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UEMK3431 Chemical Engineering Laboratory II Exp 8: Disc Bowl Centrifuge
2.0 INTRODUCTION
Centrifugal separators are used to separate solids from liquid or liquid from liquid using the
principle of centrifugal force. Liquid-liquid centrifuge separates two liquids of different
densities by spinning at relatively high speeds. Separation occurs as the heavy phase liquid
experiences a higher magnitude of centrifugal force causing it to settle on the outer collecting
ring while the lighter phase liquid is collected on the inner collecting ring.
There are two main types of centrifuge: tube bowl centrifuge and disc bowl centrifuge. Both can
be used to separate either solids from liquids or two liquids of different density. The tube bowl is
simply a tube rotated about its axis; the liquids are separate as they flow along the centrifuge or
the solids are thrown towards the wall. Overflow dams at the outlet end allow the two phases to
be collected separately.
For disc bowl centrifuge, the feed is admitted near the base and passes up through holes in the
disc (which are actually inverted cones). The discs are about 5 mm apart. The solids do not have
to travel far before hitting a disc and effectively being separated. Solids then continue to move
outwards and are either removed manually or through nozzles on the periphery as concentrated
slurry. Disc centrifuges range from 10 cm to 75 cm in diameter, spin speeds are in the 1000's or
rpm range.
The radial velocity, ur of the denser droplets or the particles is given by:
r 2
ur 1 2 d 2
18
(1)
The liquid layer thickness is small compared to the tube diameter, hence we can treat the radius
r
of rotation as a constant . This gives the distance traveled in the residence time tres as
r 2
u r t res 1 2 d 2 t res
18
(2)
If the feed is homogeneous and the distance moved is equal to half the total thickness of the
liquid layer, then half the particles with diameter d will be collected. In this case d = d50 (this
only applies if the concentration of one phase in the other is very small), thus
r2 r1
u r t res
2
(3)
V
t res
Q
(4)
V 2
d 50 r 2 1 2 V
Q
t res 9 r2 r1
g 1 2 d 502 V r 2
2
18 g r1 r2
2u t 50
(5)
V r 2
g r1 r2
=
is a characteristic of the centrifuge design only and is equal to the area of gravitational settler
required to do the same duty. For scale up on the same duty
Q1 Q2
1 2
(6)
2n r23 r13 2
3 g tan
(4)
The disc bowl centrifuge unit is designed to demonstrate the separation of a heavy phase liquid
using the principle of centrifugal force. This is a bench top unit comprises of an epoxy coated
frame, feed reservoir, collecting vessels, variable speed motor, feed system and control panel
mounted on the stainless steel frame.
The throughput of the feed system is at least 150 LPH. The speed of the motor can be varied
from 8500 to 12000 rpm using an electronic speed controller.
UEMK3431 Chemical Engineering Laboratory II Exp 8: Disc Bowl Centrifuge
Frequency Mixing
Inverter Tank
Disc Bowl
AC Motor
1. Remove the mixing tank, liquid collecting outlet tray and the disc bowl.
2. Clean it with cleaning detergent and warm water.
3. Wipe all the parts and dry them.
4. Place all the parts back to it original position.
5. Fill the mixing tank with 3 - 4 litres of hot water.
6. Run the unit by setting the frequency to about 20 Hz.
7. When all the water is drained out, switch off the machine.
6.0 EXPERIMENTS
Conduct the experiment with two different solutions at 4 different frequencies (max at 30 Hz).
Reminder:
Mix both solutions and determine the density before separation. Allow the apparatus to run for 3
minutes then record down the speed of the bowl.
By using the same setup as Experiment 1A, repeat the experiment using different ratio (mixture
with different density).
Determine the density of the test fluid (take note of the unit used).
Discuss all your results. The questions below only serve as a guideline. Your discussion should
not only limit to these questions.
1. How does the speed of the bowl affect the separation efficiency?
2. Can we separate two solutions with densities near to each other using a disc bowl
centrifuge? Why?
3. Is it possible to estimate the separation efficiency using the data you obtained in the
experiment? If Yes, show your estimations. If No, explain why it is not possible.
4. As the proportion of water to oil changes, explain how does this affects the separation
efficiency.