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(Received 22 December 1994; revised version received 17 April 1995; accepted 5 May 1995)
SLB test presented previously* is modified for the M2 B,, B22 B26 012 D22 D26
determination of energy release rate (ERR) and mode 816 B26 B66 D,6 026 D6,
M6
ratio for the case of an orthotropic specimen with a
midplane delamination. This analysis is applied to a 0
laminate and to a number of multidirectional or. in their inverted form:
laminates with delaminations at +0/ + 8 or +O/ - 8 a11 a12 al6 PI1 P12 PI6 -N
interfaces. Next, distributions of the mode I, mode II
ff12 a22 a24 P21 022 P26 N2
and mode III ERRS along the delamination fronts are
a16 a26 a66 Phi P62 P66 N6
determined for each laminate by three-dimensional =
PI1 P21 P61 611 612 616 Ml
finite element analyses. Predictions for the total ERR
and mode ratio by the two analyses are compared, and P12 P22 P62 612 622 626 M2
the results are used to make recommendations PI6 P26 P66 h6 826 866 M6 /
regarding appropriate stacking sequences and data
(2)
reduction procedures for multidirectional SLB ge-
Note that for
a midplane symmetric region,
ometries. Experimental results for these laminates are
presented elsewhere.7*
PI = [PI = PI. For an anti-symmetric region, the only
non-zero components of these two matrices are B16,
As a final note, we point out that other names have
Bx, Px, Px, Pbl and PG2.
typically been used for the SLB test, such as the
In view of the loading, we will adopt a
mixed-mode tlexure (MMF) test,13, or the modified
one-dimensional moment-curvature relationship, den-
end-notched flexure (MENF) test.5316 We prefer the
oted by: ^
name SLB, as it is more descriptive than MMF,
whereas MENF tends to invoke an image of a mode II
specimen.
where M is the moment on a face defined by a normal
vector in the positive or negative x direction, b is the
2 CLASSICAL PLATE THEORY ANALYSIS specimen width, w is the deflection in the z direction,
Consider the SLB geometry of Fig. 1. We will refer to and D is the effective bending rigidity per unit width.
the region above the crack as plate 1, and the region Standard sign convention is used for M, i.e. a positive
below the crack as plate 2. Results will be restricted to moment produces a positive stress in positive z. D
the case where t, = t2, and for which plates 1 and 2 denotes the effective bending rigidity of the untracked
each possess midplane symmetry. It will also be region, and D1 denotes the effective bending rigidity
Center-delaminated single-leg bending specimens 387
of plate 1. The term effective is used because the where the compliance, C, is defined as the
bending rigidity in either region depends upon the center-point deflection divided by the load. The crack
three-dimensional constraint conditions.21,22 If the length, a, and half-span length, L, are as defined in
constraint conditions for both regions are those of Fig. 1, and R is the ratio of flexural rigidities of the
generalized plane stress, i.e. if N2=N6=M2=M6= untracked region to that of plate 1, i.e. R = DIDI.
0, then, also noting N1 = 0, eqn (2) yields: Assuming that the specimen fabrication process is
such that the residual thermal stresses do not
DE& (4) contribute to the ERR, then eqn (7) may be
011
substituted into the relationship between ERR and
For plane strain conditions (6; = E: = K2 = Kg = 0), eqn the derivative of compliance with respect to crack
(l), along with the condition B,, = 0, yields: length:24
D =DII (5)
D2 3C
where a singular field based mode decomposition is crack-tip in both plate 1 and in the untracked region,
valid, use of this approach in the interpretation of test A, is the in-plane rigidity of plate 1, A; is its in-plane
data and the prediction of fracture should result in compliance, D1 is the flexural rigidity of plate 1, 0; is
predictions with essentially the same accuracy as when its flexural compliance, and D is the flexural
the full nature of the oscillatory field is compliance of the untracked region. For plane strain:
considered. 18~25,27 Also, for the anti-symmetric lay-ups I
considered in this work, the p = 0 approach gives A, =A,]
identical results for the mode ratio to an alternative, D, = D:, (16)
previously-proposed mode decomposition
procedure.2p-30 In the latter method, ERR com- and for plane stress:
ponents are determined numerically, based on a finite
crack extension that is large with respect to the region A,=+
a11
containing the oscillatory part of the near-tip field. As
a result of the stacking sequences chosen, and the fact
D,=& 07)
that all delaminations were at the laminate midplane, 11
the mode decomposition used herein for all laminate
types considered will also agree with the global mode where the superscript 1 denotes that these properties,
decomposition procedure described elsewhere. taken from eqn (1) or eqn (2) are for plate 1. For
Assuming that each of the cracked and untracked either plane strain or plane stress:
regions are individually specially orthotropic, and
using the above approximation for mode decomposi-
tion in the anti-symmetric lay-ups, a crack-tip element
analysis2~82~26
predicts the ERR components as:
(18)
(11) where D is defined by eqns (4) and (5).
crack-tip, and the magnitude of the non-uniformity either O/O, +15/ - 15, +15/ + W, +30/ - 30 or
can be shown to be proportional to the D, ratio of the +30/ + 30 plies. The cracked regions of all
specimen. Notice that this local problem has a width sequences are individually symmetric, the untracked
that is considerably larger than any of its other regions are either symmetric or anti-symmetric, all
dimensions and is therefore very nearly in plane regions (cracked and untracked) are specially
strain. Thus, a better approximation than the orthotropic, and within these constraints the D, ratio
two-dimensional solution presented above would be to of each sequence is minimized. Material properties
include the local loading, along with the plane strain corresponding to Ciba-Geigy C12KIR6376
properties, in eqn (11). This would be a quasi-three- graphite/epoxy are utilized for all analyses, and the
dimensional approach and would give a close unidirectional ply properties are given in Table 1.
approximation for the true distribution of G and mode The five lay-ups are presented in Table 2. Each of
mix across the delamination front; for more accurate these stacking sequences have D16 and Dz6 terms that
results, a three-dimensional crack-tip element is are at least three orders of magnitude smaller than
required.*(j Alternatively, a three-dimensional finite Dll, Dz2, D,, or Dh6. This is true for both the cracked
element method, as presented in the following section, and untracked regions. For the specimens where
may be used. Both a three-dimensional finite element growth occurs at a +f3/ - 0 interface, the chosen
or quasi-three-dimensional approach as described anti-symmetric sequences of the untracked regions
above will predict non-uniform mode I, mode II and have values of B16 and BZ6 that are essentially zero.
mode III ERRS across the specimen width. The total Each lay-up is 32-plies thick and contains a midplane
ERR for the specimen will most nearly agree with the delamination; d indicates the delamination location in
plane stress, two-dimensional plate theory predictions, the anti-symmetric lay-ups. The following abbrevia-
and the average mode mix (i.e. for the entire width) tions will be used throughout to refer to these lay-ups:
will nearly agree with the plane strain, two- the first sequence will be referred to as the [O]; the
dimensional plate theory (crack-tip element) predic- second as [Z15] (i-e. crack growth occurs at a
tions. This issue is discussed in more detail +15/ + 15 interface); the third as [f 151; and the
elsewhere,12 as the difference between the plane stress fourth and fifth sequences will be referred to as [I301
and plane strain mode mix is much more pronounced and [ f 301, respectively.
when there is an oscillatory singularity. All of the geometries studied used a half-span
length (L) of 88.9 mm, a crack length (a) of 34.29
mm, and a width (b) of 25-4 mm. These geometries
5 FINITE ELEMENT VERIFICATION
were chosen as they were utilized in our initial test
A number of three-dimensional finite element program of composite SLB specimens. In subsequent
analyses were performed to verify the preceding experimental works, we have shortened the half-span
equations for various stacking sequences. The primary length to L = 63.5 mm and reduced the crack length
issues that we will address in this section are: to 31.75 mm. These reductions were performed to
minimize the geometric non-linearity observed in the
1. whether eqn (7), with plane stress properties,
[I301 and [ f 301 specimens prior to fracture. Some
accurately predicts compliance;
guidelines on choosing specimen geometries, such that
2. whether eqns (9) and (lo), with plane stress
the effects of geometric non-linearities are insig-
properties, accurately predict ERR;
nificant, are presented elsewhere.8
3. whether eqn (ll), with plane strain properties,
accurately predicts mode mix.
5.2 Finite element analyses
The finite element results are also used to quantify The finite element models and analysis procedure is
the magnitude of the non-uniformities in the total essentially the same as those described previously.22,31-
ERR and the individual ERR components along the 33 Three-dimensional models, using eight-noded,
delamination front as a function of D,. This continuum-based three-dimensional shell elements,34
information is utilized to provide some guidelines for were used for each laminate considered. A geometri-
choosing stacking sequences for multidirectional SLB cally non-linear formulation was used; however, only
specimens.
5.1 Specimen and test geometries Table 1. Unidirectional material properties for Ciba-
Geigy Cl2K/R6376 graphite/epoxy
Five different test specimens were chosen for analysis.
These specimens use the same stacking sequences that E,, = 146.86 GPa Yxy= 0.33 G*, = 5.45 GPa
have been considered in previous analyses and test E,, = 10.62 GPa VXZ= 0.33 G,, = S-45 GPa
programs.8z2 Each specimen is chosen so that E,, = 10.62 GPa YyL= 0.33 G,, = 3.99 GPa
delamination growth occurs at a different interface; Single ply thickness = 1.27 X 1O-4 m
the five interfaces selected for study are bounded by
390 B. D. Davidson, R. Kriiger, M. Kiinig
Table 2. Stacking sequences evaluated results, mesh refinement and convergence studies
were conducted with respect to the number of
Interface Lay-up elements along the specimen width, length, and the
refinement in the crack-tip region. Total energy
o/o [Ol,*
release rates and energy release rate distributions
+ 15/+ 15 [f 15/o/ - 15/0/15/0,/15/0/ - 15/o/ F 151, obtained by models similar to those used herein have
+ 15/- 15 [ + 15/O/- 15/0/15/0,/15/O/ - 15/O/ r 15/dl also been verified to agree with those obtained from
F 15/0/15/0/-151041 -15/0/15/0/ +15] three-dimensional finite element models containing
+30/+30 [*30/O/-30/0/30/0,/30/0/-30/o/ +30], conventional 20-node brick elements.332 Contrary to
+30/ -30 [*30/O/ -30/0/30/0,/30/0/-3O/Olr 30/d/ what was expected, we did not observe an oscillatory
r 30/0/30/0/ - 30/o,/ - 30/0/30/01 f 301 singularity27-29 in our convergence studies for de-
lamination growth at a +8/ - 0 interface. Rather, the
mode ratio that was obtained for these cases
converged to that predicted by a continuum analysis if
relatively low loads were applied, and all results were it is assumed that a small but finite crack extension
observed to remain within the linear regime. A typical occurs.28-3 For the geometries considered, this
finite element model is illustrated in Fig. 2. For any definition also corresponds to that obtained by the
given laminate, the four plies nearest the delamination p = 0 approximation.8~25~27 Additional details of the
were modelled individually. The remaining plies were finite element models, mesh refinement and verifica-
subdivided into four groups, each of which contained tion studies have been presented previously.33
seven plies. That is, the continuum-based three-
dimensional shell is a brick type volume element in 5.3 Results
which the in-plane, coupling, and bending rigidities of Table 3 shows the DC ratio of each specimen. Table 4
a ply or group of plies are accurately represented.,34 presents the compliance, ERR and mode ratio of the
Energy release rate distributions were obtained by the five different specimen types, under conditions of both
virtual crack closure technique. Specific details, plane stress and plane strain, using the plate theory
describing the application of the virtual crack closure equations. All the results in both tables are identical
technique to the three-dimensional models, are given for the [ k 01 and [It?] laminates. As has been
elsewhere. In all cases, crack advance was observed in previous studies,2m23 the difference
assumed to be self-similar. between the plane stress and plane strain predictions
In order to establish the accuracy and validity of becomes more pronounced with increasing D,. All of
the specimens are less compliant, and therefore have a
lower normalized ERR, in plane strain than in plane
stress. For all of the specimen types examined, little
difference in mode ratio with changing constraint
conditions is observed.
Table 5 presents the first comparison of finite
element and classical plate theory results for the
different specimens. This table shows specimen
compliance, as determined by the finite element
analysis (FEA), normalized by both the plane stress
(Pa) and plane strain (Pe) CPT results. The results
for the [Z 131and [ f 01 specimens are identical. It is
apparent from Table 5 that the true global constraint
conditions are essentially plane stress. As expected,
the CPT plane stress predictions improve with
decreasing E,/G,, ratio, where E, is the Youngs
modulus of the specimen in the x direction, and G,3 is
the transverse shear modulus with respect to the X-Z
plane.
Figure 3 presents the finite element results for edge effect increases with increasing DC ratio. This is
energy release rate along the delamination front for consistent with results obtained in previous studies of
the [0] specimen. The horizontal axis is defined such pure mode I21,23,36 and pure mode I122,3hdelamination.
that y/b = O-5 is at the specimen center (compare with For the mode I portion of the loading, the induced
Fig. 1); thus y/b = 0.0 corresponds to the specimen transverse curvature increases the percentage of GI at
free edge. As the G distributions are symmetric about the specimen center as compared to that at its edges.
y/b = 0.5, results for only one half of the specimen Conversely, for the mode II loading, this effect causes
width are included. The distributions of G,, Grl, Gm peak ERRS to occur at the specimen edges. The mode
and GT = G1 + G,, + Grrr are shown; each data point III ERR arises from the mode II loading, and occurs
represents the energy release rate at the center of a primarily as a result of the dissimilar transverse
local area of crack closure.313 Energy release rates in contractions that the lower surface of plate 1 and the
Fig. 3 are normalized by the total energy release rate upper surface of plate 2 are trying to achieve.22 For
for the entire width, as determined by the finite pure mode II loadings, such as an ENF specimen, we
element results. To avoid confusion, we will refer to have experimentally observed that the non-uniform
the energy release rates (either mode I, mode II, ERR distributions cause crack growth to first occur at
mode III or GT) for the entire width as average the specimen edges.6 This is particularly true of the
values. Average energy release rates were determined [:30] and [ f 301 specimens. However, we have not
by multiplying the energy release rate for a given area observed any sub-critical crack advance in any of the
of crack closure by that area of crack closure, five sequences when tested in the SLB geometry.
summing these values across the specimen width, and Next, note that the ERR distributions of Fig. 4 and
dividing by the total area of crack closure. Notice Fig. 5 are slightly asymmetric. Referring to Fig. 1, the
from Fig. 3 that the energy release rate is fairly larger peaks at y/b = 0.0 occur because this is the
uniform across the specimen width, except very near fiber dominated edge. That is, the local orientation
the free edge. Near this edge, there is a decrease in of the fibers provides a natural load path to this edge,
G,, an increase in Glr, and the appearance of Gm; this whereas the y/b = 1.0 is a matrix dominated edge;
is primarily a result of the anticlastic curvature of the the local load path is very compliant and the peak
cracked and untracked regions.21-23 Due to the small energy release rate values are considerably smaller. It
D, ratio for this specimen, these free edge effects are is also of interest to note that the ERR distributions in
relatively small. The curves connecting the symbols in
Figs 3-5 are comprised of a series of straight lines, 1.2
::
-I *
2 0.8
Fig. 3, the energy release rates in both figures are c?
normalized by the average GT for that specimen as
determined from the finite element results. These
figures also indicate that the magnitude of the free
G-._AVG/G~AVG G~AVG.FE/G~C=LPU
Lay-up G,AVG/G-rAG GTrAVG/GTAVG
0.002 1.143
o-014 1.116
0.398 0.005 1.134
0.374 0.049 0.974
0.400 0.031 o-997
the SLB test is simple to run, it is relatively easy to Pieracci, A., Effects of mode ratio, ply orientation and
precracking on the delamination toughness of a
examined, a crack-tip element analysis provided
laminated graphite/epoxy composite. J. Rein6 Plast.
reasonably accurate predictions of mode ratio. A CRT Comp. (in press).
based method of data reduction can also be used to 9. Reeder, J. & Crews, J., The mixed-mode bending
obtain total ERR (e.g. through eqn (lo)), but for method for delamination testing. AMA J., 28 (1990)
highly accurate results, it is recommended that 1270-6.
10. Reeder, J. R. & Crews Jr, J. H., Nonlinear analysis and
compliance calibration be utilized.73s Overall, it
redesign of the mixed-mode bending delamination test.
appears that relatively small errors are obtained when NASA-TM-102777, 1991.
applying a two-dimensional analysis to unidirectional 11. Kinloch, A. J., Wang, Y., Williams, J. G. & Yayla, P.,
or multidirectional SLB specimens with D, ratios (per The mixed-mode delamination of fibre composite
cracked region) less than 0.25. materials. Comp. Sci. Technol., 47 (1993) 225-37.
12. Davidson, B. D. & Sundaraiaman, V., A single leg
bending test for interfacial fracture toughness deter-
ACKNOWLEDGEMENT mination. Znt. J. Fract. (submitted).
13. Russell, A. J. & Street, K. N., Moisture and
temperature effects on the mixed-mode delamination
This work was partially supported (B.D.D.) by the fracture of unidirectional graphite/epoxy. Delamination
Federal Aviation Administration under Grant 94-G- and Debonding of Materials, ASTM STP 876, ed. W. S.
022. Johnson. American Society for Testing and Materials,
Philadelphia, PA, 1985, pp. 349-70.
14. Charalambides, M., Kinloch, A. J., Wang, Y. &
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