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The following remarks and recommendations are not complete and should be looked at as a
guideline.
General remarks on scientific work: .................................................................................. 1
Recommendations for reports and scientific paper:............................................................ 2
Structure of a report or paper: ......................................................................................... 3
Citing within the text flow, samples: ................................................................................. 3
Reference sample:........................................................................................................... 3
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Before you do a field sampling campaign, think about which parameter are necessary,
useful or crucial to investigate or to measure and why are they important for the scientific scope of your work.
Before you go into the field, you are experienced with the sampling technique, the
equipment and the laboratory techniques, as well. Check your technique and the
equipment at the institute (e.g. in the back yard) and know how to handle and how to
repair it in the field.
Take sufficient amounts of samples! Try to calculate the mass or volume needed for an
excellent analysis and consider reserves for additional experiments or analyses.
All methods or techniques are verified by a minimum of triple experiments, you always
check or know the analytical, physical or chemical limits of your methods or techniques.
Laboratory experiments are performed as triple experiments with so called "blank" experiments (no reaction, no compound, "clean condition", and so on) in parallel. Use a
standard as a sample to proof your analytical method (standard = sample with known
concentrations, e.g. a spiked soil or water sample).
You should know the possible errors of your methods, as well as fundamental parameters such as reproducibility, recovery, exactness, and so on.
If an experiment fails, check your physico-chemical, laboratory and/or system conditions, repeat your experiment and vary 1 condition, keep other conditions in the same
state. Repeat systematically the experiment until you find the problem. Never change 2
or more conditions or factors at the same time, thus you will not be able not separate
the problem or the influence of a certain factor on your experiment design.
Sampling intervals within time dependent experiments should be considered in linear
(equidistant interval) or logarithmic scales. Think about possible processes or events,
which can lead to an increase, decrease or tailing of a parameter. For instance a tracer
field test or column laboratory test shows often a long tailing period, which requires
sampling intervals, such as 1, 3, 7, 10, 15, 30(time units, e.g. hours or days, even
weeks).
Experiments from the literature should be proofed with the conditions described in the
original scientific paper. If it does not work after all, contact the author. Do not vary any
conditions before you get the expected result described in the original paper.
All steps of your field and laboratory work and remarkable events (including the
weather) are recorded in a field or laboratory book, which is always stored at a safe
place. A simple (arti)fact, problem or boundary condition could be sometimes the rea-
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son for a failed experiment. Do not hesitate to ask your colleague about a problem or
discuss a problem with your advisor.
Always make a time, work package and/or milestones plan. Write down at which time
scales a problem should be solved or an aim should be reached. Draw graphical plots
of your plans. Define reasonable deadlines for interim- and end-reports.
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We never make intentionally errors or failures (e.g. laboratory work), but we describe
the errors and failures, which occurred and try to quantify them if required or suitable.
Summary (short, only the most important facts and information, if possible several
languages)
Content, Outline
Reference sample:
Schiedek, T. (1995): Impact of Plasticizers (Phthalic Acid Esters) on Soil and Groundwater
Quality.- Proceedings 'International Conference on Groundwater Quality: Remediation and
Protection (GQ95)' IAHS, Publ. no. 225: 149-156.
Schiedek T, Beier M, Lerch C (2004): Quantification of fuel-related organic contaminants in
urban areas of Germany.- In: Zhu, Y., Balke, K.-D., Prinz, D. (eds.): Proceed. Water and Development II, Proceed. Hangzhou, China, Geological Publishing House Beijing, P.R.C, 57
60.
2.0
Cl concentration Cwm
1.8
Cl flux F
1.6
1.4
1.2
1.0
0.8
0.6
0.4
0.2
31
30
to
30
to
29
28
to
29
27
26
to
26
to
25
24
to
25
23
22
to
22
to
21
20
to
21
20
19
to
19
37
to
18
17
to
17
to
16
15
to
16
15
13
to
14
to
12
11
to
12
0.0
Fig. 1: The Cl concentration vs. Cl flux for selected Zs; the data represent the Cwm (see
equation (4)) and the calculated flux F (see equation (1)) for the Z borders; concentrations
and fluxes are normalized to mean values.
Table 1: Occurrence of PAH and implication of biodegradation due to decreasing concentrations of potential electron acceptors, such as SO4, NO3, and the occurrence or increase of
Fe2+ and Mn2+; values deviating clearly from mean in bold; location of the GMW see Fig. 4.
Sampling
campaign
2001
PAHa
SO4
HCO3
NO3
[ng l-1]
NH4
Fe2+
Mn2+
[mg l-1]
219
8.0
232
26
0.01
0.10
0.05
GMW 29, Z4
275
111
494
67
0.18
0.10
0.08
GMW 12
2352
130
214
3.7
0.01
0.84
0.32
7580
202
574
4.0
0.06
0.14
0.61
580
n.d.
0.05
0.45 0.28
GMW 56, Z10 23451
126
Sum of 16 PAH according to US Environmental Protection Agency