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clear, concise meaning: rapid freezing of a material at a very low temperature
followed by rapid dehydration by sublimation in a high vacuum.
Vacuum-drying is the process used to dry wetted (non-frozen) materials by
evaporation in a vacuum chamber at relatively higher pressures (low vacuum) and at
temperatures above the freezing point.
Deep freeze drying requires only a freezer. It is a non-vacuum process which has
been described by several names: simply freeze-drying, ambient freeze-drying, cold
storage drying, non-vacuum drying. The deep freeze method dries a solid by
dehydration. The same laws of physics that govern sublimation apply here also. The
process is quite familiar to those who have placed unwrapped food in the freezer
compartment of a domestic refrigerator. Over a period of time the food becomes
dehydrated; it froze, acquired a vapor pressure higher than the point of coldest
temperature (freezing unit), its water vapor molecules were drawn to the freezer
unit and trapped there.
Deep freeze as a method of drying is relatively well-known and has bees used by a
number of conservators in the past. However, the technique has not caught on perhaps
because of the time required to dehydrate the frozen materials. But in a recently
published article, Smith (16) describes the use of a commercial upright freezer
which was modified to dry 200 to 300 wetted books in two to four weeks (and it can
also be used to exterminate insects in books). The model is self-contained, has a
vertical glass door freezer, and was chosen for availability of maintenance centers
internationally, and its ability to cope adequately with minor disasters in
libraries. The modification include the establishment of a temperature differential
between book compartment and the evaporator (freezing unit), the elimination of
unnecessary heat sources, installation of temperature controls, indicating
thermocouple, signal devices and timers.
5.3 Natural freeze-drying
Natural freeze-drying is mentioned briefly as a matter of interest and to avoid
confusion with the other methods in use for drying. It is a technique for a specific
purpose and is limited to those parts of the worldwhere winter climates prevail et
temperatures below freezing. Note how similar it is to the other methods already
described.
Gratten and McCawley (17) write of the method; they call it "exterior
freeze-drying'. in which waterlogged wood is freeze-dried without the need of a
vacuum chamber. They take advantage of Canadian winter: the low temperature, the
daily hours of sunshine to offset the latent heat of sublimation, and the wind
conditions to help remove the water-saturated air from the frozen object. A
tent-like housing with polyethylene walls protects the object undergoing treatment
from undesired exterior conditions.
Conceivably, frozen documents and books could be dried under the same conditions as
waterlogged wood. The process would be quite slow, but it would still be a form of
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freeze-drying "au nature!."
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