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CDB 3062 Chemical Engineering Lab

Sept 2016

CDB 3062
Chemical Engineering Lab 3
September 2016
Course Outline
1.

General Information & Course Administration

Coordinator
1.

Dr. Nasser Mohamed Ramli

nasser_mramli@petronas.com.my

05-3687634

Lab Instructors
1.

Alireza

alireza_rafiei63@yahoo.com

Control valve characteristics

2.

Asif Jamil

asif.jamil8@gmail.com

Flowmeter measurement

3.

Muhammad Babar

engr.babar2009@gmail.com

Temperature control

4.

Tazien

trtazien8@hotmail.com

Level transmitter calibration

5.

Muhammad Yasir
Shamim

myasir_1986@hotmail.co
m

Ratio control

6.

Hosein Ghaedi

ghaedi.hosein63@gmail.com

Pressure measurement

7.

Muhammad Mubashir

engr.mubashir37@gmail.com

Level Flow control

8.
9.

Khurrum Shehzad
Quraishi
Tran Thi To Nga

10. Farukh Iqbal


11.

Muhammad Mubashir

qureshiksq@gmail.com

pH, DO and conductivity measurement


Frequency response of couple tank

tonga.tnt@gmail.com
mfarukhiqbal@gmail.com
engr.mubashir37@gmail.com

Digital PID controller


Heat exchanger

Laboratory Technologists

1.

Suleiman Hakimi Zainal


Abidin

suleiman_hakimi@petronas.com.my

05-3687541

03-01-09

2.

Khairul Afizan Saidin

khairulafizan@petronas.com.my

05-3687540

03-00-08

CDB 3062 Chemical Engineering Lab


Sept 2016

2.

Laboratory Objectives

The objective of this laboratory is to extend the knowledge of chemical process dynamics, instrumentation
and control into practical work. The laboratory content will offer you the application of the fundamental
concepts and theory of the subjects as applied to the chemical engineering unit operations and everyday life.
COURSE SYNOPSIS:
This practical course requires several groups of 5 students perform experiments related to process
instrumentation, dynamics and control.
COURSE OUTCOME:
1.
2.

Apply appropriate sensors, instrumentation and/or computing tools to measure physical quantities.
Device suitable procedures and implement them in order to characterize dynamic and control
systems.
3. Analyze and interpret experimental data for writing and presenting technical reports.

MAPPING OF THE COURSE/MODULE TO THE PROGRAMME LEARNING OUTCOMES


Programme Outcomes (POs)

Course Learning Outcome

PO4

CLO1

Apply appropriate sensors, instrumentation


and/or computing tools to measure
physical quantities.

CLO2

Device suitable procedures and implement


them in order to characterize dynamic and
control systems.

CLO3

Analyze and interpret experimental data


for writing and presenting technical
reports.

PO5

PO9

PO5

Investigate complex chemical engineering problems using research-based knowledge and


research methods including design of experiments, analysis and interpretation of data, and
synthesis of information to provide valid conclusions
Select and apply modern engineering and IT tools to evaluate complex chemical engineering
activities

PO9

Communicate clearly on complex chemical engineering activities with the engineering


community and society

PO4

3.

Laboratory Schedule and Assignments

a)
Group
7 11

Day
Tuesday

16

Tuesday

18 22

Thursday

12 17

Thursday

Time
Morning
9:00 13:00
Afternoon
2:00 6:00
Afternoon
2:00 6:00
Morning
9:00 13:00
2

Venue
03-00-03 (process control lab)
03-01-07 (instrumentation lab)
03-00-03 (process control lab)
03-01-07 (instrumentation lab)

CDB 3062 Chemical Engineering Lab


Sept 2016

a)

You will be divided into groups of 5 students.

b)

You will carry out experiment sessions and group projects in the semester as per the attached schedule.

c)

In case of lab falls on the public holiday, lab will be replaced at other suitable time subjected to
availability (Friday slots are reserved for such events).

d)

In case of equipment breakdown, you will run another experiment in the following week. However,
cases below will apply:

If equipment breakdown is more than half of the experiment requirement, the student must
proceed with the available results.

If equipment breakdown less than half of the experiment requirement, the experiment must be
replaced with other available experiment/equipment.

EXPERIMENTS AND SCHEDULE:


WEEK
W1

DATE
12 16 Sept
2016

MODULES

GROUP

Introduction
Brief Lab Content
Group Organizations
Open-ended Lab Project

VENUE
03-00-03

ALL

EXPERIMENT

W2

W3

W4

W5

W6

W7

W8

Control valve characteristics

7,18

4,15

1,12

9,20

6,17

3,14

11,22

Flowmeter measurement

8,19

5,16

2,13

10,21

7,18

4,15

1,12

Temperature control

9,20

6,17

3,14

11,22

8,19

5,16

2,13

Level transmitter calibration

10,21

7,18

4,15

1,12

9,20

6,17

3,14

Ratio control

11,22

8,19

5,16

2,13

10,21

7,18

4,15

Pressure measurement

1,12

9,20

6,17

3,14

11,22

8,19

5,16

Level flow control


pH, DO and Conductivity
measurement
Frequency response of couple
tank

2,13

10,21

7,18

4,15

1,12

9,20

6,17

3,14

11,22

8,19

5,16

2,13

10,21

7,18

4,15

1,12

9,20

6,17

3,14

11,22

8,19

Digital PID controller

5,16

2,13

10,21

7,18

4,15

1,12

9,20

Heat exchanger

6,17

3,14

11,22

8,19

5,16

2,13

10,21

WEEK
W9
W10
W 11

DATE
8 November 2016
18 November 2016
22 and 24 November
2016

OBJECTIVE TEST
PROJECT
ORAL PRESENTATION (Project)

END OF SEMESTER
This schedule is subjected to changes. Students will be informed from time to time.
3

GROUP
ALL
ALL
ALL

VENUE
Test room block,N
03-00-03

CDB 3062 Chemical Engineering Lab


Sept 2016

4.

Report Submission

a)

There will be TWO (2) types of report as follows:

Types

Length

Mark

Due Date

Submit To

Experiments
17

Short Report
(max: 10 pages)

70
(10 each)

One week after


completion of an
experiment

Lab
Instructor

Project

Long Report
(max: 20 pages)

20

Week 10

Main
Coordinator

b)
c)

Remark

For each of the report,


please submit the
softcopy to the Main
Coordinator

Contents of the report: Please refer to elearning.


Submit report on time. Late submission will result in mark deduction:

1 day late 5 marks deducted.

Afterwards zero mark.

5.

Laboratory Assessment
Assessment Task

Mark

Assessment Type

40

Group

15 + 5

Group + Individual

Pre-experiment Viva Voce

10

Individual

Lab Test

30

Individual

TOTAL

100

Lab Report
Project (Report + Oral Presentation)

GRADING SCALE:
Grade
A
AB+
B
C+
C
D+
D
F

Meaning
High Distinction
Distinction
High Credit
Credit
High Pass
Pass
Redeemable
Redeemable
Fail

Grade Points
4.00
3.75
3.50
3.00
2.50
2.00
1.50
1.00
0.00

Range
85.0 100
80.0 84.9
75.0 79.9
65.0 74.9
55.0 64.9
50.0 54.9
45.0 49.9
40.0 44.9
0.0 39.9

LAB MANUAL:
1. Lab manual and instructions are available at http://www.elearning.utp.edu.my.
2. Open-ended lab instruction is available at http://www.elearning.utp.edu.my.

CDB 3062 Chemical Engineering Lab


Sept 2016

6.

Attendance

a)

Attendance is compulsory, i.e., you must attend all lab sessions.

b)

In case of absentees due to sickness, a Medical Certificate must be submitted to the Lab Coordinator.

c)

In the case of other commitment (student activities, family matters, etc) an authorization letter from the
relevant personnel is required.

d)

In case of emergency or any unavoidable circumstances when you cannot attend the lab session, you
are required to inform the Lab Coordinator prior to the event. This needs to be supported by a letter.

e)

Your lab session would not be replaced due to absenteeism. Therefore, you will not be graded for the
short report. (Except that a supporting document is given to the Lab Coordinator, the mark will be
exempted)

7.

Attire

a)

Properly attired. Wearing your lab coat is COMPULSORY. Other personal protective equipment
(PPE, such as goggles, safety helmet, ear plugs, ear muff, etc) will be provided.

b)

These clothing are not allowed in the laboratory: national costumes (baju kurung, cheongsam saree,
etc), jubah, skirts (short or long), sarongs, shorts, sandal, slippers and uncovered shoes) while
conducting experimental work. You are NOT ALLOWED to proceed with your laboratory work if
you fail to do that.

c)

For those who are wearing tudung or hijab, and with long hair, you are required to keep them neat.

d)

Besides the lab instructor, the lab technologists have the authority to ask you to leave the lab if you do
NOT ADHERE to the above regulations.

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