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1.0 INTRODUCTION
Soap is a salt of a fatty acid. Soap is mainly used for washing, bathing, and cleaning, but
soaps are also important components of lubricants. Soaps for cleansing are obtained by
treating vegetable or animal oils and fats with a strongly alkaline solution. Fats and oils
are composed of triglycerides: three molecules of fatty acids attached to a single
molecule of glycerol. The alkaline solution, often lye, promotes a chemical reaction
known as saponification. In saponification, fats are broken down (hydrolyzed) yielding
crude soap. Fats are transformed into salts of fatty acids and glycerol is liberated,
leaving glycerin as a byproduct. Soaps are key components of most lubrication greases,
which are usually emulsions of calcium and lithium soaps in a mineral oil. Lithiumbased greases are widely used. Many other metal ions are used, including aluminium,
sodium, and mixtures of various metal ions. Such soaps are sometimes classified as
thickeners, meaning that they elevate the viscosity of the oil. In ancient times,
lubricating greases were prepared by the addition of lime to olive oil.
Toilet Soaps, to this class belongs to the finer kinds of scented soaps, which have
emollient properties. They are rarely made direct by the perfumer, the body or basis
being a well-selected white soap, subsequently cleaned and purified. For the choicest
grades, the body should be made of a mixture of olive and sweet-almond oil, as the fat
stock. Lard and beef tallow make the next best stock; and for palm soap a small quantity
of bleached palm oil is to be added to them. Cocoa oil and pale yellow resin
saponaceous matters also enter into the composition of certain toilet soaps. These body
soaps may be obtained as wanted from any well-conducted soap factory. To be adapted
to the purposes of perfumery they must be perfectly neutral, firm, free from unpleasant
odor and all tendency to crust in cold, or sweat in damp weather. They should,
moreover, give a rich lather without wasting too rapidly in the water. Soaps, generally,
in their original condition, are usually deficient in many of those points; and must, for
the purposes of perfumery, undergo a refining procests.
Main objective
To design a plant to manufacture 50 tonnes/day of toilet soap from animal fat.
Specific Objective
The specific objectives are the processes we need to go through in order to achieve the
main objective and these are as follows:
CHAPTER 2
2
Hot process
In the hot-process method, lye and fat are boiled together at 80100 C until
saponification occurs, which before modern thermometers, the soapmaker determined
by taste (the bright, distinctive taste of lye disappears once all the lye is saponified) or
by eye; the experienced eye can tell when gel stage and full saponification have
occurred. Beginners can find this information through research, and classes. It is highly
recommended to not "taste" soap for readiness. Lye, when not saponified is a highly
caustic material. After saponification has occurred, the soap is sometimes precipitated
from the solution by adding salt, and the excess liquid drained off. The hot, soft soap is
then spooned into a mold. The soap lye is processed for recovery of Glycerine.
Cold process
A cold-process soapmaker first looks up the saponification value of the fats being used
on a saponification chart, which is then used to calculate the appropriate amount of lye.
Excess unreacted lye in the soap will result in a very high pH and can burn or irritate
skin. Not enough lye, and the soap is greasy. Most soap makers formulate their recipes
with a 4-10% deficit of lye so that all of the lye is reacted and that excess fat is left for
skin conditioning benefits.
The lye is dissolved in water. Then oils are heated, or melted if they are solid at room
temperature. Once both substances have cooled to approximately 100-110 F (37-43
C), and are no more than 10F (~5.5C) apart, they may be combined. This lye-fat
mixture is stirred until "trace" (modern-day amateur soapmakers often use a stick
blender to speed this process). There are varying levels of trace. Depending on how
additives will affect trace, they may be added at light trace, medium trace or heavy
trace. After much stirring, the mixture turns to the consistency of a thin pudding.
"Trace" corresponds roughly to viscosity. Essential oils, fragrance oils, botanicals,
herbs, oatmeal or other additives are added at light trace, just as the mixture starts to
thicken.
The batch is then poured into molds, kept warm with towels, or blankets, and left to
continue saponification for 18 to 48 hours. Milk soaps are the exception. They do not
require insulation. Insulation may cause the milk to burn. During this time, it is normal
for the soap to go through a "gel phase" where the opaque soap will turn somewhat
transparent for several hours, before once again turning opaque. The soap will continue
to give off heat for many hours after trace.
4
After the insulation period the soap is firm enough to be removed from the mold and cut
into bars. At this time, it is safe to use the soap since saponification is complete.
However, cold-process soaps are typically cured and hardened on a drying rack for 26
weeks (depending on initial water content) before use. If using caustic soda it is
recommended that the soap is left to cure for at least four weeks.
Molds
Many commercially available soap molds are made of silicone or various types of
plastic, although many soap making hobbyists may use cardboard boxes that are lined
with plastic wrap. Soaps can be made in long loaves that are cut into individual bars,
block molds that are cut into loaves and then bars, or individual molds.
Purification and finishing
The common process of purifying soap involves removal of sodium hydroxide, glycerol
and some impurities. These components are removed by boiling the crude soap curds in
water and re-precipitating the soap with salt.
Most of the water is then removed from the soap. This was traditionally done on a chill
roll which produced the soap flakes commonly used in the 1940s and 1950s. This
process was superseded by spray dryers and then by vacuum dryers.
The dry soap (approximately 6-12% moisture) is then compacted into small pellets.
These pellets are now ready for soap finishing, the process of converting raw soap
pellets into a saleable product, usually bars.
The batch is then poured into molds, kept warm with towels, or blankets, and left to
continue saponification for 18 to 48 hours. Milk soaps are the exception. They do not
require insulation. Insulation may cause the milk to burn. During this time, it is normal
for the soap to go through a "gel phase" where the opaque soap will turn somewhat
transparent for several hours, before once again turning opaque. The soap will continue
to give off heat for many hours after trace.
Soap pellets are combined with fragrances and other materials and blended to
homogeneity in an amalgamator (mixer). The mass is then discharged from the mixer
into a refiner which, by means of an auger, forces the soap through a fine wire screen.
From the refiner the soap passes over a roller mill (French milling or hard milling) in a
5
manner similar to calendering paper or plastic or to making chocolate liquor. The soap
is then passed through one or more additional refiners to further plasticize the soap
mass. Immediately before extrusion it passes through a vacuum chamber to remove any
trapped air. It is then extruded into a long log or blank, cut to convenient lengths, passed
through a metal detector and then stamped into shape in refrigerated tools. The pressed
bars are packaged in many ways.
Sand or pumice may be added to produce a scouring soap. The scouring agents serve to
remove dead skin cells from the surface being cleaned. This process is called
exfoliation. Many newer materials are used for exfoliating soaps which are effective but
do not have the sharp edges and poor particle size distribution of pumice.
Nanoscopic metals are commonly added to certain soaps specifically for both coloration
and anti-bacterial properties. Titanium powder is commonly used in extreme "white"
soaps for these purposes; nickel, aluminium and silver are less commonly used. These
metals provide electron-robbing behavior when in contact with bacteria, stripping
electrons from the organism's surface and thereby disrupting their functioning (typically
killing the bacteria when it has lost too many electrons). Because some of the metal is
left behind on the skin and in the pores, the benefit can also extend beyond the actual
time of washing, helping reduce bacterial contamination and reducing potential odors
from bacteria on the skin surface.
CHAPTER 3
3.0 EQUIPMENT LIST AND PROCESS DESCRIPTION
6
Item no.
Service
Quantity
Type
VE-101
Vertical Cylindrical
VE-105
Vertical Cylindrical
VE-110
Saponifier vessel
Vertical Cubic
VE-205
Vertical Cylindrical
DA-101
Soap dryer
Vacuum Shelf
HE-101
SE-101
Static Seperator
CO-101
Washing Column
CE-201
Centrifuge
VE-105
Neutralizer Vessel
Tubular Centrifuge
Lye
Tallow
Static Separator
Saponification vessel
wet soap
NaOH
Lye
Washing Column
Fresh lye
Glycerine
35% Glycerine
65% lye
Washed soap
20% lye
Lye
Centrifuge
Centrifuge
0.3% NaOH
wet soap
0.5% NaCl
68.2% Solids
Salt produced
Toilet soap
Vacuum Dryer
Vacuum Dryer
Neutralizer
Neutralizer
Neutralizer
Additives
31% H2O
88% Solids
68% Solid
12% H2O
1% Impurities
Water
This is a continuous process which uses a plant. The process is best understood in terms
of two streams: soap flowing in the order given below against a counter-current of lye.
Step 1 - Saponification
The raw materials are continually fed into a reactor in fixed proportions.
Tallow: 735.29 kg hr-1
NaOH solution: 272.33 kg hr-1
Lye: 35.22 kg hr-1
These ingredients alone would give a low water, high glycerine soap. Soap needs to be
about 30% water to be easily pumpable, and even then needs to be held at around 70oC,
so excess lye is added to hydrate the soap and dissolve out some of the glycerine. The
lye added is known as "half spent lye" and is the lye discharged from the washing
column. This lye already contains some glycerine, but it is further enriched by that
formed in the saponification reaction.
Step 2 - Lye separation
The wet soap is pumped to a "static separator" - a settling vessel which does not use any
mechanical action. The soap / lye mix is pumped into the tank where it separates out on
the basis of weight. The spent lye settles to the bottom from where it is piped off to the
glycerine recovery unit, while the soap rises to the top and is piped away for further
processing.
Step 3 - Soap washing
The soap still contains most of its glycerine at this stage, and this is removed with fresh
lye in a washing column. The column has rings fixed on its inside surface. The soap
solution is added near the bottom of the column and the lye near the top. As the lye
flows down the column through the centre, a series of rotating disks keeps the soap / lye
mixture agitated between the rings. This creates enough turbulence to ensure good
mixing between the two solutions. The rate of glycerine production is calculated and the
rate at which fresh lye is added to the washing column then set such that the spent lye is
25 - 35 % glycerine. Glycerine is almost infinitely soluble in brine, but at greater than
35% glycerine the lye no longer efficiently removes glycerine from the soap.
The soap is allowed to overflow from the top of the column and the lye ("half spent
lye") is pumped away from the bottom at a controlled rate and added to the reactor.
Step 4 - Lye separation
The lye is added at the top of the washing column, and the soap removed from the
column as overflow. As the lye is added near the overflow pipe the washed soap is about
9
20% fresh lye, giving the soap unacceptably high water and caustic levels. Separating
off the lye lowers the electrolyte levels to acceptable limits.
The soap and lye are separated in a centrifuge, leaving a soap which is 0.5% NaCl and
0.3% NaOH, and about 31% water. The lye removed is used as fresh lye.
Step 5 - Neutralisation
Although the caustic levels are quite low, they are still unacceptably high for toilet and
laundry soap. The NaOH is removed by reaction with a weak acid such as coconut oil
(which contains significant levels of free fatty acids), coconut oil fatty acids, citric acid
or phosphoric acid, with the choice of acid being made largely on economic grounds.
Some preservative is also added at this stage.
Step 6 - Drying
Finally, the water levels must be reduced down to about 12%. This is done by heating
the soap to about 125oC under pressure (to prevent the water from boiling off while the
soap is still in the pipes) and then spraying it into an evacuated chamber at 40 mm Hg
(5.3 kPa). The latent heat of evaporation lost as the water boils off reduces the soap
temperature down to 45oC, at which temperature it solidifes onto the chamber walls.The
soap chips are scraped off the walls and "plodded" (i.e. squeezed together) by screws
known as "plodder worms" to form soap noodles. The soap is now known as base or
neat soap chip, and can be converted into a variety of different soaps in the finishing
stages. The moisture evaporated off the wet soap is transported to a barometric
condensor, which recondenses the vapour without the system losing vacuum. The
moisture can contain soap dust (.Fines.) which is removed by cyclones and returned by
augers to the spray chamber, while the water is recycled.
10
11
CHAPTER 4
4.0 MATERIAL AND ENERGY BALANCES
4.1 MATERIAL BALANCES
4.1.1 ASSUMPTIONS
1. The process is an open system
2. The process occurs at a steady-state condition.
24hours
1 year
1 day
= 7920 hours
1 year
330 days
1 day
24 hours
1000kg
1 ton
16500,000 kg
7920 hr
= 2083.333 kg/hr
12
NaOH
Tallow
SAPONIFICATION VESSEL
Lye
INPUT
OUTPUT
Component
Amount (kg)
Component
Amount (kg)
Tallow
735.29
Wet soap
3707.62
NaOH
272.33
Lye
2700
Total
3707.62
Total
3707.62
13
Lye
Crude soap
INPUT
OUTPUT
Component
Amount (kg)
Component
Amount (kg)
Wet soap
3707.62
Crude soap
3672.4
Lye
35.22
Total
3707.62
Total
3707.62
14
Fresh lye
Crude soap
Washed soap
WASHING
COLUMN
Glycerin
INPUT
OUTPUT
Component
Amount (kg)
Component
Amount (kg)
Crude soap
3672.4
Washed soap
3360.16
Fresh lye
2500
Glycerine
2812.26
Total
6172.4
Total
6172.4
15
Washed soap
Wet soap
CENTRIFUGE.
Lye
INPUT
OUTPUT
Component
Amount (kg)
Component
Amount (kg)
Washed soap
3360.16
Lye
672.03
16
Total
3360.16
Wet soap
2688.13
Total
3360.16
Soap
VESSEL.
Salt
INPUT
OUTPUT
17
Component
Amount (kg)
Component
Amount (kg)
Wet soap
2688.13
Soap
2696.07
Additives
12.57
Salt
24.394
Weak acid
19.76
Total
2720.43
Total
2720.43
Solid soap
Toilet soap
DRYER.
Water
INPUT
OUTPUT
Component
Amount (kg)
Component
Amount (kg)
Soap
2696.07
Toilet Soap
2083.33
Water
585.79
Impurities
26.96
Total
2696.07
Total
2696.07
Q= H +W S
Where
w s=12.5 kw for a turbine agitator
But for,
H=H 2H 1
H=m [ cpdt cpdt ]
70 ' c
H=m
25' c
cpdt cpdt
25 ' c
25' c
Hence
[ ]
70 ' c
H=m
cpdt
25 ' c
Where
Cp (wet soap)=1.22kjkg.k
M(mass flow rate)=3707.48kghr
T at 250c=298.15 k
T at 700 c=343.15k
20
Then
H=3707.48
kg
kj
h
1.22
( 343.15298.15 ) k
h
kg . k
3600 s
|)
H=56.5 kw
Q= H +W S
Where
( 56.5+12.5 ) kw
Q= 69.04 kw is the amount of heat energy required by the
saponification vessel.
2. Energy balance on washing column
H=QW S
Q= H +W S
Where
w s=12.5 kw for a turbine agitator
But for,
H=H out H
Where
Hout
H glycrinee+ H
H = H
wet soap
+ H lye
wet soap
: T at 80
: T at 70
c=353.15k
c=343.15k
For
21
80 c
2812.26
kg
kj
1h
2.43
( 353.15343.15 ) k
h
kg . k
3600 s
H glyc erine=18.98 kw
H
80c
3360.16
kg
kj
1h
1.22
(353.15343.15 ) k
h
kg . k
3600 s
H washed soap=11.39kw
H
80 c
lye=m cpdt
70 c
2500
kg
kj
1h
3.1
(353.15343.15 ) k
h
kg . k
3600 s
H lye=21.53 kw
H
80c
3672.4
kg
kj
1h
1.22
( 353.15343.15 ) k
h
kg . k
3600 s
H crude soap=12.45kw
22
Hence
H=H out H
( 18.98+11.39 ) ( 21.53+12.45 )
30.3733.98
H=3.61 kw
Then
Q= H +W S
3.61+12.5
Q=8.89 k w
3. Energy balance on centrifuge
The energy consumption of a tubular bowl centrifuge handling dilute slurries is 1.49kw
Tubular centrifuge bowl diameter =4.25in
Maximum centrifuge force gravity =13200
Ref.(Robert H.Perry and Don W. Green,Perrys chemical engineershandbook, 7th
edition ,page 18-112,table 18-12)
Where Q=WS
Q=1.49kw
Separation factor (ks)
23
s=
s=
39.48 n r
g
k
39.48 ( 2502 ) 4.125
9..81
k
s= 1037557.3
k
Compound
is by definition
f (kj mol)
NaOH
- 469.43
H3PO4
- 1294.23
H2O
- 1748.1
NaHPO4
- 285. 85
24
Hence
reactants
v i f
i
products
vi f
rxn =
)( V NaOH f NaOH +V H 3 PO 4 f H 3 PO 4 ) ]
Where
T sa =feed temperature
T v =vapourization temperature
T sb =final solidstemperature
T va=final vapour temperature
C PS ,C pl ,C pv =h eat capcities of solids , liquidvapour
Then
25
C pl =
4.187 kj
.k
kg
C pv =
4.285 kj
.k
kg
C PS=
1.22 kj
.k
kg
0c
X b =0.12
ms=2083.33 kg /h
Qs
Qs
=1.22 ( 318.15343.15 ) + ( 0.3 ) ( 4.1897 ) ( 373.15343.15 ) + ( 0.310.12 ) 225+ ( 0.12 )( 4.1897 ) (318.1
ms
Qs
=(30.5 )+ (38.964 ) + ( 42.75 ) 27.652+ 3.986
ms
Qs
=58.152+85.7
ms
Qs
=27.548
ms
Qs=ms (27.548)
Q s=2083.33(27.548)
26
Qs=57391.6
1h
|kjh |3600
s
Qs=15.94 kw
Hence the enegy needed by the dryer is 15.94kw
CHAPTER 5
5.0 EQUIPMENT SPECIFICATION AND PIPELINE SCHEDULE
5.1 EQUIPMENT SPECIFICATIONS
Equipment specification typically includes the determination of vessel dimensions and
description of other internal parts of the equipment. It also involves the determination of
parameters like speed, power and any other operating parameters pertaining to the
particular equipment. Specification of equipment can be approached from a duty
specification viewpoint.
(Cheremisinoff, 2000)
27
Material handled
Material of construction
Information and data used are from Peter and Timmerhaus, McCabe and Smith and
Chemical Engineering handbook, 5th edition.
Saponification vessel
Duty: To react sodium hydroxide, tallow and lye.
Type: Non reversible
Capacity: 50 tonnes/hr
Number required: 1
Static separator
Duty: separates the soap from the lye.
Type: a settling vessel which does not use any mechanical action
Material of Construction: carbon steel
Area: 2.0m2
Width: 1.15m
Length: 1.725m
Storage Tank 1
Duty: To serve as a stock pile for the tallow.
28
Number required: 1
Material of construction: Carbon Steel
Neutralizer
Duty: to react weak acid with sodium hydroxide.
Type: Continuous Stirred Tank Reactor
Capacity: 185m3
Height: 8 m
Diameter: 5m
Material of Construction: Carbon Steel
Storage Tank 3
Duty: To temporarily store lye solution before entering saponifier.
Description: Vertical cylindrical tank with flat ends.
Capacity: 124.8 m3
Height: 11m
Diameter: 3.8m
Thickness: 7mm
Number required: 1
Material of construction: Carbon Steel
Dryer
Duty: to reduce water levels to about 12% in the toilet soap
Type: vacuum shelf dryer
Number: 1
Capacity: 2083.33kg/hr
Moisture content: 3%
Column diameter: 0.9m
Number of trays: 10
Hole diameter: 20mm
Distance between trays: 20mm
30
Centrifuge
Duty: To separate soap and lye
Type: Tubular centrifuge
Diameter: 4.25in
Number: 1
The energy consumption of a tubular bowl centrifuge handling dilute slurries is 1.49kw
Tubular centrifuge bowl Maximum centrifuge force gravity =13200
Separation factor ( kS ) ; 1037557.3
Pipeline
Fluid
Location
Mass
Fluid
Diamete Sched
Material
Transport Flow
Velocit
r, In.
ule
Of
ed
y, m/s
Numb
Construct
er
ion
40-S
304
Rate,
(kg/hr)
Between the
Wet soap
3707.62
9.67
saponification
Stainless
Steel
static separator
31
Between the
Crude
static separator
soap
3672.4
9.67
40-S
304
stainless
steel
column
Between the
Washed
washing colunm
soap
2812.26
2.73
40-S
304
stainless
and the
steel
centrifuge
Between
Wet soap
2688.13
2.23
40-S
304
centrifuge and
stainless
neutralizer
steel
Between
Soap
2696.07
2.22
40-S
304
neutralizer and
stainless
the vacuum
steel
shelf dryer
From vacuum
Toilet
shelf dryer
soap
2083.33
2.34
1.5
40-S
304
stainless
steel
32
CHAPTER 6
6.0 PLANT SITING AND LOCATION
6.1 PLANT SITING AND LAYOUT
Application of sound engineering principles, exhaustive costing and profitability
analysis only will not be enough for successful operation. The success and profitability
of the plant is largely dependent on so many factors. These factors are:
1
Plant location
Marketing areas
Maintenance
Storage facilities
10 Pollution control
11 Quality control
b. Prior existence of similar chemical plants and location of other industrial centers
c. Existing roads and services and also appropriate terrain, sub surface, drainage
etc.
d. Suitable access for transportation for transportation of raw materials and
chemicals and for construction of a chemical plant.
e. Availability of a local workforce and distance from local communities.
f. Environmental discharge regulation and cost of land and services etc
g. Climatic condition
h. Proximity to both the raw materials supply and the market for the product
chemical.
i. Political and strategic considerations.
j. Location community considerations.
k. Proximity to major transportation networks e.g. roads, railways.
l. Availability of suitable land etc.
The importance of the geographical location of the plant cannot be over emphasized.
The locations considered for the sitting of the toilet soap plant are Kumasi in the
Ashanti Region, Tema in the Greater-Accra Region and Takoradi in the Wetern Region.
After detailed analysis of the various locations appropriate for sitting the toilet soap
plant has been done, the location of the toilet soap plant will be Takoradi in the Western
Region of Ghana.
Some of the factors considered were:
and some of its surrounding towns produce a high level of animal fat which is
obtained at the abattoir and thus imply a good availability of tallow in that area. It being
a coastal town, NaOH can easily be imported from overseas for the purpose of soap
production and thus if the plant is sited in Takoradi , raw materials will not be a
problem.
Generally, skilled labour must be brought in for the construction of the plant. However,
there must be adequate labour (skill and unskilled) in the locality for the operation of
the plant. The availability of cheap labour in developing countries including Ghana and
therefore, favours this possible plant location.
Takoradi having attained metropolitan status and the regions jubilee field (crude oil)
sector in particular and agriculture in general attracts migrants to Takoradi. The migrant
population shows that males are attracted to the town than females. With the advent of
the toilet soap plant in that area, the youth will be employed on the plant site in various
forms of casual work. Unemployment among the youth like any other densely populated
area is high. Thus labour, especially unskilled labour will not be a problem. Skilled
labour can also be brought in for special purposes.
Market Areas
The local consumption and export needs are the primary focus for production, since
future expansion would seek to explore opportunities in the West African Region as well
as other parts of the world. Because transportation cost takes up a significant fraction of
the sales price, it is one of the reasons why our plant will be situated close to the
primary market and closer to the seaport and habour which is also in this town Takoradi.
Moreover the major market for the highly manufactured toilet soap is the foreign
market. Since a higher percentage of the product would be exported out of the country.
With the plant site being Takoradi which has a Sea Port renders the site very suitable.
The local market can also be served with adequate supply of toilet soap by the means of
good road and rail networks in the region and across the other regional and district
capitals.
Climate
This is considered a very important factor when choosing a location for the plant.
Generally, adverse climate conditions at a plant site will increase cost. Ghana has two
major seasons (dry and rainy seasons) which is common to all the possible plant
location. This factor thus favours the possible plant location.
Political and strategic considerations
Sometimes, the choice of location provides certain benefits from the government in
terms of capital grants, tax concessions and other inducements. For this factor however,
36
since government benefits of this sort are spread around Ghana, the possible location is
also favoured by this factor.
Local community consideration
It is important to locate the plant in a safe community and where it is accepted. The
community should also be able to provide adequate facilities for plant personnel such as
schools, banks, housing, and recreational and cultural facilities. Since Takoradi is the
regional capital; schools, banks, housing and other recreational facilities are present
with more to be created upon the establishment of the plant thus making it a favourable
location.
CHAPTER 7
7.0 ECONOMIC ANALYSIS
This plant design project aims to present a process that is capable of operating under
conditions which will yield profit. As a necessity the economic viability of this
manufacturing business must be addressed considering the society and government with
which it will operate. The primary concern of an investor lies in the rate of return
(ROR) based on accurate cost estimates and sound data.
Since net profit equals total income minus all expenses, it is essential that all the costs
involved in manufacturing processes are considered. A capital investment is required for
any industrial process and the determination of the process consists of fixed capital
Investment of physical equipment and facilities in the plant plus necessary investment is
37
an important part design project. The total investment for any working capital which
must be available to pay salaries, keep raw materials and products on hand and handle
other special items requiring a direct cash outlay. Thus in this analysis income tax is
taken into consideration.
Using the payback period, rate of return and unit product cost a profitability analysis
will be conducted to see the viability of this plant design.
Basis of economic analysis:
Process: Continuous
necessary for the installed process equipment with all auxiliaries needed for
a complete process operation (e.g. purchased equipment cost, equipment
installation cost, instrumentation and control cost, piping cost, electrical
equipment and material cost, building (including services) cost, yard
improvement cost, service facilities coat, land cost, etc)
Working Capital is the capital needed for the daily running of the plant. In other words ,
it is the additional investment capital needed over and above the fixed capital
investment to start the plant, to operate it to the point when income is earned. This
consists of the total amount of money invested in
Start up
Raw material and supplies carried in stock
Finished and semi finished products in stock
Accounts receivable and payable
Cash kept on hand for monthly payment of operating expenses
Taxes payable
Item no.
VE-101
Service
Cost $
14904
39
VE-105
VE-110
Saponifier vessel
VE-205
8280
DA-101
Soap dryer
7300
HE-101
2505.3
SE-101
Static Separator
649,600
CO-101
Washing Column
21,900
CE-201
Centrifuge
6900
VE-105
Neutralizer Vessel
6505
146302
265,700
Source: Perrys
Total Equipment Cost = $1,129,896.3
Piping Cost
40
This refers to the cost for raw material, intermediate-product, finished-product, steam,
water, and waste products piping (Peter et al). Items involved in the complete erection
of all piping used directly in the process which include the labour, valves, fittings, pipe,
support etc. The piping cost is estimated to be 30% of purchased equipment cost (Peter
et al, 1990).
41
Cost of Land
The plant will be sited at Takoradi in the Western Region. The cost of land per plot
(30mx30m) is GH600. The number of plots needed for the construction of the plant is
10, making room for future expansion of the company, 25% of the land needed will be
added, and the total land needed is 11,025m2. The total cost will be GH7500
($5357.14)
Contingency Fees
A contingency amount is included in all estimates of total capital investment in
recognition of the fact that, there will be unexpected events and changes that will
inevitably increase the cost of the project (i.e. strikes, price changes, small design
changes, storms, floods etc). This component is estimated as 8% of the total direct and
indirect cost (Peter et al, 1990).
Estimated Cost,
Item
1129896.3
1955890.93
625885.1
Piping (installed)
2347069.116
Electrical (installed)
938827.65
3677075
Yard improvements
782356.37
Service facilities
2347069.116
Land
5357.14
13,809,426.72
Estimated cost
1640247-531
Construction expense
2050309.414
Contractors Fee
1025154.707
Contingencies
1640247.531
TOTAL TIC
6355959.183
20165385.90
3024807.885
The two basic components that affect product pricing are costs of manufacture and
competition in selling. It is unprofitable to sell a product below the manufacturers
production costs and unfeasible to sell it at a price higher than that at which comparable
merchandise is being offered. Other variables also affect pricing. Company policy may
require a minimum profit on new product lines or a specified return on investments, or
discounts may be offered on purchases in quantity.
This involves the estimation of cost for operating the plant and selling the products.
Total product cost is broken down into two:
Total Product Cost = Manufacturing Cost + General Expenses
The manufacturing cost (direct product cost) is also subdivided into the fixed charges,
plant overheads and variable production cost. The fixed charges are costs that do not
vary with production rate, where as the variable production cost is the cost dependent on
the amount of product produced. Plant overheads comprise hospital and medical bills,
general plant maintenance cost safety services among others (Peter et al, 1990).
The general expenses comprise administrative expenses, distribution and marketing
expenses and research and development expenses.
An additional 12.5% 0f the total cost for direct and indirect labour is included to
account for the social security contributions for each employee.
44
Operating Labour
Table 7.3: Direct and Indirect Labour Costs (DLC and ILC)
Direct Labour Cost (DLC)
Staff
Number
Head, $
Plant Manager
80,000
80,000
Production Manager
70,000
70,000
Chemical Engineer
65,000
130,000
Mechanical Engineer
63,000
126,000
Electrical Engineer
63,000
126,000
Quality Assurance
55,000
55,000
Supervisors
45,000
225,000
Lab Technicians
18,000
90,000
15
4,800
72,000
Total (DLC)
34
Manager
974000
Staff
Number
Total Annual
Head, $
Salary, $
Managing Director
80,000
80,000
Human Resource
50,000
50,000
Sales Manager
45,000
45,000
Accountant
40,000
80,000
Store Keeper
15,000
30,000
Receptionist and
10,000
10,000
Cleaners
2,400
12,000
Drivers
3600
21,600
Security men
3000
24,000
Manager
Secretary
Total (ILC)
352600
(DLC + ILC)
1326600
Social Security
12.5%(DLC +
165825
Contributions
ILC)
TOTAL LABOUR
1492425
COST
46
Unit Cost/kg,
Raw Material
Annual Quantity
Tallow
Sodium
5823496.80 kg
0.714/20kg
207,898.84
2156853.60 kg
0.178
383,919.94
hydroxide
591,818.78
Total
Utilities
This includes the cost of the total cost of electricity, process cooling water, and other
forms of utility that is required to keep the plant in operation. This component is
estimated as 10% of the total equipment cost.
Maintenance and repairs
If a plant is to be kept in efficient operating condition, a considerable amount of
expenses is necessary for maintenance and repairs. Since the annual cost for the plant is
high, this component is estimated as 6% of the fixed capital investment.
Operating supplies
This includes the cost of items such as lubricants, test chemicals, charts etc, required to
keep the plant functioning efficiently. It is assumed to be 15% of maintenance and
repairs.
Laboratory Charges
This involves cost of laboratory tests for control operation and product quality control.
It is taken as 20% of operating labour.
Description
Raw Materials
591,818.78
Operating Labour
1,492,425
Operating Supplies
181,488.47
112,989.63
1,209,923.15
Laboratory Charges
298,485
3,887,130.03
CHAPTER 8
8.0 PLANT SAFETY AND POLLUTION CONTROL
8.1 PLANT SAFETY
Every organisation (company or industry) has the moral and legal obligation to protect
the health and welfare of its employees as well as that of the general public. Therefore,
good safety measures have to be put in place to ensure the safety of lives and prevent
damage to equipment. The primary aim of these safety measures therefore is to prevent
or minimize workers exposure to the potential hazard, injury to workers, loss of lives,
and destruction of properties. They are also needed to ensure safe as well as efficient
operation.
These safety measures are employed in industry mainly to prevent or control hazards.
A hazard is a property which in particular circumstances could lead to harm. Common
safety hazards in the manufacturing industry include; dangerous machinery, explosion
to fires, faulty electrical connections and falling materials due to poor housekeeping
among others.
48
The potential hazards that could be present in the toilet soap plant include hazards due
to materials handling and hazards due to the various processes.
Hazards due to materials handling
Potentially hazardous situations include handling and packaging operations, equipment
cleaning and repair, decontamination following spills and equipment failure. Hazards
that workers are likely to be exposed to can be prevented by a number of ways, example
of which is the provision of PPEs (Personal Protective Equipment). These equipments
include chemical splash goggles, overcoat/chemical suit, rubber boots, ear plugs, face
shield, etc. These equipment are worn to protect the worker from the dangers of
handling some of the chemicals especially sodium hydroxide.
Hazards due to various processes
Hazards that might be caused during processes in this plant include fire hazards,
electrical and mechanical hazards.
Fire Hazards: During the process of heating the raw materials, for example,
heating takes place at high temperatures of about 600-650C with the production
of hot flue gases through a chimney. Care must be taken near or during operation
of the saponification vessel for example the control of temperature. Labourers
are so careless and tend to attempt checking temperature manually. This and
many other careless practices may lead to a fire hazard. Overheating of vessel
With the above mentioned safety measures, the plant can be safe to work on.
49
50
CHAPTER 9
9.0 DISCUSSION
At this end, one can envisage that the production process is a feasible one within the
confines of the country. With the abundance of tallow in Ghana and its neighboring
country, Ivory Coast, the possibility of raw materials shortage is extremely low.
This plant can be duplicated in regions in the country in which the raw materials are
readily available. The establishment of this plant in other locations will provide
employment.
From the literature, the tallow, when left to decompose, tend to be very toxic to the soil.
This process introduces a way out whereby almost all of the tallow would be utilized in
this very lucrative venture.
The glycerine, also, obtained after the saponification process, serves as a valuable
source of product for export and other purposes. With the advancement of this project
some measures will have to be put in place to ensure that the quality of the toilet soap
remains unaltered. Thus the farmers (animal rearers) will have to be motivated to
produce a high quality of tallow required for efficient production.
With the high rate of return over the plant life, this project is very viable and rewarding
to investors and the nation (product is for exportation).
51
A continuous operation is preferred for the plant due to the following reasons (Peters et
al, 1991):
1. A specific product (toilet soap)
2. The production rate is far greater than 16500 tonnes per annum.
The chosen process for the production of toilet soap will be the best since the batch
method will not be cost effective.
CHAPTER 10
10.0 RECOMMENDATION
We recommend that, in the near future, the industry should partner with the
abattoirs and oil companies to reduce the purchase cost of raw materials.
Due to the cost intensive nature of this project, a lower annual production rate
should be used.
The issue of safety and control should be enforced at all levels and times to
ensure the smooth running of the plant, to protect lives and the environment as a
whole.
The marketing department should market the product to raise the profitability
52
REFERENCES
Perry Robert H., Green Don W., (1999), Perrys Chemical Engineers Handbook,
53
APPENDIX
MATERIAL BALANCE ON THE PRODUCTION OF 50TONS TOILET SOAP
PER DAY
ASSUMPTIONS
The process is an open system
The process occurs at a steady-state condition.
PLANT ATTAINMENT
This is defined as a percentage of available hours in a year that plant operates usually
between 90-95%. The process plant will operates three shifts of 8 hours per day.
The total downtime (maintenance, shutdowns and holidays) will take 35days per year.
330days
24hrs
1year
1day
Basis: kg/hr
Productivity is 50 tonnes per day
In a year, productivity is 50 tonnes 330days = 16500tonnes per year
Converting,
54
16500
1year
1day 1000kg
1year
330days
24hrs 1ton
= 16500 000kg
7920hr
=2083.33kg/hr
3[C17H35COONa] + C3H5(OH)3
mol
1000g
306g
1kg
= 2083330
306
= 6808.27mol/hr
Hence,
1 mol Tallow
6808.27mol/hr
3mol Soap
= 2269.42mol/hr
But,
n= m/M
m=nM
m = 2269.42mol
hr
324g
mol
1kg
1000g
55
= 735293.16
1000
= 735.29kg/hr
Also,
n(NaOH) = n(Soap)
n(NaOH) = 6808.29
m=nM
= 6808.29mol 40g
Hr
1kg
mol
1000g
= 272.33kg/hr
Amount of lye to be used at the saponification vessel = 2700kg/hr
Lye
= 3707.48 3672.4
Lye
= 35.08kg/hr
56
BALANCES ON NEUTRALIZER
Neutralization reaction
NaOH + H3PO4
NaH2PO4 + H2O
NaOH Balance
0.003 (2688.126) = 8.064kg/hr
Therefore,
1 mol NaOH
1 mol H3PO4
But n = m
M (NaOH) = 40g/mol
M
n (NaOH) = 8.064 kg
mol
1000g
Hr
40g
1kg
n = 201.6mol/hr
Therefore,
1 mol H3PO4
201.6 NaOH
1mol NaOH
n (H3PO4) = 201.6mol/hr
m (H3PO4) = n M
= 201.6 mol
Hr
98g
mol
1kg
1000g
m (H3PO4) = 19.76kg/hr
201.6 NaOH
1 mol NaOH
= 201.6mol/hr
M (NaH2PO4) = 121g/mol
n=m/M
m (NaH2PO4) = 121g
201.6mol 1kg
58
mol
hr
1000kg
m (NaH2PO4) = 24.349kg/hr
Then,
Total Material Balance
W.S + H3PO4 + Additives = S + NaH2PO4
2688.13 + 19.76 + Additives = 2696.04 + 24.394
Additives = 12.54kg/hr
For Impurities
0.01 (2696.07) = 26.96kg/hr
59
60