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ABSTRACT
The rate of change of viscosity with rate of shear is referred to as
shear susceptibility and, like initial viscosity, can be considered as an
intrinsic property of the asphalts. Many researchers have indicated
that absolute viscosity alone can not specify the complete rheological
behavior of paving asphalts, and other parameters like shear suscepti-
bility and/or temperature susceptibility are needed. Hence, it has been
the intent to study the shear susceptibility parameter in relation to the
performance of the in-service pavements.
Six viscosity graded asphalts from different sources were used
during 1964 in the construction of wearing course on Legislative Route
219 in Clinton County, Pennsylvania. In the construction of these six
test pavements, the only significant variable is the asphalt type. Tests
to determine the properties of the original asphalts as well as the as-
phalt recovered from time to time during the last 8 years, have been
conducted. Pavement performance evaluation has been carried out by a
team of five engineers.
Very good correlation was observed between aging indices and
shear susceptibility values of the aged asphalts. Aging index-shear
susceptibility relationship appears to determine the pavement perform-
ance, Control of gain in shear susceptibility and aging index seems to
be a necessary specification requirement for paving asphalts. It is in-
dicated that the ratio of Asphaltenes to Nitrogen Bases affects the shear
susceptibility of asphalts.
INTRODUCTION
Several factors are involved in the performance and durability of as-
phalt pavements. Studies relating to more durable pavements must
consider the engineering properties of the pavement structure as well
as the physical and chemical properties of the asphalt component of the
pavement, be it only the minor component volumetrically. The func-
tions of the asphalt binder film are to effect cohesion of the aggregate
components, to waterproof the pavement, and to effectively transmit the
energy resulting from transient or sustained loads, without unduly de-
forming the structure or fracturing the asphalt film (1).
Recent research (l), (2), (3), (4), (5), (6) has indicated that absolute
viscosity alone can not specify the complete rheological behavior of
paving grade asphalts, and other parameters like shear susceptibility
and/or temperature susceptibility are needed. The rate of change of
viscosity with rate of shear is referred to as shear susceptibility and
like initial viscosity, can be considered as an intrinsic property of the
99
100 KANDHAL, SANDVIG AND WENGER
6.4 percent was also held consistent. Marshall test data on the field
mixtures are given in Table 2. Properties of the six asphalts used in
the project are shown in Table 3. It will be observed from the data that
five asphalts conform to Pennsylvania AC-2000 (AASHO AC-20) asphalt
cements, since for project samples permissible viscosity is 2000 600
poises. Asphalt 4 conforms to AASHO AC-l0. The initial air voids and
subsequent decreasing trend of the air voids, with time under traffic, is
graphically illustrated in Figure 1.
Thus, in this closely controlled research project, the only signifi-
cant variable is the asphalt type. Since construction of these six pave-
ments, periodic core samples have been obtained in order to determine
Asphalt Type 1 2 3 4 5 6
Viscosity
Viscosity at 140 F., 1613 1447 1544 966 2200 2649
poises (AC-20) (AC-20) (AC-20) (AC-20) (AC-201
Viscosity at 215 F.,
339.6 475.4 343.0 318.5 509.4 556.7
Viscosity at 39 F., at
0.05 1.19 4.22 10’ 2.65 9.50 1.68 2.57
Viscosity at F., at
0.05 3.05 4.83 1.06 9.15 105 1.32 1.85
Viscosity at 115 F., at
0.05 2.09 104 1.15 104 1.54 104 1.15 2.19 2.80 104
Shear Susceptibility at
39.2 F. 0.20 0.35 0.20 0.45 0.32 0.32
Susceptibility at
F. 0.05 0.11 0.02 0.06 0.12 0.09
Shear Susceptibility at
115 F. 0.02 0.04 0.03 0.03 0.04 0.02
Penetration
Penetration at 39.2 F.,
g., 5 sec. 9 28 11 19 15 12
Penetration at 71 F.,
100 g., 5 sec. 62 149 92 114 94 80
Standard Ductility at
39.2 F. 1 cm.
per cm. 14.0 101.0 53.3 23.5 68.3 21.9
Composition Analysis)
(A), percent 16.30 26.80 18.74 19.98 25.05 26.18
Nitrogen Bases
percent 25.65 15.90 24.56 20.63 24.08 21.75
First
percent 18.62 14.70 15.84 14.32 21.11 20.23
Acidaffins
percent 26.51 30.90 26.78 21.91 20.96 21.84
percent 12.92 11.70 14.08 17.10 8.80 10.00
Coefficient 1.123 0.718 0.988 0.775 1.518 1.318
Ratio A/N 0.64 1.69 0.76 0.97 1.04 1.20
*No data available. These were determined from Figure 4 of the paper by and
(ASTM, STP. No. 309, which gives relation between Percent of Original Penetration
Viscosity Aging Index for Thin Film Test.
102 KANDHAL, SANDVIG AND WENGER
2 -
5 I I 24 I 30 I 36 I 42 54 78 1
the percent air voids in the pavements and the rheological properties of
the aged asphalts. The last core sampling was done 78 months after the
construction.
Rutting (inch)
Cracking (shrinkage) Slight None None
Surface Texture Average Closed Average Closed Average
to open
Aging Index .
aging and life expectancy of the test pavements. This will be evident
from Figure 3 when compared with the pavement ratings.
Raveling was observed in Asphalt 1 test pavement after 24 months
when the aging index (based on viscosity at 77 F., 0.05 exceeded
12. Due to inadequate compaction under traffic, test pavement contain-
ing Asphalt 1 maintained higher air voids which most likely accelerated
the aging phenomenon. Asphalt 2 and 6 are beginning to show moderate
raveling after 80 months on just exceeding aging index of 12 (Figure 3).
Shear Susceptibility
The shear susceptibility (or shear index) value as employed in this
study is the tangent of the angle of log shear rate (X-axis) versus log
viscosity (Y-axis) determined during performance of the viscosity test
using the microviscometer . Shear susceptibility values have been
Months
Asphalt Type
Original 12 18 24 30 36 42 46 78
Type
Viscosity at 77 F.,
megapoises 3.05 21.5 33.0 46.3 39.0 40.5 39.0 55.5 66.5
Shear susceptibility
at 77 F. 0.05 -- 0.41 0.39 0.43 0.55 0.56 0.52 0.50
T y p e
Viscosity at 77 F.,
megapoises 0.46 3.6 3.9 3.5 3.7 4.2 4.0 5.5 6.2
Shear susceptibility
at 77 F. 0.11 __ 0.26 0.24 0.26 0.24 0.25 0.26 0.36
T y p e
Viscosity at 77 F.,
megapoises 1.06 6.3 6.2 4.9 7.0 8.0 6.5 7.6 9.0
Shear susceptibility
at 77 F. 0.02 __ 0.17 0.14 0.13 0.17 __ 0.20 0.24
T y p e
Viscosity at 77 F.,
megapoises 0.92 6.6 5.8 5.0 6.8 6.2 1.1 10.1 10.6
Shear susceptibility
at 77 F. 0.06 __ 0.31 0.32 0.24 0.36 0.32 0.36 0.45
Type
Viscosity at 77 F.,
megapoises 1.32 7.6 6.2 6.6 6.9 7.8 12.1 10.2 10.5
Shear susceptibility
at 77 F. 0.12 __ 0.26 0.20 0.20 0.25 0.32 0.32 0.33
Type
Viscosity at 77 F.,
megapoises 0.19 9.8 13.5 13.2 12.7 13.1 16.0 15.2 22.2
Shear susceptibility
at 77 F. 0.09 __ 0.26 0.26 0.29 0.32 0.35 0.42 0.38
SHEAR SUSCEPTIBILITY TO PERFORMANCE 105
ASPHALT 1
----
ASPHALT 3 - - - - -
;
determined for the six asphalts after increasing periods of aging (Table
5). Results are shown graphically using smooth curves in Figure 4.
Having observed that pavement performance is indicated by the
aging index based on viscosity at 77 F., it was attempted to find out
whether shear susceptibility values of the asphalts affect their aging
indices. Shear susceptibility values at 77 F. of the six aged asphalts
after 30, 42 and 78 months’ period were obtained from Figure 4 and
plotted with the corresponding aging indices. Very good correlation
was obtained between aging indices and the shear susceptibility values
for these asphalts (Figure 5). Correlation between viscosity and shear
susceptibility values of all the asphalts, was observed to be poor (Fig-
ure 6).
In Figure 3, three distinct groups of asphalts can be seen accord-
ing to aging indices and pavement performance ratings after 80 months
in service:
106 KANDHAL, SANDVIG AND WENGER
1Group
Asphalt 1 High shear susceptibility (> performance
poor
2Group
Asphalt 2
Asphalt 6 Intermediate shear susceptibility (0.35
Asphalt 4 performance fair to good
3Group
Asphalt 3 Low shear susceptibility performance good
Asphalt 5 to very good
ASPHALT 1
ASPHALT 2 --------
ASPHALT 3 - - - - -
ASPHALT 4
ASPHALT 5
0.58
SHEAR SUSCEPTIBILITY S.S.
TIME MONTHS
ASPHALT 2 ---------
ASPHALT 3 - - - - -
ASPHALT 4
ASPHALT 5
TIME MONTHS
o
42 M O.
+
2 LOG Y 0.579 +
CORR. COEFF. 0.893
with aging (Figure 7). After 78 months aging, this ratio is minimum
for Asphalt 1 which is poorest, and maximum for Asphalt 3 which is
very good in performance. It seems that the temperature susceptibility
parameter may have more significance in case of low viscosity grade
asphalts. This is further confirmed by the absence of any crack pat-
tern on these test pavements, which can be attributed to temperature
susceptibility.
T. 2-
!
l o ’ -
5-
8
3-
2- +
CONCLUSIONS
Based upon the rheological properties of the six asphalts studied
and the preceding discussions, the following conclusions can be drawn:
1. Aging indices based on viscosity at 77 F. conform to the pavement
performance ratings and thus seem to be more meaningful to indi-
cate comparative aging and life expectancy of the test pavements.
2. Very good correlation was observed between aging indices and shear
susceptibility values of the aged asphalts. Thus shear susceptibility
is one of the important factors affecting the pavement performance.
The aging index-shear susceptibility relationship seems to deter-
mine the pavement durability and performance.
ASPHALT 3 - - - - -
ASPHALT 4
ASPHALT 5
0 IO 20 30 40 50 60 70 80
TIME MONTHS
0.06
Y= -0.0034 + 0.076X
ACKNOWLEDGMENTS
Thanks are due to Messrs. David Streby and Richard Basso for all
the viscosity test data, to Edward for preparing the illustrations
to June Viozzi for compiling the test data.
The opinions, findings and conclusions expressed in this paper are
those of the authors and not necessarily those of Pennsylvania Depart-
ment of Transportation.
112 KANDHAL, SANDVIG AND WENGER
LITERATURE CITED
Discussion
PROF. H. E. SCHWEYER: We certainly are pleased to see this
paper because in a paper that we are presenting on Wednesday we have
shear susceptibility as one of the parameters that we studied in our
field program. I would like to point this out as a comment and if the
blackboard was available I’d give a lecture. The shear susceptibility as
measured in this paper differs a little bit from the commonly used
shear susceptibility definition as will be shown for the analysis of shear
stress versus rate of shear data.
SHEAR SUSCEPTIBILITY TO PERFORMANCE 113
In the ordinary plot log of shear stress, versus log shear rate,
with the power law valid, the following applies
where the slope of the line is C-l with C being the same C as in Eq.
Thus, in the author’s paper the negative value of shear suscepti-
bility is mathematically correct (for C less than 1) and can be recon-
ciled with the value normally used.
MR. W. I have a question regarding initial force and
the ultimate force as shown in one of these graphs. This gives me the
impression that the initial compaction was less than, say, 95 percent of
the final volume weight. In this respect, I would like to remark that in
our country (Netherlands), there is a requirement for a minimum of 95
percent of the volume weight that can be obtained by laboratory com-
paction for the first base course layer, while for the subsequent layers
the minimum is 98 percent. I guess that in our country it is quite im-
possible to have such an enormous deformation after compaction of the
pavement as you have shown here.
MR. L. D. SANDVIG: We have similar requirements in Pennsyl-
vania now. During 1964, when this research project was undertaken,
we allowed 2 to 8 percent air voids in the Marshall design and the re-
quired compaction was 95 percent of the design. This got us into this
situation with the high voids in the placed mat to the extent of 10.3 per-
cent. Today it would be substantially less. We were rather new in the
compaction procedures of bituminous surfaces during the early 1960’s.
It was from this data we learned that we should have something better.
MR. L. W. CORBETT: If I understand you correctly you are favor-
ing the use of low shear susceptibility asphalt, is that right?
MR. SANDVIG: Yes.
MR. CORBETT: Also you are looking at aging index as a quality
criterion?
MR. SANDVIG: Yes.
MR. CORBETT: There’s one thing that bothers me in this re-
spect and that is, most specifications tend towards trying to define as-
phalt cements with good temperature susceptibility or high shear
114 SANDVIG AND WENGER
skid resistance later on, we do have some numbers. I don’t think I said
that a way of handling the void situation was through asphalt necessar-
ily. We’re trying to solve the void situation by gradation and fillers,
etc. other than asphalt. We are conscious of this skid resistance and I
would agree with you, not having the skid numbers with me, that prob-
ably the surface which went first probably did have the highest skid
resistance.
MR. R. NADY: This is rather a comment on one of Dr. Lee’s re-
marks. Looking at the table and also Figure 1 of the paper, one ob-
serves that the rutting recorded and the void contents of the mixes
correlate rather well. This indicates that the Number 1 asphalt, a
little stiffer, did not densify quite as much. This tells me, at least I
interpret in this manner, that the rutting noted was more a
tion of the mix and a reduction of the void contents rather than a shear-
ing failure or a lateral shoving of the mix itself.
MR. SANDVIG: I’d agree on that.
MR. C. FOSTER: Mr. Sandvig, I have no comment on your corre-
lation of shear susceptibility and aging index at the months at which it
becomes apparent. But looking at the original data I cannot find any
way to predict which one of these asphalts is going to reach that posi-
tion after 80 months. So shear susceptibility in the original asphalt is
of no help in making this prediction. Also the aging index on either the
original asphalt or after TFO, does not seem to be any help in making
this prediction. Now Mr. Beagle, I want to address a comment to you
and the rest of the Board of Directors. I think your policy on not hav-
ing these papers in advance is detrimental to the quality of the com-
ments we get here, because a lot of the comments presented here would
not have been necessary if we had the papers in advance. I think the
policy should be changed and these papers made available in advance.
MR. C. W. BEAGLE: That will be
MR. T. R. J. FABB (Prepared Discussion): The authors of this
paper cite some of the recent research which has that abso-
lute viscosity alone can not specify the complete rheological behaviour
of paving grade asphalts, and other parameters like shear susceptibil-
ity and/or temperature susceptibility are needed.” They state that
purpose of this report based on data from a research project, is
to determine the effect of shear susceptibility parameter on pavement
durability and performance.” One of their conclusions is of
gain in shear susceptibility and aging index appears to be a necessary
specification requirement for paving asphalts.
At the BP Research Centre we completely concur with the authors’
view on the inadequacy of viscosity alone for specifying the rheological
of bitumen. Indeed, limits for temperature and shear suscep-
tibility were embraced in the specifications for bitumens proposed by
J. L. Duthie (1) where it was also shown that the AASHO specifications
SHEAR SUSCEPTIBILITY TO PERFORMANCE 117
PENETRATION
X VISCOSITY
7 -
,
x
x
I I I I I I I I I
20 30 LO 50 60 70 80 90
BITUMEN PENETRATION AT 77
\
\
\
AFTER MONTHS
I I I I I I
2 3 ‘5 6
FINAL AIR VOIDS CONTENT
13. Since the authors have shown that hardening and shear suscep-
tibility are highly correlated with each other there does not seem to be
anything to be gained by including both properties in a specification. If
hardening during service in the pavement is to be limited by specifica-
tion, yet another test would be required to predict such hardening, over
and above that which occurs during mixing and laying. Apart from the
fact that the degree of hardening to be predicted will vary according to
the permeability of the mix, the severity of the laboratory test condi-
tions that would be required to produce the degree of hardening experi-
enced by the authors would be such as to confer a very high uncertainty
factor on the relationship between predicted and observed bitumen
performance.
AGEING INDEX
VISCOSITY AT 77 AFTER AGEING SERVICE)
VISCOSITY AT 77 BEFORE MIXING
I I I I I I I
6 11 20 22
AGEING INDEX
14. The time available for the preparation of this contribution does
not allow for a full presentation of our own data concerning the effect of
shear susceptibility on pavement performance or for the translation of
our shear susceptibility parameters into the parameter used by the
authors. Nevertheless, we feel that the following evidence shows that
the rate of hardening in dense, impermeable asphalt surfacings, and the
consequential increase in shear susceptibility, are negligible compared
with that experienced by the authors in their work.
Figure E of this contribution is reproduced from and relates to
four of the eight bitumens used in a comprehensive trial of 110 test
surfacings laid in southern France in May 1963. The shear susceptibil-
ity is a function of the parameter b and it should be noted that shear
SHEAR SUSCEPTIBILITY OF PERFORMANCE 121
I O
/ - -- - - - _ _ _
,
,
2
BITUMEN
CODE No
2
4 -
9 - - - - - -
- - - - - -
_ - - - -
-- 9
4
1
I I I
20 40
TIME IN SERVICE-MONTHS
1
SHEAR SUSCEPTIBILITY =
APPARENT VISCOSITY AT
APPARENT VISCOSITY AT
0
6 0
- 7 6
i i
8
72
- 7 0
- 6 6
60
56
2.2
SHEAR SUSCEPTIBILITY OF BITUMEN
Although the relationships are not very good, a clear trend is evi-
dent, particularly at the more critical higher speed. As with the as-
phalts discussed under 14 (above), voids contents are low, hardening in
service has been minimal, and after 4 years trafficking the test sections
are in very good condition.
These results, which will be included in a further publication on
this subject, have been quoted in an attempt to offset the impression
given by the authors that high shear susceptibility is undesirable.
16. From a rheological/mechanical point of view, high shear sus-
ceptibility can convey definite advantages, one of which, indicated in
earlier publications is a reduction of the change of asphalt
stiffness with temperature and loading time. This property can be em-
ployed to reduce both the tendencies of asphalt to crack at very low
temperatures and to deform at high temperatures.
17. It is pertinent to record that the effect of bitumen hardening in
service (i.e., increase in Newtonian viscosity) on increase of stiffness
at thermal and traffic loading times is very much reduced by the asso-
ciated increase in shear susceptibility of the bitumen. (Study of Fig-
ures 2 and 3 of Reference (1) will make this clear.) Thus, far from
being undesirable, the increase of shear susceptibility helps to alleviate
the situation created by the hardening of the bitumen.
In conclusion, we feel that from the results of their trial the authors
are not justified in attributing differences in road performance to in-
creases in shear susceptibility.
Literature Cited
1. J. L. Duthie, “Proposed Bitumen Specifications Derived from Fundamental
Parameters, Proceedings of the Association of Asphalt Paving Technolo-
gists, Vol. 41 pp. 70-117.
2. E. H. Chipperfield, J. L. Duthie, and R. B. Girdler, Characteristics
in Relation to Road Performance Proceedings of the Association of Asphalt
Paving Technologists, Vol. 39 pp. 575-613.
3. J. Huet, J. Reichert, and P. Outer, en
Asphaltiques-Bitumes et Technique Rout&e, (Brussels), Vol.
14, No. 2 pp. 37-40.
4. J. Huet, “Enseignements des Routes en
Asphaltiques (Grand Meise, Hoeilaart),” La
(Brussels), Vol. 17, No. 1 pp. 3-28.
5. Road Research Laboratory, Research on Road Safety. London: Her Ma-
jesty’s Stationery Office, 1963.
6. E. H. Chipperfield and T. R. J. Fabb, “Development of More Durable Road
Surfacings, Proceedings of the Canadian Technical Asphalt Association
pp. 157-180.