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Preparation of 0.1M and 0.1N
Volumetric analysis titration Standards
This page gives info on the weight of salt required to make up 250 ml volumetric analysis standards
for titration against acid base, permanganate, dichromate, iodine, sodium thiosulphate and silver
nitrate. The weight was calculated according to the reaction process of the particular determination.
Concentrations are expressed in molarity, normality and equivalents.
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On this page:
Acid / base titrations
Oxidation / Reduction
permanganate and dichromate
Iodometry
iodine and thiosulphate
Precipitation titrations
silver nitrate
Sodium carbonate
Na2CO3, FW = 106,
Eq. =53g/l
250ml 0.05M =
1.325g = 0.1N
In this example, the FW or Formula weight (Molecular weight) of the salt is 106. Eq. is the
equivalent weight which is 53 grams per liter. And 1.325 grams dissolved up to mark in 250
ml volumetric flask will give a 0.05 M standard solution or a 0.1N standard solution.
Ammonium sulphate
(NH4)2SO4. FW = 132.14, Eq. = 66g/l.
250ml 0.05M = 1.325g = 0.1N
Adipic acid
Barium hydroxide
Benzoic acid
Calcium carbonate
Furroic acid
Hydrochloric acid
Oxalic acid
Sodium hydroxide
Sodium carbonate
Sodium oxalate
FeSO4(NH4)2SO4.6H2O, FW = 392,
Eq. 392g/l
250ml 0.1M = 9.8g = 0.1N (add a few
drops of conc. H2SO4 to clear)
Hhdrogen peroxide
FeNH4(SO4)2.12H2O, FW = 482.19,
Eq. =241g/l
Ammonium oxalate
20 Vol. = 6% = 1.8M
100 Vol. = 30%
250ml 0.05M = 12.50ml of 20 Vol. = 0.1N
1 liter 0.05M = 50ml of 20 Vol. = 0.1N (add 2 mls
conc. H2SO4 per liter soln)
1 liter 0.05M = 10mls of 100 Vol.
1 liter 0.05M =35mls of 30 Vol.
Volume strength = 11.2/34 x strongth of peroxide
in g/l
Sodium nitrite
Potassium permanganate
Potassium dichromate
Tin, Sn,
Potassium iodide
Sodium thiosulphate
Iodine, I2
FW = 253.18, Eq. =
127g/l
1 liter 0.05M = 12.7g =
0.1N
(use 13g Iodine and add
25g KI
Potassium iodate
Copper sulphate
Bleaching powder
Na2SO3.5H2O, FW =
126.04, Eq. = 63g/l
250ml 0.05M = 1.57g =
0.1N
Silver nitrate
Potassium chromate
Ammonium thiocyanate
Potassium thiocyanate
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