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Article history:
Received 9 September 2015
Received in revised form 12 December 2015
Accepted 8 January 2016
Available online 16 March 2016
Keywords:
Mining waste
Process tailings
Valorization
Paste backfill
Uni-axial compressive strength
a b s t r a c t
Mine waste and process tailings storage is one of important challenge for which mining operations are
increasingly confronted. Treatment discharges of plants and main part of waste rock development are
generally stored on surface areas. The volume and chemical characteristics of these materials generate
serious problem for required storage spaces and mainly environmental degradation. Paste backfill
(PBF) is one of ingenious solutions to minimize the quantity of tailings to store. PBF is basically defined
as a combination of mine processing tailings, binder, and water mixing. The purpose of this paper is to
present backfilling components characterization and formula verification for a waste valorization solution through paste backfilling technology in Imiter operation. Obtained results and realized analysis
demonstrate PBF conformity and adequacy with assigned underground functions. However the studied
recipe can be more ameliorated to obtain an optimal mixture ensuring the required mechanical strength.
2016 Published by Elsevier B.V. on behalf of China University of Mining & Technology.
1. Introduction
More than 20 years ago, concentrator treatment discharges of
mining plants were wholly stored on tailings parks on surface
areas. The quantity and chemical characteristics of these tailings,
often rich of sulfurs, generate serious problem for storage requiring
spaces and mainly environmental degradation due to acid mine
drainage.
Moroccan mining operations use different kinds of backfill
depending on the extraction method. The most used backfills are
mechanical backfill (only waste material) and hydraulic backfill
(cemented backfill).
The environmental legislation, increasingly requiring, leads
mining societies to minimize as possible, the volume of tailings
stored on the surface. Morocco is one of countries which are going
to make the environment preservation as the first preoccupation
during and at the end of mining activities.
Cemented paste backfill has become increasingly widespread,
mainly because it reduces by 50%60% the quantity of sulphidic
tailings deposited on surface, increases ore recovery, and minimizes stoping sequences [1]. Its a mixture of total mill tailings
generated during mineral processing, Portland cement or blended
cement with supplementary cementitious material (lime,
pulverized fly ash, and ground granulated blast furnace slag), and
Corresponding author. Tel.: +212 662111920.
E-mail address: abdelhadikhaldoun@gmail.com (A. Khaldoun).
http://dx.doi.org/10.1016/j.ijmst.2016.02.021
2095-2686/ 2016 Published by Elsevier B.V. on behalf of China University of Mining & Technology.
A. Khaldoun et al. / International Journal of Mining Science and Technology 26 (2016) 511516
Binding agents
(SiO2+Al2O3)/
(CaO+MgO)
CaSO4 %
Tailings
Sulfides %
Grain size
distribution density,
specific gravity
Mixing water
SO42- content
soluble lime
Additives
2000
1050
460
2.8
Solids %, Cw
(78%-85%)
Binder %
(3%-7%)(by weight)
UCS28-jourw
(kPa)
512
4.8
6.8 7.0
% ciment
Water content
(expected slump)
8.7 9.3 30
W/C
55
70 3.38
% fine (20 m )
3.45 3.50
t (g/cm3)
Paste
backfill
Several works focused on the problematic of backfill transportation since their introduction PBF product must be delivered from
surface to underground via boreholes and pipes at the highest
practical density (Fig. 3) [1013]. Practically, it is not easy to have
real proprieties of PBF rheology because of experimental dispositive complexity.
It makes difficult or even impossible determination or prediction of paste viscosity which depends on several factors [3].
Generally, the slump test and flow-loop test are used to evaluate the paste consistence and pressures drop along the transporting network.
Backfill plant
Mixer
Gravity/pump
system
Pump/gravity
system
Pump
Gravity
system
Pump ?
Paste
backfill
Open stope
A. Khaldoun et al. / International Journal of Mining Science and Technology 26 (2016) 511516
The prepared PBF should be pumped through pipelines reticulation network without causing any plugging. The pumpability of
PBF is measured by the slump height. The fresh PBF behaves as a
non-Newtonian fluid. That is, applied pressure is required to initiate flow [2].
2.7. In-situ behavior
Once the PBF is deposed in underground voids, it undergoes
various transformations and interactions.
The PBF interactions with rock mass depend mainly on void
dimension but also on pressure at the bottom and over the stope
barricade. Barricade should be designed with appropriate strength
and permeability or drainage by taking into account the backfill
total pressure, pore water pressure, and loads from blast, liquefaction and piping [15].
Like the case of conventional concrete, hydration reactions is
the main phenomena that give PBF solidification. Researches and
tests made by demonstrate that the use of sulphated water contributed to the refinement of the porosity and the increase of
UCS [16]. This has been explained by a combination of the behavior
of the binder and a potential precipitation of sulphated minerals in
the pores which decrease bigger pore proportion.
In addition to hydration reactions which give the mechanical
strength of hardened backfill, other processes occur during the curing time of PBF, mainly drainage of excess water. Settlement and
consolidation, and settlement of saturated fresh mine backfill
depend on the materials coefficient of consolidation cv, which
combines permeability coefficient (or saturated hydraulic conductivity: ksat) and stiffness, and on the filling rate [17].
The strength of pastefill in the filled stope is related to the water
flow which is a function of the paste properties [18]. Transformations and interactions of PBF have to be monitored in the short,
middle and long term. This monitoring will show the impact of
selected recipe and material characteristics on the mechanical
strength of PBF. Adjustment can then be made to find the most
appropriate recipe.
The stress components in backfilled openings are affected not
only by the weight of the fill, but also by interaction between the
fill and the opening walls. Some of the stress in the backfill is thus
transferred to the adjacent walls through shearing forces between
the fill and walls. This leads to a decrease of stress in the fill compared to the overburden stress. This phenomenon is known as the
arching effect [19]. The interaction between backfill and adjacent
rock mass can be quite complex, especially when one of the supporting walls is removed [4].
3. Imiter Mine operation
Imiter Mine is an operation situated in Ouarzazate region,
southern of Morocco, 30 km from Tinghir locality and 150 km from
Ouarzazate city. The exploitation concerns a rich silver ore body.
3.1. Geological overview
Imiter Mine is located in NE edge of the Ouarzazate Basin (Eastern Saghro, Anti-Atlas). The deposit is hosted in the volcanosedimentary series of the Precambrian II and secondarily in
volcano-clastic formations of the Precambrian III. Fig. 4 presents
regional geological and metallogenic context of Imiter deposit.
513
514
A. Khaldoun et al. / International Journal of Mining Science and Technology 26 (2016) 511516
Sidi flah
Ag
West African
Cration
Tafrent
Au
Zgounder
Ag
Atlas
Central
Igherm
Anti
Kerdous
A
tla
nt
ic
O
ce
an
SAF
Agadir
E
Ougnat
ro
Sagh
Sirwa
N
W
Tamlelt
Au
South
Ouarzazate
High
Abidjan
Fault
Atlas
Atlas
15
500 km
Bou Maadine
Cu-Pb-Zn-Au-Ag
Imiter
Ag-Hg
Ifni
as Fault
Tagmout
Cu-Ag
Bou azzer
Co-Ni-As-Ag-Au
Akka
Tiouit
Au-Cu
Anti-Atl
Zenaga
Au
100 km
Ordovician
Late Ediacaran to
Cambrian
Bleida
Cu-Au
Ediacaran
Cryogenian and
Paleoproterozoic
Iourirn
Au
Fig. 4. Location of the main ore deposits in the Anti-Atlas belt [20].
Plant
O
TSF-7
TSF-5
TSF-9
TSF-6
TSF-4
TSF-8
TSF-3
TSF-2
200 m
Fig. 5. Satellite image showing main installation of Imiter operations area, TSF = tailing storage facility (Adapted from Google Maps).
Table 1
Laboratory characterization of Imiter paste backfill gravel (%).
Laboratory testing
Flatness coefficient
Superficial cleanliness
Sand equivalent
Testing result
Standard NM10.1.27
23
625
0.3
63
15
630
56
P60
Table 2
Tailing fine particle distribution.
Particle size (PS) (l)
Proportion (%)
PS < 2
2 < PS < 20
20 < PS < 80
18
38
20
H
UCSdesign SF cb H 1
L
where FS is the safety factor, cb the PBF bulk unit weight, kN/m3; H
the PBF height, m; and L the stope width, m.
The required UCS was calculated for different safety factors
based on Imiter ore geometry in case of each mining method. A
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A. Khaldoun et al. / International Journal of Mining Science and Technology 26 (2016) 511516
100
90
80
Passing (%)
70
60
50
40
30
20
10
0
31.50
16.00
8.00
4.00
2.00
1.00
0.50
0.25
Sieving analysis
0.13
63.00
Sieve bores
31.50
16.00
8.00
3.15
1.60
1.00
0.40
Sedimentation analysis
Table 3
Chemical composition of tailings.
Chemical element
AL2O3
CaO
Fe2O3
K2O
MgO
MnO
Na2O
P2O5
SiO2
TiO2
LOI
Total
13.86
2.81
6.33
3.59
3.96
0.18
1.61
0.19
57.37
0.72
8.47
99.12
Table 4
Semi-quantitative mineralogical composition of tailings.
Mineral
Dolomite
Quartz
Muscovite
Albite
35
24
16
14
Table 6
Mechanical testing-cement CPJ45.
Item
Testing result
Standards NM 10-1-004
After 2 days
After 7 days
After 28 days
18.7
27.3
P20
39.5
P32.5
Table 7
Chemical analysis of mixing water.
Chemical
parameter
Ph
Material in
suspension
(mg/L)
Testing
6.60 0.5
result
Standards P4 62000
NM 101-008
Dissolved
salt (mg/
L)
Sulfates
(mg/L)
Chlorides
(mg/L)
Organic
material
(mg/L)
617
153.60
194.70
65000
62000
6500
6200
Table 8
Imiter PBF mixture.
Component
Quantity
Gravel (kg)
Sand (kg)
Tailings (kg)
Water (L)
Cement (kg)
Total weight (kg)
600
1000
340
500
40
2480
The mechanical performance of the formulated PBF was evaluated by the uniaxial compressive strength test and analytical prediction model. Table 11 presents values of analytical prediction of
the long term uniaxial compressive strength made in chapter 4
Table 5
Physical testingcement CPJ45.
Physical parameter
Setting time
Expansion (mm)
Testing result
Standards NM 10-1-004
2 h 00 min
P1 h 30 min
1.7
610
2470
P2200
516
A. Khaldoun et al. / International Journal of Mining Science and Technology 26 (2016) 511516
Table 9
UCS design calculation according to safety factor.
Item
Safety factor
Cut-and fill
Sublevel stoping
1.0
36.0
56.8
1.1
39.6
62.5
1.2
43.2
68.2
1.3
46.8
73.8
1.4
50.4
79.5
Table 10
UCS results for Imiter PBF.
Age (day)
7
14
21
28
17.9
17.2
17.0
16.9
0.40
0.72
1.08
1.33
Table 11
Predicted UCS design instead experimental values.
PBF function
54
85
1330
1330
1.5
54.0
85.2
1.6
57.6
90.9
1.7
61.2
96.6
1.8
64.8
102.3
1.9
68.4
108.0
2.0
72.0
113.6