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Documente Profesional
Documente Cultură
STANDARD OPERATING
PROCEDURES MANUAL
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Revision No.: 0
Effectivity Date:
_______________October 2015
1.0 Purpose
This document gives the general procedure for the conduct of sensory evaluation in
order to ensure that the same procedure is always applied to the same sensory
problem. The procedure outlines each step in the evaluation and identifies the
personnel responsible for each step. If applicable, all the necessary control in the
generation of results was also included. Ignoring these considerations increases the
possibility of bias and error in the result.
2.0 Scope
The document relates to major product development activities and connects the
sensory objectives to recommended methods for the sensory evaluation.
Recommendations are suitable for application in conjunction with specific sensory
methods detailed in Sensory Evaluation Procedures (SEP) Manual.
3.0 References
3.1.
3.2.
3.3.
3.4.
Approved by:_________________________
This document shall not be copied in whole or in part; if not stamped in red, this document is uncontrolled.
FNRI-SEL
CONDUCT OF SENSORY
EVALUATION:
With INTERNAL QUALITY CONTROL
SOP-_______-0
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5.2 Panel leader, possessing relevant qualifications, assists the sensory analyst in
conducting sensory test activities and implements quality control procedures.
5.3 The sensory panel technician assists the panel leader or sensory analyst in
performing sensory tests, including necessary preparation measures before the
test and activities after the test.
5.4 Reporting and interpretation of results are the responsibilities of the competent
staff, either the sensory analyst or the panel leader.
6.0 Procedure
6.1. Identify the problem that can be resolved through sensory evaluation. These are
problems answerable by measuring the reaction of panelist to stimuli from the
use or consumption of a product. Given the steps in product development,
determine whether the solution needs to compare between product/parameters
or to describe the product characteristic. And these are generally answered
through analytical type of sensory evaluation (discriminative and descriptive
tests). Another solution is to evaluate the degree of liking/disliking or whether one
product is preferred over another product through affective tests.
6.2.Conduct sensory evaluation to investigate the problem or to come-up with
possible solution/decision. Determine the objective of the test which can be one
of the following:
a. to know whether there is perceivable difference between products or
formulations (discrimination tests),
b. to describe the difference or the sensory characteristics
c. to determine the nature of difference or to quantify the sensory characteristics
d. to determine preference or acceptability
6.3.Identify the appropriate sensory test method that will satisfy the test objective.
Figure 2 illustrates the various applications of different sensory evaluation
methods along the product development process. The laboratory uses verified
standard sensory evaluation procedures that is updated and documented in the
SEP Manual for use as reference of the personnel.
6.4.Prepare an experimental design. Consider all possible parameters that can
introduce bias or error to the evaluation. Aim for the best conditions of
experimentation to minimize these biases. Consider the following in the
experimental design:
a. Determine the sample plan. Some test method have requirement for balance
sample presentation. Refer to the latest SEP Manual for the specific
requirement of each test method,
b. Decide on the test variables or attributes to be used,
c. Type of scale to be used in your scoresheet (rating, ranking or category
scale). Each test method a validated scale to go with their evaluation. Refer to
the latest SEP Manual for the appropriate scale for a particular test method,
d. Include in the design one of the following internal quality control (IQC) check:
i. conduct of replicate analysis of samples,
ii. introduced random repeat samples into the sample analysis system at
appropriate intervals or
__________________________________________________________________________________________
This document shall not be copied in whole or in part; if not stamped in red, this document is uncontrolled.
FNRI-SEL
CONDUCT OF SENSORY
EVALUATION:
With INTERNAL QUALITY CONTROL
SOP-_______-0
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g. Number and type of panelist. Analytical test uses trained panelist (Selected
Sensory Panelists) while affective test generally use consumer panelist or the
initiated (in-house) Sensory Panelists.
6.5. Identify the panelists
6.5.1. Recruit panelists from the pool of sensory panelists who passed the
recruitment criteria (see SOP-5.2-2-0 Recruitment, Screening and
Selection of Candidate Sensory Panelists). These panelists may also
be selected based on specific criteria required by the test (see specific
requirements of each test method in SEP Manual).
6.5.2. Qualified candidates shall be informed of the task they will undertake,
how much time it will take up. Statement allowing assessment of their
interest and motivation, their voluntary participation and their pledge of
confidentiality is signed in the accomplished consent form F-SOP 5.22-3.
6.5.3. Ensure panelist safety by checking for presence of ingredients that is
restricted to some panelist due to cultural standards, safety and health
reasons (declaration of possible allergens, haraam foods). The
products major ingredients and processes is declared by the
customer in the F-QM4.4-1, Request for Sensory Evaluation.
6.5.4. Selection is based on the required sensitivity/threshold for a specific
attribute or ability to discriminate and reproduce results. Performance
of panelist is monitored following the procedure stated in SOP_____
Monitoring of Panelists Performance
6.5.5. Sensory panelist performances are kept in their individual profile as
basis of their qualification on particular sensory evaluation objective.
6.5.6. Characteristic of the target group should be stated in the contract or in
the Test Report if it is deemed necessary to meet the test objective.
6.6. Schedule the test. Reservation and cancelation is done one day before the
testing date in order to manage use of resources. (see SOP-4.1-1-0 for Request
for Sensory Evaluation).
__________________________________________________________________________________________
This document shall not be copied in whole or in part; if not stamped in red, this document is uncontrolled.
FNRI-SEL
SOP-_______-0
CONDUCT OF SENSORY
EVALUATION:
With INTERNAL QUALITY CONTROL
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FNRI-SEL
CONDUCT OF SENSORY
EVALUATION:
With INTERNAL QUALITY CONTROL
SOP-_______-0
Page 5 of 3
FNRI-SEL
CONDUCT OF SENSORY
EVALUATION:
With INTERNAL QUALITY CONTROL
SOP-_______-0
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separate document with clear reference to the basis of the opinion. Whenever
possible, discussion of the result should be entertained as a form of technical
consultation with the qualified personnel and not to be confused from the
statement of product certification and no value for promotional purposes.
6.11.Prepare report
The sensory analyst or the test supervisor summarized the result of the test in
Sensory Evaluation Test Report with predetermined content and format detailed
in APPENDIX C of this manual. Test report is checked by the Technical/
Laboratory Manager, approved by the Quality Manager and endorsed by the
Director of the Institute.
7.0 Related Documents
7.1. Sensory Evaluation Procedures (SEP) Manual.
7.2. Training and Competency-SOP-5.2-1-0
7.3. Recruitment, Screening and Selection of Candidate Sensory Panelists-SOP-5.2-2-0
7.4. Consent Form-F-SOP 5.2-2-3.
7.5. Request for Sensory Evaluation-F-QM4.4-1,
7.6. Handling of Test Items-QM-5.8-0
7.7. Laboratory Inspection Checklist -F-QM5.3-1
7.8. Laboratory Monitoring Form (F-QM5.3-2)
7.9. Satisfaction survey form (F-SOP5.4-1-1).
7.10.APPENDIX C Sensory Evaluation Test Report
7.11.eSEL Users Manual
__________________________________________________________________________________________
This document shall not be copied in whole or in part; if not stamped in red, this document is uncontrolled.
FNRI-SEL
SOP-_______-0
CONDUCT OF SENSORY
EVALUATION:
With INTERNAL QUALITY CONTROL
PROCEDURE
Determine the objective(s)
of the sensory Evaluation
Identify panelist
Collect data
CONTROL MEASURES
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MONITORING
REQUIRED
None
As agreed with the customer
Documented in F-QM4.4-1,Request for
Sensory Evaluation and test method
Mastersheet
None
None
FNRI-SEL Calendar
of Activities
Laboratory
Inspection Checklist
-F-QM5.3-1
Laboratory
Monitoring Form (FQM5.3-2)
Equipment
Maintenance
Performance Check
None
None
Prepare report
Figure 1. Process flow for the conduct of sensory evaluation with corresponding IQC.
__________________________________________________________________________________________
This document shall not be copied in whole or in part; if not stamped in red, this document is uncontrolled.
FNRI-SEL
SOP-_______-0
CONDUCT OF SENSORY
EVALUATION:
With INTERNAL QUALITY CONTROL
IDEA GENERATION
STEPS in PRODUCT
DEVELOPMENT
CONCEPT TESTING/
BENCHMARKING
LAB SCALE
TRIAL FORMULATIONS
SENSORY EVALUATION
METHODS
Descriptive Test: Focus Group Discussion (small
panel, minimum of 4 panel, product expert or
researcher)
Analytical Tests: Single sample tests-DFC; Paired
Comparison: SDT, Duo-Trio, Triangle, DPCT; Multisample-Ranking, DFC (10-15= Selected Panelists)
Descriptive Test: (QDA 10-15 selected/trained
panelists)
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PRODUCT
OPTIMIZATION
BENCHMARKING WITH
REFERENCE PRODUCT
SHELFLIFE
STUDY