Page 1/9 SAA 08/08/2016 14:06: Operator: Labora Tory

novAA 350
Operator:
Page 1/9
08/08/2016 14:06
Labora SAA
tory:
SAA
Method Parameters Technique: Flame

Name:
Created:
Comment:
(Method is not saved)

28/12/1800 0:00
Version:
Operator:
Lines
Line
Elem. Wavel.
[nm]
Optic. mode Lamp
Current
[mA]
Boost
[mA]
Slit [nm]
Meas time. PMT [V]

[s]
Fe248
Fe
Single-beam HCL
0.2
3.0
248.3
300
Evaluation/Background correction
Line
Background
Int.mode AZDK
Smooth
D2 cur. [mA]
HC/BC rat.
Fe248
no background
Mean
on
off
Flame Parameters
Type:
C2H2/air
Burner type:
50 mm
Line
C2H2/air
[L/h]
Ox. control:
Burner angle:
Burner height
[mm]
Fe248
65
off
0 deg
Nebulizer rate:
0 mL/min
Sample Transport
Autosampler:
Dilution if conc.
exceeded:
Injection switch:
Wash:
Yes
none
Delay time:
15 s
No
after sample
Wash time:
15 s
std. cal.
Std. prep.:
manual
Mixing cup cycles: 1
Calibration
Method:
Calibration Curve Parameters

Line
Calib.func.. Intercept
Fe248
linear
Calibration table
No.
Type
Pos
1
2
3
4
5
Cal-Zero
Cal-Std
Cal-Std
Cal-Std
Cal-Std
calculate
1
2
3
4
5
Weighting
Check
Unit
none
none
mg/L
Rec
Fe
[mg/L]
0
5
10
15
20
Statistics Parameters
Statistics:
Repl./sample:
ASpect LS 1.3.2.0
Mean stat.
3
CI calc.:
absolute
Repl./calib.samp 3
le:
Confidence level:
Repl./QC:
95.4%
3
Analytik Jena
novAA 350
Operator:
Page 2/9
08/08/2016 14:06
Labora SAA
tory:
SAA
Pre-runs:
Grubbs test:
off
QCS Parameters
No entries exist
QCC Parameters
RSD/RR% check:
ASpect LS 1.3.2.0
Calib. check:
Recal. check:
Analytik Jena
novAA 350
Operator:
Page 3/9
08/08/2016 14:06
Labora SAA
tory:
SAA
Results
Results file:
Instrument:
C:...+houda5
novAA 350
#AA101217199
Comment:
Line
Autozero
Fe248
Cal-Zero1
Fe248
Conc.1
Abs
Mean
default(1)
Technique:
SD
RSD[%]
default(1)
0
0.00037
Flame
CI
Unit
Date:
Date:
Rem.
08/08/2016 13:02
08/08/2016 13:02
mg/L
0.00022
59.6
Single values (Abs.): #1: 0.00011 #2: 0.00049 #3: 0.00050 (SEV: 275V)
Cal-Std1
default(1)
Fe248
Conc.1
Abs
5
0.05287
Date:
08/08/2016 13:03
mg/L
0.00090
1.7
Cal-Std2
default(1)
Fe248
Conc.1
Abs
10
0.10180
Date:
08/08/2016 13:04
mg/L
0.00069
0.7
Cal-Std3
default(1)
Fe248
Conc.1
Abs
15
0.15206
Date:
08/08/2016 13:05
mg/L
0.00144
0.9
ASpect LS 1.3.2.0
Analytik Jena
novAA 350
Operator:
Page 5/9
4/9
08/08/2016 14:06
Labora SAA
tory:
SAA
Line
Cal-Std4
Fe248
Conc.1
Abs
Mean
default(1)
20
0.19594
SD
RSD[%]
CI
Unit
Date:
Rem.
08/08/2016 13:06
mg/L
0.00028
0.1
Compute calib.
Fe248
Date:
08/08/2016 13:07
Date:
08/08/2016 13:07
Fe248
R(adj.): 0.998239361 Slope: 0.00981 Abs./mg/L Char.conc.: 0.44460 mg/L/1%A
Method SD: 0.27097 y=a+bx
a=0.0025411 b=0.0098066
mg/L
Autozero
default(1)
Fe248
ASpect LS 1.3.2.0
Analytik Jena
novAA 350
Operator:
Page 6/9
08/08/2016 14:06
Labora SAA
tory:
SAA
Autozero
default(1)
Date:
08/08/2016 13:13
Fe248
H29 (d100x)
default(1)
Date:
08/08/2016 13:14
Pre-DF: 1
Fe248
Conc.1
Conc.2
Abs
Wt.[g]:
-0.1545
-0.1545
0.00103
Vol.[mL]: 100
0.0257
0.0257
0.00025
AS-DF: 1.0
16.6
16.6
24.5
0.8034
0.8034
Blank corr.:
mg/L
mg/L
off
<KAL
<KAL
<KAL
H30 (d100x)
Pre-DF: 1
Fe248
Conc.1
Conc.2
Abs
default(1)
Date:
Wt.[g]:
-0.1314
-0.1314
0.00125
Vol.[mL]: 100
0.0302
0.0302
0.00030
AS-DF: 1.0
23.0
23.0
23.6
0.8024
0.8024
08/08/2016 13:15
Blank corr.:
mg/L
mg/L
off
<KAL
<KAL
<KAL
ASpect LS 1.3.2.0
Analytik Jena
novAA 350
Operator:
Page 7/9
08/08/2016 14:06
Labora SAA
tory:
SAA
Line
H31 (d100x)
Pre-DF: 1
Fe248
Conc.1
Conc.2
Abs
Mean
default(1)
Wt.[g]:
SD
4.441
4.441
0.04609
0.0171
0.0171
0.00017
RSD[%]
Vol.[mL]: 100
CI
Unit
Rem.
Date:
08/08/2016 13:16
AS-DF: 1.0
Blank corr.:
off
0.4
0.4
0.4
0.6449
0.6449
mg/L
mg/L
H32 (d100x)
Pre-DF: 1
Fe248
Conc.1
Conc.2
Abs
default(1)
Date:
Wt.[g]:
7.023
7.023
0.07141
Vol.[mL]: 100
0.0499
0.0499
0.00049
AS-DF: 1.0
0.7
0.7
0.7
0.5881
0.5881
Blank corr.:
08/08/2016 13:17
off
mg/L
mg/L
Autozero
default(1)
Date:
08/08/2016 13:18
Fe248
H33 (d100x)
default(1)
Date:
08/08/2016 13:19
Pre-DF: 1
Fe248
Conc.1
Conc.2
Abs
Wt.[g]:
0.8527
0.8527
0.01090
Vol.[mL]: 100
0.0512
0.0512
0.00050
AS-DF: 1.0
6.0
6.0
4.6
0.7639
0.7639
Blank corr.:
off
mg/L
mg/L
ASpect LS 1.3.2.0
Analytik Jena
novAA 350
Operator:
Page 8/9
08/08/2016 14:06
Labora SAA
tory:
SAA
Line
H34 (d100x)
Pre-DF: 1
Fe248
Conc.1
Conc.2
Abs
Mean
default(1)
Wt.[g]:
SD
5.461
5.461
0.05609
0.0404
0.0404
0.00040
RSD[%]
Vol.[mL]: 100
CI
Unit
Rem.
Date:
08/08/2016 13:20
AS-DF: 1.0
Blank corr.:
off
0.7
0.7
0.7
0.6190
0.6190
mg/L
mg/L
H35 (d100x)
Pre-DF: 1
Fe248
Conc.1
Conc.2
Abs
default(1)
Date:
Wt.[g]:
0.9465
0.9465
0.01182
Vol.[mL]: 100
0.0104
0.0104
0.00010
AS-DF: 1.0
1.1
1.1
0.9
0.7604
0.7604
Blank corr.:
08/08/2016 13:21
off
mg/L
mg/L
Autozero
default(1)
Date:
08/08/2016 13:22
Fe248
H36 (d100x)
default(1)
Date:
08/08/2016 13:22
Pre-DF: 1
Fe248
Conc.1
Conc.2
Abs
Wt.[g]:
5.970
5.970
0.06109
Vol.[mL]: 100
0.0369
0.0369
0.00036
AS-DF: 1.0
0.6
0.6
0.6
0.6077
0.6077
Blank corr.:
off
mg/L
mg/L
ASpect LS 1.3.2.0
Analytik Jena
novAA 350
Operator:
Page 9/9
08/08/2016 14:06
Labora SAA
tory:
SAA
Line
H37 (d100x)
Pre-DF: 1
Fe248
Conc.1
Conc.2
Abs
Mean
default(1)
Wt.[g]:
SD
2.738
2.738
0.02939
0.0074
0.0074
0.00007
RSD[%]
Vol.[mL]: 100
CI
Unit
Rem.
Date:
08/08/2016 13:23
AS-DF: 1.0
Blank corr.:
off
0.3
0.3
0.2
0.6966
0.6966
mg/L
mg/L
H38 (d100x)
Pre-DF: 1
Fe248
Conc.1
Conc.2
Abs
default(1)
Date:
Wt.[g]:
0.0313
0.0313
0.00285
Vol.[mL]: 100
0.0161
0.0161
0.00016
AS-DF: 1.0
51.6
51.6
5.6
0.7959
0.7959
Blank corr.:
08/08/2016 13:24
off
mg/L
mg/L
Autozero
default(1)
Date:
08/08/2016 13:25
Fe248
ASpect LS 1.3.2.0
Analytik Jena

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Drepturi de autor:

Formate disponibile

novAA 350

Method Parameters Technique: Flame

(Method is not saved)

Optic. mode Lamp

Meas time. PMT [V]

Mixing cup cycles: 1

Calibration Curve Parameters

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