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SPECIFICATION FOR

CARBON AND ALLOY STEEL NUTS FOR BOLTS


FOR HIGH-PRESSURE AND
HIGH-TEMPERATURE SERVICE

SA-194 /SA-194M

(Identical with ASTM Specification A 194 /A 194M-95a except for editorial differences in 4.1.1 and S5.1.) 98

1. Scope 1.5 The values stated in either inch-pound units or


SI units are to be regarded separately as standard.
1.1 This specification covers a variety of carbon,
Within the text, the SI units are shown in brackets. The
alloy, and martensitic stainless steel nuts in the size
values stated in each system are not exact equivalents;
range 14 through 4 in. [6.4 through 101.6 mm] nominal.
therefore, each system must be used independently of
It also covers austenitic stainless steel nuts in the size
the other. Combining values from the two systems may
range 14 in. [6.4 mm] nominal and above. These
result in noncomformance with the specification.
nuts are intended for high-pressure or high-temperature
service or both. Grade substitutions without the purchas- NOTE Grade 2M has been replaced with Grade 2HM. During
ers permission are not allowed. a transition period both grade markings are acceptable.

1.2 Bars from which the nuts are made shall be hot-
wrought. The material may be further processed by 2. Referenced Documents
centerless grinding or by cold drawing. Austenitic stain-
less steel may be solution annealed or annealed and 2.1 ASTM Standards:
strain-hardened. When annealed and strain hardened A 29 /A 29M Specification for Steel Bars, Carbon and
austenitic stainless steel is ordered in accordance with Alloy, Hot-Wrought and Cold-Finished, General Re-
Supplementary Requirements S1, the purchaser should quirements for
take special care to ensure that 7.2.2, Supplementary A 276 Specification for Stainless and Heat-Resisting Steel
Requirements S1, and Appendix X1 are thoroughly Bars and Shapes
understood. A 320 /A 320M Specification for Alloy-Steel Bolting Ma-
terials for Low-Temperature Service
1.3 Supplementary requirements (S1 through S6) of A 370 Test Methods and Definitions for Mechanical Test-
an optional nature are provided. These shall apply only ing of Steel Products
when specified in the inquiry, contract, and order. A 484 /A 484M Specification for General Requirements
for Stainless and Heat-Resisting Bars, Billets, and
1.4 This specification is expressed in both inch- Forgings
pound units and in SI units. However, unless the order A 751 Test Methods, Practices, and Terminology for
specifies the applicable M specification designation Chemical Analysis of Steel Products
(SI units), the material shall be furnished to inch- A 788 Specification for Steel Forgings, General Require-
pound units. ments

271
SA-194 /SA-194M 1998 SECTION II

E 18 Test Methods for Rockwell Hardness and Rockwell 4. Ordering Information


Superficial Hardness of Metallic Materials
4.1 The inquiry and order for material under this
E 381 Method of Macroetch Testing, Inspection, and
specification shall include the following as required to
Rating Steel Products, Comprising Bars, Billets,
describe the material adequately:
Blooms, and Forgings
4.1.1 Specification designation and grade,
2.2 American National Standards:
B1.1 Unified Screw Threads 4.1.2 Quantity, number of pieces,
B1.2 Gages and Gaging for Unified Screw Threads
4.1.3 Dimensions (see Section 9),
B18.2.2 Square and Hex Nuts
4.1.4 Options in accordance with 6.1, 7.2.2.1, 9.1,
2.3 AIAG Standard:
9.2, 10.3, 11, 12, and 13, and
AIAG B-5 02.00 Primary Metal Identification Tag Appli-
cation Standard 4.1.5 Supplementary Requirements, if any.

5. Manufacture (Process)
3. Terminology
5.1 The steel shall be produced by any one of the
3.1 Descriptions of Terms Specific to This Standard:
following processes: open-hearth, basic-oxygen, electric-
3.1.1 Lot: furnace, or vacuum-induction melting (VIM). The pri-
mary melting method may incorporate separate degass-
3.1.1.1 Unless otherwise specified (see 3.1.1.2), ing or refining. The molten steel may be vacuum-
a lot is the quantity of nuts of a single nominal size treated prior to or during pouring of the ingot or strand
and grade produced by the same manufacturing process. casting. The basic-oxygen process shall be limited to
steels containing not over 6% chromium.
3.1.1.2 When Supplementary Requirement S6 is
invoked on the purchase order, the following definitions 5.1.1 Quality To ensure soundness, ferritic steel
of a lot shall apply: bars shall be tested in accordance with Method E 381,
or other suitable method as agreed upon between the
For Grade 8 Nuts The quantity of all the nuts purchaser and the producer. Either the bar producer or
of a single nominal diameter and grade made from the the nut producer, as agreed upon between them, shall
same heat of steel and made by the same manufacturing perform the test. Quality control procedures shall be
process. sufficient to demonstrate that the testing was performed
and that the results were acceptable. A bar lot consisting
For All Other Grade Nuts (see 7.2 and 7.1.2.1) of one heat or 10 000 lbs, whichever is smaller, shall
All the nuts of a single nominal diameter and grade be represented by a minimum of one macroetch. Visual
made from the same heat number and heat treated in examination of transverse sections shall show no imper-
the same batch if batch-type heat treating equipment fections worse than the macrographs of Method E 381
is used or heat treated in the same continuous run of S4-R4-C4 or equivalent as agreed upon. Distinct zones
not more than 8 h under the same conditions if continu- of solidification shall not be present.
ous-type heat treating equipment is used.
5.2 Stainless steels for all types of Grade 6 and 8
3.1.2 Type: nuts shall be made by one of the following processes:
3.1.2.1 For Grade 8 Nuts Variations within 5.2.1 Electric-furnace (with separate degassing and
the grade designated by a letter and differentiated by refining optional),
chemistry and by manufacturing process.
5.2.2 Vacuum induction furnace, or
3.1.2.2 For Grade 6 Nuts Variations within 5.2.3 Either of the above followed by electroslag
the grade designated by the letter F as differentiated remelting, or consumable-arc remelting.
by chemical additions made for machineability.
5.3 The steel producer shall exercise adequate control
3.1.3 Series The dimensional relationship and to eliminate excessive unhomogeneity, nonmetallics,
geometry of the nuts as described in ANSI B18.2.2. pipe, porosity, and other defects.

272
PART A FERROUS MATERIAL SPECIFICATIONS SA-194 /SA-194M

5.4 Grades 1 and 2 nuts shall be hot or cold forged, of the steel. For strand cast materials, the requirements
or shall be machined from hot-forged, hot-rolled, or of 8.2 and 8.3 of Specification A 788 shall be met.
cold-drawn bars. Should the purchaser deem it necessary to have the
transition zone of two heats sequentially cast discarded,
5.4.1 All Grade 1 and 2 nuts made by cold forging
the purchaser shall invoke Supplementary Requirement
or by machining from cold-drawn bars shall be stress-
S3 of Specification A 788.
relief annealed at a temperature of at least 1000F
[538 C]. 6.2 The heat analysis of the nut materials shall
conform to the chemical composition requirements for
5.4.2 Grade 1 and 2 nuts made by hot forging or
the grade ordered as specified in Table 1. Nuts that
by machining from hot-forged or hot-rolled bars need
are normally furnished from stock are not identified
not be given any stress relief annealing treatment.
by heat number, and thus heat analysis cannot normally
5.5 Grades 2HM, 2H, 3, 4, 6, 6F, 7, 7M, and 16 be reported to the purchaser. (See Supplementary Re-
nuts shall be hot or cold-forged or shall be machined quirement S2.) Supplementary Requirement S6 is pro-
from hot-forged, hot-rolled, or cold-drawn bars and vided for use when heat analysis control is required.
shall be heat treated to meet the required mechanical
6.3 Steels with added lead shall not be used.
properties. However, nuts machined from heat-treated
bars need not be reheat treated. See Supplementary 6.4 Product analyses may be made by the purchaser
Requirement S4 for nuts to be used in low-temperature from a sample nut selected by the purchaser or the
applications (Specification A 320 /A 320M). These purchasers representative from each item in the ship-
grades of nuts shall be reheated above the critical range ment which shall meet the product analysis requirements
of the steel, quenched in a suitable medium, and then for the grade ordered in Table 1. Product analysis
tempered at a temperature not less than the following: tolerances are found in Tables 5 and 6 of Specification
Minimum Tempering
A 29 /A 29M, and Table 1 of Specification A 484 /A
Grade and Type Temperature, F [C] 484M.
2H 850 [455] 6.5 A starting material that specifically requires the
2HM 1150 [620]
addition of any element beyond those listed in Table
3 1050 [565]
4 1100 [595] 1 is not permitted. This does not preclude the use of
6 and 6F 1100 [595] deoxidizers.
7 and 7M 1100 [595]
16 1200 [650] 6.6 Chemical analysis shall be performed in accord-
ance with Test Methods A 751.
5.5.1 Grade 6 and 6F nuts shall be tempered for
a minimum of 1 h at the temperature.
7. Mechanical Requirements
5.6 Grades 8, 8C, 8M, 8T, 8F, 8P, 8N, 8MN, 8R,
8S, 8LN, 8MLN, and 8MLCuN nuts shall be hot or 7.1 Hardness Test:
cold forged, or shall be machined from hot-forged, hot-
7.1.1 Requirements:
rolled or cold-drawn bars.
5.7 Grades 8A, 8CA, 8MA, 8TA, 8FA, 8PA, 8NA, 7.1.1.1 All nuts shall be capable of meeting the
8MNA, 8RA, 8SA, 8LNA, 8MLNA, and 8MLCuNA hardness requirements specified in Table 2.
nuts shall be hot or cold-forged or shall be machined 7.1.1.2 Sample nuts of Grades 1, 2, 2H, 2HM,
from hot-forged, hot-rolled, or cold-drawn bars and the 3, 4, 7, 7M, and 16 which have been given the treatment
nuts shall subsequently be carbide-solution treated by described in 7.1.5.2 shall meet the minimum hardness
heating them for a sufficient time at a temperature to specified in Table 2.
dissolve chromium carbides followed by cooling at a
rate sufficient to prevent reprecipitation of the carbides. 7.1.2 Number of Tests (Grades 1, 2, 2H, 3, 4, 7,
and 16 and all types of Grade 6):
7.1.2.1 Tests on the number of sample nuts in
6. Chemical Composition
accordance with the following table shall be performed
6.1 An analysis of each heat of steel used for nuts in accordance with 7.1.5.1 by the manufacturer follow-
shall be made by the manufacturer during the pouring ing all production heat treatments:

273
SA-194 /SA-194M 1998 SECTION II

Lot Size Samples performed with consideration to (1) protect legibility


Up to 800 1 of markings; (2) minimize exterior dimensional changes;
801 to 8000 2 and (3) maintain thread fit.
8001 to 22 000 3
Over 22 000 5 7.2 Proof Load Test:
7.2.1 Requirements All nuts shall be capable
7.1.2.2 In addition, a hardness test shall be
of withstanding the proof loads specified in Table 3.
performed by the manufacturer in accordance with
However, nuts manufactured to dimensions and config-
7.1.5.2 on one sample nut selected from each nominal
urations other than those covered by ANSI B1.1 and
diameter and series from each grade and heat number
B18.2.2 are not subject to the proof load test.
following completion of all production heat treatments.
7.2.2 Number of Tests:
7.1.3 Number of Tests, Grades 2HM and 7M:
7.1.3.1 The maximum hardness of Grade 2HM 7.2.2.1 Tests on the number of sample nuts in
and 7M shall be 235 HB or 99 HRB (conversion in accordance with 7.1.2.1 shall be performed by the
accordance with Table 2B of Test Methods and Defini- manufacturer following all production heat treatments
tions A 370). Conformance to the maximum hardness except that, unless proof load testing or Supplementary
shall be insured by testing the hardness of each nut Requirement S1 is specified in the order, nuts which
by Brinell or Rockwell B methods as described in the would require a proof load in excess of 120 000 lbf
sections on Brinell Test, Portable Hardness Test, and [530 kN] may be furnished on the basis of minimum
Rockwell Test of Test Methods and Definitions A 370. hardness requirements. Proof load testing of nuts requir-
Surface preparation for hardness testing shall be in ing a proof load of over 120 000 lbf [530 kN] is
accordance with Test Methods E 18. Product which covered in Supplementary Requirement S5.
has been 100% tested and found acceptable shall have
7.2.3 Test Method The test shall be in accord-
a line under the M.
ance with Annex A3, Paragraph A3.5.1, of Test Methods
7.1.3.2 In addition, 7.1.2.2 shall be met. and Definitions A 370.

7.1.4 Number of Tests, All Types of Grade 8 7.3 Cone Proof Load Test:
Tests on the number of sample nuts in accordance with
7.3.1 Requirements This test shall be performed
7.1.2.1 shall be performed in accordance with 7.1.5.1
only when visible surface discontinuities become a
by the manufacturer.
matter of issue between the manufacturer and the
7.1.5 Test Methods: purchaser. The requirements specified in Table 4 shall
be met for the size range 14 to 11 / 2 in. [6.4 to 38.1
7.1.5.1 Test 1 The manufacturer shall perform
mm]. Nuts not in this size range and all types of
the hardness tests in accordance with Annex A3, Para-
Grade 8 nuts are not subject to this test. Also, nuts
graph A3.5.2 of Test Methods and Definitions A 370.
manufactured to dimensions and configurations other
7.1.5.2 Test 2 The manufacturer shall perform than those covered by ANSI B1.1 and B18.2.2 are not
hardness tests in accordance with 7.1.5.1 to sample subject to the cone proof load test.
nuts after the following test heat treatment. After com-
7.3.2 Number of Tests Sample nuts in accord-
pletion of all production heat treatments heat the speci-
ance with 7.1.2.1 shall be tested by the manufacturer.
men nuts to the temperatures indicated below for 24
h, then slow cool. Test at room temperature. 7.3.3 Test Method The test shall consist of
Temperature assembling a hardened cone (see Fig. 1) and the nut
Grade F [C] to be tested on a hardened steel mandrel, and applying
1 850 [455] the proof load specified in Table 4. The mandrel shall
2, 2H, 2HM 1000 [540] conform to the requirements of Annex A3, Paragraph
3, 4, 7, 7M 1100 [590] A3.5.1 of Test Methods and Definitions A 370 except
16 1200 [650] that the threads shall be in accordance with ANSI B1.1
of the appropriate thread series, Class 3A fit. The
7.1.5.3 Special Requirement, Grades 2HM and hardened cone shall be as described in Fig. 2. The lot
7M Preparation of Grades 2HM and 7M nuts for shall be considered acceptable if the sample nut with-
hardness test and the hardness test itself shall be stands application of the proof load without failure.

274
PART A FERROUS MATERIAL SPECIFICATIONS SA-194 /SA-194M

8. Retests 12. Rejection


8.1 Provisions for retests by the purchaser and his 12.1 Unless otherwise specified, any rejection based
representative are specified in Supplementary Require- on tests made in accordance with 6.4 shall be reported
ment S3. to the manufacturer within 30 days from the date of tests.

9. Dimensions 13. Certification


9.1 Nuts shall be hexagonal in shape, and in accord- 13.1 When agreed upon in writing between the
ance with the dimensions for the hex or heavy hex manufacturer and the purchaser, a certification that the
series, as required, by ANSI B18.2.2. Unless otherwise nuts were manufactured and tested in accordance with
specified, the American National Standard Heavy Hex this specification may be the basis of acceptance of
Series shall be used and nuts shall be either double the nuts.
chamfered or have a machined or forged washer face,
13.2 When specified on the order, the manufacturer
at the option of the manufacturer, and, conform to the
shall supply a test report showing the results of the
angularity requirements of ANSI B18.2.2.
mechanical and /or macroetch inspection tests performed
9.2 Unless otherwise specified, threads shall be in in accordance with this specification. The specification
accordance with ANSI B1.1 and shall be gaged in designation included on test reports shall include year
accordance with ANSI B1.2 as described in 9.2.1 of issue and revision letter, if any.
and 9.2.2.
13.3 When required in the order, the chemical analysis
9.2.1 Nuts up to and including 1 in. [25.4 mm] requirements and the minimum tempering temperature
nominal size shall be UNC Series Class 2B fit. for nuts of Grades 2H, 2HM, 3, 4, 6, 6F, 7, and 7M
shall be furnished on the certification. See 6.2 for heat
9.2.2 Nuts over 1 in. [25.4 mm] nominal size
analysis identification. (See Supplementary Require-
shall be either UNC Series Class 2B fit or 8 UN Series
ment S2.)
Class 2B fit. Unless otherwise specified, the 8 UN
series shall be furnished.
14. Product Marking
10. Workmanship, Finish, and Appearance 14.1 All nuts shall bear the manufacturers identifica-
tion mark.
10.1 Nuts shall be free of defects and shall be good
commercial finish. 14.2 Nuts shall be legibly marked to indicate the
grade and the process of the manufacturer, as prescribed
10.2 If visible surface imperfections in size 14 thru
in Table 5.
112 in. [6.4 thru 38.1 mm] and in any grade other
than Grade 8 become a matter of issue between the 14.3 For purposes of identification marking, the
manufacturer and the purchaser, the cone proof load manufacturer is considered the organization that certifies
test described in 7.3 shall be employed. the fastener was manufactured, sampled, tested, and
inspected in accordance with the specification and the
10.3 If a scale-free bright finish is required, this
results have been determined to meet the requirements
shall be specified on the purchase order.
of this specification.
14.4 Bar Coding In addition to the requirements
11. Inspection in 14.1, 14.2, and 14.3, bar coding is acceptable as a
supplementary identification method. Bar coding should
11.1 The manufacturer shall afford the purchasers be consistent with AIAG Standard B-5 02.00. If used
inspector all reasonable facilities necessary to satisfy on small items, the bar code may be applied to the
him that the material is being produced and furnished box or a substantially applied tag.
in accordance with this specification. Mill inspection
by the purchaser shall not interfere unnecessarily with
the manufacturers operations. All tests and inspections
15. Keywords
shall be made at the place of manufacture, unless
agreed otherwise. 15.1 bolting; chemical analysis; marking on fasteners

275
SA-194 /SA-194M 1998 SECTION II

FIG. 1 APPLICATION OF HARDENED STEEL CONE TO TESTING OF NUTS

FIG. 2 HARDENED STEEL CONE

276
PART A FERROUS MATERIAL SPECIFICATIONS SA-194 /SA-194M

TABLE 1
CHEMICAL REQUIREMENTS [NOTES (1), (2)]

Columbium
and Other
Grade Carbon, Manganese, Phosphorus, Sulfur, % Silicon, Chromium, Nickel, Molybdenum, Titanium, Tantalum, Selenium, Elements,
Symbol Material % % % [Note (3)] % % % % % % % %

1 carbon 0.15 min 1.00 max 0.040 max 0.050 max 0.40 ... ... ... ... ... ... ...
max
2, 2HM, carbon 0.40 min 1.00 max 0.040 max 0.050 max 0.40 ... ... ... ... ... ... ...
and 2H max
4 carbon, 0.40 0.70 0.035 max 0.040 max 0.15 . . . ... 0.200.30 . . . ... ... ...
molyb- 0.50 0.90 0.35
denum
3 AISI 501 0.10 min 1.00 max 0.040 max 0.030 max 1.00 4.0 ... 0.400.65 . . . ... ... ...
max 6.0
6 AISI 410 0.15 max 1.00 max 0.040 max 0.030 max 1.00 11.5 ... ... ... ... ... ...
max 13.5
6F AISI 416 0.15 max 1.25 max 0.060 max 0.15 min 1.00 12.0 ... ... ... ... ... ...
with sul- max 14.0
fur
6F AISI 416 0.15 max 1.25 max 0.060 max 0.060 max 1.00 12.0 ... ... ... ... 0.15 min . . .
with se- max 14.0
lenium
7, 7M AISI 4140/ 0.37 0.65 0.04 max 0.04 max 0.15 0.75 ... 0.150.25 . . . ... ... ...
4142/ 0.49 1.10 0.35 1.20
4145,
4140H,
4142H,
4145H
8, 8A AISI 304 0.08 max 2.00 max 0.045 max 0.030 max 1.00 18.0 8.0 ... ... ... ... ...
max 20.0 10.5
8C, 8CA AISI 347 0.08 max 2.00 max 0.045 max 0.030 max 1.00 17.0 9.0 ... ... 10 ... ...
max 19.0 13.0 carbon
content,
min
8M, 8MA AISI 316 0.08 max 2.00 max 0.045 max 0.030 max 1.00 16.0 10.0 2.003.00 . . . ... ... ...
max 18.0 14.0
8T, 8TA AISI 321 0.08 max 2.00 max 0.045 max 0.030 max 1.00 17.0 9.0 . . . 5 ... ... ...
max 19.0 12.0 carbon
content,
min
8F, 8FA AISI 303 0.15 max 2.00 max 0.20 max 0.15 min 1.00 17.0 8.0 . . . ... ... ...
with sul- max 19.0 10.0
fur
8F, 8FA AISI 303 0.15 max 2.00 max 0.20 max 0.06 max 1.00 17.0 8.0 . . . ... ... 0.15 min . . .
with se- max 19.0 10.0
lenium
8P, 8PA AISI 305 0.08 max 2.00 max 0.045 max 0.030 max 1.00 17.0 10.5 . . . ... ... ... ...
with re- max 19.0 13.0
stricted
carbon
8N, 8NA AISI 304N 0.08 max 2.00 max 0.045 max 0.030 max 1.00 18.0 8.0 . . . ... ... ... Nitrogen,
max 20.0 10.5 0.10
0.16
8LN, 8LNA AISI 304N 0.030 max 2.00 max 0.045 max 0.030 max 1.00 18.0 8.0 . . . ... ... ... Nitrogen,
with re- max 20.0 10.5 0.10
stricted 0.16
carbon
8MN, AISI 316N 0.08 max 2.00 max 0.045 max 0.030 max 1.00 16.0 10.0 2.003.00 . . . ... ... Nitrogen,
8MNA max 18.0 14.0 0.10
0.16

277
SA-194 /SA-194M 1998 SECTION II

TABLE 1 (CONTD)
CHEMICAL REQUIREMENTS [NOTES (1), (2)]

Columbium
and Other
Grade Carbon, Manganese, Phosphorus, Sulfur, % Silicon, Chromium, Nickel, Molybdenum, Titanium, Tantalum, Selenium, Elements,
Symbol Material % % % [Note (3)] % % % % % % % %

8MLN, AISI 316N 0.030 max 2.00 max 0.045 max 0.030 max 1.00 16.0 10.0 2.003.00 . . . ... ... Nitrogen,
8MLNA with re- max 18.0 14.0 0.10
stricted 0.16
carbon
8R, 8RA XM19 0.06 max 4.06.0 0.040 max 0.030 max 1.00 20.5 11.5 1.503.00 . . . 0.10 ... Nitrogen,
[Note (4)] max 23.5 13.5 0.30 0.20
0.40
Vanadium,
0.10
0.30
8S, 8SA [Note (5)] 0.10 max 7.09.0 0.040 max 0.040 max 3.54.5 16.0 8.0 ... ... ... ... Nitrogen,
18.0 9.0 0.08
0.18
8MLCuN, S31254 0.020 max 1.00 max 0.030 max 0.010 max 0.80 19.5 17.5 6.06.5 ... ... ... Nitrogen,
8MLCuNA max 20.5 18.5 0.18
0.22
Copper,
0.50
1.00
16 Chromium 0.36 0.45 0.035 max 0.040 max 0.15 0.80 ... 0.500.65 . . . ... ... Vanadium
Molyb- 0.47 0.70 0.35 1.15 0.25
denum 0.35
Vanadium
NOTES:
(1) The intentional addition of Bi, Se, Te, and Pb is not permitted except for Grades 6F, 8F, and 8FA, in which Se is specified and required.
(2) Product AnalysisIndividual determinations sometimes vary from the specified limits on ranges as shown in the table. The several determinations of any individual
element in a heat may not vary both above or below the specified range. Product analysis tolerances may be found in Tables 5 and 6 of Specification A 29/A
29M, and Table 1 of Specification A 484/A 484M.
(3) Because of the degree to which sulfur segregates, product analysis for sulfur over 0.060 % max is not technologically appropriate.
(4) As described in Specification A 276.
(5) Similar to grade S21800 of Specification A 276, except phosphorus is restricted to 0.040 % max.

TABLE 2
HARDNESS REQUIREMENTS

Sample Nut after Treatment as in


Completed Nuts 7.1.5.2

Rockwell Hardness Brinell Rockwell


Hardness, Hardness B
Grade and Type Brinell Hardness C Scale B Scale min Scale, min
1 121 min ... 70 min 121 70
2 159 to 352 ... 84 min 159 84
2H 248 to 352 24 to 38 ... 179 89
To 112 in. [38.1 mm], incl 248 to 352 24 to 38 ... 179 89
Over 112 in. [38.1 mm] 212 to 352 38 max 95 min 147 79
2HM and 7M 159 to 237 22 max ... 159 84
3, 4, 7, and 16 248 to 352 24 to 38 ... 201 94
6 and 6F 228 to 271 20 to 28 ... ... ...
8, 8C, 8M, 8T, 8F, 8P, 8N, 126 to 300 ... 60 to 105 ... ...
8MN, 8LN, 8MLN, and 8MLCuN 126 to 300 ... 60 to 105 ... ...
8A, 8CA, 8MA, 8TA, 126 to 192 ... 60 to 90 ... ...
8FA, 8PA, 8NA, 8MNA, 126 to 192 ... 60 to 90 ... ...
8LNA, 8MLNA, and 8MLCuNA 126 to 192 ... 60 to 90 ... ...
8R, 8RA, 8S, and 8SA 183 to 271 B 88 to C25 ... ... ...

278
PART A FERROUS MATERIAL SPECIFICATIONS SA-194 /SA-194M

TABLE 3
PROOF LOAD USING THREADED MANDREL

Proof Load, lbf [kN] [Note (1)]

Grade 1 Grades 2, 2HM, 6 6F, 7M Grades 2H, 3, 4, 7, 16


Nominal Threads
Size, in. per inch Stress Area, Heavy Hex Hex Heavy Hex Hex Heavy Hex Hex
[mm] [25.4 mm] in.2, [mm2] [Note (2)] [Note (3)] [Note (4)] [Note (5)] [Note (6)] [Note (7)]
1 [6.4] 20 0.0316 [20.4] 4 130 [18.4] 3 820 [17.0] 4 770 [21.2] 4 300 [19.1] 5 570 [24.8] 4 770 [21.2]
4
5 [7.9] 18 0.0524 [33.8] 6 810 [30.3] 6 290 [28.0] 7 860 [35.0] 7 070 [31.4] 9 170 [40.8] 7 860 [35.0]
16
3 [9.5] 16 0.0774 [49.9] 10 080 [44.8] 9 300 [41.4] 11 620 [51.7] 10 460 [46.5] 13 560 [60.3] 11 620 [51.7]
8
7
16 [11.1] 14 0.1063 [68.6] 13 820 [61.5] 12 760 [56.8] 15 940 [70.9] 14 350 [63.8] 18 600 [82.7] 15 940 [70.9]
1 [12.7] 13 0.1419 [91.5] 18 450 [82.1] 17 030 [75.8] 21 280 [94.6] 19 160 [85.2] 24 830 [110] 21 280 [94.6]
2

9 [14.2] 12 0.182 [117] 23 660 [105] 21 840 [97.1] 27 300 [121] 24 570 [109] 31 850 [142] 27 300 [121]
16
5 [15.9] 11 0.226 [146] 29 380 [131] 27 120 [121] 33 900 [151] 30 510 [136] 39 550 [176] 33 900 [151]
8
3 [19] 10 0.334 [215] 43 420 [193] 40 080 [178] 50 100 [223] 45 090 [200] 58 450 [260] 50 100 [223]
4
7 [22.2] 9 0.462 [298] 60 060 [267] 55 440 [247] 69 300 [308] 62 370 [277] 80 850 [360] 69 300 [308]
8
1 [25.4] 8 0.606 [391] 78 780 [350] 72 720 [323] 90 900 [404] 81 810 [364] 106 000 [472] 90 900 [404]

118 [28.6] 8 0.790 [510] 102 700 [457] 94 800 [422] 118 500 [527] 106 700 [475] 138 200 [615] 118 500 [527]
114 [31.8] 8 1.000 [645] 130 000 [578] 120 000 [534] 150 000 [667] 135 000 [600] 175 000 [778] 150 000 [667]
138 [34.9] 8 1.233 [795] 160 200 [713] 148 000 [658] 185 000 [823] 166 500 [741] 215 800 [960] 185 000 [823]
112 [38.1] 8 1.492 [962] 194 000 [863] 170 040 [756] 223 800 [996] 201 400 [896] 261 100 [1161] 223 800 [996]
All Types of Grade 8

Heavy Hex Hex


[Note (8)] [Note (9)]
1 [6.4] 20 0.0316 [20.4] 2 540 [11.3] 2 380 [10.6]
4
5 [7.9] 18 0.0524 [33.8] 4 190 [18.6] 3 930 [17.5]
16
3 [9.5] 16 0.0774 [49.9] 6 200 [27.6] 5 810 [25.8]
8
7
16 [11.1] 14 0.1063 [68.6] 8 500 [37.8] 7 970 [35.4]
1 [12.7 13 0.1419 [91.5] 11 350 [50.5] 10 640 [49.8]
2

9 [14.2] 12 0.182 [117] 14 560 [64.8] 13 650 [60.7]


16
5 [15.9] 11 0.226 [146] 18 080 [80.4] 16 950 [75.4]
8
3 [19] 10 0.334 [215] 26 720 [119] 25 050 [111]
4
7 [22.2] 9 0.462 [298] 36 960 [164] 34 650 [154]
8
1 [25.4] 8 0.606 [391] 48 480 [216] 45 450 [202]

118 [28.6] 8 0.790 [510] 63 200 [281] 59 250 [264]


114 [31.8] 8 1.000 [645] 80 000 [356] 75 000 [334]
138 [34.9] 8 1.233 [795] 98 640 [439] 92 450 [411]
112 [38.1] 8 1.492 [962] 119 360 [531] 111 900 [498]
GENERAL NOTEProof loads are not design loads.

NOTES:
(1) See limit for proof load test in 7.2.2.1. The proof load for jam nuts shall be 46% of the tabulated load.
(2) Based on proof stress of 130 000 psi [895 MPa].
(3) Based on proof stress of 120 000 psi [825 MPa].
(4) Based on proof stress of 150 000 psi [1035 MPa].
(5) Based on proof stress of 135 000 psi [930 MPa].
(6) Based on proof stress of 175 000 psi [1205 MPa].
(7) Based on proof stress of 150 000 psi [1035 MPa].
(8) Based on proof stress of 80 000 psi [550 MPa].
(9) Based on proof stress of 75 000 psi [515 MPa].

279
SA-194 /SA-194M 1998 SECTION II

TABLE 4
PROOF LOAD USING 120 HARDENED STEEL CONE [NOTE (1)]

Proof Load, lbf [kN]

Grade 1 Grades 2, 2HM, 6 6F, 7M Grades 2H, 3, 4, 7, 16


Nominal Threads
Size, in. per inch Stress Area, Heavy Hex Hex Heavy Hex Hex Heavy Hex Hex
[mm] [25.4 mm] in.2, [mm2] [Note (2)] [Note (3)] [Note (4)] [Note (5)] [Note (6)] [Note (4)]
1 [6.4] 20 0.0318 [20.5] 3 800 [16.9] 3 550 [15.8] 4 400 [19.6] 4 000 [17.8] 5 150 [22.9] 4 400 [19.6]
4
5 [7.9] 18 0.0524 [33.8] 6 150 [27.4] 5 700 [25.4] 7 100 [31.6] 6 400 [28.5] 8 300 [36.9] 7 100 [31.6]
16
3 [9.5] 16 0.0774 [49.9] 8 950 [39.8] 8 250 [36.7] 10 300 [45.8] 9 300 [41.4] 12 000 [53.4] 10 300 [45.8]
8
7
16 [11.1] 14 0.1063 [68.6] 12 000 [53.4] 11 100 [49.4] 13 850 [61.6] 12 450 [55.4] 16 150 [71.8] 13 850 [61.6]
1 [12.7] 13 0.1419 [91.5] 15 700 [69.8] 14 500 [64.5] 18 100 [80.5] 16 300 [72.5] 21 100 [93.8] 18 100 [80.5]
2
9
16 [14.2] 12 0.182 [117] 19 650 [87.4] 18 150 [80.7] 22 700 [101] 20 400 [90.7] 26 500 [118] 22 700 [101]
5 [15.9] 11 0.226 [146] 23 900 [106] 22 050 [98.1] 27 550 [123] 24 800 [110] 32 150 [143] 27 550 [123]
8
3 [19] 10 0.334 [215] 33 650 [150] 31 050 [138] 38 850 [173] 34 950 [155] 45 300 [202] 38 850 [173]
4
7 [22.2] 9 0.462 [298] 44 300 [197] 40 900 [182] 51 100 [227] 46 600 [207] 59 650 [265] 51 100 [227]
8
1 [25.4] 8 0.606 [391] 55 150 [245] 50 900 [226] 63 650 [283] 57 300 [255] 74 250 [330] 63 650 [283]
118 [28.6] 8 0.790 [510] 68 000 [302] 62 800 [279] 78 500 [349] 70 650 [314] 91 600 [407] 78 500 [349]
114 [31.8] 8 1.000 [645] 81 250 [361] 75 000 [334] 93 750 [417] 84 400 [375] 109 350 [486] 93 750 [417]
138 [34.9] 8 1.233 [795] 94 250 [419] 86 950 [387] 108 750 [484] 97 800 [435] 126 850 [564] 108 750 [484]
112 [38.1] 8 1.492 [962] 106 700 [475] 98 500 [438] 123 100 [548] 110 800 [493] 143 600 [639] 123 100 [548]
NOTES:
(1) Based upon following equation (this equation cannot be used for extrapolating values beyond the size ranges listed in this table):

CPL p (1 0.30D) f As

where:
CPL p cone stripping proof load lbf [kN],
D p nominal diameter of nut, in. [mm],
f p minimum proof stress of nut, psi [MPa]; see [Notes (2),(3),(4),(5),(6)],
As p tensile stress area of nut, in.2 p 0.7854 [D 0.9743/n]2, and
n p threads per inch [25.4 mm].
(2) Based on proof stress of 130 000 psi [895 MPa].
(3) Based on proof stress of 120 000 psi [825 MPa].
(4) Based on proof stress of 150 000 psi [1035 MPa].
(5) Based on proof stress of 135 000 psi [930 MPa].
(6) Based on proof stress of 175 000 psi [1205 MPa].

280
PART A FERROUS MATERIAL SPECIFICATIONS SA-194 /SA-194M

TABLE 5 98
MARKING OF NUTS

Nuts Hot- Nuts Machined Nuts Manufactured


Grade and Forged or from Bar in Accordance
Type Cold-Punched Stock with 5.7

1 1 1B ...
2 2 2B ...
2H[Note (1)] 2H 2HB ...
2HM [Note (1)] 2HM 2HMB ...
3 3 3B ...
4 4 4B ...
4L [Note (2)] 4L 4BL ...
6 6 6B ...
6F 6F 6FB ...
7 7 7B ...
7L [Note (2)] 7L 7BL ...
7M [Note (1)] 7M 7MB ...
8 8 8B 8A
8C 8C 8CB 8CA
8M 8M 8MB 8MA
8T 8T 8TB 8TA
8F 8F 8FB 8FA
8P 8P 8PB 8PA
8N 8N 8NB 8NA
8MN 8MN 8MNB 8MNA
8R 8R 8RB 8RA
8S 8S 8SB 8SA
8LN 8LN 8LNB 8LNA
8MLN 8MLN 8MLNB 8MLNA
8MLCuN 8MLCuN 8MLCuNB 8MLCuNA
16 16 16B
NOTES:
(1) The letters H and M indicate heat-treated nuts (see Section 5).
(2) See Supplementary Requirement S4.

281
SA-194 /SA-194M 1998 SECTION II

SUPPLEMENTARY REQUIREMENTS

One or more of the following supplementary requirements shall be applied only


when specified by the purchaser in the inquiry, contract, or order. Details of these
supplementary requirements shall be agreed upon in writing by the manufacturer
and purchaser. Supplementary requirements shall in no way negate any requirement
of the specification itself.

S1. Strain-Hardened Austenitic Steel Nuts S4. Low-Temperature Requirements for (Grade
4 or) Grade 7 Nuts
S1.1 Strain hardened Grades 8, 8C, 8T, 8M, 8F, 8P,
8N, or 8MN nuts may be specified. When Supplemen- S4.1 When low-temperature requirements are speci-
tary Requirement S1 is invoked in the order, nuts shall fied for Grade 4 or Grade 7 nuts, the Charpy test
be machined from cold drawn bars or shall be cold procedures and requirements as defined in Specification
forged to shape. No subsequent heat treatment shall A 320 for Grade L7 shall apply. Depending on the
be performed on the nuts. Nuts made in accordance size of nuts, separate test samples of the same heat
with this requirements shall be proof load tested in may be required and shall be processed through heat
accordance with 7.2.2.1 and shall withstand the proof treatment with the nuts for which the test is to apply.
load specified in Table S1.1. For nut requiring proof Full-size impact specimens cannot be obtained if the
loads over 120 000 lbf [530 kN], Supplementary Re- bar stock is smaller than 58 in. in diameter.
quirement S5 is invoked. The hardness limits of Table
S4.2 An L shall be added to the marking, as 98
2 do not apply to strain hardened nuts. Nuts made in
shown in Table 5, for nuts so tested.
accordance with this requirement shall be marked with
the Grade symbol underlined.
S5. Proof Load Tests of Large Nuts
S5.1 Proof load testing of nuts requiring proof loads
S2. Chemical Composition Certification of over 120 000 lbf [530 kN] may be required. When
specified, the test is to be performed in accordance
S2.1 The purchaser shall be provided with a statement with 7.2 to the loads required by Table S5.1. The
certifying that the nuts meet the chemical composition maximum load will be based entirely on the equipment
requirements specified in Table 1. available.

S6. Control of Product by Heat Number


S3. Retests by Purchasers Representative
S6.1 When control of nuts by actual heat analysis
S3.1 The purchasers representative may select two is required and this supplementary requirement is speci-
nuts per keg (200-lb unit [90-kg]) for sizes 58 in. [15.9 fied, the manufacturer shall identify the completed nuts
mm] and smaller, one nut per keg for sizes over 58 in each shipment by the actual heat number. When
in. [15.9 mm] up to and including 112 in. [38.1 mm], this supplementary requirement is specified, a certificate
and one nut per every two kegs for sizes larger than including the results of the actual production tests of
112 in. [38.1 mm], which shall be subjected to the each test lot together with the heat chemical analysis
tests specified in Section 7. shall be furnished by the manufacturer.

282
PART A FERROUS MATERIAL SPECIFICATIONS SA-194 /SA-194M

TABLE S1.1
PROOF LOAD TESTING OF STRAIN HARDENED NUTS USING THREADED MANDREL

Proof load, lbf [kN] [Note (1)]

Nominal Threads Stress Area, All Other Types All Other Types
Size, in. per in. in.2, Grade 8M Grade 8M of Grade 8 of Grade 8
[mm ] [25.4 mm] [mm2] (strain hardened) (strain hardened) (strain hardened) (strain hardened)
Heavy Hex Hex Heavy Hex Hex
[Note (2)] [Note (3)] [Note (4)] [Note (2)]
1 [6.4] 20 0.0316 [20.4] 3 480 [15.5] 3 160 [14.0] 3 950 [17.6] 3 480 [15.5]
4
5 [7.9] 18 0.0523 [33.8] 5 760 [25.6] 5 240 [23.3] 6 550 [29.1] 5 760 [25.6]
16
3 [9.5] 16 0.0774 [49.9] 8 510 [37.8] 7 740 [34.4] 9 675 [43.0] 8 510 [37.8]
8
7
16 [11.1] 14 0.1063 [68.6] 11 690 [52.0] 10 630 [47.3] 13 290 [59.1] 11 690 [52.0]
1 [12.7] 13 0.1419 [91.5] 15 610 [69.4] 14 190 [63.1] 17 740 [78.9] 15 610 [69.4]
2

9 [14.2] 12 0.182 [117] 20 020 [89.0] 18 200 [80.9] 22 750 [101] 20 020 [89.0]
16
5 [15.9] 11 0.226 [146] 24 860 [110] 22 600 [100] 28 250 [126] 24 860 [110]
8
3 [19] 10 0.334 [215] 36 740 [163] 33 400 [148] 41 750 [186] 36 740 [163]
4
7 [22.2] 9 0.462 [298] 46 200 [206] 41 580 [185] 53 130 [236] 46 200 [206]
8
1 [25.4] 8 0.606 [391] 60 600 [270] 54 540 [243] 69 690 [310] 60 600 [270]

118 [28.6] 8 0.790 [510] 75 050 [334] 67 150 [299] 82 950 [369] 75 050 [334]
114 [31.8] 8 1.000 [645] 95 000 [422] 85 000 [378] 105 000 [467] 95 000 [422]
138 [34.9] 8 1.233 [795] 110 970 [494] 98 640 [439] 123 300 [548] 110 970 [494]
112 [38.1] 8 1.492 [962] 134 280 [597] 119 360 [531] 149 200 [664] 134 280 [597]
GENERAL NOTE Proof loads are not design loads.

NOTES:
(1) The proof load for jam nuts shall be 46% of the tabulated value.
(2) Based on proof stress of 110 000 psi [760 MPa] up to 34 in. [19 mm]; 100 000 psi [690 MPa] 78 to 1 in. [22.2 to 25.4 mm]; 95 000
psi [655 MPa] 118 to 114 in. [28.6 to 31.8 mm]; 90 000 psi [620 MPa] 138 to 112 in. [34.9 to 38.1 mm].
(3) Based on proof stress of 100 000 psi [690 MPa] up to 34 in. [19 mm]; 90 000 psi [620 MPa] 78 to 1 in. [22.2 to 25.4 mm]; 85 000 psi
[585 MPa] 118 to 114 in. [28.6 to 31.8 mm]; 80 000 psi [550 MPa] 138 to 112 in. [34.9 to 38.1 mm].
(4) Based on proof stress of 125 000 psi [860 MPa] up to 34 in. [19 mm]; 115 000 psi [795 MPa] 78 to 1 in. [22.2 to 25.4 mm]; 105 000
psi [725 MPa] 118 to 114 in. [28.6 to 31.8 mm]; 100 000 psi [690 MPa] 138 to 112 in. [34.9 to 38.1 mm].

TABLE S5.1
PROOF LOAD FOR LARGE HEAVY HEX NUTS [NOTE (1)]

Proof Load, lbf (kN) [Note (2)]


Nominal Threads
Size, in. per Stress Area, Grades 2, 6, 6F Grades 2H, 3, 4, 7, 16
[mm] in. [25.4 mm] in.2 [mm2] Grade 1 Heavy Hex Heavy Hex Heavy Hex

158 [41.2] 8 1.78 [1148] 231 400 [1029] 267 000 [1188] 311 500 [1386]
134 [44.4] 8 2.08 [1342] 270 400 [1203] 312 000 [1388] 364 000 [1619]
178 [47.6] 8 2.41 [1555] 313 300 [1394] 361 500 [1608] 421 800 [1876]
2 [50.8] 8 2.77 [1787] 360 100 [1602] 415 500 [1848] 484 800 [2156]
214 [57.2] 8 3.56 [2297] 462 800 [2059] 534 000 [2375] 623 000 [2771]
212 [63.5] 8 4.44 [2864] 577 200 [2568] 666 000 [2962] 777 000 [3456]
234 [69.8] 8 5.43 [3503] 705 900 [3140] 814 500 [3623] 950 250 [4227]
NOTES:
(1) ANSI B18.2.2 in the size range over 112 in. [38.1 mm] provides dimensions only for heavy hex nuts. Refer to 7.3.1.
(2) Proof loads for nuts of larger dimensions or other thread series may be calculated by multiplying the thread stress area times the proof
stress in the notes to Table 3 or Table S1.1. The proof load for jam nuts shall be 46% of the tabulated load.

283
SA-194 /SA-194M 1998 SECTION II

APPENDIX

(Nonmandatory Information)

X1. STRAIN HARDENING OF AUSTENITIC


STEELS
X1.1 Strain hardening is the increase in strength and
hardness that results from plastic deformation below
the recrystallization temperature (cold work). This effect
is produced in austenitic stainless steel by reducing
oversized bars to the desired final size by cold drawing
or other process. The degree of strain hardening achiev-
able in any alloy is limited by its strain hardening
characteristics. In addition, the amount of strain harden-
ing that can be produced is further limited by the
variables of the process, such as the total amount of
cross-section reduction, die angle and bar size. In large
diameter bars, for example, plastic deformation will
occur principally in the outer regions of the bar, so
that the increased strength and hardness due to strain
hardening is achieved predominantly near the surface
of the bar. That is, the smaller the bar, the greater the
penetration of strain hardening. Thus, the mechanical
properties of a given strain hardened fastener are depen-
dent not just on the alloy, but also on the size of bar
from which it is machined.

284

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