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1
ACKNOWLEDGEMENT
Table of Contents
Types of Tube Failures 3
Boiler Chemistry 9
Condensate and Feedwater Parameters and Treatment
Cycle
12
The Metallurgy of Power
Boilers..
14
Acoustic Sound Level Detection
18
Boiler Tube Leakage incidents at Maithan and their Analysis
.22
4
TYPES OF TUBE FAILURES
CAUSTIC ATTACK
SYMPTOMS: Localized wall loss on the inside diameter (ID) surface of the tube,
resulting in increased stress and strain in the tube wall.
CAUSES: Concentration of caustic can occur as a result of steam blanketing
(layer of steam between the tube ID and the boiler water), which allow salts to
concentrate on metal surface (due to quick vaporisation on the metal surface at
point of localized overheating thus leaving behind conc. caustic solution) which
causes the dissolution of the protective magnetite layer causing loss of the base
metal and eventual failure. The metal must be stressed and a least trace of silica
must be present. Caustic attack can be controlled by the phosphate/pH control
method. Phosphate buffers the boiler water, reducing the chance of large pH
changes due to the formation of caustic.
Na2HPO4 + NaOH
Na3PO4 + H2O
OXYGEN PITTING
SYMPTOMS: Aggressive localized corrosion and loss of tube wall, most
prevalent near economizer feedwater inlet on operating boilers. Flooded or nondrainable surfaces are most susceptible during outage periods.
CAUSES: Oxygen pitting occurs with the presence of excessive oxygen in boiler
water. It can occur during operation as a result of in-leakage of air at pumps, or
failure in operation of preboiler water treatment equipment. This also may occur
during extended out-of-service periods, such as outages and storage, if proper
procedures are not followed in lay-up. Non-drainable locations of boiler circuits,
such as superheater loops, sagging horizontal superheater and reheater tubes,
and supply lines, are especially susceptible. More generalized oxidation of tubes
during idle periods is sometimes referred to as out-of-service corrosion. Wetted
surfaces are subject to oxidation as the water reacts with the iron to form iron
oxide. When corrosive ash is present, moisture on tube surfaces from
condensation or water washing can react with elements in the ash to form acids
that lead to a much more aggressive attack on metal surfaces.
HYDROGEN DAMAGE
SYMPTOMS: Intergranular micro-cracking. Loss of ductility or embrittlement of
the tube material leading to brittle catastrophic rupture.
CAUSES: in high pressure boilers, contaminants due to the condenser leakages
can lower the pH to a significant amount so that the acid reacts with the steels
producing hydrogen. This occurs under hard, porous, adherent deposits. The
hydrogen pressure at these points can build up to such high levels that the
hydrogen penetrates the metal tubing. This hydrogen reacts with the carbon
present in the steel to form methane. Methane being larger in size cannot
penetrate the metal and soon the pressure build up gets too high, causing the
5
metal to rupture along the grain boundaries where methane has formed. The
cracking that is formed is primarily intercrystalline or intergranular and
decarburization occurs at the point of rupture.
ACID ATTACK
SYMPTOMS: Corrosive attack of the internal tube metal surfaces, resulting in an
irregular pitted or, in extreme cases, a Swiss cheese appearance of the tube
ID.
CAUSES: Acid attack most commonly is associated with poor control of process
during boiler chemical cleanings and/or inadequate post-cleaning passivation of
residual acid.
6
CAUSES: Fireside ash corrosion is a function of the ash characteristics of the fuel
and boiler design. It usually is associated with coal firing, but also can occur for
certain types of oil firing. Ash characteristics are considered in the boiler design
when establishing the size, geometry and materials
used in the boiler. Combustion gas and metal temperatures in the convection
passes are important considerations. Damage occurs when certain coal ash
constituents remain in a molten state on the superheater tube surfaces. This
molten ash can be highly corrosive.
SHORT-TERM OVERHEAT
SYMPTOMS: Failure results in a ductile rupture of the tube metal and is
normally characterized by the classic fish mouth opening in the tube where the
fracture surface is a thin edge.
CAUSES: Short-term overheat failures are most common during boiler start up.
Failures result when the tube metal temperature is extremely elevated from a
lack of cooling steam or water flow. A typical example is when superheater tubes
have not cleared of condensation during boiler start-up, obstructing steam flow.
7
Tube metal temperatures reach combustion gas temperatures of 1600F or
greater which lead to tube failure.
LONG-TERM OVERHEAT
SYMPTOMS: The failed tube has minimal swelling and a longitudinal split that is
narrow when compared to short-term overheat. Tube metal often has heavy
external scale build-up and secondary cracking.
CAUSES: Long-term overheat occurs over a period of months or years.
Superheater and reheat superheater tubes commonly fail after many years of
service, as a result of creep. During normal operation, alloy superheater tubes
will experience increasing temperature and strain over the life of the tube until
the creep life is expended. Furnace water wall tubes also can fail from long-term
overheat. In the case of water wall tubes, the tube temperature increases
abnormally, most commonly from waterside problems such as deposits, scale or
restricted flow. In the case of either superheater or water wall tubes, eventual
failure is by creep rupture.
GRAPHITIZATION
SYMPTOMS: Failure is brittle with a thick edge fracture.
CAUSES: Long-term operation at relatively high metal temperatures can result in
damage in carbon steels of higher carbon content, or carbon-molybdenum steel,
and result in a unique degradation of the material in a manner referred to as
graphitization. These materials, if exposed to excessive temperature, will
experience dissolution of the iron carbide in the steel and formation of graphite
nodules, resulting in a loss of strength and eventual failure.
EROSION
SYMPTOMS: Tube experiences metal loss from the OD of the tube. Damage will
be oriented on the impact side of the tube. Ultimate failure results from rupture
due to increasing strain as tube material erodes away.
8
CAUSES: Erosion of tube surfaces occurs from impingement on the external
surfaces. The erosion medium can be any abrasive in the combustion gas flow
stream, but most commonly is associated with impingement of fly ash or soot
blowing steam. In cases where soot blower steam is the primary cause, the
erosion may be accompanied by thermal fatigue.
MECHANICAL FATIGUE
SYMPTOMS: Damage most often results in an OD initiated crack. Tends to be
localized to the area of high stress or constraint.
CAUSES: Fatigue is the result of cyclical stresses in the component. Distinct from
thermal fatigue effects, mechanical fatigue damage is associated with externally
applied stresses. Stresses may be associated with vibration due to flue gas flow
or sootblowers (high-frequency low-amplitude stresses),
or they may be associated with boiler cycling (low-frequency high-amplitude
stress mechanism). Fatigue failure most often occurs at areas of constraint, such
as tube penetrations, welds, attachments or supports.
Erosion on tube OD
10
Corrosion fatigue on
the tube ID adjacent to
attachment
Transverse view of
surface crack
Surface appearence of
tube showing fireside
ash corrosion on ID
Photomicrograph
showing graphitization
11
BOILER CHEMISTRY
It is very important to maintain proper feed water quality for the trouble
free operation of the steam boilers and turbines. The feed water required
for the High Pressure boiler parts should be demineralized to meet the
stringent quality standards of the operating fluid. Without proper water
quality it is not possible to obtain the optimal quality of steam for
operations of superheaters and reheater tubes and turbines. Also, it may
lead to deposits and corrosion in the boiler tubes and failures.
In spite of the demineralization process, the tubes may become deposited
over a long period of operation and proper cleaning process has to be
carried out whose frequency is determined by the cleanliness of the boiler
and operational requirements. The cleaning has to be carried out in such a
way that the integrity of the tube is maintained. During shutdown
processes, the boiler tubes have to be properly laid up, so that the tubes
does not get damaged by oxidation. The lay-up is done by keeping the
tubes filled with treated water and nitrogen blanketing.
PARAMETERS TO BE MAINTAINED
IONIZED SALTS: The ionized salts have to be removed for the elimination
of boiler tube scaling, turbine blade fouling and corrosion. The
demineralization plant deals with this problem to a considerable extent by
removing of the ionizing salts.
DISSOLVED OXYGEN: Dissolved oxygen must be reduced to about 10-20
ppb at the economizer inlet to prevent the oxidation of the HP
components. Generally, the deaerator considerably reduced the oxygen
content to about 10 ppb. Hydrazine is added for further scavenging of the
dissolved oxygen. Further the hydrazine forms a protective layer on the
magnetite layer of the tube ID thus protecting it from erosion by fluid
drag.
SILICA: Demineralizers can reduce silica conc. to about 20 ppb. Silica
conc. has to be maintained according to the working pressure as the
amount of dissolved silica in the saturated steam increases with the
operating pressure. Silica carryover to the turbine blading is abrasive and
deposits are difficult to remove. Further silica can react with calcium and
aluminium salts in boiler water to form hard scales which are detrimental
to heat transfer properties of the tube material.
12
During the initial commissioning of the boiler, it is likely to get high silica
content. This silica has to be brought into control by proper blowdown. The
pressure should not be raised until the silica conc. has been brought to the
specified limits. If proper boil out operations have been carried out, the
silica levels is brought down to the specified limits within some days of
operations. During normal operation, the main source of silica
contamination is condenser leakages and demineralizers. The specified
limits for operation at specified pressures is shown below to minimize the
carryover of silica to 20 ppb:
13
OTHER SALTS : The intent of providing phosphate in the boiler water is to
provide conditions conducive to the precipitation of calcium and
magnesium salts as Calcium Hydroxyapalite 3Ca 3(PO4)2Ca(OH)2 and
Serpenline 3MgO 2SiO2.2H2O. The addition of Phosphate is also done in a
co-ordinated Phosphate-pH method as stated below to maintain the pH of
the system as alkaline, absorbing any caustic which in the free form is
harmful to the system causing deposition known as caustic gouging. This
leads to material erosion leading to tube failures.
pH : Demineralized is often called hungry water as it is highly corrosive
in nature. Further a low pH means higher H+ ion conc. which is reactive
with the tube materials (decarburization)
leading to strength loss. Thus an alkaline pH has to be maintained to
avoid this. This is generally done with the help of ammonia dosing. TSP(Tri
sodium phosphate) used for sludge formation in the Drum also has basic
nature and is also judiciously used for maintain an alkaline environment.
The recommended phosphate levels for pH control is shown:
14
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15
STANDBY PROTECTION
The boiler tubes are susceptible to atmospheric corrosion during the down
time in the presence of moisture and oxygen. Thus proper laying up of the
boiler becomes an absolute necessity. Keeping the high capacity boiler
absolutely dry is a very difficult task owing to the complex nature of the
construction. The tubes can be dried to a considerable extent by
evacuating at a hot state. But the non drainable portions are not drained.
Thus condensation can take place. Thus in most of the high capacity
boilers, wet lay up is carried out. During the down times, the tubes are
filled with demineralized water dozed with
ppm of ammonia and 200
ppm of Hydrazine. This is further blanketed with a nitrogen gas
environment at about 5 psi(g).
BLOW DOWN
Blow Down must also be conducted on regular basis (When Boiler is in
Low Steaming Stage) from side wall, rear & front wall headers; so that
sludge accumulation in these headers may be avoided; which otherwise
would rise in furnace tubes creating conditions for circulation restrictions/
blockage, thus overheating at local spots.
16
Carbon steel
SA 210
P12
P22
C
steel,
Cr-1.25,
Mo- SA 213
0.5,Mn- 0.30-0.60, Ni- 0.51.0
C steel, Cr-2.25, Mo- 1.05
SA 213
T11
T22
Pipe,
finished
seamless
Tube,
seamless
Pipe,
rolled
seamless
Pipe,
rolled
seamless
Tube,
seamless
Tube,
USEF
UL
TEMP.
Hot 455
455
Hot 435
Hot 580
550
580
17
Austenitic steel, Cr- 17,
SA 213
Ni-9, Columbium &
Tantalum- 1
C steel, Cr-9, Mo-1, V-0.25, SA 213
Mn-0.3-0.6, Ni-0.25-1.0
TP347H
P91
------
SA335
SA 299
T91
seamless
Tube,
seamless
Tube,
hot 541
rolled
seamless
Pipe, seamless 420
plates
369
INFLUENCE
UPON FERRITE
INFLUENCE
UPON
AUSTENITE
(HARDENENABILI
TY)
815
PRINCIPAL FUNCTION
OF THE ELEMENT.
18
Chromium(
Cr)
Hardens slightly;
increased
corrosion resistance
Increases
hardenability
moderately, similar
to manganese
Manganese
(Mn)
Hardens, ductility
somewhat reduced
Similar to Ni
Molybdenu
m
(Mo)
Age-hardening
system in high
Mo-Fe alloys.
Increases
hardenability
strongly
Nickel (N)
Strengthens and
toughens by solid
solution
Increases
hardenability
slightly, austenite
retention with higher
carbon
Vanadium
(V)
Hardens moderately
in solid solutions.
Increases
hardenability very
strongly as dissolved
19
Apart from this, other special alloying elements are added for specific
property rendering in the steels. The Austenitic grades having high
chromium content has a tendency to sensitize, that is, form chromium
carbides along the austenite grain boundaries. The formation of these
carbides reduces the chromium content of the austenite grains at the
boundary, and, therefore, reduces the local corrosion resistance along the
grain boundaries.
To prevent sensitization, additions of columbium and tantalum to form 347
were invented. If these alloys are given a second heat treatment, called a
stabilization anneal, at 1600-1650o F after the solution anneal, titanium
carbide or columbium-tantalum carbide will form preferentially to
chromium carbide. With all of the carbon removed as innocuous carbides,
no chromium carbide can form. There is no loss of chromium at the grain
boundaries, and no loss of corrosion resistance, and thus no sensitization.
However, in boiler applications, these grades are not given stabilization
anneal.
One other microstructural constituent will form at elevated temperatures,
and that is a chromium-iron intermetallic called "sigma phase."
Both the sensitization and the formation of sigma phase occur over long
periods at ill-defined temperatures. Both will occur at temperatures
beginning at about l,000oF and will form more rapidly at slightly higher
temperatures. Since the formation of chromium carbide and sigma phase
are governed by the ability of individual atoms to move or diffuse through
the lattice, these atomic movements will occur more rapidly at higher
temperatures. As the temperature is increased above 1200 oF, however,
chromium carbide begins to redissolve in the austenite; thus the rate of
carbide formation and growth decreases. By about 1600 oF, chromium
carbide is completely gone from the microstructure. Sigma phase is
unstable and redissolves above a temperature of about 1600 o F; the exact
temperature depends on the composition.
Unfortunately, from an estimation of operating-temperature perspective,
all of these changes within the microstructure of austenitic stainless steel
occur over a range of temperatures and over a range of times. There are
no discrete temperatures that indicate with any degree of precision the
peak failure or operating temperature. Thus there are only estimates of
operating temperature and not an accurate "calling card" within the
microstructure as there are in the ferritic steels.
The 18 chromium-8 nickel austenitic stainless steels have been used for
several decades in high-temperature applications within a steam
generator. They have excellent high-temperature tensile and creep
strengths and excellent corrosion resistance. The microstructural changes
during long-term operation are more subtle than in the ferritic steels. In
20
addition to this, the ductile-brittle transition temperature for these steels
are at very low temperatures compared to the operating temperatures
and hence recommended.
21
combustion efficiency, outstripping the metallurgical developments. Sonic tube
leak detection system address this issue.
TECHNICAL DISCUSSION
OVERVIEW
As a leak develops in a pressurized system, turbulence created by escaping fluid
generates pressure waves within the contained fluid itself, throughout the low
pressuremedium (usually a gas) into which the fluid is escaping, and within the
container structure. These are commonly referred to as fluid-borne, airborne, and
structure-borne acoustic waves, respectively. To detect leaks, the energy
associated with these mechanical waves can be converted into electrical signals
with a variety of dynamic pressure transducers (sensors) that are in contact with
the medium of interest. Several methods of signal processing are available that
allow the voltages generated by these sensors to be evaluated for the presence
of a leak. As mentioned above, leaks in a pressurized system generate sound
waves in three media. The decision regarding which types of acoustic waves are
most reliably detected is important from both functional and economical
considerations. This decision, in some cases, is not simple. Factors such as
background noise level, sound attenuation within the medium, signal processing
strategy, and installation costs play a role.
22
23
BACKGROUND NOISE
In leak detection applications, the most important factor to consider is
background noise within the propagation
medium of interest. Almost all background noise can be characterized as white
noise combined with discrete frequency noise. White noise can be defined as
containing components at all frequencies within a range or band of interest. Both
normal boiler noise and leak noise are considered to be white noise. Boiler noise
is best described as low frequency white noise (rumbling) while leak noise is best
described as higher frequency white noise (hissing). Discrete frequency noise is
usually composed of a fundamental single frequency (tone) and several
associated harmonic frequencies. These sounds are best described as whistling
or humming noises.
24
angle of 45 to the walls of the boiler, 1.5 m away from the wall. It houses the
transducer in a Teflon protective coupling. Purging can be carried out on timely
basis to avoid the deposition of ash and soot particles.
SENSOR
OUTPUT
AMPLIFIER
FILTER LOW
FREQUENCY
COMBUSTIO
N NOISE
V/I
CONVERTER
0-20 mA AC
OUTPUT
25
INPUT
FROM THE
FIELD
AMPLIFIER
UNIT
I/V
CONVERTE
R
FILTER
ABSOLUTE
VALUE
CIRCUIT
DECIBEL
CONVERTE
R
BACKGROU
ND NOISE
SUBSTRACT
OR
ALARM SIGNAL
26
The design pressure and temperature of these tubes are 202.1 ksc, 363
deg C(51 OD) and 214.4 ksc and 397 deg C (63.5 OD) respectively. All the
tubes are rifled and to ASME SA 210 gr C specifications.
Preliminary examination of the tubes revealed:
1. No marks of corrosion or pitting or deposits in the tube ID of any of
the samples.
2. One 51 OD tube has a through crack starting at the end of the
support plate weld and the support weld has a weld defect of non
uniform weld throat thickness and thinning due to the weld run
deposit. This crack does not exhibit any deformation to indicate that
the failure has initiated from the steam side.(uniform diameter
around the crack)
3. 63.5 OD tube has a large window like opening showing no erosion
marks around. The tube has a diameter change in one direction. No
ballooning, swelling, overheating type of wall thinning is observed.
The 30 X 20 mm opening appears like a small portion of the tube
failed and got separated.
Physical tests, chemical analysis and metallographic tests is
carried out:
Table 1 : Tensile test results
Values
identification
Specimen
section
Tube size
51 OD X 5
thk
Tube size
51 OD X 5
thk
Tube size
63.5 X 7.5
thk
ASME SA 210
gr C specs.
6.55 thk
12.61 wide
Yield
strength
N/sq mm
X 421.6
UTS
N/sq mm
Elongation
%
548.91
25.94
533.37
29.18
546.14
26
485
30
275
Identificati
Carbon %
Silicon %
Manganes
e%
Sulphur%
Phosphoru
s%
27
on
Tube
51 0.23
OD
Tube 63.5 0.24
OD
ASME SA 0.35
210 gr C
0.25
0.7
0.015
0.02
0.2
0.7
0.023
0.02
0.10
0.29-1.06
0.035
0.035
Hardness :
51 OD (tube site sample no 7) BHN 180-184
63.5 OD tube
BHN 215-217
tubes
across
the
openings/failure
are
taken
for
28
The leak apparently has started from this opening and the release steam
has damaged the nearby tubes, its portions and supports. While the
external wall thinning was sustained by the other tubes until their internal
pressure and temperature load crossed the threshold. The yielding and
thinning after this threshold has led to the other leaks.
29
LTSH FAILURE REPORT ON 4TH MAY, 2012
INTRODUCTION
Maithan Power Limited reported a failure in U #1 LTSH area on 4.5.2012.
The failed tubes were received at CTDS for Component Damage Analysis
on 22.05.12.
The particulars of the tubes are:
Material to SA 213 gr T11.
Design Pressure 105.3 Bar; Design Temperature 464 deg C
Size (specified) is 47.63 OD X 5.6 mm thk.
Corrective Action carried out by the station:
a) Inspection of the area around the leakage and the neighbouring
area.
b) Replacement of the portions of tubes in the affected area and its
immediate vicinity.
ROOT CAUSE ANALYSIS:
The sound portion of the sample tubes received fron Maithan was
subjected to tensile tesr and the results are found to conform to the
ordered ASME SA213 gr T11 specifications:
As per Specs
UTS (415)
YS (205)
%
elongation
(30)
Actual
473.48
379.79
31.20
The spectro chemical analysis was carried out on the two of the failed
tubes and the welds and the result conforms to ASME SA 213 gr T11.The
tube has failed due to overheating caused by an excess penetration in the
adjacent butt joint. The tube is at the beginning of the bank of tubes close
to the LTSH inlet header which could be the source of debris which got
entangled in the sharp internal defect of the weld. The primary failure has
resulted in external corrosion of the neighbouring tubes, the weld quality
apparently harbouring foreign material from the header is the root cause.
PREVENTIVE ACTIONS:
A. It is suggested at the next opportunity to carry out radiography test
or UT on all such joints to identify similar defects, repair the welds
which have these defects and inspect close to th headersany OD
ballooning and attend the same.
30
B. Photograph of the location of failure from site suggest that the
freedom for movement of the tubes in that area is to be restricted
by the use of standard fixtures to permit the tubes only for thermal
expansion in the necessary direction. In case site engineers agree
that the supports are not adequate then at the next opportunity the
design drawing for supports may be verified and the supports put in
place.
31
BOILER OPERATION TO MINIMIZE TUBE
LEAKAGES
Efficient operation of the boiler, during startup, normal operation and shut
down is an essential pre-requisite for minimizing boiler tube leakages. Just
after erection, certain milestones have to be achieved in order to declare
the boiler as suitable for operation.
After erection, the following procedure is carried out:
1. HYDROTEST : the first hydrotest that is carried out on the boiler is
done at a pressure of about 315 ksc(1.5 times the design pressure
of the boiler design pressure) by a hydrotest pump maintained by
the station. The hydrotest is carried out on the non drainable tubes
first and then on the drainable and non drainable tubes together.
This hydrotest is primary importance as it points out the maximum
number of weld defects and tube leakages (during precommissioning works) which cannot be determined by Radiography
test.
2. BOILER LIGHT UP
3. CHEMICAL CLEANING
After lighting up the boiler, the boiler tube must be made free from
the debris lodged during commissioning for facilitating efficient heat
transfer, maintaining steam purity and preventing local heating
which may be an important cause of boiler tube leakages. Cleaning
process can be broadly classified as:
a. Alkali Boil out : carried out to remove oil, grease and rust.
Normally soda ash and TSP is used. Sodium sulphite is used to
reduce oxygen corrosion and sodium nitrite reduces caustic
embrittlement.
The boil out operation is carried out at about 0.2 times the rated
operating pressure of the boiler. The boiler drum is filled with
water upto the normal operating level and thw chemicals are
introduced in the syste via the normal dosing inlets. Since this is
the first time the boiler is being lighted, to facilitate checking up
free and uniform expansion of the unit while raising pressure, the
firing is to be maintained at a minimum. The silica and oil content
is monitored till oil content is below 1ppm. Then the boiler is
boxed up and allowed to slow cool. Hot dm water is flushed into
the boiler followed by cold rinsing.
32
b. Acid cleaning : An inhibited acid solution of EDTA (Ethylene
Diamine Tetra Acetic acid) is circulated for 4-5 hours by acid
circulation pumps. This cleaning is carried out to clear the tubs of
any scale deposits as well as for chelation, which forms the
protective magnetite film by reacting with the base metal on the
tube ID. Further, the iron iron content, silica etc are to be
dissolved to a considerable extent. After hot and cold rinsing,
neutralisation may be doenby soda ash. After passivation,
hydrazine and ammonia is charged and the boiler is laid up for a
predetermined time.
4. THERMAL FLOW TEST : The thermal flow test is carried out to
check the chocking of the superheaters, reheaters, waterwalls, etc.
by a thermal flow meter.
Purge the boiler for at least 5 min before start up and shut down
with adequate air flow to dilute the combustible matter in the
furnace to avoid explosion.
Before introducing any fuel into the furnace, ensure sufficient
ignition energy. Whenever fuel intake is increased or reduced,
flame stability has to be kept in mind. While increasing fuel
input, load the burners to their rated capacity before cutting in
the other burners. While reducing fuel input, the load on the
adjacent burners must be kept above 50% before cutting the
remote burners.
The varying of temperature in the boiler causes stresses in the
boiler pressure parts. The rate of temperature variation is
restricted. The cooling range is more stringent than the heating
rate because the temperature stresses are acting in the same
direction as the pressure stresses while cooling while it is
opposing at the time of heating. Also, during heating the
temperature is controlled by adequate draft.
33
The Hot, Warm and Cold Start Up characteristics are given as below:
34