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The key components selected are n-C4 and i-C5 as light and heavy key respctively.
Components
Xf
i-C4
n-C4
i-C5
5N5
2,2 DMC4
2,3 DMC4
2MC5
3MC5
5N6
6N6
6N7
K-Value (HK)
Avg Temp T
0.1895
0.2032
0.314
0.0238
0.0623
0.018
0.0652
0.04
0.0426
0.039
0.0025
1.2430511515 i-C5
153.15 F
Xd
0.4789
0.5052
0.0159
0
0
0
0
0
0
0
0
Xb
K-Values
0
0.0064
0.5082
0.0394
0.1032
0.0298
0.1079
0.0661
0.0704
0.0644
0.0042
3.4805390744
2.652914257
1.2430511515
0.7257098147
0.6721397855
0.5315962478
0.5025371437
0.4576320077
0.3656216515
0.2939287917
0.153777559
67.31 C
Nm
Nm
10.332829229
11
Rm+1
Rm
2.3865911998
1.3865911998
Sum
-Value 1.4
0.0602859725
1.2 Rm
1.6639094397
0.5809923375
R/R+1
0.6246118636
Vis A
0.32
11
34.375
35
302.51
265.84
367.32
406.69
438.44
444.19
170.2
160.2
191.58
231.67
226.67
228.86
384.13
372.11
208.27
207.55
440.52
653.62
528.41
243.24
290.84
271.58
0.1744866103 mNs/m2
Relative volatility a
a*a
2.134195567
0.3723885502
60 %
35
Eo
0.6
Actual Plates
Nth/Eo
Vis B
N
N
58.333333333
59
Feed-point location:
Using Krikbride empirical equation
here
log (Nr/Ns)
Nr/Ns
B
D
1402 lbmol/hr
915.4 lbmol/hr
-0.085755998
0.820812577
59
32.40311537
33
N-Ns
26
27
0.5 m
Rectifying Section:
Following are the necessary physical properties for Diameter calculation taken from HYSYS
v
10.96 Kg/m3
542.5 Kg/m3
9.416 dyne/cm
Lw
Vw
FLV
or
0.009416
45670 kg/hr
70180 kg/hr
0.0924960216
from graph
K1
0.07
for values other than 0.02N/m surface tension a correction is applied for K 1
K1
0.06021
0.3564075993 m/s
6403 m3/hr
1.778611 m3/s
An
5.0
Ac
5.67
8.8
9.0
Stripping Section:
Following are the necessary physical properties for Diameter calculation taken from HYSYS
v
13.87 Kg/m3
560 Kg/m3
8.261 dyne/cm
Lw
Vw
FLV
or
0.008261
117600 kg/hr
67860 kg/hr
0.2727329961
from graph
K1
0.065
for values other than 0.02N/m surface tension a correction is applied for K 1
K1
0.05
0.2904976303 m/s
4891 m3/hr
1.358611 m3/s
An
4.7
Ac
5.31
D=((At 4)/)
Dia
2.6011287735 m
or
8.5
Both diameters differ less than 20%, therefore we will have same diameter through out the column.
Therefore, governing Diameter
9
Plate Areas:
Ac
Ad
An
5.91 m2
0.7093202392 m2
Aa
Ah
12% of Ac
Ac-2Ad
Aa
4.4923615148 m2
Hole area
normally 10% of Aa
Ah
0.4492361515 m2
Weir Dimensions:
Recommended values for columns operating above atmospheric pressure for Weir Height
hw
hw
40-50mm
50 mm
Weir length of 0.77 times Dc is recommended or we can use graph for weir length
Ad/Ac
From graph the ratio
0.12 or
12
lw/Dc
lw
0.77
2.1122639324 m
or
370.6 gpm
83.160042245 in
4.4564671926 gpm/in of weir
924.3 gpm
83.160042245 in
11.114712968 gpm/in of weir
Both top and bottom liquid flow rate are in the given recommended range.
So we have selected singe pass cross flow with sgmental downcomer.
0.5 m
5 mm
5 mm
Tray Hydraulics:
Weep Point:
from HYSYS
Weir crest
117600 kg/hr
32.66667 kg/s
70 %
22.86667
Maximum
Minimum
how
how
At minimum rate
K2
From graph
68.52363 mm of liq
54.02221 mm of liq
hw+how
104.0222 mm
31
3.3939765976
Minimum Vapor rate/Ah
2.1169885252
1
0.1 or
from graph
Co
0.84
Uh
3.0242693217
now
hd
16.3734789572
hr
22.321428571 mm of liq
ht=hd+hr+(hw+how)
157.2185337 mm of liq
now
P
863.69573671 N/m2
for total pressure drop across all trays
or
here
Am is either the downcomer area or clearance area under the downcomer Aap, whichever is smaller
Taking height of Apron
hap
Area
Aap
Aap
hdc
hap=hw-10
40 mm
hap*lw
0.0844905573 m
79.127114099 mm of liq
hb
354.8693 mm of liq
0.354869 m
tr
4.3151307135 s
3s
Entrainment Check:
percentage flooding = Un (act velocity based on net area)/Uf (flooding velocity based on net area)
Un
Uf
percentage flooding
0.261186896 m/s
0.341761918 m/s
0.7642363944
76.42363944 %
FLV
0.2727329961
from graph
fractional entrainment
ah
dh
ah
ah
Number of holes
5 mm
* dh2/4
1.96375E-005 m2/hole
22876.443106
22877 holes
59
0.5
tray space*N
29.5
Top and bottom clearance usually amount to 15% of that required by trays
Top and Bottom Clearance
Tray thickness
total thickness
4.425
5
0.295
34.22
112.2703448
113
reflux ratio
(i * Xid)/(i - )
0.9578011419
1.4685400578
-0.03975
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2.3865911998
Viscosity
0.1291676051
0.1322513834
0.145068836
0.2748272451
0.2256947407
0.2310974422
Xf * Viscosity
0.0244772612
0.0268734811
0.0455516145
0.0065408884
0.0140607823
0.004159754
0.1922573469 0.012535179
0.1995690888 0.0079827636
0.3039804678 0.0129495679
0.4703941072 0.0183453702
0.4039792283 0.0010099481
Sum
0.1744866103
N/m
sctional area
m2
m2
ft
ft
N/m
sctional area
m2
m2
ft
iameter through out the column.
ft
83.1600422453 in
pm/in of outletweir .
m/s
m/s
10
m/s
mm of liq
0.8636957367 KPa
50.9580484661 KPa
owncomer area
Setisfactory
Setisfactory
m
m
m
mm/plate
m
m
ft
ft