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Whereas the Parliament of India has set out to provide a practical regime of right to
information for citizens to secure access to information under the control of public authorities,
in order to promote transparency and accountability in the working of every public authority,
and whereas the attached publication of the Bureau of Indian Standards is of particular interest
to the public, particularly disadvantaged communities and those engaged in the pursuit of
education and knowledge, the attached public safety standard is made available to promote the
timely dissemination of this information in an accurate manner to the public.
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Indian Standard
SPECIFICATiON FOR
MUSTARD OIL
(SecondRevision)
Sixth Reprint AUGUST 2007
(Incorporating Amendment No. 1 and Including Amendment Nos. 2, 3, 4, S & 6)
UDC 665.334.83
Copyright 1980
November 1975
IS I 546 -1975
Indian Standard
SPECIFICATION FOR MUSTARD OIL
(Second Revision)
Oils and Oilseeds Sectional Committee, CAFDC 5
Ch4i,m4n
DB J. S.
SBRI
SUBI
SHRI
RtprlsI",inl
Swastik Household &. Industrial Products
Bombay
BADAMI
M,m6"1
R. M. DESAI
Dr J. s. Badami)
S. K . B0811
D. S. CHADHA.
Altemat to
B. 'l.
SHRI
KANTAK:
THAKUR
S. KABTRA
M. S.
DB A. R.
R. D.
SBBI
DB. S. N.
KAWATBA
MABAPATRA
Ltd,
C) Copyright
1980
IS 15461975
( COlltiftUld from /HJ"
1)
M,mIJn,
R,pr,smti"1
Regional
Research
Laboratory
(CSIR)
Hyderabad
SUBI M. SATYANABAYANA
The Tata Oil Mills Co Ltd, Bombay
SSRl T. S. RAMASWAMY ( All'mDt,)
DB A. K. SEN
Ministry of Defence
SURI P. N. AGABWAL ( Alumat )
S BRI S. C. SINGHAL
The Vanaspati Manufacturers' Association of India,
RBPBBUNTATIVB
DB M. R.
.
SunDARAM
Bombay
Directorate of Sugar & Vanaspati (Atfinistry
Agriculture ), New Delhi
or
DB I. A. SIDDJQt ( Alumat )
Oil Technological Research Institute, Anantapur
S. D. THIRU)tAI 1\ RAO
SHIn D. ATCBYUTABAMAYYA
SBRI
( Alumat )
DB G. M. SAXENA,
Director (Chem)
S, crd ar.1
SURI
R. K.
SINGH
DB S. M.
PATEL
M""IJ.,
K. BALAltRISRN AN ( All""",,, to
Dr S. M. Patel)
SHill G. J. AOARWAL
Bombay Oilseeds and Oils Exchange Ltd, Bombay
SHRI C. V. MABIWALA. (A/ternal, )
DB A. C. CUHATBAPATI
The Vanaspati Manufacturers' Association of India,
Bombay
Indian Soap and Toiletries Makera' Association.
SHltI S. C. GUOSE
Calcutta
SRBI P. V. GUJABATHI
Khadi &. Village Industries Commission. Bombay
SHJn
181546-1975
( Ctmtinrud from pag, 2 )
M",,"'rs
R,pr,s,nting
SaBI M.
SATYANARAYANA
The Tata Oil Mills Co Ltd, Bombay
SHBI T. S. RAMASWAMY ( All,rnal,)
DB A. K. SEN
Ministry of Defence
SUBI P. N. AOABWAL (Alt,mat,)
SRBI HARI8H SBTBI
Directorate of Oilseeds Development
DB M. R.
SUDDARAM
DB I. A. SIDDIQI ( Altmaat, )
S. D. TUIBUMALA RAO
SIIBI
( Ministry of
Agriculture ), Hyderabad
Directorate of Sugar & Vanaspati (Ministry or
Agriculture ), New Delhi
( Page 8 clause 6.2 ) - Add the following new clause after 6.1:
t
'6.2.1 The containers may also be marked with the Standard Mark.
NOTE - The use of the Standard Mark is governed by the provisions of tho
Bureau of Indian Standards Act, 1986 and the Rules and Regulations made thereunder. The Standard Mark on products covered by an Indian Standard conveys
the assurance that the, have been produced to comply with the requirements
that standard under a well-defined system of inspection, testing and quality
control which is devised and supervised by BIS and operated by the producer.
Standard marked products are also continuously checked by DIS (or coonformlty to that standard as a further safeguard. Details of conditions under which
a licence for the use of the Standard Mark may be granted to manufacturers
or producers, may be obtained from the Bureau of Indian Standards!
or
:Methods of sampling and test for oils and fats: Part 2 Purity tests (third
,evl,IDn ).
(CAFDC 5)
Al\'IEND~IENT
TO
IS 546: 1975 SPECIFICATION FOR MUSTARD OIL
( Second Revision)
[ Page 7, Table 1, SI iVO. (v), Iodine value (lVijs) J- Substitute '98 to 112' for
'98 to 110'.
(FAD44 )
TO
IS 546: 1975 SPECIFICATION FOR MUSTARD OIL
( Second Revision)
( Page 4, Foreword, clause 0.6 ) - Add tbe following clause 0.7 after 0.6
and renumber the subsequent clause:
4.6.2.4 The product shall not contain any of the toxic metals in excess of the
quantities prescribed in Table 2.
TABLE 2 LIMITS FOR TOXIC METALS
SL No.
i)
CHARACI'EIUSnc
REQUIREMENT
S.O
MElHOD OF TEsT,
REF 10
IS of IS 1699: 1995
ii)
Arsenic, m~,Max
O.S
do
iii)
Cadmium.meJkg, Max
1.0
do
iv)
Mercury (total)
m&fkg.Max
0.25
do
( Page 6, clause S.1 ) - Add the following clause 5.1.1 after 5.1:
'5.1.1 For ECO Mark the product shall be packed in such packages whicb are
Blade from recyclable ( that is which can be re-processed to manufacture any
useful product) orbiodegndable materials.'
(Page 6, clause 6.1 ) - Add the following clause 6.1.1 after 6.1:
"6.1.1 For ECO Mark the contalners shall be marked with the following
information:
DETERMINATION OF AFlATOXIN
A-1 REAGENTS
A-Z PROCEDURE
A-l.1 Dissolve30 g sample in 100 ml hexane.
A-Z.2 Extract with 3 x 50 ml 70 percent acetone.
A-Z.3 To the extract add 60 ml distilled water and 20 mllead acetate.
A-Z.4 Boil to reduce volume to 150 mi. Cool to about 20C.
A-Z.5 Filter and wash with 20 percent acetone.
A-Z.6 Extract filtrate and washings with 3 )( 50 ml chloroform,
A-Z.7 Pass chloroformlayer tbrough anhydrous sodium sulphate.
A-Z.8 Concentrateto 50 ml and spot on TLC plate.
A-3 CALCUlATION
.
Aflatoxin, mg/kg
= VxsxlOOO
vx m
where
(FAD44)
(FAD44 )
(FAD 13 )
IS I 54& -1975
Indian Standard
SPECIFICATION FOR MUSTARD OIL
(Second Revision)
o.
FOREWORD
No,
Botanical Name of
Plant Sptcies
(1)
(2)
Sl
iv)
var toria
Brassica juncea Linn.
Czern. & Coss.
Common Name
in English
(3)
Common Name
in Hindi
(4)
Yellow SARSON
PILI SARSON
Brown SARSON
liALI Lc;ARSON
TORIA
TORIA OR LAHI
(mfun lff ~)
RAI (uf)
Mustard
S
(~~T)
(;mft ~~T)
'
IS 1546 .1'75
0.3.1 With regard to the relationship that these oilseed crops bear to
the corresponding crops in Europe, RAJ corresponds to mustard) SARSON
to colza and TORIA to rape. Brassica napus Linn. is not grown in India
at all.
0.4 Large quantities of the oil are used for edible purposes; in fact, the
characteristic pungent odour of the oil is at times taken as the criterion
for judging its quality. Inferior quality oil is generally used as an
illuminant and as a lubricant for axles of carts. The oil is also used for
pharmaceutical purposes.
0.5 In this revision the oil obtained by the process of solvent-extraction
has also been included. The earlier version of the standard covered the
oil obtained by the process of expression only. Care has also been taken
to ensure that the material is free from argemone oil which is reported to
cause epidemic dropsy. After the issue and implementation of the
Solvent Extracted Oil, Deoiled Meal and Edible Flour ( Control) Order
of 1967, the refined grade of solvent-extracted oil has been widely
accepted for edible purposes and the solvent-extracted rape and mustard
seed oil is one such example. Amendment No. I ofJanuary 1969 issued
to this standard has also been incorporated in this revision.
1. SCOPE
1.1 This standard prescribes requirements and methods of sampling and
test for mustard oil used for edible and industrial purposes.
2. TERMINOLOGY
2.1 For the purpose of this standard, the definitions given under 2 of
IS: 548 ( Part I )-1964t and the following shall apply.
*Rules for rounding ofT numerical values ( rtvised).
tMethods of samrling and te~t for oils and fata: Part I
'lhysical and chemica teats ( r,vis,d ).
Method. of sampling,
IS I 546 1975
2.1.1 Semi-refin,d Mwtard Oil- Mustard oil obtained by the process
'Of solvent-extraction which has been neutralized with alkali, without or
with bleaching with bleaching earth or activated carbon or both, no other
chemical agent being used.
2.1.2 R,ji",d Mustard Oil - Mustard oil obtained by the process of
expression or solvent-extraction which has been refined by neutralization
with alkali, bleached with bleaching earth or activated carbon or both,
and deodorized with steam, no other chemical agent being used.
3.1.1 The refined grade mustard oil of the expressed and solventextracted types and the raw grades of the expressed type are suitable for
direct edible consumption (see Note).
NOTB - Raw Grade 1 and Grade 2 of the expressed oil correspond to Grade 1
( Edible) and Grade 2 ( Edible) respectively of ' AGMARK ' specification. of the
Directorate of Marketing and Inspection, Ministry of Agriculture, Government of
India.
4. REQ,UIREMENTS
4.1 De.criptloD - The material shall be obtained from good quality
mustard cake or from clean and sound seeds of Brassica compestris Linn.,
Brassica Ju",ea Linn. Czern. & Coss, or a mixture of these seeds, all
belonging to the family Cruciferae, by a process of solvent-extraction or
from the mustard seeds by the process of expression.
IS I 546 1975
4.1.1 Solvent-extracted oil shall be obtained from the oleaginous.
material using solvent hexane conforming to IS: 34701966*.
4.2 The material shall be clear and free from adulterants, sediment,
suspended and other foreign matter, separated water and added colouring
and flavouring substances. When tested as prescribed in 20 of IS : 548( Part I )-] 964t the rna terial shall have peroxide value not more than
10 milliequivalents peroxide oxygen per kg of it and shall have
acceptable taste and odour.
4.2.1 The clarity of the material shall be judged by the absence of
turbidity after keeping the filtered sample at 300 for 24 hours.
4.3 Admixture with Other Oils - The material shall be free from
admixture with other oils, when tested according to the methods.
prescribed in IS : 548 (Part II )-1974:.
4.4 Freedom from Argemone Oil and Hydrocyanic Acid - The
material shall be free from argemone (argemone mexicana Linn. ) oil and
hydrocyanic acid when tested as prescribed in 10 and 11 of IS: 548
( Part II )-1974:.
4.5 The material shall also comply with the requirements given in
Table 1.
s, PACKING
5.1 The material shall be supplied packed in suitable well..closed
containers as agreed to between the purchaser and the supplier.
6. MARKING
6.1 The containers shall be marked with the following particulars:
a) Name, type and grade of the material;
b) Mass of the material in the container;
c) Manufacturer's name and his recognized trade-mark, if any;
or
.......,
(3)
Flash point,
Pensky-Martens
( closed ), C, A/in
30
15
50
50
90
1-00
(8)
100
1"25
(9)
13
5&
025 to
0-60
060
0'10 to
250
0'60---.
125
100
90
27"5----------~
~--O-IO to
1964
1970:
J3 of IS : 548
( Part II )-1974t
P:2J of IS: 1448-
17
I
I
J
r (Part 1)-
IIS: 548
61
,
,I
(10)
CLNo_
METHOD 0.,
TEST,
RUTO
------}"4646 to 1-4666--------+ 10
169 to 177--------~ 15
--+ 1498 to 110
7
2-0
4-0
0-5
1-5
12
60
8
1-5
20
1-2
20
1'2
1"2
0-25
(7)
0-1
(6)
0-25
(5)
0-25
(4)
Re- Semi-
Raw
Raw
fined refined Grade 1 Grade 2
.A.-
Solvent-Extracted
-.
renswn ).
Methods of sampling and test for oils and fats: Part I Methods of sampling, physical and chemical tests (r'l'ised)_
fMethods of sampling and test for oils and fats: Part II Purity tests ( second recision )
.t.Methods of test for petroleum and its products, P : 21 FJash point (closed) by Pensky Martens apparatus (first
x)
-A.-____._
Expressed
ReRaw
Raw
fined Grade J Grade 2
Max
(2)
(1)
i)
CBAlLAO'l'EBISTIC
SL
No_
DaM6-1975
In addition in the case of semi-refined grade and raw Grades t and 2
of the solvent-extracted type, the following information shall be suitably
marked, either printed on the label affixed to the container or litho-graphed or stencilled thereon with indelible ink in a type size not lesa
than 50 mm:
6.~
b) Raw Grade 2
C FOR
INDUSTRIAL NONEDIBLE USES ONLY J.
7. SAMPLING
7.1 Representative samples of the material shall be drawn as prescribed
under 3 of IS : 548 ( Part I )-1964*.
8. TESTS
8.1 Tests shall be carried out as prescribed in IS: 548 ( Part 1)-1964*"
IS: 548 (Part II )-1974t and IS: 1448 [P: 21 ]-1970~ reference to which
is given in 4.2 to 4.~ and col 10 of Table 1.
8.2 Q,uaUty of Reagent. - Unless specified otherwise, pure chemicals
and distilled water (se, IS : l070-1960) shall be used in tests.
NOT. - C Pure chemicals shal] meaD chemicals that do not contain impuritiea.
which affect the results of anal ylfs.
------_._--
M~thod. of aampling and test for oib and fau: Part I Methods of sampling.,
physical and chemicals teats ( "vis,d ).
tMethods of sampling and telt for oil! and fats: Part II Purity telt. (second reoisio ).
~Methodl of telt for petroleum and ita products, P : 21 Flash point ( clcsed ) by
Pensky Marten. apparatus (firs' "vision ).
ISpecification for water, distilled quality ( "vistd >:
Reglon"Offlcils:
Central
Manak Shavan, 9 Bahadur ShahZafarMarg, NEWDELHI 11 0002
Eastern 1/14CITScheme VIIM V I P Road, Kankurgachl KOLKATA 700054
Northern SCQ335-336, Sector34-A, CHANDIGARH 160022
Southern CIT Campus, IV CrossRoad, CHENNAI600113
tWestern Manakalaya, E9,MIDC, Behind MarolTelephone Exchange,
Andhen (East), MUMBAI400093
Branch OfflcBs:
Pushpak', Nurmohamed Sharkh Marg, Khanpur, AHMEDABAD 380001
Peenya IndustrialArea, 1 Stage, Bangalore-Tumkur Road, BANGALORE
Commercial-cum-Oflce Complex, Opp Dushera Mardan, AreraColony,
Blttan Market, BHOPAL462016
62-63 Ganga Nagar, UnitVI, BHUBANESHWAR 751001
5th Floor, Koval Towers, 44BalaSunda, amRoad, COIMBATORE 641018
SCQ21,Sedor 12,Fandabad 121007
Savltn Complex, 116G. T Road, GHAZIABAD 201001
53/5WardNo 29,R G. Barua Road, 5th By-lane, Apurba SinhaPath,
GUWAHATI 781003
5-8-56C, L N Gupta Marg, Nampally Station Road, HYDERABAD 500001
Pnthavi RajRoad, OPPosite Sharat Overseas Bank, C Scheme, JAIPUR 302001
11/418 B, Sarvodaya Nagar, KANPUR 208005
SethiShawan, 2nd Floor, Betund leela Cinema, NavalKishore Road,
LUCKNOW 226001
H No 15,Sector-3, PARWANOO, Dlstt Solan (H P) 173220
Plot NoA-2o-21, InstltutlonalArea, Sector62, Goutam BudhNagar, NOIDA201307
Pathputra Industnal Estate, PATNA800013
PlotNos 657-660, Market Yard, Gultkdl, PUNE411037
"SahaJanand House" 3"'Floor, Bhaktlnagar Circle, 80FeetRoad,
RAJKOT 360002
T C No 2/275 (1 &2),NearFoodCorporation of India, Kesavadasapuram-Ulloor Road,
Kesavadasapuram, THIRUVANANTHAPURAM 695004
111Floor, Udyog Bhavan, VUDA, Sinpuram Junction, VISHAKHAPATNAM-Q3
*Sales OfficeIS at 5Chownnghee Approach, PO Pnncep Street, KOLKATA 700072
tSales Office(WRO) PlotNo E-9,MIDC, Rd No 8, Behind Telephone Exchange,
Andhen (East), Mumba,-400 0093
Pnnted by the Manager, Government of IndiaPress- Farldabad, 2007
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