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Document Name: ASTM D665: Standard Test Method for Rust-Preventing
CFR Section(s):
Standards Body:
Official Incorporator:
THE EXECUTIVE DIRECTOR
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Designation: D 665 - 98
E1
Designation: 135193
Standard
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1. Scope
Copyright ASTM, 100 Barr Harbor Drive, West Conshohocken, PA 19428-2959, United States.
272
~ffi~ D 665
5.2 Beaker-A 400-mL, Berzelius-type, tall-form heatresistant glass ll beaker without pourout, as shown in Fig. 1,
approximately 127 mm (5 in.) in height measured from the
inside bottom center and approximately 70 mm (2% in.) in
inside diameter measured at the middle.
5.3 Beaker Cover- A flat beaker cover of glass or poly(methyl methacrylate) (PMMA) (Note 4), kept in position by
suitable means such as a rim or groove. Two holes shall be
provided on any diameter of the cover; one for a stirrer 12 mm
(15/32 in.) in diameter with its center 6.4 mm (V4 in.) from the
center of the cover; and the other, on the opposite side of the
center of the cover, for the test rod assembly (see Section 8), 18
mm (45/64 in.) in diameter with its center 16 mm (% in.) from
the center of the cover. In addition, a third hole 12 mm (15132
in.) in diameter shall be provided for a temperature measuring
device, with its center 22.5 mm (VS in.) from the center of the
cover and on a diameter of the cover at right angles to the
diameter through the other two holes.
rusting of ferrous parts can occur. This test indicates how well
inhibited mineral oils aid in preventing this type of rusting.
This test method is also used for testing hydraulic and
circulating oils, including heavier-than-water fluids. It is used
for specification of new oils and monitoring ,of in-service oils.
NOTE 2-This test method was used as a basis for Test Method D 3603.
Test Method D 3603 is used to test the oil on separate horizontal and
vertical test rod surfaces, and can provide a more discriminating evaluation.
5. Apparatus
NOTE 4-An inverted petri dish makes a suitable cover, as the sides of
the dish aid in keeping it in position. Fig. 2 shows a PMMA resin cover
11
THERMOMETER
HOLE
0,8 DIA PI N
11/32.")
STIRRER
TEST
ROD
ASSEMBLY
70 (27"4") APPROX
INSIDE DIA MIDWAY
0,6 THICK
(0,024")
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.NOTE
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f~r the beaker whIch has been found to be suitable. An 'optional fearilre is
sl).own, 'consisting ota slot, '1.6 by 27 1lim {V16 cby',lV16 in.), wIllClLis
~()entered,;Qn;a g,iaIp,eterQf t;!1e stirrer hole at right .,angles to'the covet
dill1neter through the test rod hole and stirrer hole. ;This feature allows
'vithd~~w"ai
Qf the
stirrer while
th~ beak~r' cover is. in' ' ;place.Whenth~te,~t
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method test IS used for other fluids such as synthetics, the beaker cover
.should be made fj:Orticliemically resistant material such as polymonochlorotrifluoroethylene, (pCTFE).
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, (0.4.5 9,,:-.0.479")
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TYPE 1
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TEST RO,D .
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BREAK SHARP
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(1/64)
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SAWCUT
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(0/(;" WHITWORTH)
CH UCK BODY
22.2
(1Is" )
39.7
A/F
MI6X2
giL
24.54
11.10
4.09
1.16
0.69
0.20
0.10
HaBOa
SrCI2 6H2 0
NaF
0.03
0.04
0.003
MgCI2 6H 2 0
CaCI2 (anhydrous)
SrCI2 6H2 0
Dissolve and dilute to 7 L
3885 9
406 9
14 9
KCI
NaHCOa
KBr
Ha B03
NaF
Dissolve and dilute to 7 L
483 9
140 9
70 9
21 9
2.1 9
,275
NOTE 7-Whtln making a check test, the steel test rod that showed rust
should not be reused. Test rods that repeatedly sh~)Y rust in tests of various
oils can be imperfect. Such test rods should be used with oils known to
pass the' test. If rusting occurs in repeat tests;, tbese test rodS' should be
discarded.
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~~r~ D 665
9.3 Continue stirring for 30 min to ensure complete wetting
of the steel test rod. With the stirrer in motion, remove the
temperature measuring device temporarily and add 30 mL of
distilled water through this hole, discharging the water on the
bottom of the beaker, and replace the temperature measuring
device. Continue stirring at a speed of 1000 50 rpm for 24
h (see Note 10) from the time water was added, maintaining the
temperature of the oil-water mixture at 60 1C (140 2P).
Stop stirring at the end of the 24-h period, remove the test rod,
allow to drain, and then wash with ASTM precipitation
naphtha or isooctane, or IP 60/80 petroleum spirit. If desired,
the test rod may be preserved by lacquering.
9.5 DIA
6.3 D/A - - - ,
BLADE
0.6 THICK
[0.024)
8 RAZE -----./
DRILL AND TAP TO FIT
3mm SETSCREW
(No.4 ALLEN)
(::I/e ")
(1/4" )
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9.5
(~/8")
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NOTE
13. Report
13.1 The test report shall contain,the f6Uowirig:
13.1.1 The type and identific;:atiQri of the product used.
13 .1.2 The date of the test.
'
13.1.3 A reference to this ASTM-IP standard, indicating
whethe~.Pt()cedbre A, B, or C was used. Since Procedure C
15. Keywords
15.1 circulating' oils; heaviet~thari-water fluids; hydiaulic
oils; inhibited mineral oil; rust-preventing characteristics;
steam-turbine, oils
The
The American Society for Testing and Materials takes no position rel;Pectingthe validity of any patent rights asserted In connection
with any item mentioned in this standard. Users of this standard are expressly'advised that determination of the validity of any 'such
patent righis, and the risl[ of.lnfringenient of such rights, are entirely their own responsibility.
,
" This, f/tancjwd is subject tq reyision I'ltl3ny tiroe by the ;Ejsponsible technical commitfe~ and' must be rdviewed every five' years and
,if not revised, either reapproved or withd(~wn. '((Jur comments are invited either for revision of this standard or fo( additional standards
'and snould be addfessed t6 ASTM Headquarters. Your comments will 'feceive careful consid~ration at a meeting ot the respo,risible'
technical committee, which you may attend. If you feel that your comments hilve not reoeivea a fair'hearing you should make your
views known to the ASTM Committee on Standards, 100 Barr Harbor{Jrivei West ,Conshohocken; PA 19428.
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This standard is copyrighted by ASTM, , 100 Barr Harbor Drive, West Conshohocken, PA 19428-2959, United, States. Individual
reprints (single or multiple copies) of this standard may be db/ained by coniaCting ASTM at the above adqress, or at 610-832-FJ585
(phone), 610-83;2-f}555 (fall), or service~as~rr;org (e-mall); or through the ASTM'webslte (http://wWw;astm.org).
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