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Introduction :The flow of fluids through beds composed of stationary granular particles is
a frequent occurrence in the chemical industry and therefore expressions are
needed to predict pressure drop across beds due to the resistance caused by the
presence of the particles. For example, in fixed bed catalytic reactors and drying
columns containing silica gel or molecular sieves, gases are passed through a bed
of particles.
The resistance to the flow of a fluid through the voids in a bed of solids is
the resultant of the total drag of all the particles in a bed. Depending on the
Reynolds number, DpG0/, laminar flow, turbulent flow, form drag, separation, and
wake formation occur. As in the drag of a single solid particle, there is no sharp
transition between laminar and turbulent flow like that occurring in flow through
conduits of cross section. The most common methods of correlating total pressure
drop through a bed of solids to the drag of the individual particles are based ob
estimates of the total drag of the fluid on the solid boundaries of the tortuous
channels through the bed particles.
a) Ergun Equation:
fP = [(1/ReP).150(1-)/s] + 1.75; (for 1<ReP<1000)
b) Kozeny-Carman Equation:
fP = [(1/ReP).150(1-)/s]; (for ReP<1)
c) Blake-Plummer Equation:
fP = 1.75;
(for ReP>1000).
(Where ReP=particle Reynolds number=voDp/)
s= (6/Dp) / (sp/vp)
Or,
sp /vp= (6/sDp)
ERGUN Equation:
It is the most general correlation between f p and (1/Rep) for flow through
packed bed. The main contribution to the pressure drop, due to flow of fluid through
packed bed, occurs due to the kinetic losses caused by changes in channel cross
section and flow direction. As the fluid passes between particles, the channel
becomes smaller and then larger, and the maximum velocity is much greater than
the average velocity. Since the channel area changes rapidly, most of the kinetic
energy of the fluid is lost and this loss is repeated at each layer.
An equation covering the entire range of flow rates can be obtained by assuming
that the viscous losses and the kinetic energy losses are additive. The result is
called the
ERGUN equation:
fp= [(1/Rep)150(1-)/s]+1.75
This equation fitted data for spheres, cylinders, and crushed solids over a wide
range of flow rates.
KOZENY-CARMAN Equation:
For low Rep values, the first term on the RHS of the ERGUN equation is >>1.75, so
that the term 1.75 may be neglected, and the resulting equation is called the
KOZENY-CARMAN equation. This is applicable for flow through beds at particle
Reynolds numbers up to 1.0. There is no sharp transition to turbulent flow at this
Reynolds number, but the frequent changes in shape and the direction of the
channels in the bed lead to significant kinetic energy losses at higher Reynolds
numbers. For a given system, the equation:
fp = [(1/Rep)150(1-)/s]
indicates that the flow is proportional to the pressure drop and inversely
proportional to the fluid viscosity. This statement is also known as Darcys law,
which is often used to describe flow of liquids through porous media.
BLAKE-PLUMMER Equation;
As the flow rate through a packed bed increases, the slope of the p-versus-V 0
plot gradually increases, and at very high Reynolds numbers, p varies with the 1.9
or 2.0 power of the superficial velocity. An empirical correlation for pressure drop in
packed beds at high Reynolds number (R ep > 1000) is the BLAKE-PLUMMER
equation:
p/L=[(1.75V02)/(gcsDp)][(1-)/]
Simplifying and approximating we get:
fp= 1.75
Therefore,
For low ReP values (i.e. ReP <1) the Kozeny-Carman equation is valid and the
plot of fP -vs- (1/ReP) should be a straight line passing through origin.
For intermediate ReP values (i.e. 1<ReP<1000) the Ergun equation is valid
and the plot of fP -vs- (1/ReP) should be straight line having y intercept is =
+1.75.
And for high ReP values (i.e. ReP>1000) the Blake-Plummer equation is valid
and the plot of fP -vs- (1/ReP) should be a straight line parallel to (1/ReP) axis.
Apparatus Used:
The main lab setup that was used is shown in the figure 1 above.
The additional apparatus those were used are:
1. Collecting vessel: Bucket was used for higher flow rates and measuring
cylinder of capacity 1lit was used for lower flow rates.
2. Stop Watch.
Packing Materials:
Two types of packing materials were used.
water
= 996 kg/m3
Ns/m2
Manometric fluid Hg
mercury = 13550 kg/m3
1.
2.
3.
4.
5.
6.
7.
8.
9.
Manometer reading ( cm of Hg )
LHS
121
126
132
152
156
158
161
136
143
RHS
106
104
97
77
72
70
68
93
86
difference
15
22
35
75
84
88
93
43
57
0.17
0.62
0.96
2.52
1.77
1.76
1.8
1.13
1.56
10
10.51
10.64
15.59
10.21
10.11
10.04
10.12
10.12
Volumetric
flowrate
(m3/s)
0.00001707
0.00005923
0.00009059
0.00016229
0.00017406
0.00017478
0.00018000
0.00011211
0.00015477
Where,
Total weight ( in Kg ) weight of empty bucket( in Kg ) = net weight of water ( in
Kg )
Volumetric flow rate of water (m3 / sec) = W / ( t*
water
1.
2.
3.
4.
5.
6.
7.
Manometer reading ( cm of Hg )
LHS
120
123
134
137
143
147
149
RHS
108
104
96
93
88
83
80
difference
12
19
38
44
55
64
69
Net mass
of water
(Kg)
Time taken
(s)
Volumetric
flowrate
(m3/s)
0.62
0.98
1.89
2.01
2.43
2.67
2.84
9.98
9.96
10.21
9.83
9.94
10.23
10.21
0.00006237
0.00009879
0.00018586
0.00020529
0.00024545
0.00026205
0.00027928
1.
2.
3.
4.
Length
of
Raschi
g Ring
(cm)
1.7
1.5
1.7
1.7
Mean
Length
(cm)
L
Outer
diameter
(cm)
Mean
Outer
Diameter
(cm)
Inner
Diameter(cm
)
D0
1.65
1.5
1.4
1.6
1.6
1.525
D1
1.1
1.0
1.11
1.1
0.00117
0.00089
Mean
Inner
Diamete
r (cm)
0.00056
1.0775
Dp
L
L= D0
Sphere
Raschig Ring
s
1.0
0.58(for D1/ D0=0.5)
0.33(for D1 / D0=0.75)
m2
Volumetric
flow rate of
water (m3 /
sec) ( Q )
Superficial
Velocity
V0 = v
(m/sec)
Manometer
Reading
( in m )
h
0.00001707
Actual
average
linear
velocity)
v = Q/A
(m/sec)
0.0159
Pressure
drop
p= h ( Hg
- water )*g
0.0076
0.015
(in Pa)
1847.321
0.00005923
0.00009059
0.00016229
0.00017406
0.00017478
0.00018000
0.00011211
0.00015477
0.0551
0.08429
0.1510
0.1619
0.1626
0.1675
0.1043
0.1440
0.0264
0.0403
0.0723
0.0775
0.0778
0.0802
0.0499
0.0689
0.022
0.035
0.075
0.084
0.088
0.093
0.043
0.057
2709.404
4310.416
9236.606
10345
10837.62
11453.39
5295.654
7019.82
Friction
Factor,
fp
Particle
Reynolds
Number,
Rep
118.607
9
14.4166
9.8425
6.5529
6.3874
6.6401
6.6036
7.8871
5.4839
153.7575
0.006504
534.105
815.3194
1462.719
1567.922
1573.991
1622.546
1009.539
1393.933
0.001872
0.001227
0.000684
0.000638
0.000635
0.000616
0.000991
0.000717
1/Rep
raschig
Superficial
Velocity
V0 = v
(m/sec)
0.00006237
Actual
average
linear
velocity)
v = Q/A
(m/sec)
0.0580
Manometer
Reading
( in m )
h
0.0441
0.012
0.00009879
0.0919
0.0699
0.00018586
0.1729
0.00020529
Pressure drop
p= h ( Hg
- water )*g
Friction
Factor,
fp
Particle
Reynolds
Number,
Rep
1477.857
7.9484
871.6089
0.019
2339.94
5.0093
1381.53
0.1316
0.038
4679.88
2.8265
2600.992
0.1910
0.1453
0.044
5418.809
2.6847
2871.764
0.00024545
0.2285
0.1737
0.055
6773.511
2.3482
3433.072
0.00026205
0.2438
0.1855
0.064
7881.903
2.3959
3666.292
0.00027928
0.2599
0.1977
0.069
8497.677
2.2741
3907.417
1 / Rep
(in Pa)
0.00114
7
0.00072
4
0.00038
4
0.00034
8
0.00029
1
0.00027
3
0.00025
6