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LABORATORY MEASUREMENT OF VELOCITY

AND RESISTIVITY ON DIFFERENT


SATURATED RESERVOIR ROCKS
Amir Mustaqim bin Majdi
Bachelor of Technology (Hons) Petroleum Geoscience
Universiti Teknologi Petronas
Tronoh, Perak Darul Ridzuan
Email: amir.mustaqim103@gmail.com

Abstract Understanding the basic rock elastic properties such well as macroscopic of core sample. However, different data
as porosity, density, P and S wave propagation, reflectivity, scale has differences in term of resolution or data quality.
acoustic impedance and electric property such as resistivity are Seismic image covers the vertical and horizontal resolution of
very important in hydrocarbon exploration. To be precise, these larger area but the data is low in resolution. Meanwhile, well
properties have relationship which can help in doing reservoir
data has better horizontal resolution but the data only limited to
interpretation. The main purpose of this project is to understand
the behavior of wave velocity and resistivity for different type of the particular drilled well hole only. Core sample has finer data
fluid filling the reservoir rock. In this project, Berea Sandstone resolution than well data and will give better understanding on
core sample is used which represent the reservoir rock. the reservoir properties. This project will focus on determining
Laboratory measurements of velocity and resistivity were taken the behavior of wave velocity and resistivity responses of
for the core in dry, saturated with brine, saturated with fresh different type of saturated reservoir rock for the macroscopic
water and partially saturated. Velocity measurement is done by scale. A laboratory test will be conducted using a sandstone
using OYO SonicViewer- SX meanwhile resistivity is done using core sample which representing the reservoir rock. The results
SCIP (Sample Core I.P.) tester. The findings shows that wave obtained from the laboratory measurement can help people such
travel faster through denser material such as fluid saturated core
as geoscientists and engineers to understand the velocity and
sample compared to dry or gas saturated core sample. Meanwhile,
material which have higher electrical conductivity such as brine resistivity readings especially in reservoir monitoring.
solution will enhance the movement of electrical current hence
reducing the electrical resistivity value. Pure electrical insulator 1.2 PROBLEM STATEMENT
material such as silica minerals did not support the movement of
electrical current, hence increase the electrical resistivity value of Understanding the velocity and resistivity properties of rock
the material. through large data scale such as seismic image is very difficult
and complex. This is because the data obtained is low in
Keywords- Rock elastic properties, Vp, Vs, resistivity.
resolution as the image is captured by the low frequency waves
INTRODUCTION and includes anisotropy and heterogeneity. Furthermore, the
processes for obtaining the data will cost a lot of money. For
example, in order to obtain the seismic and well data, seismic
1.1 BACKGROUND survey and well drilling need to be done. This matter become a
limitation and lead to lack of proper understanding upon
Understanding the basic rock properties are very important velocity and resistivity. However, the understanding by core
in hydrocarbon exploration. Some examples of the rock sample measurement is more advantage and can be done as it is
properties that can be measured are the porosity, density, P and much cheaper. In addition, we able to control the parameters
S wave propagation, reflectivity, acoustic impedance and also that affect the responses of wave velocity and resistivity such
resistivity. All of these elastic properties are related to each as type of fluid, fluid concentration, clay content, porosity,
other and they can be helpful in doing reservoir interpretation pressure and others.
especially in identifying the type of reservoir rock and fluid that
saturated within them. The understanding of these properties 1.3 OBJECTIVE
also can be done through different data scales such as
mesoscopic of seismic image, megascopic of well data and as
The objective of this project is to study the wave applied in various direction. There are three main elastic moduli
velocity and electrical resistivity for different type of fluid which related to each type of deformation which is Young
saturated of reservoir rock which represented by Berea Modulus (E), Bulk Modulus (K) and also Shear Modulus ().
Sandstone core sample. Youngs Modulus (E) can be defined as the ratio of extensional
stress to extensional strain in uniaxial stress state. Simple
1.4 SCOPE OF STUDY example for this modulus is the change of length of a rubber rod
when it being pull apart the ends of the rod. Bulk Modulus (K)
The study includes a laboratory measurement of the velocity can be defined as the incompressibility of a medium. When a
and resistivity responses for different condition of a sandstone small cube of material is being squeezed on all side, the volume
core sample. The core sample will be prepared into different will change. Large value of K indicates the volume did not
condition such as below: change much and compression cannot being done very much as
i. Dry (gas saturated) the medium is very stiff. Meanwhile, if the value of K is small,
ii. Fully saturated with brine the material can be compress a lot such as gas. Lastly, the Shear
iii. Fully saturated with fresh water Modulus () tell the difficulty to deform a cube of material
iv. Partially saturated when shearing force being applied. Large value of indicates
the shape of the material cannot be changed easily. Gas and
LITERATURE REVIEW liquid do not support shear forces which means the value of
will be zero. In addition, Poissons Ratio () is an additional
2.1 RESERVOIR ROCK parameter which related to stress and strain of a material.
Poissons Ratio is the ratio of transverse contraction strain to
Society of Petroleum Engineers Glossary has defined the longitudinal extension strain in the direction of stretching force
reservoir rock as a type of rock that contains porosity, (Lakes, 2016). Furthermore, Yun-ping (2007) also explained
permeability, sealing mechanism and also sufficient amount of that the elastic constant such as elastic modulus and the
hydrocarbon accumulation (Ishimwe, 2014). Furthermore, all Poissons ratio are the basic mechanical properties that is
hydrocarbon created by the source rock will not be economical necessary to be considered in rock engineering project analysis
and useful to be extract unless it being stored in a container and design.
which known as reservoir rock. Normally, the type of reservoir In interpretation of seismic data, the wave velocity are one
rock is influenced by their contents, composition, morphology of the great interest to the geoscientist. There are two type of
and also sedimentology. The most common type of rock wave velocities which are P-wave and S-wave. As being
associated with hydrocarbon are sedimentary rocks which explained by Fjr et al., (2008), the velocity of the propagation
includes sandstone and carbonate mud or dolomite. Sandstone wave depends mainly on the elastic stiffness and the density of
has numerous pore spaces that provide spaces for trapping the the rock. The E, K, and density of a material will affect the
hydrocarbon. This is the reason why sandstone being classified velocity of wave that propagate through it. The equations below
as the most common reservoir rock. shows how the properties related to compressional velocity, Vp
It takes millions of years for the decaying organic matter and shear velocity, Vs.
such as algae and planktons to be converted into hydrocarbon.
This process occurs within the source rock. They were buried +
4
by the sedimentation process and being cook at certain = 3

temperature. Lastly, they were converted into liquid
hydrocarbon which migrated upward, trapped by the seal of
= (1)
reservoir rock.

Fluid that accumulated within the reservoir rock are K is the bulk modulus, is shear modulus and is the
normally three phases, which is water, oil and gas. These three density. In relation with that, this project will able to explain
fluid types are very important for the petroleum engineers to the behavior of velocities responses when wave propagate
identify the preferable method of extracting them. The fluid through different density of sandstone core sample which
content within the reservoir is estimated by studying the rock represented by different type of fluid saturation. As mentioned
properties itself either direct way or indirect. The direct way is by Dvorkin & Nur (1998), the interpretation which relate the
by doing field data acquisition through well logging. velocity and to pore-fluid compressibility are among most
Meanwhile, the indirect way can be done by conducting important deliverable of rock physic. In addition, there are
laboratory measurement on core samples of the reservoir rock many factors which can affect the density. One of them is the
which what will be done for this project. fluid type that filling the pore spaces. The following equation
can be used to determine the bulk density by assuming the rock
having both single type of mineral and fluid filling the pores.
2.2 ELASTIC PROPERTIES OF ROCK
= (1 ) + (2)
Elastic property can be describe as the measurement of the
propensity of a rock to deform non-permanently when stress is
b is the bulk density of rock, is the porosity, m is bulk and electrical conductivity are determined mostly by the water
density of rock matrix and f is the bulk density of fluid. In this content. Benjamin and Paul (2013) mentioned that correlating
project, the fluid involved are gas, freshwater and also brine resistivity measurements with geophysical resistivity models
solution. helps constrain these models to the geology and lithology of an
Furthermore, Hamada (2004) also discussed that the use of area. Generally, the higher the conductivity of a medium, the
ratio of compressional wave velocity to shear wave velocity, lower the resistivity. Crain, (n.d.) describe that the pure water
Vp/Vs, is a good tool in identifying the fluid type in the is a very poor conductor and if an amount of salt is added to the
reservoir rock. In fact, as the light hydrocarbon saturation water, the solution become more conductive. This is because
increase, the compressional wave decrease and shear wave higher quantity of charged ions enhance the conductivity of the
velocity increase. This makes the Vp/Vs ratio more sensitive fluid. The reservoir rock saturated with gas, oil and also fresh
toward the changes of fluid type comparing by using Vp or Vs water will show high resistivity value. Meanwhile, for rock
separately. The denser rock tend to have high velocity, which is saturated with brine will showing low resistivity value as it is a
rock saturated with water compared to dry rock or gas- good conductor.
saturated. Moreover, Vp is always higher than Vs for any type
of rocks (Yilmaz, 2015).
2.5 RESERVOIR MONITORING

2.3 FLUID SUBSTITUTION MODELLING Time-lapse seismic reservoir monitoring which known as
4D seismic is the comparison of the 3D seismic surveys in the
According to He, T., & Schmitt, D. (2006), fluid same geographic location at different times (Fanchi et al.,
substitution modelling is a method which able to explain the 1999). This powerful technique able to monitor changes which
behavior of the rock properties with the changes of fluid happens within the reservoir during production in the
saturation within the reservoir. Besides, this technique can be dimension of x,y,z and time. In addition, Fanchi et al. (1999)
used also for evaluating the changes of wave velocity when also explained that the analysis of 4D seismic enhance the
there is increase or decrease of pore fluid saturation as well as ability to image fluid movement hence improving the quality of
the type. In addition, this technique normally associated with reservoir characterization, identification of fluid movement
the application of Gassmanns equation (1951) which have interfaces and also helping operators locating bypassed
been rearranged by Mavko et al as shown below; reserves. Anderson et al. (1996) stated that 4D seismic is most
effective in offshore fields due to its higher quality of 3D
seismic data and 4D seismic also works better in soft
= + (3)
( ) unconsolidated sands than the carbonate reservoir.
Besides, injections of water or gas normally being done
(2) (2) (1) (1)
= during hydrocarbon production in order to improve the
(2) ( (2)) (1) ( (1))
recovery. At the same time, 4D seismic technology can be used
(4) to monitor the variation of changes from it. The changes of
subsurfaces elasticity can be monitored by comparing the
The application of Gassmanns is based on certain assumptions differences in some properties measurement such as travel
such as the rock sample is homogenous and isotropic, complete times, reflection amplitude and also seismic velocities. Fig. 1
connection of the rocks pore spaces, low elastic stiffness and below shows the 4D seismic acquisition of Gullfaks field. As
lastly low seismic frequency. Smith, T. M., Sondergeld, C. H., the time changes from 1985 to 1999, the oil is being replaced
& Rai, C. S. (2003) stated that the shear modulus of an isotropic by water. The seismic amplitude changed and this information
material is not depend on pore fluid, hence remain at constant able to tell location and how much oil is present there at a time.
during fluid substitution process.

2.4 ELECTRICAL RESISITIVITY OF WATER-


BEARING ROCKS

Hersir and rnason, (2009) stated that the conductivity of


rock near the earths surface is dominated by the electrolytic
conduction in aqueous solution of common salts distributed
through the pores of the rock. The rock matrix itself is actually
the insulator and examples of the parameters which influence
the electrical resistivity of the rocks are the porosity, amount of
water, salinity of water and also the temperature (Hersir and
rnason, 2009). In addition, Parkhomenko, (1967) also
explained that although solid minerals are the main constituent
Figure 1 4D seismic acquisition, example form Gullfaks field (Eltvik, P.,
of a rock, the other properties such as dielectric permeability 2010)
Statoil petrophysicists have compared sonic logs responses 3.2 VELOCITY AND RESISTIVITY TEST
from the Gullfaks field in order to to monitor the oil-water-
contact (OWC). Higher velocities readings were obtained in The velocity measurement will be conducted by using the
the water-filled zones than in those zones filled with oil. OYO SonicViewer-SX and resistivity will be measured using
Furthermore, when periodic logging being done at the same SCIP (Sample Core I.P.) tester in the laboratory.
well using Reservoir Saturation Tool (RST), the OWC was OYO SonicViewer-SX is an instrument which produce
rising 13 m per year. At above OWC, the sonic logs readings compressional and shear waves velocities readings upon the
were same from one year to another but at below OWC, sonic measurement of ultrasonic waves travel time through a core
velocities increased due to the replacement of oil by water. sample. During measurement, the core sample will be placed in
Carbon Capture and Storage (CCS) is another technology between two transducers as shown in Photo 1. Wax is wiped on
which involve in reservoir monitoring. CCS is an initiative for the surface contact of the core with the transducer in order to
reducing greenhouse gas emission that increase earth provide a good reading. One of the transducer will generate the
temperature nowadays. It is able to capture carbon dioxide ultrasonic wave and the other one will receive the propagated
(CO2) and stored them deep inside the depleted oil and gas field wave. Average readings of Vp and Vs are calculated and
or saline formation. Huppert and Neufeld (2014) explained that recorded.
for efficient injection and storage, CO2 should be pumped into SCIP (Sample Core I.P.) tester is an instrument which
the storage reservoir at depth greater than 800 m. These depths measure the apparent resistivity and time domain induced
ensures the CO2 is stored in supercritical conditions which in polarization (IP) of core sample. During the measurements,
denser than gaseous, hence more CO2 per volume is stored core sample is placed into the core holders as shown in Photo 2
(Bachu et al., 1994). In addition, the viscosity of CO2 is lower below. The readings are taken when the contact resistance
than formation water. This condition caused CO2 injected to become stable. Average reading of the resistivity is calculated
spread and accumulate above the formation water phase and recorded.
(Suekane et al., 2005). A study has been done by Lamech
Omondi regarding acoustic velocity and electrical resistivity RESULT AND DISCUSSION
responses in sandstone reservoir when injection of CO2 is done.
The results showing that, in the CO2 injection process, Vp 4.1 VELOCITY
decrease drastically while Vs changes slightly and the
resistivity increase monotonously. The mass of the gas filling or dry core sample increase as
being saturated with freshwater and also brine solution. As fluid
METHODOLOGY
replacing the pore spaces, the core sample gain more mass. In
addition, each fluid has their own density. The density of gas is
A Berea Sandstone core sample is used for the lab 0.0098 g/cm3, freshwater is 1 g/cm3 and 30 000 ppm brine is
measurement. The dimension of the core is measured precisely 1.02 g/cm3. According to the equation (5), bulk density (b) is
using the electronic caliper. The porosity and grain density are directly proportional to the fluid density (f). Density of
measurement directly using the PoroPerm instrument porosity, freshwater and brine are greater than gas, causing the higher
grain density, bulk density, permeability (air) and other bulk density. Meanwhile, brine is denser than freshwater,
perimeters. causing higher bulk density for it. Increase of fluid saturation
(Sw) also lead to the increase of bulk density (b) as shown in
3.1 SATURATING CORE SAMPLE Fig. 2 below.

Core sample saturation being done before velocity and


resistivity measurement. The core sample need to be prepared
in dry (gas saturated), fully saturated with brine, fully saturated
with fresh water and also partially saturated. The equipment
used are oven, desiccator with pump, beakers and electronic
balance. 30 000 ppm brine solution is prepared why dissolving
30 grams of sodium chloride, NaCl into 1 liter of distilled water.
Dry (gas saturate) core sample is prepared by drying it in
the oven for 2 days and mass is measured using electric balance
and recorded. Full freshwater and brine saturated is prepared by
saturating the core using glass desiccator which air have been
pumped out for a day. Partially saturated is done by saturating
them for half day. Sw is checked by the calculation using
Figure 2 Graph of bulk density vs fluid saturation
equation (5) below;

b = (1 )m + [Sww + (1 Sw)g] (5) In this project, the results in Fig. 2 shows that Vp is reduced
significantly for the core sample which in partially saturated
condition and increase as the core sample being fully saturated proportional to Vp, it cause the Vp to increase as the density
(Fig. 3). Moreover, Vp for fully brine saturated core sample is and K increase. Since density of brine is higher than freshwater,
greater compared to fully freshwater saturated and dry core is the Vp of brine saturated core is bigger (Figure 7). is not
the lowest. supported by gas or liquid and the value is considered zero.
Wang et. al. (1990) also mentioned that Vs have very small
sensitivity toward fluids. Meanwhile, as the is zero,
theoretical value of Vs should decrease as density increase.
However, this project shows that Vs increase from dry to fully
saturated for both freshwater and brine. This happens due to the
low effective stress upon the core sample as the measurement
is taken at normal atmospheric condition. This results is similar
to the experiment conducted by Tao, G., King, M. S., & Nabi-
Bidhendi, M. (1995). They observed that Vs is higher for brine
saturated sandstone compared to dry sandstone at low effective
pressure. Meanwhile, for high effective pressure, the S-wave
velocities for the brine saturated sample are lower than the dry
sample. The sudden increase of Vs for partially freshwater
saturated core sample can be related to some errors. The human
error can be the unparalleled positioning of core sample to the
both transducers and also the wax put to the core is not spread
Figure 3 Graph of Vp vs fluid saturation
evenly. In addition, the significant decrease of Vp for partially
fluid saturated core also can be related to the presence of gas in
Besides, different trend occurred to the measurement of Vs. the rock sample. Ali, T., Din, Z. U., Khalid, P., & Ahmed, N.
Vs significantly increase as core sample being saturated by the (2013) explained that the increase of gas saturation will
brine. However for freshwater saturated, Vs increase in partial decrease the bulk modulus as well as density and Vp. For
saturated condition and decrease at full saturation. Both Vs for partially saturated condition, small amount of gas saturation
fully freshwater saturated is still higher than Vs for dry core able to reduce the Vp.
(Fig. 4).
4.2 RESISTIVITY

The resistivity readings of dry core is much greater compare


to the wet core (Fig. 5).

Figure 4 Graph of Vs vs fluid saturation

Density of medium and fluid saturation have great impact


on the behavior of the Vp and Vs. The density factor which
influences the changes of Vp and Vs for this project is similarly
discussed by Han, D. H., & Batzle, M. L. (2004).
Figure 5 Graph of resistivity vs fluid saturation
Based on the velocity equations (1), density () is
inversely proportional to the velocity which means velocity
decrease as density increase. In addition, bulk modulus (K) and
shear modulus () modulus are also considered along with CONCLUSION
density As the rock being saturate by freshwater and brine, the Based on this project, the density of fluid which filling the
rock become stiffer and greatly lead to the increase of the pore spaces of the Berea Sandstone core sample is greatly affect
compressibility (K increase). Yilmaz . (2015) also explained the rocks elastic properties such as bulk modulus (K) and shear
that there is slow change of Vp for fluid saturated sample modulus (). Bulk density is greater for denser type of fluid
compared to dry sample. As great change of K is directly saturated the sandstone. The consequent of the change of these
elastic properties influence the change of velocity of wave. The conditions, Journal of Central South University of
velocity of wave especially Vp for the denser, stiff material will Technology, pp. 210215, Apr. 2007.
be higher compared to the less dense, less stiff material. Vp is [6]. Crain's Petrophysical Handbook - Resistivity Concepts
better in analyzing the fluid type compared to Vs which is less -- Ohm's Law, Crain's Petrophysical Handbook -
sensitive to gas and fluid. In reservoir monitoring, the velocity Resistivity Concepts -- Ohm's Law. [Online]. Available:
and density of gas sand will be much lower than oil sand, https://spec2000.net/06-resistivityohm.htm. [Accessed:
freshwater sand will be higher than oil sand and brine sand will 02-Apr-2017].
be the highest. In term of seismic amplitude, the highest [7]. D. E. H. Han and M. L. Batzle, Gassmann's equation
negative reflection coefficient will be the changing of denser
rock to gas sand, followed by oil sand, freshwater sand and and fluid saturation effects on seismic velocities,
brine sand. The resistivity measurement will be highest for the Geophysics, vol. 69, no. 2, pp. 398405, 2004.
material that have less electrical conductivity such gas sand,
followed freshwater and the lowest which is brine water. [8]. D. Ishimwe, Reservoir rock properties, Reservoir rock
properties - SPE Connect, 29-Sep-2014. [Online].
Available:http://connect.spe.org/blogs/donatien-
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This project can be improved by using more type of core
samples from many area in order to observe their velocity and [9]. F. T. Westlye, Measurements of Young's Modulus on
resistivity response. Furthermore, in order to provide a core Rock Samples at Small Amplitude and Low
sample which fully saturated with fluid such as brine and fresh Frequency, thesis, Institutt for fysikk, 2011.
water, longer duration of immersion is preferable. In addition, [10]. G. Tao, M. King, and M. Nabi-Bidhendi, Ultrasonic
mineralogy need to be identify under thin section since Berea wave propagation in dry and brine-saturated sandstones
Sandstone is not a clean sandstone. Since there are many as a function of effective stress: laboratory
parameters that affect the velocity of wave through the rock, measurements and modelling1, Geophysical
comparison between two or three sample that having different Prospecting, vol. 43, no. 3, pp. 299327, 1995.
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ACKNOWLEDGMENT Predicting Strength Properties of Rocks from P-Wave
I would like to thank my supervisor, Mr. Luluan Almanna Velocity Under Different Degrees of Saturation, Rock
Lubis for the opportunity given to conduct this project and also Mechanics and Rock Engineering, vol. 46, no. 5, pp.
guidance provided throughout my final year project course. My 981999, 2013.
sincere appreciation also goes to the laboratory technologists [13]. J. Dvorkin and A. Nur, Time-average equation
for their help in completing the laboratory works. Lastly, revisited, Geophysics, vol. 63, no. 2, pp. 460464,
special thanks to my family and fellow colleague for their moral 1998.
support. [14]. J. R. Fanchi, T. A. Pagano, and T. L. Davis, State Of
The Art Of 4D Seismic Monitoring: The Technique, The
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