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BRITISH STANDARD

Bituminous mixtures
Test methods for hot
mix asphalt
Part 42: Amount of coarse foreign
matter in reclaimed asphalt

The European Standard EN 12697-42:2005 has the status of a


British Standard

ICS 93.080.20

12&23<,1*:,7+287%6,3(50,66,21(;&(37$63(50,77('%<&23<5,*+7/$:

BS EN
12697-42:2005

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BS EN 12697-42:2005

National foreword
This British Standard is the official English language version of
EN 12697-42:2005.
The UK participation in its preparation was entrusted by Technical Committee
B/510, Road materials, to Subcommittee B/510/1, Coated macadam and hot
asphalt, which has the responsibility to:

aid enquirers to understand the text;

present to the responsible international/European committee any


enquiries on the interpretation, or proposals for change, and keep
UK interests informed;

monitor related international and European developments and


promulgate them in the UK.

A list of organizations represented on this subcommittee can be obtained on


request to its secretary.
Cross-references
The British Standards which implement international or European
publications referred to in this document may be found in the BSI Catalogue
under the section entitled International Standards Correspondence Index, or
by using the Search facility of the BSI Electronic Catalogue or of British
Standards Online.
This publication does not purport to include all the necessary provisions of a
contract. Users are responsible for its correct application.
Compliance with a British Standard does not of itself confer immunity
from legal obligations.

Summary of pages
This document comprises a front cover, an inside front cover, the EN title page,
pages 2 to 8, an inside back cover and a back cover.
The BSI copyright notice displayed in this document indicates when the
document was last issued.

This British Standard was


published under the authority
of the Standards Policy and
Strategy Committee
on 23 December 2005

BSI 23 December 2005

ISBN 0 580 47466 6

Amendments issued since publication


Amd. No.

Date

Comments

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EUROPEAN STANDARD

EN 12697-42

NORME EUROPENNE
EUROPISCHE NORM

November 2005

ICS 93.080.20

English Version

Bituminous mixtures - Test methods for hot mix asphalt - Part


42: Amount of coarse foreign matter in reclaimed asphalt
Mlanges bitumineux - Mthodes d'essai pour mlange
hydrocarbon chaud - Partie 42: Quantit de matriaux
trangers prsents dans les agrgats d'enrobs

Asphalt - Prfverfahren fr Heiasphalt - Teil 42:


Fremdstoffgehalt in Ausbauasphalt

This European Standard was approved by CEN on 30 September 2005.


CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European
Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national
standards may be obtained on application to the Central Secretariat or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation
under the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the official
versions.
CEN members are the national standards bodies of Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France,
Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Slovakia,
Slovenia, Spain, Sweden, Switzerland and United Kingdom.

EUROPEAN COMMITTEE FOR STANDARDIZATION


COMIT EUROPEN DE NORMALISATION
EUROPISCHES KOMITEE FR NORMUNG

Management Centre: rue de Stassart, 36

2005 CEN

All rights of exploitation in any form and by any means reserved


worldwide for CEN national Members.

B-1050 Brussels

Ref. No. EN 12697-42:2005: E

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EN 12697-42:2005 (E)

Content

Page

Foreword ..........................................................................................................................................................3
1

Scope ...................................................................................................................................................6

Normative references .........................................................................................................................6

Terms and definitions.........................................................................................................................6

Principle...............................................................................................................................................6

Apparatus ............................................................................................................................................7

Preparation of the sample ..................................................................................................................7

Procedure ............................................................................................................................................7

Expression of results..........................................................................................................................8

Test report ...........................................................................................................................................8

10

Precision data .....................................................................................................................................8

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EN 12697-42:2005 (E)

Foreword
This document (EN 12697-42:2005) has been prepared by Technical Committee CEN/TC 227 Road
materials, the secretariat of which is held by DIN.
This European Standard shall be given the status of a national standard, either by publication of an identical
text or by endorsement, at the latest by May 2006, and conflicting national standards shall be withdrawn at the
latest by January 2008.
WARNING The methods described in this draft European Standard require the use of solvents that
are hazardous to health and are subject to occupational exposure limits as described in relevant
legislation and regulations. Exposure levels are related to both handling procedures and ventilation
provision and it is emphasised that adequate training should be given to staff employed in the usage
of these substances.
This document is one of a series of standards as listed below.
EN 12697-1, Bituminous mixtures Test methods for hot mix asphalt Part 1: Soluble binder content.
EN 12697-2, Bituminous mixtures Test methods for hot mix asphalt Part 2: Determination of particle size
distribution.
EN 12697-3, Bituminous mixtures Test methods for hot mix asphalt Part 3: Bitumen recovery: Rotary
evaporator.
EN 12697-4, Bituminous mixtures Test methods for hot mix asphalt Part 4: Bitumen recovery:
Fractionating column.
EN 12697-5, Bituminous mixtures Test methods for hot mix asphalt Part 5: Determination of the
maximum density.
EN 12697-6, Bituminous mixtures Test methods for hot mix asphalt Part 6: Determination of bulk density
of bituminous specimens.
EN 12697-7, Bituminous mixtures Test methods for hot mix asphalt Part 7: Determination of bulk density
of bituminous specimens by gamma rays.
EN 12697-8, Bituminous mixtures Test methods for hot mix asphalt Part 8: Determination of void
characteristics of bituminous specimens.
EN 12697-9, Bituminous mixtures Test methods for hot mix asphalt Part 9: Determination of the
reference density.
EN 12697-10, Bituminous mixtures Test methods for hot mix asphalt Part 10: Compactability.
EN 12697-11, Bituminous mixtures Test methods for hot mix asphalt Part 11: Determination of the
affinity between aggregate and bitumen.
EN 12697-12, Bituminous mixtures Test methods for hot mix asphalt Part 12: Determination of the water
sensitivity of bituminous specimens.
EN 12697-13, Bituminous mixtures Test methods for hot mix asphalt Part 13: Temperature measurement.

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EN 12697-42:2005 (E)

EN 12697-14, Bituminous mixtures Test methods for hot mix asphalt Part 14: Water content.
EN 12697-15, Bituminous mixtures Test methods for hot mix asphalt Part 15: Determination of the
segregation sensitivity.
EN 12697-16, Bituminous mixtures Test methods for hot mix asphalt Part 16: Abrasion by studded tyres.
EN 12697-17, Bituminous mixtures Test methods for hot mix asphalt Part 17: Particle loss of porous
asphalt specimen.
EN 12697-18, Bituminous mixtures Test methods for hot mix asphalt Part 18: Binder drainage.
EN 12697-19, Bituminous mixtures Test methods for hot mix asphalt Part 19: Permeability of specimen.
EN 12697-20, Bituminous mixtures Test methods for hot mix asphalt Part 20: Indentation using cube or
Marshall specimens.
EN 12697-21, Bituminous mixtures Test methods for hot mix asphalt Part 21: Indentation using plate
specimens.
EN 12697-22, Bituminous mixtures Test methods for hot mix asphalt Part 22: Wheel tracking.
EN 12697-23, Bituminous mixtures Test methods for hot mix asphalt Part 23: Determination of the
indirect tensile strength of bituminous specimens.
EN 12697-24, Bituminous mixtures Test methods for hot mix asphalt Part 24: Resistance to fatigue.
EN 12697-25, Bituminous mixtures Test methods for hot mix asphalt Part 25: Cyclic compression test.
EN 12697-26, Bituminous mixtures Test methods for hot mix asphalt Part 26: Stiffness.
EN 12697-27, Bituminous mixtures Test methods for hot mix asphalt Part 27: Sampling.
EN 12697-28, Bituminous mixtures Test methods for hot mix asphalt Part 28: Preparation of samples for
determining binder content, water content and grading.
EN 12697-29, Bituminous mixtures Test methods for hot mix asphalt Part 29: Determination of the
dimensions of a bituminous specimen.
EN 12697-30, Bituminous mixtures Test methods for hot mix asphalt Part 30: Specimen preparation,
impact compactor.
EN 12697-31, Bituminous mixtures Test methods for hot mix asphalt Part 31: Specimen preparation,
gyratory compactor.
EN 12697-32, Bituminous mixtures Test methods for hot mix asphalt Part 32: Laboratory compaction of
biuminous mixtures by a vibratory compactor.
EN 12697-33, Bituminous mixtures Test methods for hot mix asphalt Part 33: Specimen prepared, by
roller compactor.
EN 12697-34, Bituminous mixtures Test methods for hot mix asphalt Part 34: Marshall test.
EN 12697-35, Bituminous mixtures Test methods for hot mix asphalt Part 35: Laboratory mixing.
EN 12697-36, Bituminous mixtures Test methods for hot mix asphalt Part 36: Determination of the
thickness of a bituminous pavement.

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EN 12697-42:2005 (E)

EN 12697-37, Bituminous mixtures Test methods for hot mix asphalt Part 37: Hot sand test for the
adhesivity of binder on precoated chippings for HRA.
EN 12697-38, Bituminous mixtures Test methods for hot mix asphalt Part 38: Common equipment and
calibration.
EN 12697-39, Bituminous mixtures Test methods for hot mix asphalt Part 39: Binder content by ignition.
EN 12697-40, Bituminous mixtures - Test methods for hot mix asphalt - Part 40: In-situ drainablility
EN 12697-41, Bituminous mixtures Test methods for hot mix asphalt Part 41: Resistance to de-icing
fluids.
EN 12697-42, Bituminous mixtures Test methods for hot mix asphalt Part 42: Amount of foreign matters
in reclaimed asphalt.
EN 12697-43, Bituminous mixtures Test methods for hot mix asphalt Part 43: Resistance to fuel.
According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following
countries are bound to implement this European Standard: Austria, Belgium, Cyprus, Czech Republic,
Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Slovakia, Slovenia, Spain, Sweden, Switzerland
and United Kingdom.

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EN 12697-42:2005 (E)

Scope

This document (EN 12697-42:2005) specifies a visual method of determining the amount and components of
coarse foreign matter in reclaimed asphalt. This method does not completely categorise the foreign matter
that can occur in asphalt.
NOTE 1
For the use of reclaimed asphalt in asphalt mixtures, it is important to know the components in the reclaimed
asphalt and to what extent coarse foreign matter is present that can influence the properties of the asphalt mix.
NOTE 2
The method is not intended to categorise all foreign materials but rather to ensure that the amount of coarse
foreign materials are minimised.

Normative references

The following referenced documents are indispensable for the application of this document. For dated
references, only the edition cited applies. For undated references, the latest edition of the referenced
document (including any amendments) applies.
EN 932-1:1996, Test for general properties of aggregates Part 1: Methods for sampling.
EN 933-2, Test for geometrical properties of aggregates Part 2: Determination of particle size
distribution Test sieves, nominal size of apertures.

Terms and definitions

For the purposes of this document, the terms and definitions given in EN 932-1:1996 and the following apply.
3.1
reclaimed asphalt
asphalt made reusable by milling of asphalt road layers, by crushing of lumps torn up from asphalt pavements
and asphalt from surplus production
3.2
coarse foreign matter
matter in reclaimed asphalt not derived from asphalt pavements or surplus production, and cold asphalt
produced with cut-back bitumen
3.3
primary source
quarry or pit from which aggregate has traditionally been used successfully in the manufacture of one or more
types of asphalt
3.4
secondary source
quarry, pit or other source from which aggregate has not traditionally been used successfully in the
manufacture of any type of asphalt

Principle

The test methodology for determining the amount and components of coarse foreign matter in reclaimed
asphalt consists of the visual inspection and determination of the composition of two sub-samples, taken from
a representative sample of reclaimed asphalt.

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EN 12697-42:2005 (E)

Apparatus

5.1

Sieve, with a nominal aperture size of 8 mm, conforming to EN 933-2.

5.2

Balance to weight to 1 g.

5.3

Sampling divider, conforming to either EN 932-1 or EN 12697-27.

5.4

Hydrochloric acid, 1 mol/l.

5.5

Hydrocarbon solvent (Dichloromethane/methylene chloride or trichloroethylene).

5.6

Water.

Preparation of the sample

6.1 The reclaimed asphalt on the feedstock shall be visually inspected for the presence of coarse foreign
materials.
When coarse foreign matter is present, take a representative sample of reclaimed asphalt from the feedstock.
The sample shall be at least 20 kg.
6.2 Sieve the sample using the sieve described in 5.1. Take the portion of the sample remaining in the
sieve and divide it into two sub-samples by means of the sampling divider.
NOTE
The composition of the fraction of the sample remaining in the sieve is taken to be representative of the
composition of the total amount of reclaimed asphalt from which the sample was taken.

Procedure

7.1 The two sub-samples shall be visually inspected for the presence of coarse foreign matter and the
composition of each sub-sample shall be established as specified in 7.2. Each sub-sample shall be visually
inspected and its composition determined and the two analyses shall be independent of each other.
NOTE 1
Cold asphalt produced with cut-back bitumen may be hard to distinguish from "asphalt". However in that case
the cold asphalt may be considered as asphalt: any cut-back in the reclaimed asphalt will affect binder. Distinction is
favourable as the presence of flux may influence the final binder properties to an unwanted level or may lead to safety
risks during the production of recycling asphalt.
NOTE 2
Because of the strong influence of the analyst on the test result executing the test twice by two independent
analyses is required.

7.2

Each sub-sample shall be sorted into:


a) material derived from asphalt;
b) coarse foreign matter derived from asphalt (cold asphalt produced with cut-back bitumen);
c) coarse foreign matter not derived from asphalt, divided into site materials and other materials.

NOTE 1
Site materials include, for example: cement concrete and cement concrete products; bricks; unbound
pavement materials including fine natural aggregate, from secondary sources; cement mortar. Other materials include, for
example: metals; synthetic materials; plastic; wood.
NOTE 2
If necessary, washing the material with water before inspection may be helpful in order to facilitate the
inspection.

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EN 12697-42:2005 (E)

NOTE 3
In case of doubt, the presence of concrete can be proved by use of hydrochloric acid, and asphalt by use of
dichloromethane.

7.3 The mass of asphalt, cold asphalt produced with cut-back bitumen and coarse foreign matter not
derived from asphalt (divided into side materials and other materials), shall each be determined to an
accuracy of 1 g.
7.4 Calculate the content of asphalt, cold asphalt produced with cut-back bitumen and coarse foreign
matter not derived from asphalt (divided into side materials and other materials) in the sub-sample, as a
percentage by mass, to an accuracy of 0,1 % by mass.
7.5 If the mass of coarse foreign matter obtained from the sub-samples by each independent analyse
differs from that obtained by the other independent analyse by more than 5 % by mass, the cause of this
difference shall be investigated.
NOTE
If no explanation for a difference in mass is found, a new representative sample should be taken and the test
should be performed once more.

Expression of results

Calculate the content of material derived from asphalt, coarse foreign matter derived from asphalt and coarse
foreign matter not derived from asphalt, expressed as the average of the results of both analyses, to an
accuracy of 0,1 % by mass.

Test report

The test report shall include the following information:


a)

identification of the feedstock;

b)

source of reclaimed asphalt (mix-groups from which the feedstock has been derived);

c)

tonnage of the feedstock;

d)

content of material derived from asphalt, coarse foreign matter derived from asphalt and coarse foreign
matter not derived from asphalt, expressed as the average of the results of both independent analyses, to
an accuracy of 0,1 % by mass;

e)

date on which and the time at which the test was carried out.

10 Precision data
Precision data are not available.

blank

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BS EN
12697-42:2005

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