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Oleochemicals
Category:
FPG Crude Glycerin
Originator:
Vijay
1.0
Date Approved:
January 2015
Subcategory:
Glycerin Evaporator Condensate Tank (S-307)
- Protocol
Owning Area:
Technical Standard #:
Utilities
OBJECTIVE
This is to provide a documented evidence that relocation of pH probe and caustic injection point
in Glycerin Evaporator Condensate Tank (S-307) will still produce the same specification crude
glycerin hot well product .The objective of this modification is to enhance the mixing of NaOH
(diluted caustic) with hot well product and better pH control. This will reduce the variation of pH
control in Glycerin Evaporator Condensate Tank (S-307). Failure to maintain the neutralization
pH between 6 to 8 can also lead to downstream process upset. It will also pose a danger of the
downstream equipment structural damage due to the acidity condition. If he condition is too
alkaline, vacuum will fluctuate indicating foaming in MeOH Concentrator.
2.0
SYSTEM DESCRIPTIONS
FPG
Oleochemicals
Category:
FPG Crude Glycerin
Originator:
Vijay
3.0
Date Approved:
January 2015
Subcategory:
Glycerin Evaporator Condensate Tank (S-307)
- Protocol
Owning Area:
Technical Standard #:
Utilities
BOUNDARIES
4.0
TEST PLAN
4.1
Location
Critical Parameters
Range
Target
Glycerin Hotwell
Hotwell pH
Hotwell level
6-8
40 - 60
7
50
4.2
Frequency
Sample
Size
Analysis
(A.M.#)
2
Who
Limit
FPG
Oleochemicals
Category:
FPG Crude Glycerin
Originator:
Vijay
Date Approved:
January 2015
Sampling
point
5.0
Subcategory:
Glycerin Evaporator Condensate Tank (S-307)
- Protocol
Owning Area:
Technical Standard #:
Utilities
1 x 500
ml
1). pH
(60065133)
OA
6.0 8.0
Items
1.
Action Plan
To collect Glycerin Evaporator Hot well sample and
analyze as per sampling plan.
Responsibility
Operation
Associates
When
Twice / per shift
7.0
What
pH
ABORT CRITERIA
No.
What
Product quality at
Glycerin
Evaporator
Condensate Tank
(S-307)
Abort Criteria
Any parameter that does not meet the in process control limit.
FPG
Oleochemicals
Category:
FPG Crude Glycerin
Originator:
Vijay
8.0
Date Approved:
January 2015
Subcategory:
Glycerin Evaporator Condensate Tank (S-307)
- Protocol
Owning Area:
Technical Standard #:
Utilities
VALIDATION DATA
S307 pH
monitoring.xlsx
SIGNATURES
Role
Name
Originator
Vijay
Validation System
Owner
Operation
Manager
QA Manager
Signature
Rahman
Date