Documente Academic
Documente Profesional
Documente Cultură
DOI 10.1007/s00170-014-6111-1
ORIGINAL ARTICLE
Received: 12 December 2013 / Accepted: 25 June 2014 / Published online: 8 July 2014
# Springer-Verlag London 2014
Abstract A new constitutive relation for powder materials fabricate high-performance and complex-shaped metal parts
used in finite element analysis (FEA) of hot isostatic pressing within a short period. However, the final geometry of the HIP
(HIP) complex-shaped parts was derived from Perzynas products differs from that desired in both shape and scale due
elastic-viscoplasticity equations, and the stickslip boundary to the container stiffness and temperature gradient during the
modelling and thermomechanical coupling solution were densification process [1]. Using finite element analysis (FEA)
achieved. The temperature-dependent mechanical and thermal to predict those changes is very effective, especially for near-
parameters were determined through experiments. A net shaping complex-shaped parts. Yuan et al. [2] produced a
complex-shaped turbine disc from Inconel 625 alloy has been small casing component from Ti6Al4V powder by HIP and
simulated and produced. The predicted dimensions and rela- compared the predicted dimensions with the experimental
tive densities have been compared with those measured from measurements. Comparisons of the predicted and measured
the experiments, which shows a good agreement for most two-dimensional (2D) configures for a small casing sample
regions of the turbine disc. The reasons for local predicted showed a good agreement.
discrepancies and physical defects were discussed, and future Metal materials will yield at a low stress under high tem-
improvements for FEA simulation and HIP process were peratures, and then deform with time. Considering the cou-
outlined. pling influence of temperature and pressure, a variety of
viscoplasticity models have been developed based on macro-
Keywords Finite element analysis . Perzynas scopic approach, in which the macroscopic deformation of the
constitutive relation . Hot isostatic pressing . Near-net powder is estimated based on the conventional material yield
shaping . Inconel 625 theory. Most of the proposed constitutive models belong to
porous material models that are based on the classical von
Mises model [3]. Abouaf et al. [4] proposed an equivalent
1 Introduction stress equation based on the yield theory of porous metals for
FEA of HIP and used a hyperbolic sine power-law equation to
Hot isostatic pressing (HIP) can densify loose powder into describe the equivalent strain rate. This method obtained good
near-full dense metal parts, with the combined processing of 2D simulation accuracy for HIP of a complex-shaped turbine
high temperature and pressure. Therefore, it is suitable for disc. Svoboda et al. [5] used the same equivalent stress and
manufacturing metal parts from difficult-to-cut and precious power-law equations with Abouafs models [4] to simulate the
materials. Combined with mould technology, it can be used to HIP of hot-working martensitic steel. They described in detail
the solving process of finite element implementation and
Q. S. Wei (*) : P. J. Xue : G. C. Liu : H. Lu : J. Huang :
validated 2D simulation examples with experimental mea-
Y. S. Shi (*) surements. To consider the strain strengthening effect on the
State Key Laboratory of Materials Processing and Die and Mould powder, Gillia et al. [6] modified the Abouafs models [4] and
Technology, School of Materials Science and Engineering, simulated the HIP of blanket shield components for ITER
Huazhong University of Science and Technology,
applications.
Wuhan 430074, China
e-mail: wqs_xn@163.com In addition to the power-law models proposed by Abouaf,
e-mail: shiyusheng@mail.hust.edu.cn the models in different forms for FEA of HIP were developed
1668 Int J Adv Manuf Technol (2014) 74:16671677
by other researchers. Based on the equivalent stress equation the whole process of HIP discussed above, this study is
proposed by Abouaf, Hggblad and Li [7] used a microbased concerned with attempts to use Perzynas model for simulat-
densification rate equation to replace the power-law equation ing the viscoplasticity behaviour of powder during HIP pro-
in Abouafs models. The prediction error of the radial shrink- cess. The objectives are to build the finite element models
age for HIP of a turbine disc was less than 2 %. Jeon and Kim based on Perzynas constitutive relation, and to determine the
[8] implemented a FEA for HIP of 316 L stainless steel model parameters through experiments with Inconel 625 su-
powder, based on the Abouafs model and another power- peralloy; to simulate the mould deformation and the powder
law model. The comparison showed that the predictions for an densification during near-net shaping a turbine disc by HIP;
axisymmetric part by both models agreed well with the ex- and to validate the simulation accuracy of the new method by
perimental data of densification and deformation. Jinka [9] experimental results.
simulated the HIP of Astroloy powders using power-law
equations in two different forms. The simulation results
showed that the powder was not in a hydrostatic pressure state
during the normal cycle of HIP, whereas during isothermal 2 Simulations
and isotropic heating the isostatic pressure distribution was
achieved. Kim [10] incorporated the power-law creep model 2.1 The constitutive relations for powder during HIP process
with various diffusion models, and applied to the simulation
for HIP of 316 L stainless steel powder. The result indicated The equivalent stress for powder is defined by a double-
that the contribution of diffusional mechanisms was not sig- parameter equation as the following [15]
nificant for the powder densification compared with those
2eq A J 2 BI 21 1
from the plastic and creep deformation.
The creep deformation of metal materials will occur when
the processing temperature exceeds 30 % of the melting
temperature and have to be considered when the temperature where, eq is the equivalent stress. J2, I1 are the second and
is higher than 50 % of the melting point [11]. During the first invariants of the stress tensor, respectively. Variables A
whole HIP process, the operating temperature gradually rises and B are the functions of relative density D, can be expressed
to 5070 % of the melting temperature of the powder from as [16]
room temperature, keeps at that temperature value for a period
A 2 D2 2
of time, and then descends to room temperature through air
cooling. Consequently, at the beginning of heating and the end
of cooling, which is almost half of the HIP cycle, material
creep deformation does not happen because the processing
temperature is lower than the critical value of creep genera- .
B 1D2 3 3
tion. Therefore, it may not be reasonable to describe the
powder behaviour in the HIP process using creep models.
Constitutive equations, including Perzynas model [12],
Peirce model, Logarithmic model and Johnson-Cooks model, According to Eq. (1), the yield function F can be described
were usually used to describe the thermal deformation of as
metal materials. Among them, the constitutive equation de- p q p
rived by Perzyna, a Polish researcher, was widely used for F eq y A J 2 BI 21 y 4
calculating elastic-viscoplasticity deformation of geomateri-
als. Using a nonlinear model combined with the viscoplastic
Perzynas law, Belaychi et al. [13] dealt with a where, y, is the yield stress for the dense material, varying
micromechanical analysis for the nonlinear behaviour of a with temperatures. is the geometric strengthening parameter,
composite-like rock material. The numerical results were in changing with the relative density , can be expressed as [17]
agreement with experimental findings. In addition, the
Perzynas model was also successfully used to simulate the 11 5
process of die-forging complex-shaped aluminium compo-
nents at high temperatures [14]. The above studies show that
the Perzynas model can not only describe the flowability of The Perzynas constitutive relation is expressed as [12]
metal powder similar to that of rock-soil, but also predict the
high-temperature deformation of metal materials. Considering
ij ije h F i 6
the irrationality of using power-law creep models to describe ij
Int J Adv Manuf Technol (2014) 74:16671677 1669
where,ij , ije are the total strain rate and the elastic strain rate, Combining Eqs. (4), (9), and (10) gives
respectively. is the viscoplastic flow coefficient, and is the q
plastic potential function. Expression of x is the Macaulay A 3B F ij
eq p
vp
A2 J 2 2B2 I 21 13
function, which can be defined as 3A 18B eq y
2 2
0; x 0
h xi 7
x; x>0 2.2 Modelling for the boundary friction during HIP process
q where, dvp T
ij , dij are the viscoplastic and thermal strain incre-
2
For dense materials, A=1 and B=0, then C 3 . ments. dTij can be expressed as
Ni Cr Mo Nb Fe Si Mn N Al O Ti C
Mass ratio (%) bal 21.4 8.9 3.48 1.49 0.42 0.39 0.12 0.10 0.06 0.02 0.02
1670 Int J Adv Manuf Technol (2014) 74:16671677
Table 2 Material parameters against temperature of hot isostatic pressing Inconel 625 powder
Test temperature/C
Z
dTij dT ij 17 T T T T T T T
T c kx ky kz TQ d
Z t
Z x x y y z z
Tqd ThT a T d 0
2 3
18
where, is the thermal expansion coefficient, and dT is the
temperature increment. The temperature field during the HIP where, c is the specific heat capacity (J/(kg K)); t denotes the
process can be calculated by the Galerkin weighted residual time (s); kx, ky and kz are the thermal conductivity coefficients
method, expressed as [20] in x, y and z directions (W/(m K)). Q is the heat resource
HT KT P 20
where, Keij, Heij are the heat conductivity and capacity matrixes
for each mesh unit, respectively. PeNi is the thermal load vector
applied on the outside surface of the powder domain, and
equals to the temperature on the internal surface of the mould.
Ni,Nj are the finite element interpolation functions for mesh
units. The temperature values on all mesh nodes at different
time can be calculated by Eq. (20). And then, the whole
temperature field can be solved by Eq. (19). Finally, the
thermal strain can be obtained by Eq. (17).
MSC.MARC, a commercial finite element programme,
was used to solve the models described above. In the process
of finite element calculation, the effect of temperature on the
material properties and thermal strains was considered, but the
effects of the deformation and phase transition on the temper-
ature were ignored. An updated Lagrangian incremental solu- Fig. 3 3D finite element meshes of a quarter of the turbine disc and the
tion was performed as follows: update the geometric shape of mould
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The powder, denoted Inconel 625 chosen in this study is a A simplified turbine disc, as shown in Fig. 1, consists of four
high-temperature alloy produced by Belgium Hoganas inner passages. The inner passages are expected to be near-net
Company using a gas atomisation process. The powder com- shaped through HIP, but the outer surfaces can be machined
position is given in Table 1. The particle size ranges between into the final geometry.
22.49 and 56.2 m, and the average size is about 45 m. The assembled mould was designed as shown in Fig. 2.
Series cylindrical specimens (8 mm12 mm) with a relative The cores in the internal and at the bottom have a relatively
density of more than 99.5 % were made by HIP process (ABB large volume, are expected to have no or small deformation
Inc., Mini-HIPper QIH-15). The high-temperature compres- during the HIP process, and thus play a role of controlling
sion testings at room temperature, 200, 400, 600, 800, and complex shapes. The external container with a relatively thin
1,000 C on these specimens were performed using Gleeble- thickness can create a vacuum cavity for powder materials,
3500 (Dynamic Systems Inc.) thermal simulated test machine. which is the necessary condition for the HIP process. The
The strain rate was set to 0.001 s1, and the compression rate container greatly deforms under the coupling loads of temper-
was higher than 25 %. The temperature-dependent material ature and pressure, which drives the powder to densify. The
parameters from high-temperature compression testings are containers at the top and bottom ends were 2 mm in thickness
listed Table 2. In addition, the study assumed that the thermal and 15 mm in thickness for the external cylinder container.
related parameters were not affected by the relative density, The container has a top ventilation plug for degassing.
and the equations for calculating Poissons ratio and Youngs The finite element modelling of a quarter of the turbine disc
modulus at different relative densities are expressed as [21] and its mould, using the eight-node hexahedron meshes is
Int J Adv Manuf Technol (2014) 74:16671677 1673
illustrated in Fig. 3. In the process of finite element solution, shown in Table 3. In general, the prediction of the final
the domains of both container and core were assumed to be a consolidated shape compares well with the CMM measure-
whole, given the same material parameters. In order to im- ment of the physical part.
prove the computational accuracy, the meshes of areas where The discrepancy between the prediction and measurement
large deformation occurs are refined. is defined as
100jmeasuredpredictedj
3.3 HIP implementation e % 24
measured
A hot isostatic press (ABB Mini-HIPper QIH-15) was used
for HIP of Inconel 625 powder. Both the core and the con-
tainer were made from 45 mild steel by machining methods. The maximum discrepancy in axial direction (y-axis) is
The container was cleaned by the ultrasonic method. The about 4.5 % and 6.3 % in radial direction (x-axis). The
mould assembled by the core and the container was filled by container in the upper is designed to generate large compres-
Inconel 625 powder, and then vibrated to attain the tap density sion for powder densification. Quite good match is especially
of 0.67. The edge between the top plug and the container was shown in those regions, which just proves the applicability of
welded. Then the powder in the container was degassed for the proposed simulation method. However over amplification
5 h at 450 C. HIP was done under 110 MPa at 1,050 C by of powder surface distortion by the current simulation is
referring to our previous study results. Figure 4 shows the recognised at some regions. This may be partially caused by
test condition for temperature and pressure during HIP, the following two reasons: (1) refer to the experience data of
which is also used for finite element calculation stated in other superalloys mechanical parameters (see Eqs. 5, 22 and
Sect. 2.3. 23); (2) neglect the influence of relative density on thermal
properties. Therefore, the follow-up experiments for determin-
ing the mechanical and thermal parameters of specimens with
different relative densities should be done.
4 Results and discussions
P Q R S P Q R S
The measured coordinate values 73.01 64.84 61.46 68.56 0 17.58 48.46 51.32
The predicted coordinate values 73.90 61.95 60.29 69.90 0 18.61 51.13 54.56
Discrepancies (%) 1.2 4.5 1.9 2.0 0 5.9 5.5 6.3
4.2 Powder densification during HIP of a complex-shaped node 1834 are somewhat lower than those of nodes 1847 and
turbine disc 1870 at the same time, but both exceed about 0.95 at the end of
HIP. However, the value of node 1765 in the bottom is
The simulated result of Fig. 7 shows that the powder domain obviously lower than those of other four nodes. At the begin-
has large volume shrinkage. The relative density at the end of ning of raising temperature and pressure, the relative densities
HIP presents a nonuniform distribution. The shape change of of all nodes do not rise but fall. It may be explained by the
the powder domain indirectly reflects the mould deformation. thermal expansion of both powder and mould. After that, the
The top container is compressed faster than other parts of the powder begins a fast densification because the temperature
mould due to its thin wall thickness. That makes the powder in and pressure loads exceed the shielding limit of the mould.
upper region (nodes 1847, 1870 and 1794) to densify rapidly. The densification rates of nodes 1847 and 1870 are the
The continuous compression during HIP results in a high highest, those for nodes 1834 and 1794 are the second highest,
relative density for the powder in that region. On the contrary, and the lowest for node 1765. That densification law shows a
the powder in lower region (node 1765) has a relatively low good agreement with the expectation that the container and the
density. This phenomenon may be explained by the fact that core are designed for different functions. After entered into the
the internal core in those regions has no or small deformation stage of preserving temperature and pressure, the powder
during HIP, so the compression on the powder by the mould is densification rate reduced gradually. During that stage
relatively low. That just indicates that the core is capable to the plastic deformation has developed fully, and the
near-net shaping a complex geometry that it was designed for. powder densification only come from the contributions
The evolution of the relative density on the five nodes of creep and diffusion owing to high temperatures. In
labelled in Fig. 7 is shown in Fig. 8. The tendencies of the spite of the decrease of temperature and pressure in
density evolution for nodes 1847 and 1870 in upper region are uploading stage, the larger temperature difference
basically identical. The relative densities of node 1794 and existing within the compacted powder domain will lead
4.3 Microtopographies of the compacted powder from simulations (Fig. 7). Most pores present a round or near-
round shape, which may be caused by the residual gas in the
Figure 10 shows the micro-morphologies using optical micro- powder. That gas may be derived from the atomisation process
scope for the regions labelled in Fig. 9a. A few micron pores or the remnant during the degassing process. In the process of
can be found in all regions, which is the reason why the HIP these enclosed gases will expand, and then gather togeth-
compacted powder does not reach a full dense state. The er into some scattered pores. These micro pores can reduce the
pores number and the scale for region A in the lower of mechanical property of the HIP-ed parts greatly. Therefore the
the power domain are greater than those of other regions. That gas contents in the raw powder and the sealed container have
shows good agreement with the relative density distribution to be strictly controlled.
Fig. 10 Micro morphologies of different regions shown in Fig. 9a. (without corrosion)
Int J Adv Manuf Technol (2014) 74:16671677 1677