Universidad Central de Ecuador

Alejandro Delgado
UCE-FIQ
Ecuador

Quotation
Transaction No.: 359801
Quotation No.:
1485
Project:
Date:
Your No.:
Inquiry Date:
Contact Person:
E-mail:
Telephone:
Fax:

3598
04.04.2014
04.04.2014
Ulrich Ahlers
Ulrich.ahlers@spx.com
+49 (0) 2581 63601-159
+49 (0) 2581 63601-20

Debitor Tel.:
Debitor Fax:
E-mail:
For any queries please indicate the transaction no.
and the document no.!

Order of Costs
e&e Small Scale Extract Production Plant

Table of contents
1.0 SPX/e&e CPP Pilot 2- effect extraction plant; 2 x 100 l
2.0 SPX/e&e CPP Pilot 1- effect evaporation plant; 200 kg/h
3.0 SPX/e&e CPP Pilot rectification plant; 150 kg/h
4.0 SPX/e&e CPP Pilot aroma recovery plant; 50 l/h
5.0 SPX/e&e CPP UHT sterilisation plant
6.0 SPX/e&e CPP Pilot drying cabinet; 3 m2
7.0 SPX/e&e Installation supervision
8.0 SPX/e&e Commissioning and training
9.0 GMP Documentation (OPTION)

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SPX/e&e CPP Pilot 2- effect extraction plant; 2 x 100 l

...
2 x 100 l Percolator Volume
The extraction plant is used for the extraction of vegetable or animal raw
materials. The plant consists of 2 extractors which can be operated in 1- or
2-effect operation. Due to the very flexible construction, varying operation
modes with variable pressures, temperatures and solvents are possible. The
direction of extraction can be chosen either from top to bottom or vice versa.
Moreover, the extraction material can be damped and the extraction can
take place under vacuum or pressure.
e&e CPP System: Connect - Plug - Produce
The plant is ready for operation, incl. switch cabinet, and mounted on a
stainless steel frame. Before being delivered to the customer the plant is
checked for functioning in e&es workshop.
All components are ex-proof according to
ATEX. Technical Data:
Solvent:

Watery and non-water-soluble, combustible and

non-combustible solvents
(Other solvents are only allowed to be used after
consultation with e&e)
Flow rate:
100 - 800 l/h
Operating temp.:
10 - 100C
Operating pressure:
-1...+0,5 bar
Extract concentration: depending on the basic material and the process
conditions

Utilities Requirements:
Steam:
3,0 barg
Steam demand:
approx. 120 kg/h (preheating)
approx. 100 kg/h (damping)
Electrical power:
4,7 kW
Electrical connection: 230/400 V, 50 Hz, PE/N
Ex protection:
EEx de II T3
3
Cooling water:
approx. 3,8 m /h (25 - 35C)
Chilled water
6 - 12 C for vacuum pump
Compresses air:
6 barg

Einzelpreis
Unit price

18

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Size:
Length x width x height: approx. 5.000 x 1.900 x 2.450 mm
Materials:
All product-contacting parts are made from AISI 316/316 L. Other parts are
made from AISI 304, resp. grey cast iron or something similar. The frame is
fabricated from AISI 304.
Gaskets are made from EPDM, partially from PTFE.
The plant is designed and fabricated according to the effective DIN, AD and
VDE standards and directives as well as to all applicable EU Directives.
The layout corresponds to the rules of the food and pharmaceutical industry.

Einzelpreis
Unit price

18

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SPX/e&e CPP Pilot 1- effect evaporation plant; 200 kg/h

...
1-effect, 200 kg/h Water evaporation
The plant is used for the concentration of watery or organically dissolved
extracts. The plant consists of a plate evaporator with a downstream centrifugal
separator. The evaporated vapours are condensed in the plate condenser in
the vacuum or at ambient pressure.
The evaporation temperature can be adjusted according to the product-specific
boiling curve through the applied vacuum. This way, even temperature-sensitive
extracts can be concentrated.
e&e CPP System: Connect - Plug - Produce
The plant is ready for operation, incl. switch cabinet, and mounted on a
stainless steel frame. Before being delivered to the customer the plant is
checked for functioning in e&es workshop.
All components are ex-proof according to
ATEX. Technical Data:
Solvent:

Watery and not water-soluble, combustible and

non-combustible solvents
Evaporative power:
200 kg/h (water)
Feeding quantity:
100 - 1000 l/h
Feeding temperature: 20 - 60C
Extract concentration: Depending on the feed material and the
process conditions

Utilities requirements:
Steam:
Steam demand:
Electrical power:
Electrical connection:
Ex protection:
Cooling water:
Chilled water
Compressed air:

3,0 barg
approx. 220 kg/h
7,5 kW
230/400 V, 50 Hz, PE/N
EEx de II T3
3
approx. 15 m /h (25C inlet, 35C outlet)
6 - 12 C for vacuum pump
6 barg

Size:
Length x Width x Height: approx. 3,600 x 1,400 x 2,100 mm

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Materials:
All product-contacting parts are made from AISI 316/316 L. Other parts made
from AISI 304, resp. cast iron or something similar. The frame is made from
AISI 304.
Gaskets are made from EPDM, partly from PTFE.
The plant is designed and built according to the effective DIN, AD and VDE
standards and directives as well as to all applicable EU Directives.
The layout corresponds to the rules of the food and pharmaceutical industry.

Einzelpreis
Unit price

18

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SPX/e&e CPP Pilot rectification plant; 150 kg/h

...
The plant is used for concentration of Ethanol / Water solution by
rectification. The feed quantity is charged into the column by a pump and can
be preheated by bottom product.
After filling the bottom, the steam- heating of the bottom evaporator is started.
The entering liquid is in contact with the rising vapours. At the head the
enriched vapours are condensed. Part of the condensed liquid is pumped back
to the column as reflux, the main part is cooled in a heat exchanger by cooling
water and leaves the plant.
The bottom is equipped with an overflow by level. The overflow is pumped
through a heat exchanger for pre-heating the feed bevore leaving the
plant. The plant operates under atmospheric conditions.
e&e CPP System: Connect - Plug - Produce
The plant is ready for operation, incl. switch cabinet, and mounted on a
stainless steel frame. Before being delivered to the customer the plant is
checked for functioning in e&es workshop.
For transportation the column has to be dismounted and reassembled on
site. Therefore the column will be delivered without insulation.
All components are ex-proof according to ATEX, temperature class T3.
Technical Data:
Feeding quantity:
150 - 200 kg/h
Feed concentration:
approx. 60 Vol-%
Ethanol concentration: approx. 85 Vol-%
Bottom concentration: <1 Vol-%
Utilities requirements:
Steam:
Steam demand:
Electrical power:
Electrical connection:
Ex protection:
Cooling water:
Compressed air:

3,0 barg
approx. 130 kg/h
7,5 kW
230/400 V, 50 Hz, PE/N
EEx de II T3
approx. 10m3/h (25C - 35C)
6 barg

Size:
Length x Width x Height: approx.4,000 x 1,600 x 10,500 mm

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18

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Materials:
All product-contacting parts are made from AISI 316/316 L. Other parts made
from AISI 304, resp. cast iron or something similar. The frame is made from
AISI 304.
Gaskets are made from EPDM, partly from PTFE.
The plant is designed and built according to the effective DIN, AD and VDE
standards and directives as well as to all applicable EU Directives.
The layout corresponds to the rules of the food and pharmaceutical industry.

Einzelpreis
Unit price

18

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Total

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SPX/e&e CPP Pilot aroma recovery plant; 50 l/h

...
The plant is used for enrichment of aromatic components from the
extraction solvent by stripping / rectification.
The feed quantity is charged into the column from a buffer vessel by means
of vacuum or a pump.
After filling the bottom, the steam- heating of the evaporator is started. The
entering liquid is in contact with the rising vapours. At the head the enriched
vapours are condensed. A share of the condensed liquid is discharged as
aroma, the remaining main part is going back to the column (reflux).
The final product can be cooled in a heat exchanger either with cooling or chilled
water. It will be collected in a buffer vessel.
The bottom is equipped with an overflow by level. Two bottoms product
vessel can collect the liquid and discharge it vice versa.
The plant can operate under atmospheric or vacuum conditions.
e&e CPP System: Connect - Plug - Produce
The plant is ready for operation, incl. switch cabinet, and mounted on a stainless
steel frame. Before being delivered to the customer the plant is checked for
functioning in e&es workshop.
For transportation the column has to be dismounted and reassembled on
site. Therefore the column will be delivered without insulation.
All components are ex-proof according to ATEX, temperature class T3.
Technical Data:
Feeding quantity:

10 - 70 l/h

Utilities requirements:
Steam:
Steam demand:
Electrical power:
Electrical connection:
Ex protection:
Cooling water:
Chilled water
Compressed air:

3,0 barg
approx. 60 kg/h
7,5 kW
230/400 V, 50 Hz, PE/N
EEx de II T3
3
approx. 4 m /h (25 - 35C)
6 - 12 C for vacuum pump
6 barg

Size:
Length x Width x Height: approx. 3,700 x 1,400 x 6,000 mm

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Materials:
All product-contacting parts are made from AISI 316/316 L. Other parts made
from AISI 304, resp. cast iron or something similar. The frame is made from
AISI 304.
Gaskets are made from EPDM, partly from PTFE.
The plant is designed and built according to the effective DIN, AD and VDE
standards and directives as well as to all applicable EU Directives.
The layout corresponds to the rules of the food and pharmaceutical industry.

Einzelpreis
Unit price

18

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SPX/e&e CPP UHT sterilisation plant

...
The plant is used for sterilisation of watery or organically dissolved extracts. This
is done by heating the extracts up to 145 C by the means of sterilized steam at
approx. 3.5 bar g, keeping the extracts hot during approx. 2 - 4 seconds
(variable), cooling down by flashing under vacuum and condensation of the
vapours.
The plant consists of a clean steam generation, a deep sterilisation head with
injection nozzle and holding tube, a flash separator with plate condensor and
vacuum pump, a feeding tank and several pumps.
e&e CPP System: Connect - Plug - Produce
The plant is ready for operation, incl. switch cabinet, and mounted on a stainless
steel frame. Before being delivered to the customer the plant is checked for
functioning in e&es workshop.
All components are ex-proof according to ATEX, temperature class
T3. Technical Data:
Feeding quantity:
50 - 400 l/h
Product:
various extracts
Solvent:
water / ethanol
Product viscosity:
max. 1000 cp at feeding temperature
Feeding temperature:
20 - 60C
Sterilisation temperature: approx. 143 C
Keeping the extract hot: 2 - 4 seconds (variable, keeping the extracts hot
by modifying the sterilisation section)
Utilities requirements:
Steam:
3,0 barg
Steam demand:
approx. 10 - 100 kg/h
Electrical power:
7,5 kW
Electrical connection:
230/400 V, 50 Hz, PE/N
Ex protection:
EEx de II T3
3
Cooling water:
approx. 11 m /h (25 - 35C)
Chilled water
6 - 12 C for vacuum pump
Compressed air:
6 barg
Size:
Length x Width x Height: approx. 3,400 x 1,400 x 1,900 mm

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Materials:
All product-contacting parts are made from AISI 316/316 L. Other parts made
from AISI 304, resp. cast iron or something similar. The frame is made from
AISI 304.
Gaskets are made from EPDM, partly from PTFE.
The plant is designed and built according to the effective DIN, AD and VDE
standards and directives as well as to all applicable EU Directives.
The layout corresponds to the rules of the food and pharmaceutical industry.

SPX/e&e CPP Pilot drying cabinet; 3 m2

9-0004015
2

e&e Pilot Drying Cabinet Plant, 3 m Heating surface

The plant is used for batchwise drying of liquid or viscous products, especially of
thickened extracts. The plant mainly consist of the drying cabinet, a tempering
device, a vacuum and condensation system as well as a control cabinet.
The product is poured into drying trays and then shifted onto the heating plates of
the drying cabinet. A vacuum is created for drying and the trays will be heated
from the bottom by direct-contact heat and from above by radiant heat. The

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evaporating temperature can be adjusted according to the product-specific

boiling curve through the applied vacuum so that temperature-sensitive
extracts can be dried as well.
The vapours will be extracted and liquefied in the condenser.
The plant will be delivered ready for operation and is mounted on a stainless
steel frame, incl. a control cabinet. The drying cabinet has a mounting frame
with which it can be attached to a wall. Thereby, the anterior part reside in a
clean room whereas the posterior part with the auxiliary equipment can be
stored in an engineering room.
The cabinet can be cleaned by wiping it clean or washing it out. For this,
the heating plates can be removed separately if required.
Technical Data:
Heating surface:
6 plates 0.5 m2 (750 x 750 mm)
Front door:
attached to the right or to the left (changeable)
Sight opening:
2 sight glasses DN 100 with sight glass lamp
Operating pressure:
10 mbar (abs.)
Operating temperature: 120C
Operating pressure
Heating plates:
3 bar g
Heating capacity:
6/12 kW (switchable)
Cooling capacity:
20.000 kcal/h at 120C
Utility requirements:
Fresh water:
Cooling water:
Electrical power:
Electrical connection:
Protection category:
Size:
Overall size
Wall opening:
Swing range door:
Materials:
Drying Cabinet:
Piping:
Sealing:
Insulation:

for filling the tempering device

3
3,5 m /h (4C - 10C)
approx. 18 kW
230/400 V, 50 Hz, PE/N
IP 54

2.900 x 1.200 x 2.090 mm (L x W x H)

1.100 x 1.205 mm (W x H)
1.200 mm (max. radius)

1.4301, dead surface

1.4301, dead surface
O-ring-seal in the door frame, EPDM
other sealings EPDM
50 mm rock wool with stainless steel casing all around,
screwed together with the corpus.
The insulation of the door is hermetically welded.

The scope of delivery includes 48 pc. stainless steel trays made of 1.4301, type

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Gastro-Norm, 325 x 345 x 65 mm, deep-drawn and stackable.

The control is carried out via On/Off Switches and feelers with signal lamps
which are installed in a stainless steel control cabinet for wall fastening. The
control cabinet is installed in the clean room near the cabinet door.
The plant is built ready for operation on a stainless steel frame with height
adjustable base. The control cabinet is connected to the plant with 5 m
cable harness and has to be installed on the wall next to the dryer door after
assembly.
The plant must be assembled in the explosion-proof area.
The plant is designed and built according to the effective DIN, AD and VDE
standards and directives as well as to all applicable EU Directives.
The layout corresponds to the rules of the food and pharmaceutical industry.

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SPX/e&e Installation supervision

...
Since the Pilot plants are constructed acc. to the e&e system
CPP: connect-plug-produce (plant completely assembled, wired and
function-tested in the e&e workshop), the only works remaining on site to
be carried out by the buyer are:
- Allocation and connection of utilities:
- steam
- cooling water
- chilled water
- compressed air
- electricity
- Reassembling, duct work and insulation of the columns (Position 4 and 5).
SPX/e&e makes one senior supervisor available, who supervises and controls
the connection works and tightness tests on site and conducts a first test
operation of the plant with water.
We assume that the period for the SPX/e&e supervision will take 24 days (incl.
travel).
24 days SPX/e&e installation supervision incl. travel / flight costs and
incurred expenses / allowance.
Hotel costs (min. 4 star hotel), transfer between airport and hotel, transfer
between hotel and construction site as well as an allowance fee (meals) are
to be paid by the buyer.
The estimated 24 days for the SPX/e&e installation supervision shall be
conducted without interruption.
The mechanical and electrical installation of the supply lines (incl. installation
material such as pipes, flanges, fittings, etc. in stainless steel AISI 316/316 L) as
well as the connection of the plant incl. pressure and tightness tests are to be
conducted by the staff of the buyer.
In case the SPX/e&e supervisor needs more than 24 days and his support is
demanded by the buyer, the additional costs will be invoiced at a daily rate of
1.250.- acc. to actual expenditures.

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SPX/e&e Commissioning and training

...
The SPX/e&e commissioning engineer commissions the completely installed
e&e CPP Pilot plants and tests all mechanical and electrical functions.
After completion of the functional tests the SPX/e&e commissioning engineer
will conduct miscellaneous test runs with water and product that is to be
provided by the buyer.
- Test production (extraction) with one or more raw materials / products
(to be provided by the buyer).
- Introduction and training for the operating personnel of the buyer.
- Final acceptance.
Please note:
- that the raw material / products for the commissioning provided by
the buyer shall demonstrably not be toxic
- that the extraction cut of the raw material / products shall have a
particle size of 3-5 mm
- that the dust content in the product / raw material shall not exceed 20 %
- that as solvent solely water or a mixture of water and ethanol will be used
We assume that the period for the SPX/e&e commissioning und training
will take approx. 36 days (incl. travel).
36 days SPX/e&e commissioning and training incl. travel / flight costs
and incurred expenses / allowance.
The buyer ensures the proper supply of steam, cooling water, chilled water,
pressed air and electricity during the entire period of the commissioning and
training, furthermore the buyer provides sufficient and qualified personnel for
the entire period of the commissioning and training. The buyer guarantees that
the product / raw material / solvent will be provided in a sufficient amount and
quality during the entire period of the commissioning and training.
The estimated 36 days for the SPX/e&e commissioning and training shall
be conducted without interruption.
Hotel costs (min. 4 star hotel), transfer between airport and hotel, transfer
between hotel and construction site as well as an allowance fee (meals) are
to be paid by the buyer.
In case the SPX/e&e commissioning engineer needs more than 36 days and
his support is demanded by the buyer, the additional costs will be invoiced at a
daily rate of 1,250.- acc. to actual expenditures.

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GMP Documentation (OPTION)

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...
According the EU GMP Guideline SPX qualifies to ensure the required product
quality.
SPX is not responsible for the GMP relevant room concept, ventilation
system or provision of according utilities!
The Qualification is prospective (parallel) to the planning, installation and
commissioning of the plant and consists of the following steps/documents:
- URS (User Requirement Specification)
- RA (Risk Analysis from plants point of view)
- FDS (Functional Design Specification)
- HDS (Hardware Design Specification) and SDS (Software Design
Specification)
- DQ (Design Qualification)
- IQ (Installation Qualification), Leak Test, I/O-Check, etc.
- OQ (Operational Qualification), Alarm Check, Performance Test (with
water), etc.
SPX provides Qualification Plans for the DQ, IQ and OQ which need to be
approved by the customer before the corresponding Qualification Steps
activities can start. In these steps the Plans are filled out and become reports
together with the corresponding annexes.
Deviations are documented and rated in deviation reports. If they do not affect
the next Qualification Step, that one can start and the deviation reports can be
closed later. If they affect the next Qualification Step, they need to be closed
before starting it.
The following documents are provided for GMP qualification:
- Tube marking according DIN 2403 with labels
- Component marking with Tag-No. with labels
- For product contacted components additionally
- 2.2 test reports according DIN EN 10204-2.2 for material
and surfaces
- Declaration of FDA conformity for gaskets
- Welding documentation (manual isometrics, welders
qualification)
- Calibration Certificates for quality-relevant measuring devices

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-optional-

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Commercial Conditions
1

SPX/e&e CPP Pilot 2- effect extraction plant; 2 x 100 l

198.800,00

SPX/e&e CPP Pilot 1- effect evaporation plant; 200 kg/h

177.900,00

SPX/e&e CPP Pilot rectification plant; 150 kg/h

189.100,00

SPX/e&e CPP Pilot aroma recovery plant; 50 l/h

174.600,00

SPX/e&e CPP UHT sterilisation plant

219.800,00
2

198.700,00

SPX/e&e CPP Pilot drying cabinet; 3 m

SPX/e&e Installation supervision

32.500,00

SPX/e&e Commissioning and training

46.500,00

GMP Documentation (OPTION)

Total EUR without VAT

Option

GMP Documentation

1.237.900,00

91.700,00

Prices are only valid upon purchase of all items 1 - 6.

Delivery:

EXW (Incotherms 2010): Delivery ex works, excl. transport, insurance, not loaded.

Delivery time:

Approx. 8 12 month

Price:
All prices are net and to be understand plus the legal VAT.
The prices of this budget quotation are estimated budget prices. They were calculated on the basis of the
commercial conditions, this scope and other references or documents of this budget quotation. However, in this
phase, the prices do not represent a binding quotation that could be accepted.

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Documentation
The documentation will be delivered in one hard copy and one soft copy in English language consisting of:
- P & I diagrams
- Equipment list
- Technical documentation with description of the components and units
- Operating manuals of process components
- Maintenance guidelines
- Spare part lists (consolidated list form)
- Manufacturer certificates

Exclusions:
The following services and supplies are not part of the Sellers proposal:
- Intermediate storage tanks, raw material and product storage tanks, unless specified
- Exhaust gas and waste water handling
- Mechanical and electrical installation on site
- Supports, platforms, stairs and railing, unless specified
- Buildings, foundations, breaking into and adaptation of existing works, ventilation and
draining systems, earthing and potential equalization
- Insulation and insulation material, unless specified
- Main electrical power supply
- Low voltage distribution
- Connections for the utilities as well as the utilities
- CIP cleaning detergents
- Ex- Zone planning
- Unloading and storage of the equipment according to the Sellers instructions and marking
- Access for communications by telephone, Internet, fax etc.

Sincerely yours,
SPX Flow Technology Warendorf GmbH

Ulrich Ahlers
Sales Manager

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