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Documente Profesional
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PRODUCT SHEETS
TECHNICAL ARTICLES
AMACS History
TEG Recovery
Fractionation Trays
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Email: amacs@amacs.com
Process
Amacs
Company
HistoryTower Internals
Amacs, a specialist in Process Tower Internals, was formed through the 2011 merger
or Products
of Amistco Separation Products Inc., and the Separations & Mass Transfer
division of ACS Industries. Amistco and ACS were both well respected suppliers of a full
complement of process tower internals.
ACS was founded in 1939 in Rhode Island to manufacture knitted copper wire
mesh. By the 1950s, it had expanded into stainless steel wire mesh and established
the Separations Technology Division to manufacture entrainment separators.
To better serve the petrochemical industry, the division relocated to Houston
in 1979. Over time ACS developed process engineering capability and expanded
s into vane separators,
AMA
in Monterrey, Mexico to add capacity to meet its growing sales.
Amistco was founded in Houston in 1991 to manufacture mist eliminators based on its own wire knitting technology. It too
expanded into vane separators and mass transfer products as it expanded its in-house process engineering capability. Amistco
also invested in w edge wire screen manufacturing to serve the petrochemical as well as other industrial markets.
Today, Amacs operates factories in Houston and Monterrey. Headquarters are in Houston where its process engineering and
mechanical engineering groups provide customers with custom solutions for new build and replacement product needs. Amacs
serves a broad industry group including oil rening, natural gas processing, biofuels, and chemicals. Amacs is a vertically integrated
manufacturer with wire knitting, laser cutting, plasma cutting, metal punching, metal stamping, roll forming, welding, and assembly
capability.
Additional information is available at www.amacs.com
1-800-231-0077
www.amacs.com
Amistco Separation Products Inc, and ACS Separations and Mass Transfer Products, are Registered Trademarks of AMACS
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Table of Contents
Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Droplet Formation and Size Distributions . . . .1
Mechanisms of Droplet Removal . . . . . . . . . . .2
Types of Mist Eliminator Mesh & Materials . . .4
Design Equations . . . . . . . . . . . . . . . . . . . . . . . .6
Predicting Pressure Drop . . . . . . . . . . . . . . . . .7
Inlet Diffusers . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Vessel Configuration . . . . . . . . . . . . . . . . . . . . .8
Advanced Mist Eliminator Designs . . . . . . . .10
Mesh-Vane Assemblies . . . . . . . . . . . . . . . . . .11
Use of Geometry . . . . . . . . . . . . . . . . . . . . . . .11
MultiPocket Vanes . . . . . . . . . . . . . . . . . . . . .11
In practice, designers
or engineers do not
quantify or measure
droplet size distributions, rather they are
assumed based on
empirical data or experience. Fortunately, an
experienced engineer
can
assume
an
approximate distribution based on the
means or mechanism
by which the droplets are generated. Typical examples from common
mist sources are given to illustrate these concepts.
Fine droplet distributions, often called fogs (<3 m diameter particles
with an average typically in the submicron range), occur in high speed
metal stamping in which cycles of extreme frictional heating and shock
condensation of lubricating oils form droplets in the submicron range,
so-called "blue smoke". This smoke is removed to comply with health
and environmental regulations.
Fog is also produced when gas phase reactions form a liquid product as
in the case of vapor phase SO3 and water yielding H2SO4. Downstream
For fogs in which the bulk of the droplets are characterized with submicron diameters, the energy to bring
about the collision with the target is derived from
Brownian Diffusion, the random motion of fine liquid
particles as they are
FIGURE 4
pushed about by
molecular action as
4a
shown in Figure 4a.
Fog elimination with
so-called fiberbed
technology is beyond
4b
the scope of this
manual.
This manual contains basic design concepts used by
engineers to remove droplets greater than 3 m in
For particles in the
diameter, so called mists and sprays.
mist region between
4c
3-20 m, knitted wire
Mechanisms of Droplet Removal
Droplets are removed from a vapor stream through a mesh is the most comseries of three stages: collision & adherence to a target, mon type of mist
coalescence into larger droplets, and drainage from eliminator used and
the impingement element. Knowing the size distribu- interception is the
tions as explained above is important because empir- primary mechanism.
At each
curve,
liquid
droplets
strike
plates
Droplet
capture in a
Plate-PakTM unit
Plate-Pak unit
FIGURE 8
THEORETICAL EFFICIENCY VS. VELOCITY FOR VARIOUS
DROPLET SIZES (WATER IN AIR AT AMBIENT CONDITIONS
FOR TYPICAL MESH PADS AND PLATE-PAK UNITS
WITH LIGHT LIQUID LOAD)
Most designers believe that all wire mesh mist eliminators behave basically the same in terms of capacity
and removal efficiency. It is true that for meshes of
same filament diameter, the denser mesh offers superior
removal efficiency. For meshes with differing filament
diameters, a lighter (less dense) mesh may offer
considerably better removal efficiency. The key is that
Operating range is also affected by the liquid loading
the working part of the mesh is the target density, not
(proportion of liquid) of the gas. If too great, the mist
FIGURE 11
It is the amount of targets per unit volume which influences removal efficiency, not the density of mesh (the Selecting the material of mesh style(s) is also important.
greater the number of targets the greater the proba- Corrosion rates as low as 0.005"/year is not serious in
vessel walls but will quickly destroy 0.006" or 0.011"
bility of a successful collision).
wire mesh. Table 2 gives preliminary guidelines, but
In a co-knit such as a metal alloy and fiberglass, the AMACS draws wire and knits mesh with any ductile metal
alloy provides a skeleton for structural support and for special applications.
prevents the high specific surface media from collaps- When applying non-metal materials operating tempering on itself.
ature limits must be considered.
TABLE 2
Mesh Corrosion & Temp. Considerations
the upper end of the range: about 10 fps for plain wire
mesh pads, about 8.5 fps for co-knits, and 14 fps for
Plate-Pak elements. As discussed, effectiveness
drops off at lower velocities as the droplets have
sufficiently low momentum to negotiate paths through
the targets, and at higher velocities because the vapor
carried sufficient kinetic energy to re-entrain droplets.
For typical designs, acceptable velocities range
between 25% to 125% of the ideal value.
The Capacity Factor may be thought of as an indication
of ability of a mist eliminator to drain liquids and avoid
re-entrainment under various conditions. See Table 3
for some typical baseline values.
TABLE 3
Standard Souders-Br
(k factors) for mesh and Plate-Pak Units
Design Equations
Vd = k(L-G/G)1/2
where Vd
k
L
G
=
=
=
=
(1)
Note that Souders-Brown equation provides correction for only gas and liquid densities. Should any
conditions exist which affect drainage or re-entrainment,
the Capacity Factor must be pro-rated as appropriate.
K = [( L- G)Vd 2] / 9 D
(2)
Where K = dimensionless inertial parameter
V = gas velocity in fps
d = Liquid droplet diameter in ft
= Gas viscosity in lb/ft sec
D = Wire or filament diameter in ft
design consideration in certain applications, particularly vacuum systems or larger columns requiring the
movement of great quantities of gas. It has been
shown that each inch of head loss requires some 0.16
hp/scfm. A simple correlation has been developed to
describe the pressure drop through a dry mist
eliminator (no mist):
Use this calculated K value with Figure 12 to find the Pdry = 0.4VD2 GST/gc w
(3)
corresponding value of the impaction efficiency fraction
E. From Table 1, find S, the specific surface area for Where V = Gas Superficial velocity = Ft / Sec
G = Gas Density lbs / ft 3
the mesh style of interest.
Subsequently determine SO of the mist eliminator
perpendicular to vapor flow and with a correction factor of 0.67 to remove that portion of the knitted wire
not perpendicular to the gas flow:
Inlet Diffusers
FIGURE 13
ACTUAL PRESSURE DROP VERSUS VELOCITY FOR TYPICAL AMACS MESH PADS AT LIGHT AND MEDIUM LOADS
Decades ago, Dutch Shell Chemical Company introduced Schoepentoeter style bladed designs (Fig. 14).
As the fluid flows
FIGURE 14
axially towards the
shell opposite of
the inlet nozzle,
liquids are captured by specially
p l a c e d blades.
This design is
superior because it
allows the escape
of liquids over a
much
greater
region of the vessel. A simple inlet diverter ( Fig. 15)
would simply shear bulk liquids into smaller droplets
at great flow rates:
FIGURE 15
AMACS AccuFlow
Inlet Diffuser (Fig.
16) is a similiar
style of the bladed
design in which
the body of the diffuser maintains its
shape, the restriction of flow which
allows the escape
FIGURE 16
Vessel Configuration
FIGURE 17
SIMPLIFIED VIEWS OF TYPICAL MIST ELIMINATOR CONFIGURATIONS IN SEPARATOR VESSELS
There are several modifications to mesh pads and Recall the discussion on pressure drop through a mist
vanes to dramatically enhance performance.
eliminator in which liquid tends to pool in the lower layers
of mesh. The simplest technique to promote drainage
FIGURE 18
is to use a few inches of open, porous mesh such as
AMACS style 7CA (5-lb density with specific surface area
Guidelines for maintaining even flow distribution across
as low as 45 sq-ft/cu-ft) in the upstream position. As
mesh pads or vane units with axial flow in cylindrical vesdrainage occurs through the interstitial regions of the
sels. Height of vessel head is assumed to be 1/4 of vessel
diameter. Flow distribution devices can minimize required
mesh, opening the
disengagement space above mesh pads.
FIGURE 19
knit enhances liquid
Contact AMACS for assistance.
drainage.
An extension of this
approach is to use
higher specific surface
area mesh in downstream positions to
enhance separation
efficiency,
with
intermediate mesh
between the collection and drainage zones. Figure 19
illustrates a multilayer mist eliminator.
10
Mesh-Vane Assemblies
MultiPocket Vanes
Use of Geometry
11
12
Mist Eliminators
Advantages:
No Welding
Figure 3. MistFix
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Amistco Separation Products Inc, and ACS Separations and Mass Transfer Products, are Registered Trademarks of AMACS
13
Our
we
14
FIGURE 24
APPLYING COMBINATIONS OF AMACS MESH PADS
AND PLATE-PAKTM VANE UNITS TO MINIMIZE VESSEL
SIZE
L = 62.4 lb/ft 3
G = 0.60 lb/ft 3
P = 122 lb/ft 2
T = 82F
F = 60 ft 3/sec
Videal = k [ ( L- G) / G]1/2
Videal = 0.27[(62.4-0.60)/0.60] 1/2
Videal = 2.74 fps
The cross-sectional area of mist eliminator is determined by dividing the volumetric flow rate by the ideal
velocity:
Area Mist Eliminator = Volumetric Flow Rate/
Superficial Vapor Velocity
Area Mist Eliminator = [60 ft3/sec]/2.74 fps
Area Mist Eliminator = 21.9 ft2
The corresponding diameter is 63.4", rounded up to a
standard 66" scrubber vessel. Note that performing
the same calculations using a vane (and a capacity
factor of 0.50) yields an ideal vessel diameter of 46.7",
rounded up to a standard 48" ID vessel. To calculate
the removal efficiency at 5 m, several parameters
must be identified to use equation 2 to determine the
inertial parameter K:
15
K = [( L- G)Vd 2]/9 D
K = 0.32 fps
The capacity factor for 12-lb density mesh in this service is ~0.23 0.27, having been de-rated for the high
liquid viscosity of 18 cP (which retards liquid drainage)
and relatively high operating pressure. Using the gas
For ACS style 8P, the specific surface area is
2
3
density,
volumetric flow rate and cross-sectional area
(185 + 36) = 221 ft /ft , we will try both 4" and 6" thick
of the mist eliminator, the actual superficial velocity is
mist eliminator thicknesses (1/3 and 1/2ft):
readily calculated. Next, using known densities of the
gas and glycol, the actual or operating Capacity
SO = 221 x 1/3.14 x 1/3 x 0.67
Factor
k is determined:
SO 4"thick = 15.7 and SO 6"thick = 23.6
= 0.44 fps
For the 6" thick element, the removal efficiency is
84.8%. By using a composite pad containing a 2"
layer of regular monofilament polypropylene, style 8P, A Capacity Factor of 0.44 fps is almost twice as high
upstream of a 2" thick layer of 8PP, mono- and as the optimum, and is in the range of that of an AMACS
multi-filament co-knit, the removal efficiency is 99.9% . Plate-Pak Vane mist eliminator. However, the vane
will not remove particles down to 5 m, so a meshCASE STUDY #2
vane assembly was proposed. The assembly has a
Traditionally, trays are used to bring about contact
multiple layers of mesh. The first layer is composed of
between glycol and natural gas in dehydration conhighly porous mesh (AMACS style 7CA), followed by a
tactors. In recent years, the industry moved towards
layer of the high specific surface area (AMACS style 8DT)
smaller diameter columns by exploiting the higher
co-knit mesh of stainless and Dacron Fibers.
capacities achieved with structured packing.
MisterMesh drainage coils were appended to the
However, the lower capital investment associated with
bottom face of the mist eliminator. Downstream of the
a smaller diameter packed tower is often offset by
mesh was placed a Plate-Pak vane. The total
dramatically increased glycol losses.
thickness was 12" and was accommodated using the
Consider a mid-western sour gas plant operating a same supports as the mist eliminator it replaced.
96" glycol contactor and processing 1,310,000 lb/hr of
gas at 116F and 1214 psia. The gas and liquid specific Carryover from a glycol contactor occurs through two
densities were 4.4 and 68 lb/cu-ft respectively. The mechanisms, evaporative losses and mechanical
plant was experiencing 0.13 US gal of carryover per (carryover losses). In this example, simulations
mmscf, amounting to some 65 gal/day of lost triethylene showed evaporative glycol losses of 0.0054
glycol, several hundred dollars worth per day. A 10" gal/mmscfd. The total losses after the revamp were
thick wire mesh mist eliminator of 12-lb mass density less than 0.008 gal/mmscfd, and carryover losses had
been reduced from 0.13 gal/mmscfd, a 94% reduction!
was installed above the packing.
16
17
18
ADVANCED TECHNOLOGY
FOR DEBOTTLENECKING !
Our MisterMesh Mist Eliminator out performs conventional pads. The drainage rolls
accelerate liquid removal thus increasing
capacity and reducing pressure drop. Used
in conjunction with our Plate-Pak vane,
the MisterMesh drain
rolls can increase capacity
by over 200% while separating droplets down to
3 microns.
Top View
Benefits:
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P rocess design
Equipment design
Equipment fabrication,
installation and commission
Project Objective
Conventionally, the
design of distillation
column internals
involves two main
steps: process design
and optimisation, and
equipment design
design and fabrication would also
evolve from an earlier set of design
operations and drawings.
The process design and optimisa tion step mainly determines how
close the tray geometry is to reaching maximum capacity. However,
in this case, due to the nonavailability of process data, this first
step was bypassed. However,
detailed discussions with the opera tional and process staff of the gas
plant concluded that the column
and existing trays were working to
their satisfaction in terms of capac ity and efficiency, and there were
no plans to either increase or
decrease the units operations in the
near future. Hence, the decision
was taken to duplicate the existing
geometry in new trays.
Since drawings for the existing
trays were not available, an inspection crew consisting of engineers,
designers
and
drafters
was
REVAMPS 2010 37
Tray 1
Tray 2
C
Figure 2. Schematic of a four-pass tray arrangement showing panel designation
Tray geometry
Tower diameter
# of passes
# of valves
Type of valves
Valve lift
Side downcomer width
Centre downcomer width
Off-centre downcomer width
Distance of off centre downcomer from tower wall
Metallurgy
Table 1.
38 REVAMPS 2010
Measurement
156in
4
1056
0.4395in
11.75in
12in
12in
43.125in
SS 304L, 14 Ga./12Ga.
11.75in (30cm), the centre downcomer widths were 12in and the
off-centre downcomer widths were
also 12in. At the same time, and
based on the recovery of some
material from the scrap yard, some
of the downcomer panels were
reassembled, to the point where it
was possible to verify these dimen sions. It proved interesting to note
that the judgment made through
chord lengths matched closely the
widths of the downcomer panels.
Measuring between the support
rings provided an idea of tray spac ing. An inspection of the tray panel
indicated that the trays were round
floating valves with 0.4375in (1.1cm)
lift and they were 1056 in number.
Following discussions with the
operator to confirm that the existing
trays did not have any operational
problems, the tray layout was
decided upon, considering that the
existing trays were operating in
froth regime and there was no
excessive entrainment, excessive
downcomer backup or excessive
downcomer choke, with reasonable
pressure drop. Although some
corrosion and fouling was observed
on the trays, it was felt that their
condition was acceptable following
a five-year ????.
The column was required to oper ate in different cycles with varying
gas rates. As a result, the percent age turndown would be most
important. Hence, the decision was
taken to continue using floating
valves.
Given that this tower has fourpass trays, balancing the number of
passes is critical, to avoid poor
distribution of vapour and liquid,
which would reduce the efficiency
and/or the capacity of the trays. It
is important to ensure that the
vapour and liquid contact each
other uniformly across each panel
and to make sure that the vapourto-liquid ratio is as close to unity
on each of these panels. All fourpass trays have two different sets of
configurations. One set consists of
two side downcomers and a centre
downcomer, while the other set
consists of two off-centre downcomers, and these alternate in a
given column. As a result, the trays
will have four active panels, with
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Conclusion
path length
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REVAMPS 2010
39
THREE
PHASE
IN
GAS OUT
THREE
PHASE IN
GAS
OUT
LIQUID LEVEL
36" ID
LIGHT
PHASE
OUT
16"
INTERFACE
LEVEL
30"
60" ID
LIQUID LEVEL
HEAVY
PHASE
OUT
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LIGHT
PHASE
OUT
Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Stokes Settling Using Gravity . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Basic Design Concepts The Emulsion . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Basic Design Concepts Operating Principles of a Coalescer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Basis for Sizing and Selection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Intra-Media Stokes Settling . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Direct Interception . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Gravity Separation Downstream of a Coalescer Element . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Coalescer Congurations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Case Studies
-Oil-Water Separators - Environmental Response . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
-Gas Plants . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12
-Alkylation Units . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
-Oil/Water Separator on a Production Platform . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .14
-Upgrading a Three-Phase Separator . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .15
General References . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16
Ranges of Application for Coalescing Media . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16
AMACS Oil / Water Separators utilize patented* technology to separate oily waste water.
Applications include oil spill clean up for marine, power plants, reneries, vehicle terminals, and
countless others. The separated water is puried for
direct sewer or ocean discharge. The oil is captured
1992 Vaaler Award
and recycled.
for AMACS
Oil-Water Separator
20L x 8W x 9-6"H
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COALESCER DESIGN MANUAL
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Introduction
flowing and the opposing forces of buoyancy and viscous drag balance (Figure 1), the droplet has achieved
its Terminal Settling Velocity. This vertical velocity is
constant because there are no net forces acting upon
the droplet. This mechanism of separating liquids by
gravity is called Stokes Settling after the nineteenth
century English researcher Sir George Stokes.
(1)
LIQUID-LIQUID
COALESCER DESIGN MANUAL
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With Coalescer Media and Internals, unit performance can be restored. Typical applications include:
Upgrading 3-Phase Separators
and Decanters
FIGURE 2
VOLUME FRACTION FREQUENCY DISTRIBUTIONS
FOR DISPERSIONS OF VARIOUS MATURITIES
LIQUID-LIQUID
COALESCER DESIGN MANUAL
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Source
Stability
Droplet Size
Range
Weak
100-1000 microns
Moderate
50-400 microns
Strong
10-200 microns
0.1-25 microns
1000
FIGURE 4
ZONES WHERE DIFFERENT
COALESCING MECHANISMS APPLY
100
10
0.1
0.1
Table 1
10
100
1000
depend on Intra-Media Stokes Settling confine the disLiquid-Liquid Coalescers are used to accelerate the tance a droplet can rise or fall between parallel plates
merging of many droplets to form a lesser number of or crimps of packing sheets (Figure 5). This is comdroplets, but with a greater diameter. This increases pared to simple gravity separators in which the travelthe buoyant forces in the Stokes Law equation. Settling
FIGURE 5
of the larger droplets downstream of the coalescer
element then requires considerably less residence
OIL DROPLETS RISING TO A COLLECTION SURFACE
time. Coalescers exhibit a three-step method of operaL
tion as depicted in Figure 3.
FIGURE 3
THREE STEPS IN COALESCING
Submicron droplets
flow around target Several captured droplets
coalesce, forming larger
drops...
Droplets strike
target and adhere
...which trickle down
and fall, becoming
separated
LIQUID-LIQUID
COALESCER DESIGN MANUAL
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Porosity
(20-110
m
High Pressure Drop
Polymer
Mixing Valves
Capillarity
Haze from Cooling in
Glass Mat,
Bulk Liquid Phase,
Co-Knits of
7.5-45
Liquid Phases:
1-25
Surfactants Giving
Wire &
(20-110 m3/hr/m2)
Emulsions with Very
Continuous/Dispersed
Fiberglass
Low Interfacial Tension
Interfacial Tension
Continuous/Dispersed
Media
Hydro/Oleophilic Porosity Target Size Fouling/Cost
Density Difference
Metal/Plastic
H/O
98-99%
3/8" - 1"
Low/Low
Spacing/Crimps
Corrugated Sheets
Continuous Phase Viscosity
Superficial Velocity
.002" - .011"
Wire/Plastic Mesh
H/O
95-99%
FIGURE 6
Wire Wool
Coalescers work better in laminar flow for several reasons. First, as mentioned above,
8 - 10 micron
High/High
Wire/FG Co-Knits,
H
92-96%
droplets will stay in the streamlines around a
Glass Mat
wire or fiber target. Second, high fluid velocities
Table 2
overcome surface tension forces and strip
droplets out of the coalescer medium. This results in reStep 2 Droplet Coalescence
The second step is to combine, aggregate, or coa- entrainment in co-current flow and prevents droplets
lesce captured droplets. Increasing the tendency for from rising/sinking in counter-current flow. Lastly, slowdroplets to adhere to a medium, increases the proba- er velocities result in greater residence time in the
bility that subsequent droplets will have the opportuni- media and therefore more time for droplet-to-target
ty to strike and coalesce with those that already have impact, droplet-to-droplet collisions, and Intra-Media
Stokes Settling.
Wire/Polymer
Co-Knits
94-98%
21-35 micron
LIQUID-LIQUID
COALESCER DESIGN MANUAL
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Separation
Time
< 1 minute
< 10 minutes
Hours
Days
Weeks
Emulsion
Stability
Very Weak
Weak
Moderate
Strong
Very Strong
Droplet Size,
Microns
>500
100-500
40-100
1-40
<1 (Colloidal)
For liquid-liquid coalescers, as with any process equipment, successful sizing and selection is always a
combination of empirical observation/experience and
analytical modeling. Of the three steps in coalescing
droplet capture, combining of the collected droplets,
and gravity separation of the enlarged droplets the
first and the last can be modeled with good accuracy
and repeatability. The modeling of the middle and the
actual coalescing step is a complex function of surface
tension and viscous effects, droplet momentum, and
the dynamics of the sizes of the droplets in the dispersion. This has been done successfully in porous
media, but is beyond the scope of this brochure.
Droplet capture, the first step in liquid-liquid coalescing, is the most important. The next two sections
describe the formulas used for the collection mechanisms of Intra-Media Stokes Settling and Direct
Interception.
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COALESCER DESIGN MANUAL
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VC = (C1) Q h
( S.G.) d2
(2)
In a horizontal 3-phase separator, in order for efficient separation to take place, droplets of some min- Where
imum size which exist in both the gas and the liquid
VC = Coalescer volume, cubic feet
phases must be captured within the equipment.
When coalescing media is installed in the lower segment
C1 = 164 for Plate-Pak w/horizontal sheets
of the vessel, the furthest a droplet has to travel is
219 for STOKES-PAK w/horizontal sheets
from plate to plate or sheet to sheet, rather than
312 for STOKES-PAK w/vertical sheets
down from the liquid level to interface level and/or up
Q = Liquid/liquid emulsion flow, US GPM
from the vessel wall to the interface level (depending
whether the dispersed phase is heavier or lighter
h = Corrugated plate spacing or structured
than the continuous phase).
packing crimp height, inches
AMACS offers a number of Corrugated Plate Interceptors
d = Minimum droplet diameter, microns
(CPI) to enhance coalescence, such as Plate-Pak and
= Continuous phase viscosity, centipoise
STOKES-PAK crimped sheet packing (Figure 8).
FIGURE 8
COALESCING MEDIA THAT
DEPENDS ON STOKES SETTLING
h=
Emulsion
Clear liquid
Plate-Pak
Axis of Corrugation
Axis of Corrugation
9b
Stokes-Pak with
Horizontal Sheets
h
1/2"
Axis of Corrugation
Stokes-Pak
9c
They make more efficient use of a vessel volume than
a straight PPI (Parallel Plate Interceptor) since more
metal is used and the specific surface area is greater.
It can be shown from Equation 1 for Vt that the volume
of media necessary to remove virtually all droplets
equal to a minimum, typically 30-60 microns, is given
by:
Stokes-Pak with
Vertical Sheets
1/2"
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COALESCER DESIGN MANUAL
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In order to decrease solid retention the axis of the cor- can be found by trial-and-error substitution of the terminal
rugations of Plate-Pak should be parallel to the flow. settling velocity from Equation 1 into Equation 3 below
However, vessel geometry often necessitates that the
s = (vt/h)/ (vs/L) = .999
corrugations be perpendicular to the flow, especially in
(3)
round vessels. Due to its light, self-supporting struc- where
s = Fractional Collection Efficiency
ture and ease of installation, the overall project cost is
by Stokes Settling
normally less for STOKES-PAK than Plate-Pak when
vs = Superficial Velocity
L = Element Length
vt/h = Droplet Rise Time
vs/L= Droplet Residence Time
FIGURE 10
GAS OUT
OIL OUT
ADJUSTABLE
OIL WEIR
ADJUSTABLE
WEIR
OIL
WATER
OUT
FLOW
DISTRIBUTION
BAFFLE
WASTEWATER
INLET
In horizontal flow when this length is over four elements, ~32" (813 mm), the coalescer is usually split in
two or more beds with intermediate spacers or spacer
rings. Also, cross-flow designs are often used in this
situation to allow for more frequent removal of the
collected dispersed phase.
Direct Interception
SOLIDS
DRAIN
SOLIDS
DRAIN
(4)
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COALESCER DESIGN MANUAL
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FLOW
FIGURE 12
(5)
Coalescer
D
microns/in.
Wastewater
Sheen
4.5
0.037 .04
Fiberglass Mat
Fiberglass Co-Knit 8.9/0.00035 0.027 .02
Interceptor-PakTM
Caustic
Wash Drums
11.0
Teon
21/0.00083 0.019 .07
Co-Knit
Interceptor-PakTM
Impeller
Mixers
12.5
Polyester
24/0.00095 0.021 .07
Co-Knit
Interceptor-PakTM
Mixing
Valves
22.0
Wire
50/.002
Wool
Interceptor-PakTM
0.028 .40
Extraction
Columns
79.0
Knitted
152/.006
Mesh
Interceptor-PakTM
0.014 .60
Table 3
LIQUID-LIQUID
COALESCER DESIGN MANUAL
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FIGURE 13
Successful gravity separation downstream of a coalescer element depends primarily on vessel geometry.
Various schemes are used with horizontal vessels
depending on whether there is a significant amount of
gas present as with Three-Phase Separators (Fig. 14A)
and/or the volume percent of the dispersed phase. The
formation of a wedge between a coalescer and a sharp
interface level as seen in Fig. 14B is well documented.
A boot is desirable when the amount of dispersed phase
is <15% v/v (Fig. 14C) where the control of the interface
level is linear with the volume of dispersed phase discharged. A dispersed phase velocity of 10 inches (254
mm)/minute is desirable to allow disengagement of the
continuous phase, while keeping the boot diameter
<40% of the diameter of the horizontal portion to minimize the necessity for weld pads. The most common
applications for coalescers in vertical flow are
extraction/liquid-liquid absorption towers (Fig. 14D)
and entrainment knockout installations (Fig. 14E)
where the available plot plans in the plant are at a pre-
UMax = 0.78 | |
(6)
Where
UMax =Emulsion velocity, feet/minute
| | =Absolute value of the difference
between the densities of the
continuous and dispersed
phase, pounds/cubic feet
=Continuous phase viscosity,
centipoise
The successful design of a liquid-liquid coalescer starts
with knowledge of the source of the emulsion and the
streams physical properties. It has been shown that a
combination of empirical experience and analytical
modeling of available coalescing media based on
removal of 99.9% of a minimum droplet size can then
be used to predict allowable entrainment concentrations
in the effluent stream. Once the coalescer is properly
located in an existing or new vessel a project that has a
high rate of return is achieved that gives many years of
reliable service.
LIQUID-LIQUID
COALESCER DESIGN MANUAL
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COALESCER
FIGIRE 14 D
Congurations
Vertical Coalescers
Coalescer
Heavy
Stream
In
Horizontal Coalescers
FIGIRE 14 A
Trays,
Packing
or Agitated
Internals
Inlet Device
Plate-Pak
Mist Eliminator
Vapor
Outlet
Light
Stream
In
Flow
Hydrocarbon
Two
Liquid
Phases
Hydrocarbon
Aqueous
Coalescer
Aqueous
Outlet
FIGIRE 14 E
FIGIRE 14 B
2-Phase Horizontal Coalescer Vessel
Emulsion In
Wedge
Hydrocarbon
Outlet
Light Product
Light
Stream
Out
LC
Liquid
Distributor
Coalescing
Medium
Coalescer
Heavy
Product
FIGIRE 14 C
2-Phase Horizontal Coalescer Vessel with Boot
Emulsion In
Light Product
Emulsion
In
LC
Heavy
Dispersed
Phase
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COALESCER DESIGN MANUAL
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10
CASE STUDY #1
K=
=
1.083
According to Table 3 fiberglass co-knit can remove
99.9% of all droplets 4.5 microns and larger.
Therefore
D = 0.02 (1-.027)(4.5/8.9)
1.083 (1+(4.5/8.9))
= 0.00305
L = (.00035") (1-.027)ln (1-.999)
-4(0.00305) 0.027
= 22.4"
For safety each stage was supplied with a
24" thick fiberglass co-knit element.
FIGURE 15
Vc
=
=
Dual
Pre-Filters
LC
Advanced
Capacitance
Probes
Oily
water
drawn in
by suction
LC
Water
FC
Solvent
Injection
Solvent
Injection
In order to meet stringent EPA regulations for discharging wastewater overboard, two stages of A M ACS
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COALESCER DESIGN MANUAL
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11
CASE STUDY #2
162(45) 42 (.11)
(.818-.496)302
70F
Gas-Gas
Exchanger
25F
Hydrocarbon Vapor
Flash Tank
Lean
Glycol
J-T Valve
Steam
COLD SEPARATOR
WITH COALESCER
AT 250 PSIG
Reboiler
Condensate
LC
Rich Glycol
Make-up
Ethylene Glycol
Lean-Rich Exchanger
Lean Glycol
Rich
Glycol
Pump
Lean Glycol
LIQUID-LIQUID
COALESCER DESIGN MANUAL
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12
1.251 (1+(15/21))
14.3"
= 0.0163
FIGURE 17
COALESCER IN ALKYLATION UNITS
HYDROCARBON OUT
15"
STAGE 2
Teflon Multifilament Co-Knit
180" DIA.
HC/
ACID
IN
60" T/S
180" T/T
72" I.D.
CASE STUDY #3
Hydrocarbon
Acid
Liquid
Distributor
V.B.
Acid Out
Drain
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COALESCER DESIGN MANUAL
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13
Case Study #4
7.1"
FIGURE 18
VERTICAL 10,000
BPWD PRODUCED
WATER OIL SKIMMER
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COALESCER DESIGN MANUAL
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14
Case Study # 5
FIGURE 19
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COALESCER DESIGN MANUAL
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15
Plate-Pak
Coalescer
Wire Mesh
Interceptor-Pak
Teflon Fiber
Interceptor-Pak
Fiberglass
Interceptor-Pak
125 micron
75 micron
15 micron
7.5 micron
Human hair
Mist
Fog
Bacteria
Three-Phase
Separators
Static
Mixers
Extraction
Columns
Two-Phase
Pump Discharges
Mix
Valves
Caustic Wash
Drums
Condensation
in Pipelines
Anti-Foam
Surfactant
Stokes-Pak
Wire Wool
Interceptor-Pak
Polyester Fiber
Interceptor-Pak
General References:
Paragon Engineering
Services, Produced Water
Theory and Equipment
Description, Houston, TX.
Lieberman, N. P.,
Troubleshooting Process
Operations,
3rd Edition, PennWell Books,
Tulsa, OK, 1991.
Fiberglass Mat
Interceptor-Pak
Structured Packing
Applications:
Quench Towers in Steel Mill
Coker Fractionator wash section
Atmospheric Crude Unit wash section
Crude Vacuum Unit was section
40Y
40X
64Y
64X
40
40
64
64
228
228
231
231
AMACS Corrugated Grid Packings are constructed with rigid sheet metal,
held together with studs, allowing it to be replaced easily when
necessary. Manufactured to the industry standard design, corrugated
packing is available in a wide range of steel and alloy materials to
handle high fouling services.
.
AMACS
manufactures a full line of tower internals, mist eliminators and
other complimentary components critical to effective mass transfer
and separations. For more information regarding these products.
please visit our website www.amacs.com, or call to speak to one of
our product specialists.
AMACS Orifice Type Liquid Distributors are mainly suitable for low turn-down ratios.
Three basic types are available Plate Type, Pan Type for smaller sized towers and Ladder
Type.
For the Plate and Pan Type distributors, the gas flows through risers that are either round
or rectangular in shape. The liquid collects on the deck and flows through the orifices to
the packing. In Pan Type designs, the gas also flows through the annulus between the
distributor and the vessel. By varying the size and number of orifices, the distributor can
be made adaptable to a wide range of flow rates.
For high-efficiency designs, AMACS can provide drip tubes instead of orifices. Ladder Type
distributors are suitable for liquid feed under pressure, and where limited space is available
for the distributor. These provide a high amount of free area for gas flow and uniform liquid
distribution over the entire tower cross section.
All types are available in diverse materials metals, thermoplastics and FRP. The basic
distributor design can be modified for use as either Redistributors or Liquid Collectors.
For Redistributors hats are incorporated on top of the risers, while with Liquid Collectors
the orifices are not provided. Other variants include adding anti-migration bars at the
bottom of the distributors that eliminate the need for separate bed limiters.
Ladder Type
Plate Type
Distributors
Benefits:
Uniform liquid distribution
Low vapor phase pressure drop
High resistance to fouling
Minimal liquid resistance time
Optimal use of vessel height for
proper performance
Mixing capability for distribution
to other beds
Pan Type
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Amistco Separation Products Inc, and ACS Separations and Mass Transfer Products, are Registered Trademarks of AMACS
AMACS Weir Type Liquid Distributors effectively handle a wide variety of gases and
liquids. They feature a series of closed end troughs that have slots through which the
liquid is uniformly dispersed over the packed bed. Liquids feed evenly to one or more
of the parting boxes, which in turn distribute the flow to the troughs. The parting boxes
receive the liquids through sparger type feed pipes. The tower diameter and the liquid
flow determine the number of parting boxes. Up to three parting boxes may be required
depending upon tower size and flow rates. Mid-span supports are required for 120 and
larger sizes. Typical turn down ratio for LDWs is 4:1.
AMACS LDWs are self-cleaning, resistant to fouling, and are suitable for liquids with
high solids content.
AMACS offers other variations in the distributor design including:
Distributors with high drip density for low liquid flows
Rectangular slots with flow guides for precise liquid control
AMACS Separation Products, Inc. manufactures a full line of tower internals, mist
eliminators and other components critical to effective mass transfer and separation. For
more details regarding these products, visit our website or consult with an AMACS
Distributors
Benefits:
Uniform liquid distribution
Low vapor phase pressure drop
High resistance to fouling
Minimal liquid resistance time
Optimal use of vessel height for
proper performance
Mixing capability for distribution
to other beds
Separations representative.
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Amistco Separation Products Inc, and ACS Separations and Mass Transfer Products, are Registered Trademarks of AMACS
Random Packing
Applications:
CO 2 removal
Name
#1
#1 /2
#2
#3
1
Size
mm.
30
45
60
90
Gas dehydration
Demethanizing
Tall oil fractionating
Number of Pieces
ft3
m3
847
29,900
266
9,390
104
3,670
31
1,090
Free Space
%
97
97
98
98
Packing
Factor F
43
26
18
15
The AMACS AIPR tower packing high strength geometry makes them well suited to deep beds. AIPR tower packings are
available in a wide range of metal and alloy materials. AMACS Process Tower Internals, manufactures a full line of tower
internals, mist eliminators and other components critical to effective mass transfer and separation. For more details regarding
these products, visit our website or consult with an AMACS Separations representative.
1-800-231-0077
www.amacs.com
Amistco Separation Products Inc, and ACS Separations and Mass Transfer Products, are Registered Trademarks of AMACS
Mist Eliminators
Advantages:
No Welding
Figure 3. MistFix
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Amistco Separation Products Inc, and ACS Separations and Mass Transfer Products, are Registered Trademarks of AMACS
Mist Eliminators
Benefits:
Increases machine tool life
Cleans your recycled oil and other
industrial fluids
Removes metal contaminants from coolants
Applications
Oil Filtration
Fuel Filtration
Filters
Solvent Filtration
Chemical Filtration
Metal Cutting Fluids
Oily Wastewater Filtration
.006 In
Dia Wire
10
20
30
.011 In
Dia Wire
15
30
40
1
P 3/4
(PSI)
1/2
.006 In
Dial Wire
10 lbs.
7 lbs.
4 lbs.
To clean,
simply backwash
1/4
.011 In
Dial Wire
8 lbs.
3 lbs.
2 lbs.
10
20
30
40
Micron Rating
NOTE: Based on 20 gpm/per F2
NOTE
1
Refer to particle size for 99.9% removal
2
Based on 9 O.D. 36 L. filters standard
RMF-1-10
RMF-2-20
RMF-3-25
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80%
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60%
Amistco Separation Products Inc, and ACS Separations and Mass Transfer
Products, are Registered Trademarks of AMACS
P
(PSI)
Structured Packing
Applications:
High Purity Product distillations
(fragrances, flavors, dyestuff
intermediates, fluorinated
hydrocarbons, lubricating oil
additives, specialty monomers,
pesticides, rubber processing)
Mass transfer (de-aeration,
carbonation)
Solvent and Byproduct recovery(resins, coatings, fibers, films,
pharmaceuticals, plasticizers, and
custom distillations)
Scrubbing (sulfur recovery, air
purification)
PACKING DATA
Packing
Style
Strand
Diam., in.
Density
lbs3 ft.
Pct. Void
Vol.
Sp. Surf.,
ft2 per ft3
AKSP-12
0.0045
27.5
94.5
580
AKSP-8
0.0045
20.0
96.0
420
The AKSP Structured Packing is available in a wide range of metal and alloy materials. For availability and lead times consult the factory.
AMACS Separations Products, Inc. manufactures a full line of tower internals, mist eliminators and other components critical to effective mass
transfer and separation. For more details regarding these products, visit our website or consult with an AMACS Separations representative.
1-800-231-0077
www.amacs.com
Amistco Separation Products Inc, and ACS Separations and Mass Transfer Products, are Registered Trademarks of AMACS
Liquid/Liquid Coalescers
Mist Eliminators
Applications:
Oil-water separations
Removal of aqueous solutions
from hydrocarbon streams
Removal of haze from fuels
Enhanced separation of reflux
streams
Three phase separations
Advantages:
Dry Oil
Wet Oil
AMISTCO Coalescer
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Amistco Separation Products Inc, and ACS Separations and Mass Transfer Products, are Registered Trademarks of AMACS
M ist Eliminator
Installation Guide
Table of Contents
New Mist Eliminator Inspection
6-8
I n s ta l l a ti o n
9 - 13
14
Tr ou bl es h ooti n g
15
Please Note:
lines or a
ensure a snug
between the
to any
diminish
and hamper
eliminator performance.
Step One
Check the Shipment
Always make sure you have the right
mist eliminator for the job prior to
doing anything, especially removing
the old mist eliminator. Always
check your shipment to make sure
you have received the correct size
and installation hardware (if
ordered with the job) and for
potential mist eliminator damage.
U pon receipt of an AMACS mist
eliminator, inspect and verify the
dimensions. Also check for any
hardware and documentation that
Ready to Install
Lay out the sections of the mist
eliminator in a clean area close to
the vessel. For dual density pads,
check tags for correct orientation
of ow direction.
term storage.
rm you have
the drawing.
into vessel.
Step Two
Safety Considerations:
t P rior to entering any vessel, it is
important that
space
snug
J-Bolts
L atch Keys
the
Flag
Please Note:
Bottom Grid
or locknuts.
Top Grid
Wire M esh
tie
Caution:
If your mist eliminator is installed
in a critical or severe service,
AMACS recommends a more
secure hold down method. Check
with your AMACS sales representative about optional relief
doors, heavy duty grids and other
special features.
Tie Wires
J-Bolts
Offset Rings
rings are held away from the
Secure
vessel wall by a
Through Bolts
Relief Doors
D ual Support Rings
Gas
Re movable Section
of Support Ring
Relief Door
Relief door moves up and
down on the guide rods.
B asket Cages
Expansion Rings
e. You simply
pieces intact.
shell is a problem.
E xpansion Ring
to adjacent sections.
Step Three
Installation
indicate where each section edge should sit. Align the sections in
accordance to your marks as you install each section.
2. Work from the outside in on each side by placing the end sections
1. Before installing any sections, mark lines on the support ring that
Please Note:
it in. Keep
is neces-
L arge Pads :
For large pads, total compression can be several inches. It is very
to work out all of the compression when installing the last section.
AMACS recommends this easy method: Loop tie wire around adjacent
grids as the sections are installed. This loop should be close to the down
rods, where the mesh is xed to the grids. Twist the tie wire, pulling the
grids towards each other, until the grids of each section are spaced 1 1/ 2
apart. Using this procedure will ease installation of the last sections.
10
thin pieces of sheet metal or some smooth yet strong material that
extends the length of the section and is taller than the section.
You may even wish to cut handles in the aid. Place the installation
aids on either side of the mesh to reduce the friction of the mesh
surfaces. A compression
you push the
11
2. Work from the vessel wall toward the center aligning each
3. To install the
thin pieces of sheet metal or some smooth yet strong material that
extends the length of the section. You may even wish to cut handles
in the aid. Place the installation aids on either side of the mesh to
is
section into
Top View
12
In this
section remains.
thin pieces of sheet metal or some smooth yet strong material that
extends the length of the section. Place the installation aids on
either side of the mesh to reduce the friction of the mesh surfaces.
A compression
section into place. Push the section in and pull the aids out.
Final Notes:
2
correct ow orientation.
4. Be sure to remove all tools
before start-up.
13
Removing Fouled
M ist Eliminators
for Cleaning
plugging severely
mist elimi-
plugging issues.
14
Important Note:
y.
Troubleshooting
M onitoring pressure drop across
When pressure drop decreases across the mist eliminator, there are
likely holes or voids in the pad or
Corrosion over time will reduce the mesh wire diameter, mesh
density and in turn reduce pressure drop. Gaps in the mesh pad will
cause channeling and a
reduction in collection
y.
Note:
For mist eliminator design and
performance information, ask for
the AMACS Mesh and Vane Mist
Eliminator brochure.
15
come to AMACS Process Tower Internals. With the full range of separation
products, we
RANDOM PACKINGS
STRUCTURED PACKING
LIQUID/LIQUID COALESCERS
INSERTION MISTFIX
MIST ELIMINATOR
LIQUID DISTRIBUTORS
INLET DISTRIBUTORS
TRAYS
TURNKEY POLLUTION
CONTROL PACKAGES
14211 Industry Street, Houston, TX. 77511 Ph: 713-434-0934 Fax: 713-433-6201
e-mail: amacs@amacs.com www.amacs.com
Random Packing
AMACS
AMACS Raschig Ring Packing is proven in a wide range of
mass transfer applications. A full range of Raschig Ring sizes
and materials are available to tackle a wide range of separation
applications.
handles heavy
The AMACS Raschig Ring structure provides one of the largest
among tower packing options and surface areas loading,
process upsets and temperature shocks.
Applications:
Petrochemical distillation and
extraction applications
in
Absorption gas processing
and combustion plants
Desorption in water treatment
PACKING DATA
Size
in.
1/4
1/4
5/16
3/8
3/8
1/2
1/2
5/8
3/4
3/4
1
1
1 /4
1 /2
2
2 /2
3
1
Size
mm
6
6
8
10
10
13
13
16
19
19
25
25
32
38
51
64
76
Weight*
lbs/ft3
91.5
132.0
61.0
51.0
95.0
75.0
136.0
129.0
52.0
94.0
39.0
71.0
62.0
53.0
49.0
37.0
20.0
Weight*
kg/m3
1466
2114
977
817
1522
1201
2179
2066
833
1506
625
1137
993
851
785
593
320
Surface Area
ft2/ft3
213.3
215.6
191.8
152.2
153.9
130.9
132.1
106.6
91.4
92.5
67.0
68.2
53.1
45.7
39.6
33.5
22.8
Surface Area
m2/m3
700
707
629
499
505
429
433
350
300
303
220
224
174
150
130
110
75
Free Space
%
72
68
91
89
81
85
84
87
89
83
92
86
87
89
90
92
95
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Amistco Separation Products Inc, and ACS Separations and Mass Transfer Products, are Registered Trademarks of AMACS
High Capacity
Mist Eliminator
Greater Throughput
Higher Liquid Loads
Improved Separation Efficiency
High Performance for micron size fog
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Amistco Separation Products Inc, and ACS Separations and Mass Transfer Products, are Registered Trademarks of AMACS
AMACS Plate-Pak
Vane Mist Eliminators
Multipocket Vane
AMACS Multipocket Vane features a revised pocket design which enhances droplet
capture while being less intrusive in the gas flow path. This allows greater liquid
capture with less in-pocket turbulence and shearing while also reducing the inherent
pressure drop.
The 8 thickness allows easy application with minimal adaptation of existing
systems. With no tack welds or loose pieces, every part of the vane is securely
through bolted eliminating the possibility of weld failure.
The Multipocket Vane is truly bi-directional. The inlet and outlet sides are
symmetrical about the centreline, greatly simplifying installation. For models without
a flow distribution plate, the inlet and outlet sides are identical. During prototype
testing, test pieces run in both directions confirmed that performance remained
consistent with the initial orientation.
Applications:
Gas processing facilities
Inlet to gas production facilities
Compressor protection
Gas gathering stations
The Multipocket Vane is also available with perforated flow distribution plates.
For optimum performance the plate should be located on the upstream side of the unit.
0.2
0.4
0.6
0.8
1.2
6.00
0.100
0.090
0.080
0.070
4.00
0.060
3.00
0.050
0.040
2.00
0.030
5.00
0.020
1.00
0.010
Greater efficiency
Reduced pressure loss
8 Standard thickness for easy retrofit
Bi-Directional Flow easily reversible
for field installation
0.000
0.00
0
0.2
0.4
0.6
0.8
1.2
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Amistco Separation Products Inc, and ACS Separations and Mass Transfer Products, are Registered Trademarks of AMACS
Tower Internals
To support packing and aid in gas/liquid distribution, AMACS offers a wide variety of
packing support plates. These supports are available for both random and
Benefits:
structured packing.
This design supports random packing and aids liquid distribution without impeding
gas flow. The support plate consists of a series of perforated arches. The vapor
passes through the slots in the arches while liquid passes through the slots in the
deck. Normal pressure drop across the plates is usually below 1/4 W.C. with the slot
area being 80% to 110% of the tower cross-section area. The support plate rests on
support ledges which are welded to the tower. Clamps and mid-span beams are
available as required. Bed depths of 30 feet and higher can be achieved using gas
injection type supports.
Grid type packing supports are used for structured packing to provide a horizontal
contact surface and to prevent distortion of the packing. This design can also be
considered for random packing. A wide range of openings is available to prevent the
packing from falling through. The supports typically rest on support ledges. For larger
towers with manways, sectional designs are standard.
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Amistco Separation Products Inc, and ACS Separations and Mass Transfer Products, are Registered Trademarks of AMACS
Random Packing
Applications:
Absorption
Aeration
Degassing
Desorption
Distillation
Stripping
Heat Recovery
Extraction
Packing Data
Size
in
5/8
1
1 /2
2
1
Weight
LB/c F
30.78
24.23
20.16
19.15
Surface Area
ft2/ft3
100
61
39
30
Free Space
%
93
94
95
96
n umber
(Pcs./ft3)
5882
1374
374
164
AMACS Separation Products, Inc. manufactures a full line of tower internals, mist eliminators and other components critical to effective mass
transfer and separations.
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Amistco Separation Products Inc, and ACS Separations and Mass Transfer Products, are Registered Trademarks of AMACS
ACRR
Applications:
Halogen acid processing
Hydrofluoric acid manufacturing
Phosphate fertilizer manufacturing
Sodium/potassium hydroxide
scrubbers
Applications involving high
thermal shock
Packing data
Size
in
Size
mm
Weight*
lbs/ft3
Weight*
kg/m3
Surface Area
ft2/ft3
Surface Area
m2/m3
Free Space
%
Wall
Thickness in.
3/4
19
34
546
75
244
67
1/8
25
27
433
57
185
74
1/8
1 /2
38
34
546
38
124
67
1/4
51
27
433
28
91
74
1/4
76
23
369
19
62
78
5/16
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Amistco Separation Products Inc, and ACS Separations and Mass Transfer Products, are Registered Trademarks of AMACS
Saddle Ring
Saddle Rings were originally introduced to the industry under the product
Applications:
name IMPT Intalox Metal Tower Packing, a registered trademark of KochGlitsch, LP. Today, AMACS offers a similar high performance, third
generation random packing in primarily 304SS and 316SS metal alloy for
distillation
of saddle and ring styles into one high performance packing. Its unique
Demthanizer / deethanizer
ensuring the randomness and optimum surface area within the packed bed,
while the internal fingers, arches and vanes promote optimum interfacial gas/
liquid contact with minimal drag or hold-up.
Available in various sizes, this random packing type allows for combinations
of efficiency and pressure drop and can be fabricated from a variety of
metals.
High capacity and low pressure drop allow for smaller column diameter.
High efficiency and capacity
High mechanical strength
Available in a variety of sizes and materials
PACKING DATA
AHPP
Style
AHPP 25
AHPP 40
AHPP 50
AHPP 70
Number of Pieces
Per ft3
3,825
1,420
416
131
Surface Area
ft2/ft3
Free Space
%
Packing Factor
F
68
47
30
18
96.7
97.3
97.8
98.1
41
25
16
13
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Amistco Separation Products Inc, and ACS Separations and Mass Transfer Products, are Registered Trademarks of AMACS
Structured Packing
Applications:
AMACS Structured Grid Packing (ASGP) is a good choice for applications
that have fouling, erosion, coking and process upset tendencies. ASGP is
extremely structurally durable and has a high void space percent suiting it
Coker Fractionators
The AMACS structured grid packing surface design reduces coking and fouling
due to stagnant overheated droplets by providing rapid drainage. For the most
Resid Cracker
part, the rapid drainage of ASGP makes it self-cleaning. The grids install in
successive layers. They can be removed and cleaned, or replaced, easily
standard design and is available in a wide range of steel and alloy materials
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Amistco Separation Products Inc, and ACS Separations and Mass Transfer Products, are Registered Trademarks of AMACS
ribbon or strip
n B1-type packing uses a cold rolled sheet metal
ribbon or strip
n M-type packing has a curved shaped crimping
phase
n uniformly operating vapor and gas distributors
n wall wipers to avoid bypass flows and to
MONTZ-PAK TYPE A3
SPECIAL WIRE MESH PACKING TO FRACTIONATE THERMALLY INSTABLE SUBSTANCES UNDER VACUUM
Materials
n very low liquid loads (< 100 l/m /h) are possible
2
Applications include:
Corrugation angles:
n ethereal oils
n isomer mixtures
n fatty acids
Fractionating stages
n fatty alcohols
Assembly
Structure of a Montz-Pak
Type A3-500 with a diameter
of 3000mm
PAK-TYPE
SPECIFIC SURFACE
A3-500
500
A3-750
750
m2/m3
A3-1000
1000
A3-1200
1200
A3-1500
1500
A3-1900
1900
MONTZ-PAK TYPE B1
THE EFFICIENT METAL SHEET PACKING
Column Data
n high throughput
n high flexibility
Revamping
specific surface
Applications
n vacuum columns
n normal and high-pressure columns
n absorption of components and pollutants from gas
n petrochemical columns
Assembly
PAK-TYPE
SPEC. SURFACE
m2/m3
B1- 65
65
B1- 65.60
65
B1-125
125
B1-125.60
125
B1-150
150
B1-150.60
150
B1-200
200
B1-200.60
200
B1-250
250
B1-250.60
250
B1-300
300
B1-300.60
300
B1-350
350
B1-350.60
350
B1-500
500
B1-500.60
500
Column Data
n column diameter 70mm up to
SPEC. SURFACE
m2/m3
SPEC. SURFACE
m2/m3
BSH-250
250
BSH-250.60
250
Materials
BSH-300
300
BSH-300.60
300
BSH-350
350
BSH-350.60
350
BSH-400
400
BSH-400.60
400
BSH-500
500
BSH-500.60
500
BSH-750
750
BSH-750.60
750
MONTZ-PAK TYPE M / MN
THE NEW HIGH-PERFORMANCE PACKING
The Montz-Pak
Type M and Type MN are
further developments of the tried and
trusted Montz structured packing Type B1, A3
and BSH. It has its own patent coverage. The optimized
crimp geometry creates two packing types that
meet the demands for high separation efficiency
and throughput exceptionally well.
The new Type MN-series gives 30% more separation
efficiency along with higher throughput capacity when
compared to standard packing crimps. Higher purities,
small column heights and simple tower debottlenecking
are now possible.
The Type M-series allows throughput increases of 30%
compared to columns equipped with standard packing
types due to the reduced pressure drop. This packing only
offers the same efficiency as standard packing types.
Both packing types are patented in the USA and
Europe. Layer height depends upon crimp shape which
prevents liquid hold-up at the lower end of the packing
layer at high gas loads.
Type M and Type MN packing are ideal for new
columns or tower revamps. Revamps from standard
packed columns to the new high performance packing
types consistently deliver outstanding performances.
Applications
n vacuum columns
n normal-pressure and high
pressure columns
n absorption
n natural gas drying with
glycols refinery columns
n revamping existing packing,
random rings or
tray columns
Characteristics Type M
n maximized capacity
n lowest pressure drop
n same separation efficiency
compared to standard
packing types
Characteristics Type MN
n higher capacity
n lower pressure drop
n highest separation efficiency
Structure of the
Montz-Pak Type M / MN
AVAILABLE PACKING
TYPES
PAK-TYPE
SPEC. SURFACE
m2/m3
B1-250M
250
B1-350M
350
B1-250MN
250
B1-350MN
350
B1-500MN
500
SADDLE RINGS
Ideal For Both High Pressure And
Vacuum Towers
PALL RING
Perfect In-kind Replacement
Packings
ITEM
Piece
Density
pcs/m3
Surface
Area
m2/m3
Voidage
(%)
Packing
Factor
MSR # 25 135000
225.8
96.6
41
MSR # 40 50000
150.8
97.7
24
MSR # 50 15000
100
98
18
MSR # 70
60
98.5
12
10
4625
ITEM
Piece
Density
pcs/m3
344.2
93.1
81
MPR# 25mm
51000
206.7
94.8
56
MPR# 38mm
14300
130.4
96.08
40
MPR# 50mm
6500
102.1
95.9
27
LIQUID DISTRIBUTORS
KNOW-HOW FROM MONTZ FOR MAXIMUM PERFORMANCE
(distributors for 201/m2/h have been successfully applied e.g. distillation of glycerine)
flexibility: standard turn down ratio 1:3 (higher ranges of loading
e.g. 1:10 and more are possible using multi-stage distributors)
design know-how for viscous liquids
diameters range from 70 mm to 12 m and more
the same design principle applies to diameters from
200 mm to >12m
liquid feed by pre-distribution system can be adapted to
most applications
contamination is reduced because our designs are
resistant to dirt and sedimentable impurities
Can be adjusted easily with standard fitters tools
Fits solidly against the column wall
Installation and inspection can be made through manholes
for columns from DN 800; smaller columns can be accessed
through shell flanges.
Liquid distributor type R for
assembly through shell flanges
11
Channel-style Type S
Special applications
Operating ranges:
Detailed view of
the Type S
12
13
PERFORMANCE CHARTS
OVERVIEW OF PERFORMANCE AND PRESSURE DROP
Nth/meter
dP in mbar/meter
PRESSURE DROP
F-factor in Pa0.5
F-factor in Pa0.5
Nth/meter
7
6
5
4
3
2
1
0
0
0.5
1
F-Factor in Pa0.5
1.5
2.5
3.5
0
0.5
1
F-Factor in Pa0.5
1.5
2.5
3.5
Nth/meter
dP in mbar/meter
PRESSURE DROP
F-factor in Pa0.5
F-factor in Pa0.5
Nth/meter
F-factor in Pa0.5
14
PRESSURE DROP
F-factor in Pa0.5
0
1
F-Factor in Pa0.5
Nth/meter
dP in mbar/meter
PRESSURE DROP
F-factor in Pa0.5
F-factor in Pa0.5
Nth/meter
dP in mbar/meter
PRESSURE DROP
F-factor in Pa0.5
F-factor in Pa0.5
Nth/meter
dP in mbar/meter
PRESSURE DROP
F-factor in Pa0.5
F-factor in Pa0.5
Nth/meter
dP in mbar/meter
PRESSURE DROP
F-factor in Pa0.5
F-factor in Pa0.5
15
PERFORMANCE CHARTS
OVERVIEW OF PERFORMANCE AND PRESSURE DROP
Nth/meter
7
6
5
4
3
2
1
0
0
0.5
1
F-Factor in Pa0.5
1.5
2.5
3.5
10
9
8
7
6
5
4
3
2
1
0
0
0.5
1
F-Factor in Pa0.5
1.5
2.5
3.5
10
9
8
7
6
5
4
3
2
1
0
0
1
F-Factor in Pa0.5
B = 100
B = 50
B = 20 B = 10
B=2
Nth/meter
dP in mbar/meter
PRESSURE DROP
F-factor in Pa0.5
F-factor in Pa0.5
Nth/meter
dP in mbar/meter
PRESSURE DROP
F-factor in Pa0.5
F-factor in Pa0.5
Nth/meter
7
6
5
4
3
2
1
0
16
0
0.5
1
F-Factor in Pa0.5
1.5
2.5
3.5
10
9
8
7
6
5
4
3
2
1
0
B = 100
0
0.5
1
F-Factor in Pa0.5
1.5
2.5
3.5
10
9
8
7
6
5
4
3
2
1
0
0
1
F-Factor in Pa0.5
B = 50 B = 20 B = 10
B=2
Nth/meter
7
6
5
4
3
2
1
0
0
0.5
1
F-Factor in Pa0.5
1.5
2.5
3.5
10
9
8
7
6
5
4
3
2
1
0
B = 20
B = 10
B=5B=2
0
0.5
1
F-Factor in Pa0.5
1.5
2.5
3.5
0
1
F-Factor in Pa0.5
Nth/meter
7
6
5
4
3
2
1
0
0
0.5
1
F-Factor in Pa0.5
1.5
2.5
3.5
10
9
8
7
6
5
4
3
2
1
0
0
0.5
1
F-Factor in Pa0.5
1.5
2.5
3.5
10
9
8
7
6
5
4
3
2
1
0
B=20
0
1
F-Factor in Pa0.5
Nth/meter
dP in mbar/meter
PRESSURE DROP
F-factor in Pa0.5
F-factor in Pa0.5
Nth/meter
dP in mbar/meter
PRESSURE DROP
F-factor in Pa0.5
F-factor in Pa0.5
17
PERFORMANCE CHARTS
OVERVIEW OF PERFORMANCE AND PRESSURE DROP
Nth/meter
dP in mbar/meter
PRESSURE DROP
F-factor in Pa0.5
F-factor in Pa0.5
Nth/meter
dP in mbar/meter
PRESSURE DROP
F-factor in Pa0.5
F-factor in Pa0.5
Nth/meter
dP in mbar/meter
PRESSURE DROP
F-factor in Pa0.5
F-factor in Pa0.5
Nth/meter
F-factor in Pa0.5
18
PRESSURE DROP
F-factor in Pa0.5
MONTZ QUALITY
PRECISE MEASURING FOR QUALITY ASSURANCE
Our air-water test equipment is used for fluiddynamic tests of column internals in accordance with
the specific requirements of our customers .
We offer the following:
n test columns of a diameter of 100 to 2500 mm
are available
n tests of the minimum and maximum load limit
of mass-transfer trays, structured packings or
separator internals
n determination of all essential data by means
of precise measuring instruments: mass flow,
pressure drop entrainment, etc.
Liquid distributor test equipment
19
Services
800-231-0077
www.amacs.com
Continuous V
slot opening
for high intake
efficiency
Non-clogging
construction
Large filtration
area
Ease of back
wash and well
completion
Additional inlet
area reduces
inlet velocity
Wide variety
of construction
strength and
open area ratio
Unlimited slot
size design
for a broad range of well completion applications in the ground water industry.
For a wide range of industrial and process applications AMACS manufactures a complete line of Wedge Wire
industrial screens. The Wedge Wire screen products are constructed of a series of parallel V resistance welded
cold drawn wire, cold wound welded on perpendicular support rods. The result is a smooth plug resistant
screen surface that is very structurally sound. AMACS Wedge Wire industrial screens provide superior
performance in numerous process industries including chemical, petrochemical,
Advantages
support services:
process analysis, troubleshooting and recommendation
design to your performance criteria or
redesigns and retr
cost
technical support
quality assurance
and
operations.
and
bottom
cleaning.
or threaded. All
liquid or solid retention in
Nozzles, Strainers
and sand
ration or treatment
rration.
ation. These sc
screens are
e
in wastewater treatments,
Inlet and O
Outlet
utlet B
Baskets
askets
AMACS inlet and outlet baskets are designed to meet
open area, designated temper
temperature,
rature, and
rential
ential pressu
pressure
essure
performance requirements or
s. Backwash
Numerous custom
ration application
can assist you in designing a wide variety wedge wire screen and other separations products.
For applications that require very
SPECIFICATIONS
V-WIRE
WIDTH
.047
.058
.060
. 0 9 0
.069
.118
. 0 9 0
HEIGHT . 0 8 8
.085
.100
.140
.170
.185
. 1 05
SUPPORT
ROD
WIDTH
.090 F
HEIGHT
.140 H
Round
Round
Round
.098 dia.
.125 dia.
.177 dia.
individual
RANDOM PACKINGS
STRUCTURED PACKING
LIQUID/LIQUID COALESCERS
INLET DISTRIBUTORS
TRAYS
TURNKEY POLLUTION
CONTROL PACKAGES
14211 Industry Street Houston TX.77053 Ph: (713) 434 0934 Fax: (713) 433 6201 amacs@am
acs.c om
www.amacs.com
AMACS Hub laterals are designed for disc head vessels enabling the
system to collect completely to the bottom of the vessel. Header laterals
designs are available for flat bottom collector applications. Distributor systems
can be designed to accommodate side or center inlet piping.
Integral backwash systems can be designed for any hub and header lateral
for fast effective and efficient cleaning. Connections of the laterals can be
flanged or threaded. All systems are designed for effective liquid or solid
retention in a wide range of applications including exchangers, clay and
sand filtration applications, carbon towers and power plants with water systems.
Applications:
Ion Exchange
Clay and Sand filtration applications
Activated Carbon Towers
Chemical Catalytic exchangers
Industrial Softeners and
Demineralizes
Profile Wire
Slot opening
fixed or variable
Slot opening
Support rod
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Amistco Separation Products Inc, and ACS Separations and Mass Transfer Products, are Registered Trademarks of AMACS
Structured Packing
Applications:
Pharmaceuticals
Fine chemicals
Flavors and fragrances
Electronic chemicals
5 to 8
0.1 W.C. per theoretical stage
0.05 to 5 gpm/square foot
0.1 to 0.25 ft./sec
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Amistco Separation Products Inc, and ACS Separations and Mass Transfer Products, are Registered Trademarks of AMACS
Stage 2
Stage 1
Knockout
drums
Figure 2. Typical
compressor
drums
T HAPPENS in petrochemical plants, reneries, and anywhere else that the gas approaching a comp ressor is wet.
Traces of aqueous or organic liquid escape the inlet knockout drum - often intermittently - and silently damage the compressor. Telltale signs include pitting corrosion, salt deposit s,
and diluted lubricants.
Instead of trying to repair symptoms, look for the root
cause, which usually involves the mist eliminator in the knockout drum (Figu res 1 and 2). Problems may include improper
mist eliminator specications, overloading, uneven velocity
proles, incorrect installations , high liquid viscosity, waxy
deposit s, liquid slug s, foaming, and several other possibilities .
The trouble may even be that no mist eliminator was provided in the rst place - or perhaps no knockout drum at all.
But wherever free liquid drops out in a suction drum, it generates some mist that can damage the compressor unless it is
removed by a mist eliminator. Even in cases where the feed gas
never has any free liquid, there are often ne mist droplets that
coalesce into large drops on the walls of the inlet pipe or inside
the compressor. For all but the driest gas, a compressor should
be protected by an inlet mist eliminator. New high-capacity,
high-eciency mist eliminator technologies pay o the rst
you avoid a shutdown.
For optimum separation performance, compressor knockout drums must be properly designed and sized with appropri1
Mist-free gas
MESH PAD
VANE UNIT
Gas
with
mist
Figure 3.
capturing mist
and draining
dry zone,
ooded zone,
agitated by
rising gas
higher in
pad
is ooded
and
agitated
Most captured
mist is blown
away as
re-entrainment
liquid
drains
below
Low
efficiency
Reentrain
MESH PAD
Re-entrainment
Dual support
rings
Through bolts
Relief door
AMACS has endeavored to assure that all information in this publication is accurate. However, nothing herein is intended as a guarantee or warranty.
AMACS
Figure 6. S
Depending on the judgment of the designer , the design
velocity may be established at the inner or outer surface or anywhere in between. The most conservative and cautious
approach is to set the inner-surface velocity at the design value,
to make sure re-entrainment is avoided. Velocities farther out
toward the outer surface will be progressively lower.
Figure 6 depicts the application of Steps 4 and 5 above to a
typical simplified design case. A knockout drum with design
throughput of 3,600 actual cubic feet per minute has an 18-inch
gas exit nozzle. A MistFix unit is to be inserted in the nozzle,
and the proper length is to be determined. The pressure is less
than 85 psig. The owing materials are hydrocarbon vapor and
liquid with densities of 0.31 and 45.2 pounds per cubic foot.
Using a design K factor of 0.42 as discussed before
, the
design velocity turns out to be 4.91 feet per second. The crosssectional area required to achieve that velocity is 12.2 square
feet. For this MistFix unit, the length to achieve that design
velocity at the outer surface is 31.1 inches. By comparison, if a
conventional round horizontal mesh pad were used, that
design cross-section would correspond to a diameter of 47.3
inches.
sizing example
the unit, and avoiding strong turbulence and fluid shear around
and below the MistFix unit. Consultation by Amacs engineers is
especially important in this area.
To prevent uneven flow through the mesh, the bottom end
of the device should be well clear of the inlet stream - more
than about half a vessel radius above the top of the inlet nozzle.
In many cases, undesirable turbulence can be diminished by a
properly selected inlet feed device. If a manway is not available for
installing such a device, it may be possible to use a diffuser
designed for insertion through the inlet nozzle as shown in
Figure 7. To control flow inequality along the length of the
MistFix unit, variation in thickness or density of the mesh may
be incorporated.
Case Histories
Chemical
A Midwester
production plant had to shut down two
identical vertical gas-liquid separators four times a year to
replace the horizontal mesh pads due to fouling
s.
Each shutdown lasted two days because of the time required for
reach the
mesh pad. The plant was operating near maximum capacity, so
any down time dir
the companys bottom line.
The separators were 36 inches in diameter and 84 inches
high. The incoming stream consisted of
gas with a density of 0.25 lb/ft 3 and a throughput of 3,600 actual cubic feet per
minute. The feed contained less than 0.1% water with droplets
greater than 10 microns in size, and also traces
s. The
gas outlet nozzle had an inside diameter of 12 inches.
Based on the process conditions, a 12- inch MistFix unit
with a length of 30 inches for each separator, using 316 SS mesh.
MistFix is a trademark of AMACS Process Tower Internals. AMACS has endeavored to assure that all information in this publication is accu ar te. However, nothing herein is intended as a guarantee or warranty.
Applications
vacuum columns
normal and high pressure columns
absorption
gas drying/glycol columns
revamps
Characteristics Type M
capacity advantage of 30%
low pressure drop
liquid loads from 0.2 to > 250
m3/m2/h
reduced liquid hold-up
Characteristics Type MN
higher capacity
lower pressure drop
highest separation efficiency
Materials
Carbon-steel, stainless, Hastelloy,
monel, other materials are available
on request
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Amistco Separation Products Inc, and ACS Separations and Mass Transfer Products, are Registered Trademarks of AMACS
Mist Eliminator?
Save Thousands in TEG Recovery
For your next turn around or new gas
dehydration process think about cutting
your losses before you start.
$40,000
$35,000
$30,000
$25,000
$20,000
$15,000
$10,000
$5,000
$0
$31,098
Loss with Typical
Mist Eliminator
$27,988
Savings with
High Capacity
Mist Eliminator
4000
2500
2000
1500
1000
500
0
3000
3500
14211 Industry Street Houston, Texas 77053 Phone: (281) 716-1900 FAX: (281) 433-6201 www.amacs.com
AMACS
tower trays
tower trays
materials of
construction
hex nut
manway lock clamps
manway lock studs
manway (active)
(active)
tray
manway clamps
hex nut
seal plate
tray
(active)
outlet weir
downcomer truss
hex nut
standard tray
component assembly
tray
(inlet panel)
hex nut
frictional washer
tray
(inlet panel)
tray support ring
bottom tray clamp
hex-head bolt
hex nut
frictional washer
downcomer panel
downcomer bolting bar
bottom tray clamp
hex-head bolt
hex-head bolt
manway stud
seal plate
frictional washer
Pressure drop
Turndown
Capacity
Efficiency
valve trays
tower trays
slotted
bubble cap
3 piece valve
This valve consists of a light weight or
welded stud
swaged riser
extruded tray
deck opening
fixed valve
This valve is integral with the tray deck. This is the preferred
option for fouling conditions. However, it provides lower
turndown and less efficiency than floating valves
baffle trays
design assistance.
donut tray
disk tray
tower trays
additional tray
design options
For special customer requirements
AMACS include:
tray from jumping over the downcomer onto the opposing flow path.
Call our
24 hour number
1-800-231-0077
RANDOM PACKINGS
STRUCTURED PACKING
LIQUID/LIQUID COALESCERS
LIQUID REDISTRIBUTORS
INLET DISTRIBUTORS
TRAYS
TURNKEY POLLUTION
CONTROL PACKAGES