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data on unidirectional
to a Weibull two-parameter
graphite-epoxy
statistical-strength
composites
model
ABSTRACT--Tensile
data o n unidirectional composites
generated from a flexure test usually yield a higher strength
than observed from a standard tensile coupon. According to
a statistical-strength theory based on a Weibull distribution,
the presence of a stress gradient in the flexureqest results in
an apparent increase in tensile strength as compared to the
tensile test under uniform stress. In the present paper, this
concept is explored by utilizing data from unidirectional
graphite-epoxy composites to compare with theoretical
results generated from a two-parameter Weibull distribution. A
larger variation in tensile strength is observed from tensilecoupon data than from flexure data. Such differences are not
in accordance with strength theories based on a uniform
flaw distribution and raise questions concerning variability of
the test methods, as well as sources of material variability.
List of Symbols
B ( S ) = risk of rupture at stress S
b = width of test specimen, mm (in.)
L = length of tensile specimen or span of beam
h
S=
Sb =
So =So
Sb =
S t .=
X=
P~o =
Xo=
specimen, mm (in.)
thickness of test specimen, mm (in.)
maximum stress, MPa (psi)
characteristic bending strength, MPa (psi)
scale parameter in two-parameter Weibull
distribution
maximum likelihood estimate of So
adjusted maximum likelihood estimate for scale
parameter under bending load, MPa (psi)
characteristic tensile strength, MPa (psi)
adjusted maximum-likelihood estimate for scale
parameter under tensile load, MPa (psi)
normalized strength
scale parameter for normalized strength
maximum likelihood estimate of normalizedscale parameter
shape parameter in Weibull distribution
J.M. Whitney and M. Knight are Materials Research Engineers, Nonmetallic" Materials Division, Air Force Materials Laboratory, WrightPatterson Air Force Base, OH 45433.
Paper was presented at 1979 SESA Spring Meeting hem in San Francisco,
CA on May 20-25.
Original rnanuscripl submitted: October 12, 1979. Final version received:
January 29, 1980.
Introduction
Tensile data on unidirectional composites are often
used as one of the key factors in materials selection, and
also provide basic ply properties which are used in
laminate design. Such data generated from a unidirectionalflexure test usually yield higher strength than data obtained from a standard tensile coupon. It is primarily for
this reason that flexure data are not considered appropriate
for design purposes. This difference in apparent tensile
strengths can be accounted for, however, if one considers
the brittle nature of most polymeric-matrix composites.
In particular, a statistical-strength theory based on a
Weibull distribution' can be used to explain the difference
between unidirectional-tensile data generated from a
flexure test and a standard tensile coupon. Tbe presence
of a stress gradient in the flexure-test results in an apparent
increase in tensile strength compared to the tensile test
under uniform stress. Establishment of a viable relationship between the flexure test and standard-tensile-coupon
test would provide a potential basis for use of the flexure
test in the generation of unidirectional-design data. Since
flexure tests are easy to run and relatively inexpensive, a
large statistical-data base obtained with this method rather
than tensile coupons is far more economical.
A two-parameter Weibull model was used by Bullock 2
in correlating 4-point flexure and tensile-coupon data for
unidirectional graphite-epoxy composites.
Excellent
agreement was obtained between theory and experiment.
The Weibull model has been previously applied to ceramic
materials '.4 and more recently to randomly oriented
short-fiber composites.'
In the present work, unidirectional graphite-epoxy
tensile data are obtained on both 3-point and 4-point
flexure tests, as well as on straight-sided tensile coupons.
The influence of specimen thickness on tensile strength is
investigated in addition to the effect of stress gradient.
Thus, a much broader data base for comparison to
Weibull statistical theory is available in the current work
than presented by Bullock. 2 Unlike the experimental
Tension
4-PT Flex.
3-PT Flex.
T300/5208,8 Ply
T300/5208,16 Ply
AS/3501-5,16 Ply
25
20
36
--
28
25
28
21
30
Statistical.strength Model
According to the Weibull statistical-strength theory for
brittle materials,' the probability of survival, P , at a
maximum stress level S for a uniaxial-stress field in a
homogeneous material governed by a volumetric flaw
distribution is given by
>_ S ) = R ( S )
P(S/
= exp [ - B ( S ) ]
B(S)
(5)
SA = SoA -'/~
(6)
where
(1)
(2)
o(x,y,z)
= Sf(x,y,z)
= A
(So, c~> 0)
(3)
o0
(4)
A = Jv [ f ( x , Y , Z ) l ' ~ d V
Sb
S,
~L/2
"q J L
P/2
~_29cm(9in )
P/2
t
P/2
P/2
L/h=52,
b=l.27cm(O.5in.)
h = 0 0127 cm/PLY ( 0 0 0 5 in / PLY )
Fig: 1 - - G e o m e t r y of test s p e c i m e n s
212
June 1980
]]l/,~
)]
O-point)
~,~
(4-point)
(9)
(10)
--
Sb
=
St
1.52, a = 15
1.33, c~ = 25
(3-point)
(11)
Sb
=
St
1.31, a = 15
1.20, c~ = 25
(4-point)
(12)
--
P/2
J-
~.~-b -,,.{
Vt
[2 (c~ + 1)2 . - - ~ -
S~ _ [4(c~+ 112
S,
( a + 2)
L=15.2 cm ( 6 i n )
(8)
SA = S, = S o ( V , ) -''~
where
if- b.~
(7)
These values of c~ are typical of currently utilized composites such as glass-epoxy and graphite-epoxy. Thus, the
flexure test can, in theory, produce significantly higher
tensile strengths than the tensile test, with the 3-point
loading producing the highest strength. This is due to the
fact that the maximum stress is produced at the outer
surface in the center of the beam, while the 4-point
loading produces the maximum stress at the outer surface
throughout the center section. In particular, the smaller
Test
..T300/5208,
Si, MPa (kSl)
8 Ply,
A
oq
Tension
Tension *
Tensiont
4-Pt Flex
4-Pt Flex*
4-Pt Flext
3-Pt Flex
3-Pt Flex*
1790 (259)
1776 (257)
.
--.
2377 (344)
2377 (344)
17.7
20.4
.
.
---
16 Ply,
^T300/5208,
Sol, MPa (kSl)
.
41.4
42.6
1665
.
.
1734
1741
.
1790
1797
(~i
(241)
^AS/3501-5,
Sol, MPa (kSI)
16 Ply,
^i
ot
1506 (218)
13.3
1506 (218)
1624 (235)
-1624 (235)
1617 (234)
--
13.2
29.2
-32.7
22.9
--
18.5
.
(251)
(252)
29.3
28.7
(259)
(260)
36.7
36.2
S, = S o ( L b h ) . . . .
= (h,},,,,
.~,.
,
h~ > h,
(14)
(3-point)
(15)
TENSION
0 8 L
" v ~
[U]['"
&~
U~"
h, > h,
(16)
06
2~
0 4
=~184
X.
0.2
I
08
1
09
I
1.0
Experimental
Mechanics
9 213
S(MPa)
1400
I0
1600
1800
2000
I
TENSION
T500/5208
tol
0.8
St = !665 MPa
'~
X ~
06
"~
~ / - S ~ :I790MPa
(259 KSI)
u3
0.4
5~ =18 4
8 PLY
0.2
2;o
0171
:500
S(KSI)
rSpi = X o S o i
(17)
I0 ~
BENDING ~
0.8 ~
[0]
06
T3_OOJ52o8
o ss
090
095
"~,q~
Discussion of Results
too
1.05
x
Fig.4--PooledWeibulldistributionfor flexuralloading,
T300/5208graphite-epoxycomposites
00%
0.3
n+0.4
j -
(18)
where j is the survival order number (data listed in decreasing order of strength) and n is the total number of
samples tested. Pooled-shape parameters are denoted by
1600
I 014OO
O
\O
~_\
06
2200
~_~ g
O 3PT, 16 PLY
r~c~
~ 3PT, 8PLY
gb =1734MP(]
2400
BENDING
T300/5208
\o~
08
04
S(MPo)
2000
1800
~] OI
Sb=2377 MISo
~[3 O~r
"~
= 1790 MPo
02
0
200
225
,,L,
250
\q
275
StKSI)
300
325
I ~
350
S(MPa)
I100
1.0
1300
1500
1700
TENSION
0.8
AS/3501-5A
0.6
~)~
?,--128
g,
: 1499 MPa
~3
(217 KSI)
04
0.2
~0
150
175
~ '- ~ 0 ~
O608 ~
m
N
I-~
200
S(KSI)
225
ab :251
04
02
O
O 80
I
O 85
J
090
I,
095
X
I
IOO
105
JO
250
S(MPe)
1500
1300
I0,
I ~
(3 I 0
1900
~Q.~
~
0.8
1700
BENDING
(4PT)
AS/3501-5A~ _
E
Sb=1624M P o ~
(235 KSI)
~
04
02
i
017!
200
225
S(KSI)
.250
275
graphite-epoxy
composites
S(MP~)
1300
p
tO
1500
I
08
O6
0.4
BENDING
(SPT)
~
AS/SSOL-~
1900
17OO
I
Sb=1617MPo
(234KS~1
(~
~
References
I
200
225
S(KSI)
250
275
composites
It is obvious from the data presented that the experimental results do not correlate with a two-parameter Weibull statistical model. This lack of correlation may be a
result of test methodology or may simply be an indication
that the Weibull distribution is an inadequate model for
describing failure in the fiber direction for a unidirectional
fiber-reinforced composite. It is important from a design
standpoint to determine the precise source of the discrepancy. This can only be accomplished by establishing
failure mechanisms. Until this is done, it appears that any
attempt to predict tensile-coupon data from flexural data
for design purposes is premature.
Acknowledgments
~t~= 2 5 I
175
216
Conclusions
b \
02
AS/3501-5A
June 1980