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E___
RECOMMENDATIONS
FOR
ENVIRONMENT
A CONTROLLED
ENCLOSURE
INSTRUMENTATION
FOR
PACKAGES
SEPTEMBER
EG&G-1183-5068
1976
by
Buford MeClung PE
ENGINEERING SPECIALIST
APPROVED
FOR PUBLICATION
ENGINEERING
Carl F, Virchowp
DEPARTMENT
Manager
IcHIAL/
PERFORMED
UNDER
ERDA-NV
BY E. G. & G.
CONTRACT
NO.
E(29-1)-1183
,__o._ o_LABORATORY
D[STRIB_UTION
OF THIS
DOCUMENT
IS UNLIMITED
_ _.90
_ _t,i_O_,
_
DISCLAIMER
Portions of this document may be illegible in
electronic image products. Images are produced
from the best available original document.
q,
CONTENTS
Page
SECTION
1
SYNOPSIS...........................
DISCUSSION ..........................
3.1
General .........................
3.2
3.3
3.3.1
3.3.2
l0
3.3.3
12
14
3.4
4
CONCLUSIONS .........................
17
4.1
17
4.2
18
APPENDIX
A
GENERAL ...............
............
A-1
B-1
ENCLOSURE THERMALSPECIFICATION
C-1
...............
DISCLAIMER
This report was prepared as an account of work sponsored by an agency of the United States
Government. Neither the United States Government nor any agency thereof, nor any of their
employees, makes any warranty, express or implied, or assumes any legal liability or responsibility for the accuracy, completeness, or usefulness of any information, apparatus, product, or
process disclosed, or represents that its use would not infringe privately owned rights. Reference herein to any specific commercial product, process, or service by trade name, trademark,
manufacturer, or otherwise does not necessarily constitute or imply its endorsement, recommendation, or favoring by the United States Government or any agency thereof. The views
and opinions of authors expressed herein do not necessarily state or reflect those of the
United States Government or any agency thereof.
iii
.,
SECTION 1.
SYNOPSIS
An enclosure
to
protect
and temperature
environment
Division
Hill
lack
Fenton
of interest
fabrication,
use
in establishing
sure
vessel
parameters
Geothermal
a pressure
the
B is
material;
and
presented
by prospective
and
Appendix
instrumentation
size
by
Research
vendors
vessel
thermal
limintations.
downhole
site
is
use
all
and heat
recommended
in
at
specified.
was designed
insulation
C for
from the
conditions
in handling
housing
a specification
Appendix
packages
for
specifying
pressure
the
LASL Q-12
Due to
phases
of the
and specified
sink
use
severe
a general
design
for
their
requirements.
in
the
purchasing
important
the
pres-
thermal
SECTION 2.
INTRODUCTION AND GENERAL SPECIFICATIONS
In July 1976, EG&G, LAO was contracted by the Q-12 Division of the Los
Alamos Scientific Laboratory (LASL) to provide our technical support in several
areas of their Geothermal Research and Development projects (in process at their
Fenton Hill site in the Jemez Mountains).
12 hours.
2)
is 24 hours; during this time the dewar will be placed in an air ambience at
-30C to +30C temperature.
3)
S)
6)
7)
be joined end-to-end and all suspended from a logging cable; the sequential order
of packages is subject to change for each experiment.
9)
The volume required to house the Multiplex System electronics and its
'
SECTION 3.
DISCUSSION
3.1
GENERAL
Potential
tacted
in
an effort
meet
the
high
pressure.
found
general,
custom
No "off-the-shelf"
models
the
LASL packages
that
in
would
Obviously,
costs
In view
for
the
have
for
of these
EG&G to
to
if
for
interior
a mechanical
cided
the
that
would
vendors
be given
packages
factors,
it
and the
thermal
invited
the
to
option
with
other
been
bid
the
the
thermal
the
pressure
be finalized.
and material
fabricated
from
work
resulted
vessel),
LASL packages,
joining
designed;
the
interface.
(pressure
and to
and
and other
time
were
In
housing.
LASL personnel
housing
for
to bid
string
interest
analysis
could
same mechanical
shroud,
interface
had not
to
A-l).
enclosure
and fabrication
discussions
enclosure
vessel
con-
and
sparse
thermal
this
unit
page
a specification
in the
the
the
pressure
downhole
in design
all
and only
a thorough
were
temperature
Appendix
between
before
and employed
specification
the
to be lowered
savings
(ref.
type)
designed
high
located
conduct
interface
be completed
design
developing
3.2
string
of combined
were
designing
or other
or custom
TM
units
to
mechanical
tubing
the enclosure
cation
in
be realized
same mechanical
material
qualified
a significant
could
desire
and fabricated
interested
(dewar
an "off-the-shelf
conditions
seemingly
not
enclosure
environmental
Furthermore,
task
secure
designed
those
were
of a suitable
to
stringent
in
design
vendors
write
closely
write
a specification
with
packages.
Also,
analysis,
design,
vessel
in
them
it
fabrication
in
by Mr. Sheldon Reynolds, U.S. Steel metallurgist who works closely with the
petroleum industry.
threads be used with a copper plating to both the male and female threads to
insure sealing without galling.
Figure 1 illustrates the API Extreme-Line thread, (one of four standard
5.50- _ API
EXTREME-LINE CASI_GTHREADS
COPPER PLATED
API types);
tage of complicated
machining
coupling
(see Figure
advantage
require
suggested
Acme
employing
equipment
that
an extra
sealing
The coupling
the necessary
local buckling
Acme
increase
in wall
for a more
careful
tracks) ; a recommended
3.3
PRESSURE
3.3.1
VESSEL
General
Choosing
of various
O-rings
(maletogether
method
However,
up this
would
LASL
felt
type of joint
in combination
vises
is depicted
joint
and
with
the advantage
component
close
by fabricating
groove
moveof easily
include
an
and a require-
parts.
tolerance
a simple
mounted
insure
circumferential
sealing
3.
to cause
pins
the disadvantages
an O-ring
associated
in Figure
together
restraining
offers
makeup;
and V-blocks
ends
by relative
of the fragile
and their
seal
optional
interface
to accommodate
could be eliminated
to make
the package
of the O-ring;
handling
pins
Hither
compound.
O-ring
pulling
and low-torque
thickness
The restraining
press-fitting
a metallic
This mechanical
threads
several
two packages
thread machining
or metallic
enough
changing
be investigated.
acts as a turnbuckle,
plating
to join
(the coupling).
API thread
with elastomer
of accomplishing
be to use an internal
threads
of simpler
piece
temperature
threads
might
API Buttress
(free-running)
A method
ment
alternative
a coupling
A better
of requiring
that their
of not requiring
joint
to slide
on
machining
and
makeup
fixture
longitudinal
method.
MATERIAL
CONSIDERATIONS
Considerations
an appropriate
desirable
pressure
features
material
involved
trade-off
studies
including"
I)
Instrumentation
2)
Sealing
3)
Temperature
4)
Material
cost vs material
5)
Material
hardness
method
vessel
payload
volume
vs wall
vs wall thickness
vs material
strength
strength
vs material
strength
thickness
:
.
6)
Material
hardness
7)
Material
availability
8)
Material
cost
In an effort
with
of
10,000
psi,
through
0.75
125,000
to
the
a nominal
various
wall
psi,
its
0.525,
and 0.750
160,000
psi.
28,000,
and
page
sealing
of 0.750
but
still
terials
factor
realized
only
the
of
maximum stresses
in
the
range
of
Appendix
yielding
yield
(respectively)
required
wall
page
for
wall
in the
for
the
A-2).
were
three
pressure
thicknesses
range
of
of 60,000
determined
wall
0.25
Alternatively,
of a cylindrical
pressures
resulting
145,000
of
at
thickness
was determined
withstand
psi
safety
wall
at
(2500
employing
in Section
the
area
20,000
minimum
strength.
since
15,000
psi)
in
for
approximately
yield
the
maximum downhole
maximum pressure
3.3.2
the
pressure
range
strengths
psi
the
should
adequate
psi
an external
the
cause
yield
vessel
in
(ref.
to
and under
a pressure
considered
was calculated
for
technique
_nches;
having
in
for
0.500,
through
to be 22,300,
thicknesses
(ref.
A-3).
The minimum
O-ring
resulted
strength
At 150,000
inches
were
respectively
inches
32,800
of 6.0
required
yield
requirements
thicknesses
This
methods
quality
strength
diameter
pressure
vs
fabrication
vs material
outside
45,000
vessel
vs
determine
inches.
external
Appendix
to
vs machinability
3.2
psi
feet
should
the
external
This
head
preferred
the
neighborhood
ends
is
pressure
should
pressure
static
be approximately
be in
threaded
due to
presently
to
of the
maximum design
depths;
the
of
for
equate
10,000
observers
and the
reduced
ma-
to an
psi
is
(actually,
specified
9000 psi).
treatable (via oil quench and temper) to 145,000 psi minimum yield strength.
Grades SAE-4135, -4140, and -4340 can easily be heat-treated to tensile strengths
in excess of 200,000 psi in the proper cross-sections.
4340 is limited to cross-sections of approximately 3.5 inches; 4140 to approximately 0.5 inches.
treating 0.750 inch wall tubing to the desired yield strength of 145,000-1.75,000
psi; 4140 _ecomes somewhat marginal.
I0
This yield
Brinell
4340
strength
Hardness
steel.
desired
strength
as supplied
vessel
quality)
very
steels
machinability
housing),
heat
treated
specification
amount
are generally
available
treatment
to its
of the
(max. BHN =
of machining
while
required
before
for
machining
to the buyer
in "commercial"
quality"
grades
the aircraft
process
standards.
quality
to insure
Certified
of aircraft
grade
quality
only
is continuously
quality
products;
and,
(magna-flux
the steel-making
quality
supplied
in the "aircraft
difference
standards
meets high
commercial
vs the better
A_
to a
shipment
The basic
throughout
is supplied
are sometimes
loose quality
product
corresponds
choice.
grade.
monitored
312-383
psi)
this material
(enclosure
low alloy
on occasion,
- 175,000
of having
before
(145,000
range of approximately
The convenience
final
material
range
control
none
documentation
is available
for
grade.
For example:
aircraft
AMS Specification
quality
No. 6415H
low alloy
(Aircraft
quality
steel
tubing
SAE 4340)
purchased
is certified
to SAE
to meet
the following:
i)
Tolerances
2)
Chemical
analysis
3)
Steel cleanliness
4)
Quality
sampling
5)
Other
assurance
standards
controlling
the hardenability,
decarburization
depth,
maximum
hardness,
and frequency
- severity
rating.
Fabrication
tubing
of a cylindrical
of the proper
potential
vendors
pressure
(manufacturers
vessel
is obviously
can be located.
and warehouses)
simplified
Approximately
were contacted
if
fifteen
in an effort
t
mechanical
In summary,
O.D.
x .75" wall
tubing;
thickness
the results
are tabulated
ii
aircraft
in stock;
quality
on Appendix
two others
4140 or 4340
page A-4.
are willing
to
manufacture
140
lineal
it
in
the
the
AMS tubing
x 0.750
+ 0.056
wall)
_+ 0.025
x 0.750
_+ 0.045
6.030
-+ 0.030
able
coupling
fabricated
Dia.
from
their
for
given
heat
are
in
x 0.750
in
LASL requires
than
one
treated
to
range.
to be 52_F
Since
(40-
the
data
the Brinell
Hardness
the hardness
range
eliminates
at the specified
worst
alloy
steels
to
thickness
800F
for
proposed
this
these
characteristics
at 352.
BHN) recommended
Analysis
consideration
is
have
been
they
in
this
specified
temperNo.
steels.
1991
From an
is slightly
data
are
Publication
No. 11102
of the 4140
strength
from room
alloy
suitable
by ARP
exposed
are
the curve
This hardness
above
employed
Technical
that
or
is
temperatures
deterioration
for some
be
removal
of
(when
operating
be:
predict-
to
may be
4340
temperatures
a more
near
tempering
it can be concluded
to
application
loss
strength);
vs temperature
it from further
is
without
some strength
corrosion.
for
alloy
(6.000
chosen
allow
in
each
(286-325
were
temperatures
which
tensile
case
temper
operating
inches.
Dia.
tolerances
decarburization
6.000
and
typical
is listed
of stress
of
for
+ 0.060
closer
coupling
allow
to
4140
of strength
3.3.3
ultimate
our
of the 4340
possibility
inch
psi
are expected.
and
limit
ature values
analysis
per
for
below
(the
exposures
725F
180,000
IO0F
should
low
The
to
This
area
extended
work
wall.
approximately
hour
as
easily
(6.000
tolerances
heat-treated
by
liberal
size
tubing)
temperature.
approximately
in excess
to reduce
of
the
strength
temperature.
Other Steels
There
ature
that
tubing
stress
using
MIL-ttDBK-5
strength
+ 0.050
of
rather
can
the
purchased
affected
longer
source)
qualities
are
industry
wall),
an O.D.
tempering
no
and
the
A concern
they
standards
cross-section
retaining
that
small
feet).
Since
while
relatively
are a number
strength
discussed
and
low alloy
of other
steels with
better
substantially
corrosion
resistance
The problem
I Report on Elevated-Temperature
Properties of Wrought
American Society for Testing Materials, 1957.
2 Published
by the Society
of
Automotive
12
Engineers
better
high-temper-
in selecting
Medium-Carbon
(1969).
one of
Alloy
Steels,
these better
types is their
Five Percent
This family
lack of availability
Chromium
Steels
of steels most
is retained
in aircraft
3.3.3.2
Precipitation-Hardening
salient
quality
exceeding
THI050,
retention
approximately
1,000 hours. 1
of
90%
These
are
good corrosion
to 800F.
is their
up to 1000F;
Stainless
at temperatures
and Vanadium
characteristic
strength
grades
erties:
with Molybdenum
available
properties
size of tubing.
will be discussed:
in the proper
resistance
As an example
has a tensile
of their
yield
mechanical
strength
prop-
of 138,000
psi
at 800 F.
5.3.3.3
Inconel
This age-hardenable
close to 100%;
its resistance
room temperature
125,000
alloy
yield
is readily
welded
to postweld
strengths
with
cracking
of 150,000
joint
efficiencies
are outstanding.
psi; dropping
very
It exhibits
only to approximately
psi at 1200 F.
Corrosion
resistance
of this nickel-chromium
alloy
is excellent
to many
media.
It is available
forging
stock,
sheet,
AMS specifications.
larger sizes
in a range
of standard
and tube;
However,
all available
the seamless
mill
6" O.D.);
forms
including
in aircraft
tubing
quality
is not readily
larger-sized
tubes
are generally
AMS standards
I)
Seamless
2)
Sheet,
3)
Bars, Forgings,
4)
Welding
I Reference:
Tubing;
Strip,
Me,Z8
are listed
AMS-5589,
& Plate;
-5590
AMS-5596,
8 Rings;
for reference:
A_8-5662,
-5597
-5663,
-5664
Wire; AMS-5852
Handbook,
8th Hdition,
13
American
"
Society
of Metals.
per
in
rolled
3.4
order to minimize the heat flow from the high-temperature environment to the
lower temperature electronics canister (or other instrumentation package).
Preliminary analysis of the Multiplexing System electronics and its power
source (batteries) indicated that a volume of greater than 160 cubic inches
would be adequate for packaging.
surface area yields a cylinder of 5.88 inches diameter x S.88 inches length.
Since this diameter is approximately equal to the pressure vessel (pv) outside
diameter, a smaller canister diameter must be chosen to allow for wall thickness, insulation, and heat sink.
eter x 26.00 inches length was chosen; allowing for the maximum diameter (2.6
inches), commercially available, mercuric-oxide button-cells (high-temperature
batteries).
Insulation manufacturers were contacted (see Appendix page A-S) to survey
the types of insulation available; both flexible and rigid types were considered.
One of the most promising is "MIN-K" manufactured by Johns Manville; available
in the rigid and flexible forms (rigid types are favored due to ease of replacement), both in variable densities and associated thermal conductivities ("Kfactor").
For a mean temperature of 400F, the "MIN-K" molded type No. 1301
The heat sink would be self regenerating; the material changing back
to a solid as the pressure vessel cools after being removed from the hole.
2)
As compared to the common ice-packed dewars, the fusion heat sink does
not have to be dismantled at the test site for charging nor does it have to be
recharged if the experiment is delayed.
3)
14
liquid,
the
electronics
in ice-packed
dewars).
4)
cannot
be damaged
by its
vapors
(such
as steam
damage
15
SECTION 4.
CONCLUSIONS
4.1
and high
downhole
temperature
retention
at
better
its
"Hll"
has
most
importance,
is
Aircraft
appropriate
its
exhibits
excellent
corrosion
and very
However,
dictates
realizing
an alternate
an "off-the-shelf"
stock
I would
recommend
specification
for
Toward
the
its
seamless,
Hamilton
Corporation
it
6.030
+ 0.030
conforms
to
certification
for
heat
1 Metals
O.D.
are
wall
+ 0.050
closer
on file
Edition,
in
page
it
100% joint
often
(aircraft
150
stock
of
quality
Hence,
lineal
at
A4).
could
feet
the
the
they
been
assure
the
American
Society
of
shipment
this
outside
me that
can
(if
AMS
be made
desired).
Metals.
configuration
6"
mandatory
arrangements
before
of
Channing-
Although
have
after,
be provided;
vessel
B.
No.
tube
In
location
material.
testing
17
of
the
(up to
recent
Furthermore,
i,n a welded
with
(availability)
steel
tensile
2 Inconel
Alloy 718 can be considered
as in the seamless
configuration.
signifi-
procurement.
of the
alternate
tolerances.
As
temperatures.
alone
view
sought
for
elevated
material
wall
and will
accordance
material;
approximately
thickness
of
suitable
as Appendix
Appendix
slope
but
weldability
was located
(ref.
and subsequent
8th
inserted
but
pressure
AMS-6415
of tl_is
tubing
x 0.750
papers
and in
investigation
nominal
specified
Handobook,
is
warehouse
the
treatment
purchase
at
strength
enclosure
most
of time
suitably-sized
purchase
in
excellent
retention
corrosion.
of the
718 to be the
strength
Handbook.
by less
shown,
recommended
aspects
in matters
cold-drawn,
x 0.750
to
consideration
the
end of this
AMS-5415
O.D.
of
not
manufactured
resistance,
choice
Metals
(depicted
materials;
definitely
strength
the
high
of some families
room temperature
susceptibility
2 tubing
that
in
highest
listed
Alloy
good
depicted
pressure
with
representation
temperatures
technical
Inconel
efficiency),
the
other
is
I believe
the
elevated
AMS specification
housing,
nominal
at
general
the
is
of high
of materials
A graphical
only
seamless
of only
by a concurrence
consideration
not
of the
quality
consideration
4340),
direct
temperature
retention
than
created
temperatures.
vs
strength
cant
to
strength
steel
curves)
lead
elevated
of materials'
depicted,
environment
as well
4.2
ENCLOSURE
Thermal
THERmaL
analysis
ANALYSIS
of the enclosure
is not a steady-state
temperature
heat
sink
varying
vendors
competence
caution
The specification
is reached,
should
signing
may be necessary
the latent
internally
be employed
I would
[depending
upon
a Performance
in Appendix
to control
18
heat-of-fusion
(if a phase
have
when
size
their
and reputa-
Bond be considered.
C is for employment
others.
a vendor
demonstrate
their
change
run an analysis
selecting
suggest
outlined
manufacturers
fabrication.
plant be visited,
of their
until
insulation
and subsequent
to accomplish
firms; additions
at least
Several
results;
is complicated
sink material
is employed).
to do the analysis
spective
conduction;
of the heat
with widely
AND FABRICATION
of reputable
POTENTIAL
DATE OF
IN IT IAL
CONTACT
01 July
POTENTIAL
VEN DO R
'76
Noren
Inc.
Products,
PROTECTIVE-ENCLOSURE
PERSON
CONTAC_
RESPONSE
19 July
'76
Cryogenic
Technology,
Inc.
(617) 890-9400
Mr. Harry
19 July
'76
Arthur
Co.
Mr. Peter
O'Farrell
D. Little
(617) 864-5770
CO_NTS
(415) 365-0632
>
,
VENDORS
Nicoll
Very interested in
the thermal aspects
Apparently
qualified.
(has forwarded a
preliminary
sketch);
not interested in
ommended by Jermyn
Mfg. Co. as the
designer of their
the pressure
design,
heat-pipe
line,
vessel
well
Rec-
product
Apparently well
qualified.
Recommended "MIN-K"
Insulation and
Inconel 718.
Very interested,
but would like to
Apparently well
qualified -- but
19 July
'76
Cryofab, Inc.
(201) 925-2916
Mr. George
Grillo
Not interested
custom work.
19 July
'76
Minnesota Valley
Engineering,
Inc.
(612) 758-4484
Mr. Mike
Lumpkin
in
Apparently
qualified.
r -(in.)
a1
(KSi)
o2
(KSi)
3
(KSi)
k
0.3
0.4
0.5
0.6
O. 75
0.25
-52.63
-95.26
10.00
-52.63
-40.18
-70.36
10.00
-40.18
-80.36
0.00
-32.73
-55.45
10.00
-32.73
-65.45
0.00
-27.78
-45.56
10.00
-27.78
-55.56
0.00
-22.86
-35.71
10. O0
-22.86
-45.71
0.00
-62.61
-115.2
10.00
-62.61
-125.2
0.00
-105.3
q ----external
pressure
t _ wall thickness
0.00
= -10,000
psi
Formula
a _ outside R = 3 000"
t <
b--inside
.25 = t is slightly
less
than the minimum allowed
with this
formula
is
a
I0
invalid
3.00
i0
for
""
R = a - t
Fo2_nulas
= __qa2
a 2_b2
for
Stress
with
tensile).
02
and
= qa 2 (b 2+ r 2)_
r 2 (a2-b 2)
Strain,
Roark
A-2
& Young,
03
= -qa 2 ( r2_b 2)
r 2 (a2-b 2)
Mcgraw-Hill,
1975.
0e
30"
D/t
FORMULA
PYP
PP
YIELD PRESSURE
PT
(KSi)
GIVEN MATERIAL
YIELD STRENGTH
(psi)
0.5
O. 625
0.750
12.00
9.6
8.00
X
X
X
9.167
11.20
13.13
60,000
60,000
60,000
0.5
0.625
0.750
12.00
9.6
8.00
X
X
X
10.69
13.06
15.31
70,000
70,000
70,000
0.5
0.625
0.750
12.00
9.6
8.00
X
X
X
12.22
14.93
17.50
80,000
80,000
80,000
O. 5
0.625
O. 750
12. O0
9.60
8. O0
X
X
X
13.75
16.80
19.69
90,000
90,000
90,000
O.S
0.625
0.750
12.00
9.60
8.00
X
X
X
15.28
18.66
21.88
100,000
100,000
100,000
0.5
0.625
0.750
12.00
9.60
8.00
X
X
X
16.81
20.53
24.06
110,000
110,000
110,000
O.S
O. 625
O. 750
12.00
9.60
8. O0
X
X
X
18.33
22.40
26.25
120,000
120,000
120,000
O.S
0.625
0.750
12.00
9.60
8.00
X
X
X
19.86
24.26
28.44
130,000
130,000
130,000
0.5
0.625
O. 750
12.00
9.60
8. O0
X
X
0.5
0.625
0.750
12.00
9.60
8.00
X
X
0.5
0.625
0.750
12.00
9.60
8.00
X
X
t m wall
thickness;
U a outside
diameter;
140,000
140,000
26.13
30.36
Pyp -
1 Formulas
and their
applicable
2nd Edition,
November 1974.
yield
point
ranges
formula;
are
A-3
22.33
27.99
32.81
150,000
1SO,O00
150,000
23.49
29.86
35.00
160,000
160,000
160,000
PT " transition
taken
formula;
Pp _ plastic
range
No.
'
formula
5C3,
POTENTIAL
VENDORS
OF AIRCRAFT
II
QUALITY
TUBING
COST
VENDOR
Jorgensen
Steel Co.
AVAILABILITY
S/FT.
FOR FT.
Do not stock
$57.87/ft
6" round
for
(213)567-1122
Jim Miller
Aug.
II
16
Kilsby Tube
Supply, "Cris"
(303) 371-7600
Not in stock,
6-8 weeks to
manufacture
Aug.
16
Aug. 23
$25.89/ft for
Must order 40stress reliev140 ft. @ their
ed; $34.30/ft
: option.
for heat
treated
Not in stock
,.
$45.83/ft to
bore out to
4.8 in. I.D.
Total=S103.70/ft.
COMMENTS
,,,,
C.A.
Russell,
Inc., "Patty"
(214)641-1222
Not in stock
Whitaker
Metals
Not in stock
(913) 869-8661
Aug.
23
Ducumnin
Not
Metals, "Ro dney"
(713) 675-4301
Aug.
31
ChanningHamilton Corp.
Tron Carter
(213) 889-6791
Aug.
31
in stock
140 ft. of
4340 in stock
per AMS 6415
$43.14/ft
140 ft.
$57.36/ft
40 ft.
for
for
$2.00/ft for
Staitening;
$4.95/ft for
heat treating
Sept. 01
Babcox _
Wilcox,
Mr. Came
(412) 846-0100
Not in stock;
6-8 weeks to
manufacture
Sept. 01
WheelingPittsburg
(412)288-3600
Not in stock
Aug. II
through
Sept. 01
Other Steel
Vendors and
Manufacturers
Contacted
$49.98/ft for
60-110 ft.
(quantity at
their option)
Minimum buy of
5-12 tons
A-4
Contact
inquiry
via their
#4138
POTENTIAL
DATE OF
INITIAL
CONTACT
VENDOR
30 July
1976
Johns-_nville
R_D Center
PERSON
INSULATION
CONTACTED
Mr. Tony
Silva
VENDORS
INSULATION
TYPE
RI GID
FLEXIBLE
X
(305) 770-1000
"
Babcock
Wilcox
(404)
>
,
_n
798-8000
"
PittsburghComing
[412) 327-6100
,,
SONO-THERM,
Inc. Mr. Ernest
(716) 875-6625
"
E.J.
Davis Co.
(203)
239-5391
"
COMMENTS
Permali, Inc.
(412)
547-4581
Mr. Chester
Smolenski
Feine
Recommended Carborrundum
brand rigid "FIBER-FRAK"
Did not
literature
Ns. Ruth
Klingensmith
follow-up
with
as promised.
MATERIAL
SPECIFICATION,
PRESSURE
i. 0
INTRODUCTION
I.I
Scope:
This
aircraft
specification
quality
manufactured
treated
1.2
in accordance
package
5270F
pressure
for a 12-hour
SPECIFICATIONS
2.1
Vendor
2.2
Material
0.030
2.3
Preparation
2.3.1
diameter
low-alloy
and wall
steel
canister
will be sub-
emersed
in water
at
customer
that
the material
supplied
before
+_ 0.050
cold-drawn
heat-treatment:
inch wall
seamless
with
thickness
mechanical
the exception
stipulated
_+
air-
tubing
that
shall be as specified
the certification
6.030
the
herein.
in AMS-6415H.
for Heat-Treatment
permanently
the information
information
vendor
mark within
required
already
being easily
the tubing
x 0.750
tolerances
Prior to heat-treatment,
otherwise
psi.
is new material.
with AMS-6415H
thickness
furnish
to customer
to the following
in accordance
shall
vessel
heat-
a sealed
an electronics
specification
is to conform
craft quality
Vendor
to 175,000
in fabricating
The pressure
tubing
subsequently
= 145,000
to protect
environment.
in writing
inches outside
diameter
housing
mechanical
of
AND REQUIREMENTS
per this
manufactured
seamless
will be used
pressure
duration.
shall certify
to customer
cold-drawn
(0.2% offset)
vessel
to an external
2.0
with
tubing
from a hostile
forth controls
steel
strength
The specified
cylindrical
jected
low-alloy
to a yield
Purpose:
sets
VESSEL
in ink).
engrave,
impact-stamp,
per paragraph
exists
is subjected
shall
No. 5.1.I.I
Permanent
room-ambient
of AMS-6415H
marking
lighting
or
of tubing
(this
is defined
conditions
as
after
to heat-treatment.
Q
I Material
manufactured
to earlier
revisions
approval
B-I
of AMS-6415
will
for substitutions
be considered
must be given
2.3.2
maximum), the vendor shall have the option of placing any other additional
markings within the 6" limited area specified in the previous paragraph
(e.g., "Special", "Additional H.T.", etc.).
2.3.3
not
be removed
except
just
prior
to heat-treatment
at
the
heat-treatment
facility.
2.4
Heat-Treatment
2.4.1
The material
the
2.4.2
2.5
properties
shall
be oil-quench
specified
in paragraph
and temper
heat-treated
to obtain
2.5.
2.5.1
Room-temperature
elongation,
and reduction
in accordance
selected
2.5.2
yield
for
with
of area
(0.2% offset),
tests
ASTM Specification
these
tests
The allowable
2.5.3
strength
limits
strength
per
the requirements
Yield
(0.2% offset):
b)
Elongatic_:
c)
Reduction of area:
are
strength,
be run on material
No. A370.
of acceptance
a)
shall
tensile
Samples
are
to
samples
be
of AMS-2370.
as
follows:
145,000-175,000
psi
8.0% minimum
45-70%
Vendor shall provide customer with written and certified documentation of testing conditions and results and the heat-treatment procedure.
2.6
Protective Treatment:
B-2
2.8
Packaging:
3.0
REJECTIONS
Material not conforming to this specification or to authorized
modifications will be subject to rejection.
B-3
OR 4340
STEEL TUBING
COST
S/FT. FOR FT.
VENDOR
AVAILABILITY
Aug. II
Jorgensen
Steel Co.
(215)567-1122
Jim Miller
Do not stock
$57.87/ft for
6" round
$45.83/ft to
bore out to
4.8 in. I.D.
Tota1-$103.70/ft.
Aug. 11
Not in stock,
6-8 weeks to
manufacture
$25.89/ft for
stress relieved; $34.30/ft
for heat
treated
Aug. 16
Kilsby Tube
Not in stock
Supply, "Cris"
(303) 371-7600
Aug. 16
Aug. 23
Whitaker
Metals
(913)869-8661
Aug. 23
Ducumnin
Not
Metals ,"Rodney"
(713) 675-4 301
Aug. 31
Channing140 ft. of
liamiltonCorp. 4340 in stock
Tron Carter
per A_tS6415
(213)889-6791
$43.14/ft for
140 ft.
$57.36/ft for
40 ft.
$2.00/ft for
Staitening;
$4.95/ft for
heat treating
Aug. 31
Sept. 01
Babcox 6
Wilcox,
_r. Came
(412)846-0100
Not in stock;
6-8 weeks to
manufacture
$49.98/ft for
60-110 ft.
(quantity at
their option)
Sept. 01
WheelingPittsburg
(412)288-3600
Not in stock
Aug. II
through
Sept.
Ol
Other Steel
Vendors
and
Manufacturers
Contacted
CO_ENTS
Not in stock
in stock
_tinimumbuy of
5-12 tons
B-4
APPENDIX
ENCLOSURETHERMALSPECIFICATION
1.0
INTRODUCTION
!
1.1
Scope
This
specification
defines
physical
constraints,
external
environ-
ment, maximum operating time, and other parameters necessary to accomplish an analysis,
shroud
1.2
for
design,
and
an instrumentation
fabrication
of
a thermal-protective
package.
Purpose
An enclosure
and
a thermal
to protect
consisting
shroud
designed
instrumentation
lically-induced
of a previously
to this
used
in
designed
pressure
specification
surveying
is
natural
to
vessel
be employed
faults
and hydrau-
formations.
2.0
SPECIFICATIONS
(a)
(b)
(c)
(d)
Minimum time between enclosure emersions in the hostile environment is 24 hours; during this cooling period, the enclosure will
be placed
(e)
Before
interior
gas
(f)
in
the
an air
enclosure
will
ambience
is
-30C
placed
be evacuated
to a pressure
at
of 11.1
in the
of air
+ 2.0
to
hostile
and then
psia
+50C temperature.
environment
filled
(absolute
with
the
dry
nitrogen
pressure).
(g)
(h)
C-1
(j)
design
and
The longitudinal
axis
mum deviation
3.0
fabrication
from
at a later
of the
date.
enclosure
vertical
will
when emersed
be
in
limited
the
to
hostile
15 maxi-
environment.
REQUIREb_NTS
(a)
Figure C1 and its "Notes" are to be considered a part of this speciIn the
fication.
tion
(b)
should
A copy
of
take
of conflicting
precedence
Figure
interface
event
C1 shall
dimensions,
over
requirements,
Figure
be annotated
signed,
and
this
specifica-
C1.
in
red
returned
ink
to
to
show pertinent
customer
at
time
of
bid submitted.
(c)
(d)
Heat
sink,
if used,
wou_.d be in the
9.0
psia
at
(f)
withstand
at
a temperature
the
The enclosure
hostile
for
phase
of
shown
in
shall
canister
a period
of
environment;
for
an absolute
of 0-20
psia
be designed
after
interior
a period
not
of
C-2
absolute
pressure
must
of
be able
external
or distortion
require
pressure
beyond
the
materials
so that
ambient
12 hours
it
if it
the
C1.
cryogenic
interior
the
damage
sealed
external
Furthermore,
shall
as
and hermetically
280C.
Figure
shroud
(such
shroud
mum of 15 watts
emersed.
under
275C without
thermal
(electronics)
85C
of
material
The thermal
be encased
application
limits
"charging"
(g)
liquid
a temperature
to
tolerance
must
the
or
the
enclosure
while
the
rely
instrumentation
does
is
will
of
ice).
temperature
electronics
10 hours
addition
not
emersed
exceed
in
the
dissipate
a maxi-
enclosure
is
(h)
Vendor
must
shall
be in
enclosure
(i)
"
(j)
specify,
a certain
must
through
or
special
cooling
Vendor
or
If
finds
conductive
the
enclosure
methods
are
at
transported
it
canister
same at
compound shall
specified
the
time
not
during
its
for
cooling;
if
cooling
if
cooling;
of bid
the
enclosure
period;
air
if
must
or if
submitted,
any particular
and/or
annulus
and the
of bid
any
the
be blown
other
advantageous
between
heat
enclosure
must
employ
a thermal-
to
the
sink
instrumentation
(ref.
Figure
If this
surfaces
or cause
if
position.
submittal.
bond the
conditions,
submittal,
for
time
in
in
of bid
required.
necessary
compound
(electronics)
specify
position
specify,
be stored
time
be disassembled
across
shall
vendor
at
together,
corrosion
of
choice
flow
C1),
he shall
is
made the
under
the mating
the
materials.
Also, the tolerances controlling the annulus size (e.g., heat sink
I.D.)
4.0
will
be tightened.
ACCEPTANCE TESTS
It is the intention of customers to monitor, as deemed necessary,
tests
conducted
Reports
vendor's
must be prepared
Acceptance
vendor
vendor.
Certified
4.1
by the
on tests
test
Tests
reports
shall
or by an approved
conducted
by the
by laboratories
laboratory
depicting
be submitted
laboratory
the
other
conducting
results
of all
selected
than
such
by
the
tests.
required
to customer.
Schedule
Vendor
shall
schedule
the
required
tests
to be accomplished
in a
Customer Notification
Vendor shall notify customer's Project Manager (or his designated
alternate) via telephone at least seventy-two (72) hours in advance of
the beginning of the required tests; Saturdays and Sundays will not be
credited toward this time requirement.
C-3
4.3
Accuracy
o Test
Vendor
tests.
Apparatus
shall
Measuring
supply
all
test
instruments
apparatus
necessary
must be accurate
to
accomplish
the
Testing Procedure
The tests are to be run in the following ascending sequential order:
4.4.1
Shock Test
1)
b)
c)
2)
steel plate (Brinnel Hardness of 250 minimum); the electronics cavity toward
the
bottom.
strength
enclosure
3)
The stecl
and
rigidity
plate
impact,
to
to
less
limit
than
is
to
be backed
deflections
0.1
by other
of the
steel
materials
plate,
of
sufficient
induced
by
inches.
parts (parts housed within the pressure vessel) shall show no damages or
any deformations beyond their toleranced limits of Figure CI.
4.4.2
Temperature Test
I)
C-4
a)
b)
c)
e)
2)
Backfill the
interior with dry nitrogen gas to an absolute pressure of 11.1 + 1.0 psia.
3)
The exterior
One hour after the heating cycle begins, energize the IS-watt
being energized.
6)
+85C for a period of twelve (12) hours from the application of the
external heat.
@
C-S
,, ,.
.
"
7)
At the
be removed
from
room ambient
(at
time
temperature
8)
ature
around
the
the
temperature
mended method
interior
end of
Promptly,
of
12-hour
enclosure.
the
external
The enclosure
(23C
+ 7C)
bid
submittal).
must not
at the
period
rise
in accordance
While
above
end of the
heat
shall
with
source
be cooled
vendor's
cooling,
shall
the
at
recom-
canister
100C.
24-hour
cooling
period,*
5,
the Temper-
above.
This
second test is run for the purpose of demonstrating the abillty of the
enclosure heat sink to regenerate itself in the allotted time.
a)
b)
After the enclosure has cooled sufficiently, it shall be disassembled and inspected for damages and distortions of the vendor supplied
interior parts.
4.4.3
Pressure Test
This test is designed to determine the structural integrity of the
hermetically sealed heat sink and/or vacuum chamber under external pressure.
this
is
to be omitted
If
either
sequence
shall
Temperature
one or both
be run,
from the
required
of
devices
these
beginning
at
the
Acceptance
exists
eleventh
Tests.
the
hour
following
of
the
test
second
Test:
I)
Hold
the
temperature
constant
at
275C + 5C.
2)
housing).
3)
After 0'5 hours, backfill the pressure vessel with dry nitrogen
Vendor may proceed earlier if he determines that the heat sink has regenerated sufficiently.
C-6
4)
After
an additional
from around
the
step
No.
of the
sure
with
that
5)
After
assembled
the
the
remove
the
Test.
the
cooling
Also,
external
cycle
heat
source
as specified
equalize
the
in
internal
pres-
room.
enclosure
has
for
cooled
damages
sufflclently,
it
and distortions
shall
of the
be dis-
vendor
supplied
parts.
Final
If
passed
of
hours,
and begin
Temperature
and inspected
interior
4.4.4
enclosure
0.5
Acceptance
the
Shock,
with
Temperature,
no apparent
supplied
by vendor,
a signed
statement
If
any tests
corrective
and Pressure
damage to
the
the
customer's
action.
failed
pressure
Acceptance
or
required)
vessel
representative
acknowledging
are
(if
damages
Subsequently,
are
customer
interior
shall
Test
Tests
were
components
supply
vendor
with
passage.
found,
vendor
may require
shall
instigate
any or all
tests
to be re-run.
5.0
BIDDING INSTRUCTIONS
Potential vendors may bid either "Option A'
5.1
"Option B"
or both
"Option A"
The bidder (potential vendor) will supply all materials and labor
required to accomplish a thermal analysis, thermal design, fabrication
and installation
ponents
necessary
Customer
and set-screw
5.2
"Option
of
will
the
to
pressure
conform
provide
retaining
vessel
to
the
intent
a finished
rings
interior
thermal
of this
pressure
ready
shroud
com-
specification.
vessel
for
vendor's
the
raw material
(enclosure
housing)
use.
B"
Customer
necessary
(enclosure
b)
A" except:
will
for
provide
vendor
to
fabricate
(steel
the pressure
tubing)
vessel
housing).
Customer
will
pressure
vessel
provide
a thread
3age
for
the
external
threads,_
C-7
..
c}
Customer
shall
retaining
d)
Vendor will
fabricate
rings
customerts
Vendor
the
material
for
the
set-screw
rings.
retaining
e)
provide
the
pressure
from materlal
vessel
supplied
and set-screw
by customer
to
drawings.
will
threads
machine
so that
they
the
external
mate
with
pressure
a thread-gage
vessel
supplied
by customer.
6.0
REJECTIONS
Equipment not conforming to this specification or to authorized
modifications will be subject to rejection.
7.0
8.0
VENDOR WARRANTY
Vendor shall warrant that he will expediently repair or replace
any defect in workmanship and/or material found within one year from
the date of delivery.
C-8
DISTRI BUTION:
LASt
Allen
Bert
James
John
G. Blair,
Q-DO
R. Dennis,
Q-12
H. Hill,
Q-12 (3)
C. Rowley, Q-DO
EG_G
Willlam C. Anderson
William H. Bostwick
Stanley
O. Gamsby
Allan C. Johnson
Buford HcClung (5)
Carl F. Vlrcho_'
@-I-
+
-4
I
I
j
i
I
1
1
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