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"This is the pre-peer reviewed version of the following article: Convective drying of potato slices at lowtemperatures in full air

recirculation dryer, which has been published in final form at


[http://www.appleacademicpress.com/title.php?id=9781771884518]. This article may be used for non-commercial
purposes in accordance with Apple Academic Press Terms and Conditions for Self-Archiving."

To cite this article use following reference:


Zlatanovi, I., Radojii, D., Topisirovi, G. Convective Drying of Potato Slices at LowTemperatures in Full Air Recirculation Dryer. Chapter 6 in: Engineering Practices for
Agricultural Production and Water Conservation - An Interdisciplinary Approach. Part 2:
Agricultural Process Engineering. Series: Innovations in Agricultural and Biological
Engineering. Editors: Megh R Goyal, PhD, PE R. K. Sivanappan, PhD. In production. Pub
Date: Sep, 2016. Hard ISBN: 9781771884518. E-Book ISBN: 9781771884525. Apple
Academic Press. 2016.

CONVECTIVE DRYING OF POTATO SLICES AT LOW-TEMPERATURES IN FULL


AIR RECIRCULATION DRYER
Ivan Zlatanovi1, Duan Radojii, Goran Topisirovi
University of Belgrade - Faculty of Agriculture, Department of Agricultural Engineering,
Nemanjina 6, 11080 Belgrade, Serbia
Abstract
An experimental investigation of convective drying of Dsire potatoes in full recirculation
laboratory scale dryer was conducted. Potatoes sliced into chips (thickness 2 and 3 mm),
without pre-treatment, were used. The parameters of air stream over the tray with samples
were fully controlled and adjusted in several sets of experiments. Drying air temperature was
in range 35-55oC, relative humidity in range 10-30% and velocity in range 1-2 m/s. Data were
analyzed to obtain diffusivity values from the period of falling drying rate. The effective
moisture diffusivity was used to describe drying process efficiency. The obtained values for
the potato effective diffusivity coefficient were in range 1.5010-8 4.2810-8 [m2/s].
Key words
Convective drying; Potato; Experimental results; Drying air parameters; Effective moisture
diffusivity.
1. Introduction
In modern industrial production, can be said with certainty that there is no such a product
whose main raw material in one of its stages did not go through a drying process (Zlatanovic,
2012a, 2012b). Research and analysis of the drying process is essential for its further
optimization and improvement. A clear physical and mathematical description of the process
of drying biological material is still pretty much remained unresolved despite the huge
number of applied research. Most modeling methods based on the concept of the diffusion of
moisture through the material, describes a change in the average moisture content of the
material over time (Kemp, 2001).
The estimation of the effective diffusivity coefficient during the drying process of various
food materials is very common in literature. Similar researches were conducted for potato
material (Singh, 2011; Aghbashlo, 2009; Hassini, 2007; Leeratanarak, 2006; Akpinar, 2003;
1 Corresponding author:

E-mail address: ivan@agrif.bg.ac.rs

"This is the pre-peer reviewed version of the following article: Convective drying of potato slices at lowtemperatures in full air recirculation dryer, which has been published in final form at
[http://www.appleacademicpress.com/title.php?id=9781771884518]. This article may be used for non-commercial
purposes in accordance with Apple Academic Press Terms and Conditions for Self-Archiving."

Simal, 1994). The effect of air temperature, the thickness of slab and air velocity on the
moisture diffusion was usually investigated. However, unlike other, this research include
relative humidity besides all other drying parameters. The experiments were conducted in
convective dryer with full air recirculation, which makes the control of the drying agent (air)
relative humidity less complicated. This way, all important drying parameters were
considered.
2. Materials and methods
Potatoes (var. Dsire) were used in the experiments. This variety of potatoes was introduced
in Holland in 1962. It has great resistance to various diseases and it is suitable for growing in
regions with low rainfall. The annual production in Republic of Serbia is 900.000 tons. It has
excellent storage properties.
The usual shapes of the final product of dried potatoes are: french-fries shaped pieces and
chips slices. Potato chips shape is chosen because of the simplicity and solvability of the
diffusion model equations (Crank, 1975). The side dimensions of 2 and 3 mm are chosen from
the range between 0.3 and 4.3 mm, that is a normal range for this shape of the material widely
used in literature (Leeratanarak, 2006; Kingsly, 2007). This geometry shape is suitable for
describing in Descartes rectangular coordinate system. The material dimension in the
direction of z-axis is much smaller than the other two dimensions in the direction of the x-axis
and y-axis. Therefore, the main route of moisture transfer through the material will be in the
direction of the z-axis. The moisture movement through the material in the direction of x-axis
and y-axis may be omitted. This way the mass transfer equations will be simplified.
For samples preparation, potatoes were washed, peeled and cut into potato chips slices with 2
and 3 mm thickness. The chips slices were put in thin-layer on the 240x200 mm tray with net
weight of 0.1 kg. The initial moisture content of apple cubes was determined using the ovendrying method (Lengyel, 2007) with repetition in order to assure accurate initial moisture
content average values. The initial moisture content of the samples was found to be 760.3%,
with initial moisture ratio of 3.58 kg water/kg dry matter.
2.1 Experimental apparatus
Convective laboratory scale HPD system with possibility of full drying air recirculation
(Fig.1) was designed and built in order to achieve and measure all relevant drying process
parameters, and with possibility of the full control of drying air RH. It consists of a closed
loop tunnel sections with built-in drying chamber. Primary condenser (CD1) used for air
heating is positioned at the top of the vertical tunnel section above the tray section (TR) that
stands on digital weight indicator (DWI). Evaporator (EV) used for air cooling is positioned at
the bottom of the horizontal tunnel section, separated from the by-pass (BP) line. Water
condensed on EV surface drains out of the system to the graduated glass cylinder (GC) located
outside of the dryer. Desired drying air velocity is provided with an axial fan with electric
motor frequency speed control unit. The amount of air that flows through BP and EV is
regulated manually with by-pass damper (BPD) and evaporator damper (EVD).

"This is the pre-peer reviewed version of the following article: Convective drying of potato slices at lowtemperatures in full air recirculation dryer, which has been published in final form at
[http://www.appleacademicpress.com/title.php?id=9781771884518]. This article may be used for non-commercial
purposes in accordance with Apple Academic Press Terms and Conditions for Self-Archiving."

Figure 1. Laboratory HPD system with full air recirculation

The measurement equipment used in experiments has the following accuracies: temperature
measurement: 0.175oC, air relative humidity measurement: 1%, drying air velocity
measurement: 0.01 m s-1, weight measurement: 0.001 kg, measurement: 5 cm3, current
frequency measurement: 0.01 Hz.
The following measurements were performed (Fig.1):
T w
At positions 1 to 5: drying air parameters ( , , and RH);
T
At position 6: ambient air properties ( and RH);
At positions A, B, C and D: dryer components control parameters (temperatures at
CD1 and EV inlet/outlet connections);
At position E: sample weight during the drying process;
At position F: removed water volume;
At position G: electric motor parameters (current frequency).
2.2 Experimental design
All measurements and experimental procedures were carried out in accordance with the
methodology described by (Zlatanovic, 2013). Drying air temperature was in range 35-55oC,
relative humidity in range 10-30% and velocity in range 1-2 m/s. Drying air was circulating
over the wet material staggered on a tray.
2.4 Drying models
Ficks second law of unsteady state diffusion (Eq.(1)) for cube geometry, that provides
connection between effective moisture diffusivity and moisture ratio (Crank, 1975), was used
to interpret the drying process since moisture diffusion is one of the main mass transport
mechanisms that describe this process.

"This is the pre-peer reviewed version of the following article: Convective drying of potato slices at lowtemperatures in full air recirculation dryer, which has been published in final form at
[http://www.appleacademicpress.com/title.php?id=9781771884518]. This article may be used for non-commercial
purposes in accordance with Apple Academic Press Terms and Conditions for Self-Archiving."

2M 2M 2M
M
Deff 2 M Deff

2
2

y
z 2

(1)
In the case of symmetric boundary conditions, with neglecting of material shrinkage and with
the assumption that water distribution in material (2 and 3 mm chips) is homogeneous, the
moisture ratio can be determined (Crank, 1975; Akpinar, 2003; Aghbashlo, 2009) as in Eq.(2).
2 Deff
M Me
8

MR
2 exp
2

M0 Me
4
z

(2)
Taking into account the change of MR with drying time, Eq. (2) can be solved only
numerically. In this case, a linear correlation between the natural logarithm of MR and time is
obtained and can be used in Eq. (3).
2
8 Deff
ln MR n 2

4
z

(3)
ln MR f
A plot of
gives a straight line with a slope that is used to determine (Crank,
1975) effective moisture diffusivity (Deff) according to Eq. (4).
2 Deff
Slope
4z 2
(4)
Drying rate of products during drying experiments was calculated by using the following
equations:
M M
DR

(5)
3. Results and discussion
The knowledge of MR change in time opens up the possibility of mutual comparison of the
kinetics of drying of many different materials regardless of total weight of the material.
Determination of the MR was performed on the basis of the experimental results and
methodology described in subsection 2.4 (eq.2) and presented on Fig.2 and Fig.3.

"This is the pre-peer reviewed version of the following article: Convective drying of potato slices at lowtemperatures in full air recirculation dryer, which has been published in final form at
[http://www.appleacademicpress.com/title.php?id=9781771884518]. This article may be used for non-commercial
purposes in accordance with Apple Academic Press Terms and Conditions for Self-Archiving."

Figure 2. Efect of temperature, relative humidity and velocity of drying air


on MR change in time (Potato, chips 2mm)

Figure 3. Efect of temperature, relative humidity and velocity of drying air


on MR change in time (Potato, chips 3mm)

The value change of MR in the process follows the character of the changes of moisture
content.
The results of experimental research, indicate the lack of a constant-rate period of drying, ie.
only the existence of the period of falling rate of drying (Fig. 4 an Fig. 5). During the drying
process, the drying rate is declining in a constant, which can be explained by the fact that the
material is dried in a thin layer. The highest drying rate occurs at the beginning of drying,
when the average moisture content is highest. This is explained by the position of the zone of
vaporization, which is closer to the outer surface of the material at the beginning of the
process, so the resistance to the transfer of moisture through the material is smaller.

"This is the pre-peer reviewed version of the following article: Convective drying of potato slices at lowtemperatures in full air recirculation dryer, which has been published in final form at
[http://www.appleacademicpress.com/title.php?id=9781771884518]. This article may be used for non-commercial
purposes in accordance with Apple Academic Press Terms and Conditions for Self-Archiving."

Figure 4. Efect of temperature, relative humidity and velocity of drying air


on DR change in time (Potato, chips 2mm)

Figure 5. Efect of temperature, relative humidity and velocity of drying air


on DR change in time (Potato, chips 3mm)

By using the effective diffusion coefficient it is possible to include all the possible
mechanisms of the transfer of moisture that occur in the material, so that the transfer of
moisture depends only on the geometrical shape and dimensions of materials which influence
the direction and the direction of movement of moisture. In the case of material of potato,
sliced into thin sheets (chips), the thickness of the sheets (in the z direction) is several times
smaller than the other two dimensions (in directions x and y-axis), so that the direction of
movement of moisture takes the direction of the z-axis. The movement of moisture in the
directions of the x and y-axis is ignored. The characteristic length of material z that exists in
the equation (2) in this case represents the of the chips thickness. Determination of the
effective diffusion coefficient in this case is based on the assumption that the transmission of
moisture takes place in the two directions along the direction of the z-axis. The calculated
values of effective diffusivity coefficient for each experimental setup are presented in Table 1.

"This is the pre-peer reviewed version of the following article: Convective drying of potato slices at lowtemperatures in full air recirculation dryer, which has been published in final form at
[http://www.appleacademicpress.com/title.php?id=9781771884518]. This article may be used for non-commercial
purposes in accordance with Apple Academic Press Terms and Conditions for Self-Archiving."

Table 1
The results for effective diffusivity coefficient
for each experimental setup
Effective diffusivity
coefficient
Drying regime
Deff 108 [m2/s]
Experimental
potato
setup
T
RH
w
z =2
z =3
[oC] [%] [m/s]
[mm]
[mm]
E1
E2
E3
E4
E5
E6
E7
E8
E9
E10
E11
E12
E13
E14
E15
E16
E17
E18
E19
E20
E21
E22
E23
E24
E25
E26
E27

35
35
35
35
35
35
35
35
35
45
45
45
45
45
45
45
45
45
55
55
55
55
55
55
55
55
55

10
10
10
20
20
20
30
30
30
10
10
10
20
20
20
30
30
30
10
10
10
20
20
20
30
30
30

1
1.5
2
1
1.5
2
1
1.5
2
1
1.5
2
1
1.5
2
1
1.5
2
1
1.5
2
1
1.5
2
1
1.5
2

1,91
2,04
2,17
1,64
1,75
1,87
1,51
1,62
1,72
2,68
2,82
2,97
2,39
2,50
2,63
2,04
2,14
2,26
3,83
4,04
4,28
3,54
3,73
3,98
3,00
3,18
3,38

1,90
2,01
2,12
1,61
1,72
1,83
1,50
1,57
1,68
2,63
2,77
2,92
2,34
2,45
2,59
2,01
2,12
2,23
3,72
3,94
4,20
3,47
3,65
3,87
2,96
3,10
3,32

The values for the potato effective diffusivity coefficient are in range: Deff =1.5010-8
4.2810-8 [m2/s]. The effective diffusion coefficient increases with increasing temperature
humidity and velocity of moist air, and decreases with increasing relative humidity and the
characteristic dimensions of a piece of material. In table 2, the effective diffusion coefficient
are presented in a such a way that all drying parameters that have negative influence (relative
humidity and material size) on Deff are in columns and all drying parameters with positive
influence (temperature and velocity) on Deff are in rows.

"This is the pre-peer reviewed version of the following article: Convective drying of potato slices at lowtemperatures in full air recirculation dryer, which has been published in final form at
[http://www.appleacademicpress.com/title.php?id=9781771884518]. This article may be used for non-commercial
purposes in accordance with Apple Academic Press Terms and Conditions for Self-Archiving."

Table 2
Effective diffusivity coefficient Deff 108[m2/s]
Potato
Drying parameters
w=1 m/s
w=1.5 m/s
w=2 m/s

T=35oC
T=45oC
T=55oC
T=35oC
T=45oC
T=55oC
T=35oC
T=45oC
T=55oC

RH=10%
1,91
2,68
3,83
2,04
2,82
4,04
2,17
2,97
max.4,28

z=2 mm
RH=20%
1,64
2,39
3,54
1,75
2,50
3,73
1,87
2,63
3,98

RH=30%
min.1,51
2,04
3,00
1,62
2,14
3,18
1,72
2,26
3,38

RH=10%
1,90
2,63
3,72
2,01
2,77
3,94
2,12
2,92
max.4,20

z=3 mm
RH=20%
1,61
2,34
3,47
1,72
2,45
3,65
1,83
2,59
3,87

RH=30%
min.1,50
2,01
2,96
1,57
2,12
3,10
1,68
2,23
3,32

The highest values of effective diffusion coefficients were determined in experiments E21
T 55C RH 10% w 2 m s
with the set parameters of drying:
,
i
. This is explained by
the maximum values of the parameters of temperature and flow velocity of moist air, and
minimum of the relative humidity value, in the observed range of size variation. The lowest
values of effective diffusion coefficients were determined in experiments E7 with the set
T 35C RH 30% w 1 m s
parameters of drying:
,
i
. This is explained by the minimal
values of the parameters of temperature and flow velocity of moist air, and the maximum
value of the parameter relative humidity, in the observed range of size variation.
Table 3
The influence of drying parameters variation on effective diffusivity coefficient
The change of effective
The variation of
diffusivity coefficient
Drying parameter
drying parameter
Potato, chips 2 mm
Temperature

60%

100%

Relative humidity

100%

14%

Air velocity

100%

13%

The influence of drying parameters variation on the change of effective diffusivity coefficient
is presented in table 3.

"This is the pre-peer reviewed version of the following article: Convective drying of potato slices at lowtemperatures in full air recirculation dryer, which has been published in final form at
[http://www.appleacademicpress.com/title.php?id=9781771884518]. This article may be used for non-commercial
purposes in accordance with Apple Academic Press Terms and Conditions for Self-Archiving."

Figure 6. Drying time for each experiment (Potato, chips 2 and 3 mm)

Drying time was measured for potato sample dimensions of 2 mm and 3 mm in different
experimental setups (Fig.6). The maximum drying time was observed in the experiment E7
and the minimal in E21.
4. Conclusion
In this paper, the effects of drying agent (air) temperature, relative humidity and velocity as
well as the material dimension influence on the kinetics of the drying process was
investigated. Drying air temperature was in range 35-55oC, relative humidity in range 10-30%
and velocity in range 1-2 m/s. Potatoes were sliced into chips with the thickness of 2 and 3
mm.
It was found that regardless of the dimension of the test material, the drying regime, with the
highest temperature and velocity agents, and minimum relative humidity, achieves the shortest
possible duration of the drying process, and vice versa.
The influence of individual parameters on the kinetics of drying scratched discussed over the
obtained values of effective diffusion coefficient. The effective diffusion coefficient does not
change in time. The increase of the air velocity and temperature agent lead to a rise in
effective diffusivity coefficient values with predictable cause-and-effect relationship.
Obtained values of the effective diffusivity coefficient are in the range: 1.5010-8 Deff
4.2810-8 m2/s.
References
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potato slices in length of continuous band dryer, Energy Conversion and
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Akpinar, E., Midilli, A., Bicer Y. 2003. Single layer drying behavior of potato slices in a
convective cyclone dryer and mathematical modeling, Energy Conversion and
Management 44, p.1689-1705.
Crank, J. 1975. The mathematics of diffusion, Second edition, Brunel University
Uxbridge, Oxford University Press, London. ISBN 0-19-853344-6.

"This is the pre-peer reviewed version of the following article: Convective drying of potato slices at lowtemperatures in full air recirculation dryer, which has been published in final form at
[http://www.appleacademicpress.com/title.php?id=9781771884518]. This article may be used for non-commercial
purposes in accordance with Apple Academic Press Terms and Conditions for Self-Archiving."

Hassini, L., Azzouz, S., Peczalski, R., Belghith, A. 2007. Estimation of potato moisture
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10.1016/j.fbp.2011.06.006.
Zlatanovi, I. 2012a. Application of modern drying technology in the food processing
industry, Scientific Journal Agricultural engineering, 37(4), p.23-30, (ISSN
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Zlatanovi, I. 2012b. Types, classification and selection of dryers in agro industry,
Scientific Journal Agricultural engineering, 37(2), p.1-13, (ISSN 0554-5587).
Zlatanovic, I., Komatina, M., Antonijevic, D. 2013. Low-temperature convective drying of
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