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I. I NTRODUCTION
Manuscript received April 24, 2009; revised October 5, 2009. First published
December 8, 2009; current version published February 3, 2010. This work was
supported in part by the National Science Foundation (NSF) under CAREER
Award ECS-0449400 and Grant CTS-0428889, in part by the Center of
Integrated Nanomechanical Systems under the NSF National Science and
Engineering Center Grant ECS-0425914, in part by Nanoscale Exploratory
Research under Grant ECCS-0708031, and in part by the National Institutes
of Health under Grant R01 EB006745-01A1. The work of S.-J. Park was
supported by a Samsung Fellowship. The work of J. C. Doll was supported
in part by a National Defense Science and Engineering Graduate Fellowship
and in part by an NSF Graduate Fellowship. Subject Editor K. E. Petersen.
The authors are with the Department of Mechanical Engineering, Stanford
University, Stanford, CA 94305 USA (e-mail: pruitt@stanford.edu).
Color versions of one or more of the figures in this paper are available online
at http://ieeexplore.ieee.org.
Digital Object Identifier 10.1109/JMEMS.2009.2036581
138
Ewc t3c
4lc3
(3)
where Svibro and Vvibro are the velocity sensitivity and velocity
voltage signal of the vibrometer, respectively.
We simulated dopant profiles using TSUPREM4 (Synopsys,
Mountain View, CA) (Fig. 2). To compute the efficiency factor
and sensitivity of each cantilever, we used the fabrication
process steps in Table I. We compared the simulation results
with dopant profiles measured by spreading the resistance
analysis (Solecon Laboratories, Reno, NV) of test structures
(5 mm 5 mm) fabricated during the piezoresistive cantilever process [Fig. 2(d)]. The geometry factor is calculated
from finite-element analysis using COMSOL (COMSOL, Inc.,
Burlington, MA).
III. A NALYTICAL M ODEL F OR S ENSITIVITY
A. Change in Resistance Due to Applied Stress
Piezoresistivity describes the change in the electrical resistance of a material due to the applied mechanical stress [27],
[28]. To calculate the change in resistance due to the mechanical
stress, we consider arbitrary profiles of both electrical resistance and mechanical stress, i.e., dopant concentration profile
(p) and stress distribution (). Additionally, because resistivity
, carrier mobility , and piezoresistivity are a function of
dopant concentration, p, , , , and are defined locally.
Therefore, it is necessary to average the change in resistance
by integrating all local variables over the three dimensions.
In this paper, we derive the analytical solution for the sensitivity of a typical device with a U-shaped piezoresistor. We
make four simplifying assumptions. First, we consider resistivity (l ) only in the longitudinal direction of the piezoresistor.
Current flow in a U-shaped piezoresistor can be assumed 1-D,
because the piezoresistor length is much greater than its width.
Second, we assume that the doping method is uniform across
the wafer so that the dopant concentration varies only across the
thickness of the piezoresistor. Third, lateral diffusion is negligible compared with diffusion in the thickness direction, because
the width of the piezoresistor is much larger than the junction depth. Fourth, we neglect shear piezoresistivity, because
longitudinal piezoresistors are insensitive to shear stress. Assuming plane stress [28], the change in resistance is a function
of the longitudinal piezoresistance coefficient (l ), transverse
piezoresistance coefficient (t ), normal stress parallel to the
current (l ), and normal stress perpendicular to the current (t )
(1)
l (x, y, z)
l (z)
(4)
(5)
or
2f0 Vpiezo
Svibro Vvibro
(2)
139
Fig. 2. Dopant concentration profiles for the cantilever shown are simulated using TSUPREM4. The plots compare epitaxial and ion-implanted distributions.
(a) Inert N2 anneal at 1000 C for epitaxial deposition (dopant concentration: 1018 cm3 ). (b) For low-dose ion implantation (dopant dose: 2 1014 cm2 ).
(c) For high-dose ion implantation (dopant dose: 5 1015 cm2 ). (d) Comparison of dopant profiles between TSUPREM4 result and spreading resistance
analysis data.
TABLE I
P ROCESS PARAMETERS OF TSUPREM4 S IMULATION
12(lc x)z
F.
wc t3c
(7)
140
The sensitivity can be expressed in terms of force or displacement and in terms of change in resistance or voltage. We indicate the sensitivity (S) with subscripts (force F , displacementd,
resistance , and voltage V ). From (6) and (7), the force
sensitivity ((R/R)/F ) for an end-loaded beam is
SF
tc /2
12(lc 0.5lp )l,max tc /2 qpP zdz
=
.
tc /2
wc t3c
qpdz
(8)
SF ,max
tc /2
2 tc /2 qpP zdz
.
=
tc /2
tc
qpdz
(10)
tc /2
Using this efficiency factor, the force sensitivity (8) for any
arbitrary dopant profile may be expressed as
SF =
(11)
tc /2
SF V =
C. Geometry Factor
is a geometry factor defined as the ratio of the resistance
of the strained region in the piezoresistor to the total resistance
including unstrained regions, interconnects, and contact pads
[Fig. 1(c)], which act to reduce force sensitivity ( < 1). We
can estimate the ratio of the resistance of the strained region to
the total resistance by calculating the voltage distribution of a
piezoresistor using finite-element analysis (Fig. 4).
D. Efficiency Factor
Considering a balanced 1/4-active Wheatstone bridge configuration ((Vout /Vbridge ) (R/4R)), voltage force sensitivity is
(9)
(12)
(13)
141
Fig. 5. of epitaxial (a, c, and e) and ion-implanted (b, d, and f) cantilevers with various cantilever thicknesses (a and b), dopant concentration (c), implantation
dose (d), epitaxial layer thickness (e), and implantation energy (f). Lines are discontinuous because the solid solubility limit depends upon the maximum processing
temperature.
142
Fig. 6. and junction depth of piezoresistor formed by B and BF2 ion implantation. Both low-power implantation and heavier ion implantation can yield better
and force sensitivity. However, the low dose and short diffusion lengths needed to fabricate shallow piezoresistors with BF2 require a longer annealing process
to achieve better and force sensitivity than elemental boron. The cross indicates diffusion lengths where of piezoresistors with BF2 is the same as of
piezoresistors with B.
.
(14)
=P 1
tc
B. for Nonuniform Doping Profiles
Diffusion of dopant atoms during high-temperature processes leads to a nonuniform dopant profile. The electrically
active dopant concentration profile can be simulated with
TSUPREM4 [Fig. 2(a)(c)] or experimentally measured using
spreading resistance analysis [Fig. 2(d)]. In Fig. 5, we calculated for epitaxial (A, C, and E) and ion-implanted
(B, D, and F) cantilevers in various conditions such as
different cantilever thickness (A and B), dopant concentration
(C), implantation dose (D), epitaxial layer thickness (E), and
implantation energy (F). To investigate how diffusion affects
with various process conditions, in Fig. 5 was also calculated
with various annealing conditions (temperature T and time
t) and was plotted in terms of diffusion length ( Dt). The
diffusion coefficient is defined as D = Dio exp(Eia /kB T ),
where for boron Dio = 0.037 cm2 /s and Eia = 3.46 eV [34].
143
Fig. 7. and oxide thickness of ion-implanted cantilever with different annealing methods. is greater for oxidizing environments because dopant
segregation
into the oxide acts to reduce the dopant concentration in the piezoresistor and increase by the piezoresistance factor effect. Note that versus Dt of dry
and wet oxidation is discontinuous for the different annealing temperature ranges, because of dopant segregation in the oxide.
large drift and electrical noise and may not yield optimal
resolution.
3) Effect of Initial Junction Depth on : Junction depth
is defined as the depth where the doping concentration of a
piezoresistor drops to background concentration. In the case
of epitaxial piezoresistors with varying initial thickness ratios
(tp /tc ) [Fig. 5(e)], is inversely proportional to the thickness
ratio as expected. Ion-implanted cantilevers show a similar
trend [Fig. 5(f)]; the formation of shallow piezoresistors by
reducing implantation energy tends to improve for a given
dose. However, there is an exception to this trend in the case
of low-dose low-diffusion-length piezoresistors where is
actually improved with implantation energy because of the
piezoresistance factor effect.
The effect of increasing ion mass for a fixed energy is similar
to that of decreasing implantation energy [Fig. 5(f)] because
the initial dopant depth is reduced. Bergaud et al. [35] demonstrated that ultrashallow piezoresistors can be fabricated by the
implantation of more massive ions such as BF2 . We calculated
for cantilevers with boron and BF2 dopant atoms in Fig. 6.
The competition between the depth and piezoresistance factor
effects is evident in the results.
4) Effect of Annealing Atmosphere on : Next, we investigated the effect of the postimplantation annealing atmosphere
on (Fig. 7). The trend of for dry and wet oxidation
is similar to the trend for inert annealing. However, is
greater for oxidizing environments because dopant segregation into the oxide acts to reduce the dopant concentration
in the piezoresistor and increase by the piezoresistance
factor effect. Oxide thickness
is greater for wet growth than
144
Fig. 9. 1 and 2 for boron-implanted piezoresistors (50-keV energy and 2 1015 cm2 dose) with various inert (N2 ) annealing temperatures and times.
1 (piezoresistance factor effect) and 2 (depth effect) depend only on processing parameters.
=
.
(16)
t
tc
qpdz
0
tc 2
1 = 0 tp
0 qpdz
tp
qpP z dz
2 = 0 tp
.
0 qpdz
(17)
(18)
(19)
3
4
SdV, measured
l
Es l,max 1 0.5 lpc f0 Vbridge
(20)
TABLE II
L OOKUP TABLE FOR 1 AND 2 ( IN MICROMETERS ) W ITH B ORON I MPLANTATION . T HE F IRST N UMBER G IVEN I S FOR A T YPICAL P ROCESS W ITH 1500- W ET I SOLATION OXIDE W ITH N2 A NNEALING ,
W HILE VALUES IN PARENTHESES A RE FOR I NERT (N2 ) A NNEALING A LONE . T HE W ET I SOLATION OXIDE WAS G ROWN AT THE I NDICATED P ROCESS T EMPERATURE FOR 66-, 15-, AND
5-min OXIDATION T IME FOR 900 C, 1000 C, AND 1100 C, R ESPECTIVELY, AND THE WAFER I S T HEN A NNEALED AT THE S AME P ROCESS T EMPERATURE FOR THE T IME
I NDICATED IN THE TABLE. OF P IEZORESISTIVE D EVICE I S C ALCULATED U SING (17). F OR E XAMPLE, OF 10-m-T HICK D EVICE W ITH 2 1015 cm2
I MPLANTATION D OSE AT 50 KE V AND A 30-min N2 A NNEAL AT 1000 C I S 0.53 F ROM = 1 2 /0.5tc = 0.55 0.13/5
146
Fig. 10. Validation of the analytical model. (a) Comparison of analytical models for the piezoresistance factor as a function of dopant concentration and
experimental results of changes in resistance of a typical piezoresistive cantilever (2000-m-long 30-m-wide 15-m-thick cantilever with 350-m-long by
10-m-wide U-shaped piezoresistor having the dopant profile in Fig. 2(d)) based on piezoresistance factors of the theoretical values of Richter [32], Harley and
Kennys empirical model [4], and Kandas theoretical values [28]. (b) Force sensitivity of piezoresistive cantilevers with various cantilever dimensions. (c and d)
of 7- and 15- m-thick piezoresistive cantilever. Each point of (b) indicates a sensitivity result of one device with different cantilever dimensions, and each
point of (c and d) represents measured values of two to seven devices from different wafers fabricated with different process conditions. The (solid lines)
analytical model is in good agreement with (circles) experimental results.
analysis [37] including variation in lp /lc , , the Youngs modulus, density, and the piezoresistance coefficient possibly from
the misalignment of the cantilevers from the [110] direction as
well as the undercut of the clamped boundary during backside
release. Measured values from thin cantilevers depart from
the model more than thick cantilevers. We believe the cases
with larger errors due to the thermal resistance of the cantilever
and the decrease in piezoresistance with temperature [32].
For typical 7-m-thick cantilevers with 15-min wet oxidation and 10-min N2 annealing at 1000 C, = 0.50 from
TSUPREM4, = 0.46 from dopant profiles from spreading
resistance analysis [Fig. 2(d)], and = 0.49 0.04 (N = 5
devices and 1 wafer) from experimental sensitivity. Although
TSUPREM4 predicts a greater junction depth than that measured with spreading resistance analysis, is dominated by the
high-concentration regions where the agreement between the
two is excellent. In addition, we found that for various cantilever geometries (16863175 m long and 30200 m wide)
from a single wafer have only 0.04 standard deviation. This
147
lp
Rslice = 2
(z)
2lp
dy =
.
wp tslice
wp tslice
(21)
tc /2
(28)
lp
Rslice = 2
(x, y, z)
dy.
wp tslice
(22)
lp
dy = l l + t t
(23)
G=
tc /2
wp
wp
dz =
2lp
2lp
t
c /2
tc /2
1
dz.
(24)
t/2
1 Rslice
R
=
.
2
R
Rslice Rslice
(25)
z=t/2
t
c /2
tc /2
1
(l l + t t )dz.
(26)
ACKNOWLEDGMENT
This work was performed in part at the Stanford Nanofabrication Facility (a member of the National Nanotechnology
Infrastructure Network) which is supported by the National
Science Foundation under Grant 9731293, its laboratory members, and the industrial members of the Stanford Center for
Integrated Systems. The authors would like to thank the staff
of the Stanford Nanofabrication Facility for the help with
the fabrication. The authors are grateful to N. Harjee and
J. R. Mallon, Jr., for the helpful discussions.
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Beth L. Pruitt (S99M02) received the B.S. degree in mechanical engineering from the Massachusetts Institute of Technology, Cambridge, in
1991, and the M.S. degree in manufacturing systems
engineering and the Ph.D. degree in mechanical engineering from Stanford University, Stanford, CA,
in 1992 and 2002, respectively, supported by both
the Hertz Foundation Fellowship and the Stanford
Future Professors of Manufacturing Fellowship.
She was an Officer in the U.S. Navy with tours as
an Engineering Project Manager at Naval Reactors,
Washington, DC, and as an Engineering Instructor at the U.S. Naval Academy.
She joined the mechanical engineering faculty at Stanford University in 2003.
Her research interests include microelectromechanical systems, particularly
metrologies for material characterization and biological measurements, and
manufacturing and design for packaging, systems integration, and biomedical
devices.
Dr. Pruitt is a Certified Professional Engineer. She is the recipient of the
National Science Foundation CAREER Award and the Defense Advanced
Research Projects Agency Young Faculty Award.