2 hidrazin hidrat
3 Hidrazid
4 Acid clorhidric
5 nitrit de sodiu
6 bicarbonat de sodiu
7 Dietilamina
8 eter
9 Baloane
Hrtie 10 filtru
11. manta de nclzire
12 2 litri cu trei gturi balon cu fund rotund
Timp: aproximativ 36 de ore.
Procesul de:
PASUL 1: ntr-un balon de 2 litri cu trei gturi cu fund rotund
adaug la 2 grame de tartrat de ergotamin despre jumtate gram
de hidrat de hidrazin. Procedai cu atenie atunci cnd se adaug
hidrat de hidrazin, pentru c este foarte otrvitoare,
n special pentru ochi.
PASUL 2: Se pune o coloan de condensare pe una gtul
balon. Punei un dispozitiv de agitare n gt centru i
plasa o plnie de separare n gt gros. (Not:
hidrat hidrazida poate fi adugat printr-o separare
plnie dei nu este necesar.)
PASUL 3: Se pune vasul pe o manta de nclzire i se fierbe
soluia timp de 2-3 ore cu agitare din cnd n cnd.
PASUL 4: Eliminai coloana de condensare de la balon i a continua
pentru a gti timp de 10-15 minute sau pn cnd soluia iniial
este redus la jumtate.
PASUL 5: Dup ce soluia sa rcit, se toarn soluia
prin hrtie de filtru i se colecteaz cristalele care
format. Se spal cristalele ntr-o cantitate mic de
alcool absolut.
Shoping
1.(en)
1. Ergotamine tartrate-i found this with caffiene? you could buy some of this and extract
it: http://www.valuephar...m/Cafergot.html
2. Hydrazine hydratehttp://buy.ecplaza.n...ne_hydrate.html
3. Hydrazide- this looks like a pill...
http://www.allcareme...AZIDE.shtml.htm
4. Hydrochloric Acid- http://secure.scienc...-P6548C670.aspx
5. Sodium Nitrite- http://www.sciencest...hem-Rgnts/C2664
6. Sodium Bicarbonate- http://www.sciencest...hem-Rgnts/C2538
7. Diethylamine- http://www.neis.com/...ethylamine.html
8. Ether- http://www.tradekey.com/kb-ether/
2.(ro)
1 tartrat de ergotamin
2 hidrazin hidrat
3 Hidrazid
4 Acid clorhidric
5 nitrit de sodiu
6 bicarbonat de sodiu
7 Dietilamina
8 eter
ergotamina
Recipie one:
Ingrediants- Finely crushed up Cagerfoot pills
Candy thermometer
Double broiler set-up
1)Hook the candy thermometer to the top section of your doulbe broiler
2)Place in Cagerfoot Pills
3)Get the temature of the pills up to 400 degrees ferent hight (If to goes above 460, this is ruined, so be
carefull)
4)Ergotamine tartrate's melting piont is below caffine's so if all goes well it sould melt and the caffine
shoundent
5)Once the pills have become a sludge... add about 2 table spoons of water for every pill and mix well
(remebering to keep temp at 400)
6)There should be two liquids and they sould separate (i dont know the density of caffine or Ergotamine
tartrate so the Ergotamine tartrate could be the top layer or bottom layer)
7) take a turkey baster and suck of the top layer (eaither using that or using whats left)
-Remember when using the turkey baster.... its better to lose a bit of Ergotamine tartrate then have what
you do have contaminated so you may want to leave a bit of the Ergotamine tartrate in the broiler as to
not bymistake pick up some caffinated water
Recipie Two:
Ingredients--Cagerfoot pills
Hot water (at boiling piont)
Coffie strainer
1) place crushed pill in water
2) stir like theres no tomorow
3) strain and rince with water and strain again (repeat as many times as possible)
4) let water evaporate
This method is easier but will leave quite a few impurites