Documente Academic
Documente Profesional
Documente Cultură
R.Cox
1-2012
Scope
Page 1
Equipment Overview
Page 1
Safety
Page 2
P&ID
Page 3
Operating Procedure
Page 4
Valve Directory
Page 14
Equipment Description
Page 16
Air circuit
The air circuit consists of two blowers, associated valves and 2-inch schedule 80 PVC rated to 400 PSI.
The gas injection and analysis system consist of a mass flow controller and associated measuring
devices.
A detailed list of the equipment incorporated in the gas absorption experiment is included at the end of
this document.
Safety
Safety glasses and hardhats must be worn when operating this equipment.
Note that certain procedures require the coordinated efforts of two people.
When filling the mixing tank do not exceed the 50-gallon level.
The use of caustic solutions, compressed gas, large volumes of water and multiple sources of
electrical power make attention to safety paramount when operating this equipment.
Accidental flooding will result in caustic liquid exposure to equipment and personnel working on
both floors below the gas absorber experiment.
Use Chloroflex gloves and wear safety glasses and a face shield when mixing sodium hydroxide
and water.
Never add water to a corrosive. Always add corrosives to water. When mixing with water, stir in
small amounts of corrosives slowly.
Label containers. All chemical containers must be clearly labeled with the chemical contents and
concentrations. Keep containers closed when not in use. Empty containers may contain residues
which are hazardous. Triple rinse all empty containers before discarding them to the trash.
Anytime the basement neutralization tank is in use, a team member must remain in room 2505
to monitor the basement tank system for leaks.
2
Operating Procedure
This procedure describes the operation of the gas absorber experiment with the following restrictions.
Some valves are not labeled or mentioned in this SOP these valves should not be adjusted.
This operating procedure details system operation using column # 1 with blower # 2.
Prior to startup:
Meet with the lab manager to verify that all tanks are empty. Both tanks have a sight glass
indicating the tank level, however, the sight glass does not read to the bottom of the tank. If the
sight glass does not indicate liquid in the tank, it is possible that the tank may contain liquid
below the level of the sight glass, which could result in flooding. To confirm that the tanks are
empty the tank pumps must be operated until no flow is observed. This procedure must be
performed with the assistance of the lab manager.
Close both the 9500 and 9510 gas analyzer input needle valves.
To feed column # 2 set the liquid circuit valves as listed above but close V8L and open V9L then adjust
column 2 liquid input flow using V11L. Adjust column 2 output flow using V15L.
1.
2.
3.
4.
Set the valves to pump liquid from the mixing tank to the feed tank.
Open:
Close:
V1L
V2L
V3L
Once you are ready to pump the contents of the mixing tank to the feed tank, set the mixing /
feed valves as indicated above.
The mixing tank pump is controlled by two switches; 17C located on the rear switch panel and a
second 17C switch located on the front switch panel. The 17C (mixing tank switches) must both
be in the on position to power the mixing tank pump.
5.
6.
7.
Set liquid flow valves to pump liquid from feed tank to column 1.
Open
Close
V5L
V9L
V6L
V3L
V8L
V10L
V12L
V14L
To feed column # 2 set the liquid circuit valves as listed above but close V8L and open V9L then
adjust column 2 liquid input flow using V11L. Adjust column 2 output flow using V15L.
8.
Closed
V15A
V16A
V14A
V13A
V11A
V12A
V1A
To select airflow to column #2, make the following adjustments to the valve settings as shown in
the valve directory.
Set V9A to allow flow in from the top and out through the right side.
7
9.
Close V11A.
10.
11.
Monitor the liquid flow out of the column, watch for flooding at the bottom of the column, if
liquid backs up at the bottom of the column to the point where it is about to enter the gas flow
inlet immediately reduce the flow of liquid into the column and open V14L.
12.
13.
J.
K. Slowly open the 9510 needle valve while monitoring the gas flow rate to the analyzer.
L. Adjust the needle valve so that the gas flow is below 300ml/min as indicated by the yellow tape
on the 9510 flow meter.
M. Repeat the previous three steps to set the flow for the 9500 analyzer. Note the yellow tape on
the 9500 analyzer marks the maximum flow of 1 L/min for the 9500 analyzer.
10
14.
15.
Verify that the pH of the liquid in the basement / neutralization tank is within disposal range.
A. Set neutralization / basement tank valves to recycle the contents of the basement tank.
B. Set V19L flow output to the right
C. Open V16L
D. Switch on the basement / neutralization tank pump.
Monitor the pH reading on the computer, if the pH does
16.
Close
V16L
V2L
V18L
V4L
11
17.
Wear Chloroflex gloves, lab coat and face mask when working with concentrated acid.
Mix all concentrated acid solutions in the fume hood.
A. Set neutralization / basement tank valves to recycle the contents of the basement tank.
B. Set V19L flow output to the right
C. Open V16L
D. Calculate the amount of acid required to lower the pH of the liquid in the basement tank to
within the safe disposal range of (5 10pH).
E. Disconnect the acid container from the metering pump located next to the feed tank. Take the
acid container to a fume hood and add the required amount of acid.
F. Cap the acid container and return it to the the metering pump. Connect the metering pump acid
feed line to the acid container.
G. Verify that the metering pump output line is connected to the PVC acid line.
H. Start the basement neutralization pump.
I.
J.
12
P.
Store any remaining acid in the 8-liter Nalgene container remember to label the container
with the contents and concentration.
18. Set the neutralization tank valves to pump the contents of the neutralization tank to drain.
A. Open V16L
B. Set V19L to flow to the left, towards V20L.
C. Set V20L to flow to the hose.
D. Verify that V16L is open.
19.
20.
Final Shutdown:
A. Verify that all pump and blower power switches are in the off position
B. Close the main CO2 tank valve
C. Close basement tanks main valve V16L
D. Set basement valve V19L to flow output to the right
E. Close Feed tank main valve V6L
F. Unplug all blowers
G. Close the mixing tank outlet valves V1L, V2L and V3L
H. Properly label and store any chemicals in use
I.
Exit the Opto22 control software; do not log off the computer
13
J.
Location
Function
V1L
Main
Comments
V2L
V3L
V4L
V5L
V6L
V7L
Not Used
V8L
Column # 1 feed
V9L
Column # 2 feed
V10L
V11L
V12L
Column # 1 feed
ALWAYS OPEN
V13L
Column # 2 feed
ALWAYS OPEN
V14L
Column #1 drain
V15L
Column #2 drain
ALWAYS CLOSED
V16L
V17L
Basement
Not Used
V18L
Basement
14
V19L
Basement
When the flow indicating arrows on the valves V2A - V12A listed below are oriented as indicated by the arrows,
air flow will be directed to column #1.
Air Circuit Valves
Location
Function
Comments
Main
V2A
V3A
V4A
V5A
V6A
V7A
V8A
V9A
V10A
V11A
V12A
V13A
Column #2 output
15
V14A
Column # 1 output
V15A
Orifice plate
V16A
Orifice plate
Gas Absorption
Experiment
Equipment Description
Air Flow Circuit
Blower #1
Spencer Turbo-Compressor
30 CFM - 64 oz, s/n 51219, lot # 35108
Blower motor: Black & Decker 2 HP, 60 cycle,
240 VAC, 10 Amp, 10,000 RPM, Type CSC
Blower #2
Spencer Turbo-Compressor
12 CFM - 35 oz, s/n 43903, lot # 33662
Rotometer: Air Flow
Omega Engineering FL45200A series
Range: 40 - 240 SCFM
Air velocity transmitter: JLC International model EE66
Range 0-400 ft/min
16
Orifice Plate #1: 0.814 inches i.d, no bevel - Pipe Size 1.9 inch o.d, 1.5 inch i.d
Orifice Plate # 2: 0.530 inches i.d, no bevel - Pipe size 1.4 inch o.d, 1.0 inch i.d
Liquid Circuit
Pump data
Mixing tank pump motor: AMT Model 3696-975-97, Pump head # 3690-002-00
Feed Tank Pump: Eastern Industries, model B 34
Max flow rate into column #1 = 10 GPM adjustable from 1-10 GPM
Neutralization Tank Pump: Same as feed pump
Metering Pump:
17
Pulsatron E Plus Series, Maximum flow 630.9 mil/min, Min flow 6.3 mil/min
CO2 Flow Control
CO2 gas feed system
Temperature
Measurement
Type T Thermocouples
Opto22
18