFA40, after 30 days
(Fig. 10). In addition, the lower hydration level of the paste justies
the higher drying rate (Fig. 10) and the lower effect of the water
lost in the shrinkage of BFA40 (Fig. 3). The behaviour of the LWC
with type A LWA and 22% of y ash is between that found for
BFA22 and BFA40. This is probably because there is less water
available in type A LWA than in type B LWA, which means lower
levels of hydration in the LWC with type A LWA.
Fig. 11. One year shrinkage versus the percentage replacement of y ash.
cs (x10-6)
3
0
-100
-200
-300
-400
-500
-600
30
60
90
180
365
Fig. 12. Inuence of the total or partial replacement of normal weight coarse aggregate by LWA on the total shrinkage up to one year old.
1046
VLWA (L/m3)
0
35
65
100
cs (x10-6)
0
Type B (1 year)
Type A (1 year)
-200
-400
R = 0.73
-600
Fig. 13. One year shrinkage versus the percentage replacement of LWA.
cs (x10-6)
3
0
-100
-200
-300
-400
-500
-600
-700
30
60
90
180
365
Fig. 14. Inuence of the initial water content of LWA on the total shrinkage up to one year old.
100
30
60
90
180
365
cs (x10-6)
-100
-200
-300
-400
-500
-600
B450
B450_7D
B450_PR
NWC450
NWC450_7D
NWC450_PR
Fig. 15. Inuence of the specimen size on the total shrinkage up to one year old.
1047
cs (x10-6)
100
0
-100
-200
-300
-400
-500
-600
-700
-800
-900
-1000
-1100
-1200
30
60
90
180
365
cs (x10-6)
Fig. 16. Shrinkage curves and normative estimations for LWC with type B aggregate (w/c of 0.30.55).
100
0
-100
-200
-300
-400
-500
-600
-700
-800
-900
30
60
90
180
365
Fig. 17. Shrinkage curves and normative estimations for LWC with type A aggregate (w/c of 0.30.45).
In general, the expressions in the standards tend to overestimate the shrinkage of LWC with a w/c ratio up to 0.45, especially
at early ages. These expressions are not suitable for lightweight
concrete, since they do not take into account the shrinkage delay
caused by the internal curing.
Of the methods analysed, the one suggested by ACI 209R [18]
led to the best tted shrinkage curves at early ages. However, the
shrinkage estimation at later ages may be too conservative, particularly for LWC with a low w/c ratio or with LWA of high initial
water content. It is noteworthy that this report does not, for practical purposes, take into account the concrete composition and the
water content of the aggregates. The method is empirically based
and less reasonable for moderate to high-strength LWC.
The long-term shrinkage estimates from the expressions suggested by EN1992-1 [19] and MC 2010 [20] are within the experimental results obtained for low w/c lightweight concrete,
especially after a long drying period. However, the expressions
were totally inadequate for early ages. Moreover, the shrinkage
of common LWC with higher w/c ratio can be greatly underestimated in these recommendations. In fact, the long-term shrinkage
of LWC with w/c ratio above 0.45 is underestimated by more than
50% (Fig. 16). However, since multiplier factors for LWC are provided in EN1992-1 [19] and MC 2010 [20] these differences can
be smaller. Comparing just the one year shrinkage of LWC with
that of NWC with the same composition (Table 4), multiplier
f cm (MPa)
30 35 40 45 50 55 60 65 70 75 80
0
-200
-400
-600
-800
-1000
-1200
VmB425
BFA40
Type A
Type B
MND (Type A)
MND (Type B)
coefcients of about 1.3 for higher density LWA (type A) and about
1.6 for the more porous LWA (type C) are suggested.
The expressions suggested in EN1992-1 [19] and MC 2010 [20]
take the concrete composition into account indirectly through the
compressive strength. However, shrinkage does not depend on the
compressive strength but on the parameters related to the microstructure and composition of concrete, such as the volume of paste,
w/c ratio, degree of hydration and aggregate properties. Therefore,
there is a weak correlation between shrinkage and compressive
strength, as shown in Fig. 18.
5. Conclusions
The inuence of different compositional parameters on the
shrinkage of lightweight concrete was analysed by means of an
extensive experimental programme. The internal curing and the
lower stiffness of LWA are responsible for the lower initial shrinkage and the higher long term shrinkage of the LWC. Depending on
the type of LWA, the one year shrinkage of LWC was about 3065%
higher than that of NWC and about twice as high as that of NWC
when additionally there was a replacement of natural sand by
lightweight ne aggregates. The partial replacement of coarse NA
by LWA led to intermediate shrinkage curves relative to those obtained for concrete produced with only NA or LWA.
1048