AC600

AC600 Automatic
Calorimeter
Instruction Manual
Version 1.2x
Part Number 200-718
May 2013
Patents are Pending in U.S.A. and other countries

2013 LECO Corporation
Minor revisions may not be reflected in this manual.
LECO Corporation
3000 Lakeview Avenue St. Joseph, MI 49085-2396
Phone: 269-983-5531 Fax: 269-983-3850
Info@leco.com www.leco.com ISO 9001:2000 No. HQ-Q-994
Leco is a registered trademark of LECO Corporation.
Introduction AC600 11
12 AC600 Introduction
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1 Introduction
The Introduction chapter provides general information including safety
guidelines and warranty terms. This chapter also provides information
about parts and accessories.
1 Introduction ............................................................................... 15
Illustrations .................................................................................. 19
Software License ......................................................................... 112
Warranty.................................................................................... 116
WEEE......................................................................................... 118
LECO-Supplied Dell Computers ..................................................... 123
Interference to Other Devices ....................................................... 125
Declaration of Conformity ............................................................. 126
About this Manual ....................................................................... 127
Tips for Navigating the Electronic Manual ....................................... 128
Equipment Packages .................................................................... 130
Options ...................................................................................... 133
Components and Accessories List .................................................. 135
Specifications ............................................................................. 141
Certificate of Traceability.............................................................. 143
Oxygen Combustion Vessel Safety Notice ....................................... 144
Hydrostatic and Proof Testing ....................................................... 146
Combustion Vessel Hydrostatic and Proof Testing Return Form ......... 147
2 Installation ................................................................................ 21
Illustrations .................................................................................. 22
Lifting and Moving the Instrument ................................................... 23
Installing Instrument for First-Time Analysis ..................................... 24
International Installation .............................................................. 214
Installing Dual Instrument Configuration ........................................ 215
3 Option Installation ..................................................................... 31
Illustrations .................................................................................. 32
Installing Balance .......................................................................... 33
Installing Printer ........................................................................... 38
Single Sized (7L) and Dual Sized (15L) AC600 Chillers ....................... 39
Bar Code Reader ......................................................................... 317
4 System Setup ............................................................................. 41

Selecting Language ....................................................................... 44
ACWIN Software Main Window ........................................................ 45
Using Toolbars ............................................................................ 412
Customizing Sample Spreadsheet .................................................. 414
Customizing Software Main Window............................................... 418
Determining User Permissions....................................................... 426
Configuring System ..................................................................... 430
Importing Sample Data ................................................................ 432
Creating Sample Templates .......................................................... 434
Creating Transmission Formats ..................................................... 435
Creating Export Format ................................................................ 441
Creating and Modifying User Defined Fields .................................... 445
Managing Databases .................................................................... 450
5 Operation ................................................................................... 51
Illustrations .................................................................................. 53
Preparing for Analysis .................................................................... 54
Creating or Modifying Methods ........................................................ 59
Logging in a Sample .................................................................... 514
Analyzing a Sample ..................................................................... 518
Using Sample Filters .................................................................... 520
Calibration ................................................................................. 524
Recalculating Results ................................................................... 526
Viewing History of a Sample ......................................................... 527
Applying Sample Signatures ......................................................... 528
Printing Reports .......................................................................... 530
Transfer Import and Transfer Export .............................................. 534
Importing and Exporting Data ....................................................... 536
Exporting Buffers ........................................................................ 537
Transmitting Results .................................................................... 538
6 Maintenance ............................................................................... 61
Illustrations .................................................................................. 62
Periodic Maintenance Schedule ....................................................... 63
Modifying Maintenance Counters ..................................................... 66
Viewing Log ................................................................................ 610
Performing Prep Station Maintenance............................................. 611
Leak Checking Oxygen Combustion Vessel ..................................... 613
Replacing Oxygen Combustion Vessel O-Rings ................................ 614
Replacing Oxygen Charger O-Rings ............................................... 616
Rinsing Prep Station .................................................................... 617
Replacing Ignitor Wire Assembly for Thread Fuse ............................ 619
Replacing Optional Wire Fuse ........................................................ 620
Draining and Replacing Distilled Water ........................................... 622
Replacing Water Filter .................................................................. 624
Removing and Cleaning Fan Filter ................................................. 625
Polishing Bucket and Baffle ........................................................... 626
Lubricating Screw for Lift-Arm Mechanism ...................................... 632
Adjusting the Pressure Safety Release Valve ................................... 638
Replacing Ceramic Washer ........................................................... 639
7 Theory of Operation ................................................................... 71

Theory of Operation....................................................................... 72
Critical Calculations ....................................................................... 73
8 Diagnostics ................................................................................ 81
Monitoring Ambient Chart............................................................... 82
Solenoids and Switches .................................................................. 88
Using Offset Thermistors .............................................................. 810
Lift Mechanism ............................................................................ 812
Network ..................................................................................... 814
9 Service ....................................................................................... 91
Illustrations .................................................................................. 92
Installing LECO Software ................................................................ 93
Configuring the Ethernet Adapter .................................................. 911
Configuring Firewall Settings ........................................................ 920
Configuring DHCPLite ................................................................... 921
Registering Software ................................................................... 925
Troubleshooting Copy Protection Key ............................................. 931
General Troubleshooting .............................................................. 932
Jacket Temperature Troubleshooting ............................................. 934
Fault Conditions .......................................................................... 936
Software Error Codes ................................................................... 938
Aligning Bucket Lid ...................................................................... 939
Using the Dock Wizard ................................................................. 940
Adjusting Duty Cycle ................................................................... 941
10 Illustrations ............................................................................. 101
11 Schematics ............................................................................... 111
12 Glossary ................................................................................... 121
13 Index ....................................................................................... 131
Illustrations
Figure 1-1 Declaration of Conformity ................................................126

Figure 2-1 Shipping Strap ...............................................................24
Figure 2-2 Connecting Water Filter ...................................................25
Figure 2-3 Power Cord Connection ....................................................26
Figure 2-4 Pneumatic T-Fitting .........................................................27
Figure 2-5 Pneumatic and Oxygen Connections ..................................28
Figure 2-7 Vessel Prep Station Rear Connections ................................210
Figure 2-8 Ethernet Switch ..............................................................211
Figure 3-1 Balance Control Panel ......................................................34
Figure 3-2 Chiller Rear Panel ...........................................................311
Figure 3-3 Chiller Sterilizer Installation .............................................312
Figure 3-4 Water Filter ....................................................................312
Figure 3-5 External Chiller Cover ......................................................313
Figure 3-6 Drain Connection ............................................................313
Figure 3-7 Drain Tubing Installed .....................................................314
Figure 5-1 Oxygen Combustion Vessel Assembled ..............................55
Figure 5-2 Vessel Prep Station - Fill Side ...........................................56
Figure 5-3 Oxygen Fill Button ..........................................................57
Figure 5-4 Vessel Installed ..............................................................58
Figure 5-5 Bucket Lid Mating Socket .................................................58
Figure 5-6 Vessel Prep Station - Vent Side ........................................519
Figure 6-1 Orientation of Lock Vessel ................................................612
Figure 6-2 Vessel Lid ......................................................................614
Figure 6-3 O-Ring Removal Tools .....................................................615
Figure 6-4 Prep Station with Rinse Bottle Attached .............................617
Figure 6-5 Drainage Port .................................................................618
Figure 6-6 Electrode Sleeve and Slots ...............................................620
Figure 6-7 Wire Fuse in Electrode Slots .............................................621
Figure 6-8 Wire Fuse with Crucible ...................................................621
Figure 6-9 Front Panel ....................................................................622
Figure 6-10 Fan Filter .....................................................................625
Figure 6-11 Top Casting Cover Screws ..............................................626
Figure 6-12 Pneumatic Lead ............................................................626
Figure 6-13 Back Electrode Leads .....................................................627
Figure 6-14 Bolts for Front Panel ......................................................627
Figure 6-15 Screw Locations for Side and Top Panels ..........................628
Figure 6-16 Stirring Motor Gear Box .................................................628
Figure 6-17 Upper Setscrew ............................................................629
Figure 6-18 Thermistor Leads ..........................................................629
Figure 6-19 Lift-Arm Screws ............................................................630
Figure 6-20 Power Switch ................................................................632
Figure 6-24 Front Panel Bolts ...........................................................634
Figure 6-26 Lift-Arm Plate and Molding .............................................635
Figure 6-27 Side Casing for Lift Arm .................................................636
Figure 6-29 Top Casting Cover Screw Tabs ........................................637
Figure 6-30 Pressure Safety Valve ....................................................638
Figure 9-1 Jacket Temperature for Single Analysis ..............................934
Figure 9-2 Jacket Temperature for Series of Analyses .........................935
Figure 9-3 Lift-Arm Screws ..............................................................939
Figure 9-4 Duty Cycle Adjustment Knob ............................................941
Figure 10-1 Reference Card .............................................................102
Figure 10-2 Facility Requirements ....................................................103
Figure 10-3 Wiring Diagram.............................................................104
Figure 10-4 Instrument Overview .....................................................105
Figure 10-5 Instrument Overview - Panels Removed...........................105
Figure 10-6 Left Side View ..............................................................106
Figure 10-7 Rear View ....................................................................107
Figure 10-8 Oxygen Combustion Vessel Assembly ..............................108
Figure 10-9 Halogen-Resistant Combustion Vessel .............................109
Figure 10-10 Jacket Thermistor ........................................................1010
Figure 10-11 Wire Fuse Assembly ....................................................1011
Figure 10-12 Lift-Arm Screw ............................................................1012
Figure 10-13 Locking Mechanism .....................................................1013
Figure 10-14 Water Manifold Assembly View 1 ...................................1014
Figure 10-17 Oxygen Manifold Assembly ...........................................1017
Figure 10-18 Pneumatic Manifold Assembly .......................................1018
Figure 10-19 Card Control Assembly .................................................1019
Figure 10-20 Motor Stirrer Gearbox ..................................................1020
Figure 10-21 Jacket Assembly..........................................................1021
Figure 10-22 Switch for Bucket Water Level ......................................1022
Figure 10-23 Water Heater Assembly and Pump .................................1023
Figure 10-24 Bucket Sealing Cover Assembly ....................................1024
Figure 10-25 Water Inlet Assembly...................................................1025
Figure 10-26 Bucket .......................................................................1027

Figure 10-27 Lift Arm Assembly .......................................................1028
Figure 10-28 Lift-Arm Positions ........................................................1029
Figure 10-29 Flow Diagram .............................................................1030
Figure 10-30 Semi-automated Analysis Sequence ..............................1031
Figure 10-31 Top-Level Exploded View ..............................................1032
Figure 10-32 Vessel Prep Station......................................................1033
Figure 11-1 Temperature Control and Measurement ...........................113
Figure 11-2 Motion Control ..............................................................114

Software License
By installing the Licensed Software, the Licensee acknowledges that

Licensee has read it, understands it and agrees to be bound by its
terms, and further agree that this is the complete and exclusive
statement of the Software License between the parties, which
supersedes and merges all prior proposals, understandings and other
agreements oral and written, between the parties relating to the
subject matter of this Software License. In the event of any conflict
between the terms of this Software License and the terms of purchase
orders submitted by Licensee, the terms of this Software License shall
control.
This is an agreement between the Licensee and LECO Corporation

(LECO) of 3000 Lakeview Avenue, St. Joseph, Michigan 49085-2396,
owner of the Licensed Software. This Software License specifies the
conditions under which Licensee may use the Licensed Software.
I. Definitions
"Licensed Software" shall mean the software supplied with this
Software License, which is software developed and distributed by
LECO.
"Instruction Manual" shall mean a guide describing the use and

operation of the Licensed Software, together with any related
supporting documentation.
"Licensee" shall mean and include any of the Licensee's divisions and
departments within Licensee's organization, but shall not include
wholly or partially owned subsidiaries, affiliates, successors or assigns,
or independent third parties.
II. License Grant

LECO hereby grants to Licensee, and Licensee hereby accepts, subject
to the terms and conditions set forth in this Software License, a non-
exclusive, non-transferable license to use the Licensed Software and
Instruction Manual as set forth in this Software License. The term
license as used in this Software License shall mean and include:
a. the right to use a copy of the Licensed Software in executable form

by one user at a time;
b. the right to use and copy the Instruction Manual for Licensee's
internal operations; and
c. the right to make one backup copy of the Licensed Software.

In accepting the license granted by LECO, Licensee agrees that it shall
not:
1. transfer or allow transfer of copies of the Licensed Software to any

other party including any wholly or partially owned subsidiaries,
affiliates, successors, or assigns without the express consent of LECO;
2. use the Licensed Software on more than one (1) CPU at any one
time;
3. cause or permit unauthorized copying, reproduction, or disclosure of

any portion of the Licensed Software or Instruction Manual or the
distribution of any part thereof to any third person or entity, for any
purpose whatsoever. This restriction shall continue to bind Licensee
and its agents beyond the termination of this Software License; or
4. attempt to disassemble modify, or reverse engineer the Licensed

Software;
5. attempt to defeat or defeat the copy-protection mechanism;
6. attempt to or access features not purchased.
III. Enhancements And Support

LECO may make available to Licensee updates and enhancements to
the Licensed Software, which Licensee may accept at the time it is
offered to Licensee by paying any applicable update fee. LECO shall
have the sole discretion to determine the update fee. Use of all such
updates and enhancements by Licensee shall be subject to the terms
and conditions of this Software License unless supplemented or
replaced by a subsequent license.
IV. Termination Of Software License

In the event of a material default by Licensee or its agents, of any
provision of this Software License, LECO may terminate this Software
License upon thirty (30) days written notice. Upon termination of the
Software License, the Licensee shall return all copies of the Licensed
Software to LECO. This obligation shall survive the termination of this
Software License.
V. Copyright And Proprietary Information

Licensee acknowledges that the Licensed Software and the Instruction
Manual constitute valuable and copyrighted property of LECO and that
all title and ownership rights in the Licensed Software and related
materials remain exclusively with LECO. LECO reserves all rights with
respect to the Licensed Software and Instruction Manual under all
applicable laws for the protection of proprietary information, including,
but not limited to, trade secrets, copyrights, trademarks, and patents.

VI. Limitation Of Liability And Warranties
With respect to the physical media on which the Licensed Software is
delivered and Instruction Manual, LECO warrants the same to be free
of defects in materials and workmanship for a period of ninety (90)
days from the date of delivery. In the event of notification within the
warranty period of defects in material or workmanship, LECO will
replace the defective media or documentation. LECO specifically
disclaims all other warranties, expressed or implied, including but not
limited to implied warranties of merchantability and fitness for a
particular purpose with respect to defects in the media and
documentation. In no event shall LECO be liable for any loss of profit,
data, or use, or any other commercial damage, including but not
limited to special, incidental, consequential, interruptions in Licensees
operations, or other damages regardless of negligence or fault. LECO's
liability in connection with this Software License shall not exceed the
value of the amounts paid by Licensee under this Software License for
the Licensed Software which gave rise to the loss less a reasonable
amount for use, damage and obsolescence.
VII. Confidentiality
All information and materials regarding the software, provided to
Licensee by LECO which are not generally known in the trade are
confidential, are proprietary, and such information and materials are
furnished solely for the use of Licensee under this Software License.
Licensee agrees not to use or disclose any such information or material
otherwise without prior written consent from LECO and Licensee
further agrees to take all reasonable steps requested by LECO, or
otherwise necessary to protect the confidentiality of all such
information and materials. The foregoing obligations will survive
termination of this Software License, and Licensee agrees to return all
such information and materials to LECO upon request or any non-
renewal or termination of this Software License.

VIII. Miscellaneous
a) This Software License shall be binding upon and inure to the
benefit of the parties hereto and their respective successors and
assigns, provided that Licensee shall not have any right to assign its
rights or obligations under this Software License (whether by operation
of law or otherwise) without the prior written consent of LECO.
b) All notices hereunder shall be in writing and shall be sent by

registered or certified mail postage prepaid to LECO at the addresses
first written above. The date of postmark shall be deemed the date on
which such notice is given.
c) No delay on the part of LECO in exercising any right, power or

remedy hereunder shall operate as a waiver thereof, nor shall any
single or partial exercise of any such right, power or remedy preclude
any other or further exercise thereof or the exercise of any other right,
power or remedy.
d) No amendment, modification or waiver of, or any consent with

respect to, any provision of this Software License shall be effective
unless the same shall be in writing and signed and delivered by each
of the parties hereto, and then such amendment, modification, waiver
or consent shall be effective only in the specific instance and for the
purpose for which given.
e) This Software License shall be construed in accordance with and

governed by the internal laws of the State of Michigan. Wherever
possible, each provision of this Software License shall be interpreted in
such manner as to be effective and valid under applicable law, but if
any provision of this Software License shall be prohibited by or invalid
under such law, such provision shall be ineffective to the extent of
such prohibition or invalidity, without invalidating the remainder of
such provision or the remaining provisions of this Software License.
f) Licensee agrees that it is responsible for obtaining proper

authorization and complying with any export, re-export, or import laws
or regulations and that may apply if Licensee exports, re-exports, or
imports the Licensed Software, technology or technical data licensed
hereunder.

Warranty
Equipment manufactured by LECO Corporation, St. Joseph, Michigan is

warranted free from defect in material and workmanship for a period
of 1) thirteen months from date of shipment or 2) twelve months from
date of installation, whichever occurs first. Equipment not
manufactured by LECO is covered to the extent of warranty provided
by the original manufacturer and this warranty does not cover any
equipment, new or used, purchased from anyone other than LECO
Corporation. All replacement parts shall be covered under warranty for
a period of thirty days from date of purchase. LECO makes no other
representation or warranty of any other kind, expressed or
implied, with respect to the goods sold hereunder, whether as
to merchantability, fitness for purpose, or otherwise.
Expendable items such as crucibles, combustion tubes, chemicals, and
items of like nature are not covered by this warranty.
LECO's sole obligation under this warranty shall be to repair or replace
any part or parts which, to our satisfaction, prove to be defective upon
return prepaid to LECO Corporation, St. Joseph, Michigan. This
obligation does not include labor to install replacement parts, nor does
it cover any failure due to accident, abuse, neglect, or use in disregard
of instructions furnished by LECO. In no event shall damages for
defective goods exceed the purchase price of the goods, and LECO
shall not be liable for incidental or consequential damages
whatsoever.
All claims in regard to the parts or equipment must be made within ten
(10) days after Purchaser learns of the facts upon which the claim is
based. Authorization must be obtained from LECO prior to returning
any other parts. This warranty is voided by failure to comply with
these notice requirements.

Notice
The warranty on LECO equipment remains valid only when genuine
LECO replacement parts are employed. Since LECO has no control over
the quality or purity of consumable products not manufactured by
LECO, the specifications for accuracy of results using LECO
instruments are not guaranteed unless genuine LECO consumables are
employed in conjunction with LECO instruments. If purchaser defaults
in making payment for any parts or equipment, this warranty shall be
void and shall not apply to such parts and equipment. No late payment
or cure of default in payment shall extend the warranty period
provided herein.
LECO Corporation is not responsible for damage to any associated

instruments, equipment, or apparatus nor will LECO be held liable for
loss of profit or other special damages resulting from abuse, neglect,
or use in disregard of instructions. The Buyer, their employees,
agents, and successors in interest assume all risks and liabilities for
the operation, use, and/or misuse of the product(s) described herein
and agree to indemnify, hold harmless, and defend the seller from any
and all claims and actions arising from any cause whatsoever,
including seller's negligence for personal injury incurred in connection
with the use of said product(s) and any and all damages proximately
resulting therefrom.

WEEE
Disposal of WEEE and the Wheeled Bin Symbol

In 2002, the European Union introduced the Directive on Waste
Electrical and Electronic Equipment (WEEE). The main aim of the
Directive is to ensure that WEEE is collected and treated separately.
WEEE may contain hazardous substances that should not end up in the
(human) environment because it can have adverse effects on it.
Furthermore, WEEE is a vast source of raw materials. With the ever

rising worldwide demand for new equipment and the ever decreasing
volume of raw materials in nature, letting this potential source of such
materials go to waste is unacceptable.
If equipment is collected separately, the equipment can be recycled

and up to 85% to 90% of the equipment can be reused as new
material, saving the use of virgin raw materials and energy of
producing these. Separate collection and treatment of WEEE will thus
decrease CO2 emissions as well.
For the above reasons, LECO expects end users to dispose of the
material in an environmentally friendly way, being separate collection
and treatment.
Electrical and Electronic Equipment is labeled with the following

crossed-out wheeled bin symbol, indicating that the equipment
should be disposed of by the end user separate from other types of
waste.
End users should contact their dealer/distributor or our company on

disposal, collection, and recycling options in their country.

LECO-Supplied Dell Computers
Dell Support
All LECO supplied Dell PC's include Dell's ProSupport Service, which is
designed to provide a base level of customer security. This service
option can place a Dell-certified technician at your location the
following day, if necessary (after phone-based troubleshooting). In
many cases, remote troubleshooting can minimize overall system
downtime by getting the issue quickly fixed remotely or helping Dell to
dispatch the right part (if necessary).
The inclusion of Dell ProSupport with LECO supplied PCs ensures that
any computer related service issues are handled directly by the
experts at Dell. This eliminates the unnecessary step of working
through the LECO service professionals for a resolution from Dell, and
provides PC support 24 hours a day, seven days a week.
Dell ProSupport provides expert assistance when you need rapid

problem resolution to help maximize your PC system's uptime and
productivity. ProSupport provides the following benefits:
24 x 7 Access to advanced-level North American-based phone

technicians
Live Chat tech support
DellConnect remote diagnosis and resolution
Next Business Day On-Site Service after Remote Diagnostics
For more information, call 1-800-WWW-DELL (1-800-999-3355) or

access Dell's website by copying and pasting the following link into
your internet browser:
http://www.dell.com/content/topics/global.aspx/services
/prosupport/end_users?c=us&cs=555&l=en&s=biz
Please have your Service Tag and Express Service Code numbers
available when contacting Dell to expedite service. These can be
found on the back or side of the tower.

Transferring Ownership of a Dell Product
The following section explains the steps to transfer the warranty and
ownership of a Dell computer. This transfer is necessary to complete
when an equipment package that includes a Dell computer has been
purchased from LECO.
An internet connection is required to complete the transfer. If an

internet connection is not available, the transfer can be completed
by calling Dell at 800-624-9897.
To complete the transfer online through Dell's website, complete
either the Domestic Customer procedure or the International
Customer procedure as explained in the following steps.
For Domestic Customers:

1. Access Dell's website by copying and pasting or entering the
following website URL into your internet browser:
http://support.dell.com/support/topics/global.aspx/support/chang
e_order/tag_transfer?c=us&l=en&s=gen&redirect=1
It is recommended to complete the transfer of ownership from the
computer from which the ownership will be transferred. If this is not
possible, follow the instructions provided on Dell's website.
2. Complete the transfer by completing and submitting the form
provided on Dell's website.
For International Customers:

1. Access Dell's website by copying and pasting or entering the
following website URL into your internet browser:
http://support.dell.com/support/topics/global.aspx/support/chang
e_order/tag_transfer?c=us&l=en&s=gen&redirect=1
It is recommended to complete the transfer of ownership from the
computer from which the ownership will be transferred. If this is not
possible, follow the instructions provided on Dell's website.
2. Do not enter information into the fields. Instead, click

International Transfer Form located below the form fields.
3. On the form, for original owner,
A. For First Original Owner, enter "LECO Corp"
B. For Original Owner E-mail Address, enter
"service@leco.com"
C. For Country of Original Purchase, click the arrow and select
United States from the list.
4. Complete the transfer by following the remaining instructions
provided on the form.

Interference to Other Devices
This equipment has been tested and found to comply with the limits
for a Class B digital device, pursuant to Part 15 of the FCC Rules and
Regulations. These limits are designed to provide reasonable
protection against harmful interference in a residential installation.
This equipment generates, uses and can radiate radio frequency
energy and, if not installed and used in accordance with the
instructions, may cause interference to radio communications.
However, there is no guarantee that interference will not occur in a
particular installation. If this equipment does cause harmful
interference to radio or television reception, which can be determined
by turning the equipment off and on, the user is encouraged to try to
correct the interference by one or more of the following methods:
Reorient or relocate the radio or television receiving antenna.

Increase the separation between the equipment and the radio
or television receiver.
Connect the equipment to an outlet on a circuit different from
that which the radio or television receiver is currently
connected.
Consult the radio or television dealer or an experienced
radio/TV technician for help.

Declaration of Conformity
Figure 1-1
Declaration of Conformity

About this Manual
This instruction manual provides information about the AC600 as

explained below. For each chapter, there is a hyperlinked table of
contents and list of illustrations, if applicable.
The screen shots used throughout the manual are examples only and
may or may not be applicable to specific procedures.
Chapter 1, Introduction, page 15, describes general information

including safety guidelines and warranty terms. This chapter also
provides information about parts and accessories.
Chapter 2, Installation, page 21, describes hardware setup and

connection.
Chapter 3, Option Installation, page 31, describes the purchasable

options available for the instrument.
Chapter 4, System Setup, page 41, describes starting and

navigating the software and setting operating parameters.
Chapter 5, Operation, page 51, describes the procedures to analyze

samples.
Chapter 6, Maintenance, page 61, describes procedures to perform

on a regular basis to improve the instruments performance and life
span.
Chapter 7, Theory of Operation, page 71, provides a theoretical

overview of instrument operation.
Chapter 8, Diagnostics, page 81, describes how to monitor the

instrument to ensure proper operation.
Chapter 9, Service, page 91, describes service procedures. Contact

the LECO Service Department for further information.
Chapter 10, Illustrations, page 101, provides illustrations and

photographs that can assist with procedures and location of parts.
Chapter 11, Schematics, page 111, provides diagrams of circuit

boards and wiring.
Chapter 12, Glossary, page 121, provides definitions of terms.
Chapter 13, Index, page 131, provides page numbers for topics
throughout the manual. In the electronic manual available through the
software, the page numbers in the index provide a hyperlink to the
corresponding topic.

Tips for Navigating the Electronic Manual
The instruction manual is available as a pdf (portable document

format). To access the manual, push F1 on the computer keyboard, or
select Help on the Menu Bar and then select Help F1.
The appearance of the pdf will depend on the version of Acrobat

Reader loaded with your software. Refer to the Adobe Reader Help
system for further information. The following section provides some
general tips on navigating a manual.
Bookmarks
For versions prior to 8, after opening the pdf document, select the
Bookmarks tab located on the left side of the screen to access a tree
that displays main section headings. Select a heading to go
immediately to the corresponding section. If a + appears, select it to
display more section headings.
For version 8, right-click on and then select Bookmarks. Select a

heading to go immediately to the corresponding section. If a +
appears, select it to display more section headings.
Find
Select Edit on the Menu bar and then Find to highlight a search box
where you can enter a word or phrase. Each time you select Next, the
software will highlight the next occurrence of the word or phrase in the
manual. Find is most useful when the word or phrase is used
infrequently in the manual.
Search
For versions prior to 8, select Edit and then select Search on the Menu
bar to display a side bar with a search box. Enter the desired word or
phrase and each occurrence of the word or phrase in context will
display in the Results area.
For version 8, the Search box appears in a separate window rather

than a sidebar.
Search makes it easier to find words or phrases that occur several

times in the manual. Search also provides the ability to search words
or phrases in several pdf documents, if applicable. To search the
instruction manual only, select the Search this Pdf Document Only
check box.

Links
In the manual, text or a page number highlighted in blue provides a
direct link to the associated topic. In the Index, select the page
number to go directly to the associated topic. For illustrations, a label
and a page number are provided. The label links to the caption of the
illustration while the page number links to the body of illustration.
Previous and Next Arrows

Use the green view arrows located at the bottom of the screen to
toggle between views in the document once more than one page of the
document has been viewed.
In version 8, there are two types of arrows, page arrows and
view arrows . Page arrows move from one page to the next
page and follow the page numbering of the manual while view arrows
move from one view to the next and depend on the pages you have
viewed. To display both types of arrows, click Tools on the Menu bar
and then click Customize Toolbars. From the list, locate Page
Navigation Toolbar and then if all of the arrows do not appear, select
the Previous Page check box, Next Page check box, Previous View
check box, and Next View check box to display both sets of arrows.

Equipment Packages
Items listed below and repeated throughout this manual are subject to
revision. Please consult the packing slip received with the instrument.
For a complete listing of components and accessories, refer to
Components and Accessories List, page 135.
AC600SC Package (Auto Calorimeter with Computer)

1 603-300-600 ASSY AC600 SEMI AUTOMATIC CALORIMETER 230/115V
1 686-483 ASSY PC TOWER AC600
1 618-380 CASE HOLDER CD-24 BLUE/BLACK*
1 259-073 SOFTWARE KIT AC600
1 704-241 ASSY KEY COPY PROTECTION
1 710-172 MONITOR COLOR 19 FLAT SCR GRY
1 621-605-954 ASSY VESSEL COMBUSTION II
1 621-605-981 PACK ACCESSORY AC600
AC600SCR Package (Auto Calorimeter Computer Ready)

1 621-605-981 PACK ACCESSORY AC600
AC600SHC Package (Semi-Auto Calorimeter Halogen Res with Computer)

1 621-605-975 ASSY VESSEL COMBUSTION HALOGEN RES II
1 621-605-983 PACK ACCESSORY AC600 HALOGEN RESISTANT
AC600SHCR Package (Semi-Auto Calorimeter Halogen Res Computer Ready)

1 621-605-983 PACK ACCESSORY AC600 HALOGEN RESISTANT

AC600DC - PKG DUAL AC600 SEMI AUTO CALORIMETER
1 621-785 PACK SWITCH ETHERNET
1 621-605-982 PACK ACCESSORY AC600 DUAL
AC600DCR AC600 Semi-Automatic Calorimeter Dual CR

1 621-605-982 PACK ACCESSORY AC600 DUAL
AC600DHC - PKG DUAL AC600 SEMI AUTO CAL HALOGEN RES

1 621-605-984 PACK ACCESSORY AC600 DUAL HALOGEN RES
AC600DHCR AC600 Semi-Automatic Calorimeter Halogen Res CR

1 621-605-984 PACK ACCESSORY AC600 DUAL HALOGEN RES

AC600A AC600 Semi-Automatic Calorimeter Add-On
1 621-605-985 PACK ACCESSORY AC600 ADD ON
AC600AH AC600 Semi-Automatic Calorimeter Halogen Add-On

1 621-605-986 PACK ACCESSORY AC600 HALOGEN RES ADD ON

Options
603-300-6OP AC600 Options

1 259-073-CPK SOFTWARE KIT AC600 W/KEY
1 259-073UPGR SOFTWARE KIT AC600 UPGRADE
1 621-322 ASSY PRESS PELLET SAMPLE AC
1 621-605-302 KIT VESSEL COMBUSTION AC600
1 619-995 READER BAR CODE CCD USB*
1 621-435 CARTRIDGE COLOR PRNTR HP6940
1 621-436 CARTRIDGE BLACK PRNTR HP6940
1 751-300-140 KIT BALANCE L-250 4PL
1 774-235 REGULATOR PRESSURE
1 051-083 SPEC SHEET AC600
1 150-996-B/M SCHEMATIC CABINET AC600
1 621-605-482 NUT DRIVE LINEAR EXTERNAL
1 621-605-654 KIT CONNECTION ELECTRODE VESSEL AC600
1 621-605-652 KIT UPGRD DRIVE UPPER STIRRER BUCKET AC
1 774-208-150 ACID BENZOIC 1.00GR 50/BT
1 621-429 KIT ADD ON MONITOR 19 INCH PCI EXPRESS
1 621-605-705 KIT REPAIR SWITCH VERTICAL
1 621-605-750 KIT TOOL VESSEL COMBUSTION AC600
1 621-605-747 KIT REPL INSERTS STATION PREP AC600
1 621-605-757 KIT FLUSH VALVE EXHAUST STATION PREP
1 502-816 STD IARM LP50002A
1 621-605-777 KIT CONVERSION VESSEL FUSE WIRE
1 621-605-840 KIT UPGRD DRIVE STIRRER LOWER BUCKET
1 621-605-865 KIT REPL VALVE WATER AC600 S/N 3110 DN
1 621-446 CARTRIDGE COLOR PRINTER WORKFORCE 30
1 621-447 CARTRIDGE BLACK PRINTER WORKFORCE 30
1 621-445-110 KIT PRINTER INKJET WORKFORCE 30
1 621-605-866 LAMP UV REPL STERILIZER WATER AC600
1 621-605-867 SLEEVE QUARTZ REPL STERILIZER WATER AC
1 621-605-854 KIT ADDON STERILIZER CHILLER POLYSCI 13L
1 502-680 STD RM COAL PROX PLUS LOW
1 502-681 STD RM COAL PROX PLUS MED
1 502-682 STD RM COAL PROX PLUS HIGH
1 633-101-920 SWITCH ETHERNET 16 PORT POWER CON 2816
1 621-605-882 KIT REPL POWER SUPPLY AC600 SN3162DN
1 621-605-895 KIT ADDON STERILIZER CHILLER F25-EH
1 621-605-897 KIT ADDON STERILIZER CHILLER LJT180
1 621-605-902 KIT REPL ELECTRODE VESSEL SN370 DN
1 621-605-905 KIT UPGRADE STATION PREP VESSEL

1 621-605-925 KIT REPL ELECTRODE VESSEL HALOGEN RES
1 621-605-940 KIT WARRANTY ARM PREP VESSEL
1 709-806-719 CORD POWER ASSY 10FT 15A/250V
1 621-605-775G KIT ADD-ON FILTER AIR CHILLER SGL AC600
1 621-605-962 FILTER AIR REPL CHILLER MODEL 9502
1 709-806-808 RECEPTACLE SNGL 15A 250V BLK
1 709-806-809 COVER RECEPTACLE SNGL SST
1 621-605-972 KIT REPL BASE MTG DRIVE STIRRER
1 621-605-803 ASSY WIRE IGNITER FUSE VESSEL 5/PACK
1 621-605-977 KIT UPGRD CONNECTION VESSEL COMBUSTION
1 621-605-978 KIT VESSEL COMBUSTION II
1 621-605-979 KIT VESSEL COMBUSTION HALOGEN RES II
1 203-505-431 FORM INSPECTION VESSEL INTERMEDIARY
1 621-605-994 KIT UPGRD CONNECTION VESSEL COMB HAL/RES
1 621-605-995 KIT REPL CARD CONTROL AC600
1 619-592-407 KIT REGULATOR PRESSURE 2-STAGE AIR
1 621-606-101 KIT UPGRD BEARING/SEAL VENT VESSEL
1 621-448-110 KIT PRINTER OFFICEJET HP6100
1 621-449 CARTRIDGE BLACK PRNTR OFFICEJET HP6100
1 621-450 CARTRIDGE CYAN PRNTR OFFICEJECT HP6100
1 621-451 CARTRIDGE MAGENTA PRNTR OFFICEJET HP6100
1 621-452 CARTRIDGE YELLOW PRNTR OFFICEJET HP6100
1 621-606-155 KIT ADDON STERILIZER CHILLER POLYSCI 7/15L
1 621-606-160 KIT CHILLER RECIRCULATING 7L 120V AC600
1 501-439 SAMPLE PARAFFIN 118/ML
1 621-656-001 O-RING 237 3.375X 3.625X .125

Components and Accessories List
603-360-070 AC600 Component Pack

1 621-778 ASSY INLET WATER AC600
1 621-821 ASSY TUBE DRAIN
1 776-692 ASSY HOSE OXYGEN HI-PRESSURE
1 620-677 CABLE ASSY CAT 5 15' RJ45 SHLD
1 776-997 CORD POWER SHLD 16/3GA SJT 115
1 617-482 ASSY TUBE DRAIN TANK COOLANT
1 776-562 WASHER FLT .187X .500X.12CER
2 190-269 SCREW MPHP 8-32X .38 SST
2 193-234 WASHER FLT .169X .304X .03 SST
20 619-590-821 TUBING FLX POLYU BLK .166ID X .042W
1 200-718 MANUAL INSTR AC600
621-605-270 Accessory Pack - Auto Calorimeter
1 501-241 LUB GREASE VACUUM 5.3 OZ

2 621-777 STRIP TEST HARDNESS WATER
1 774-649 ASSY BRUSH CLEANING
1 776-978 SCOOP GLASS 1.5 ML
1 762-515 TOOL O-RING REMOVAL
1 621-605-408 BEAKER 2000ML POLYPROP W/HANDLE & SPOUT
2 502-051 TWEEZER CURVED FINE POINT*
3 502-461 FUSE THREAD COTTON 10CM 375/PK
1 769-434 LUB GREASE LUBRIPLATE 2
1 774-204 CRUCIBLE SST 10/PK
1 621-605-517 ASSY TOOL REMOVAL INSERT VESSEL AC
1 621-605-525 ASSY LABEL SET BARCODE 0-9 BAGGED
1 621-605-557 ASSY CABLE CONNECT STATION PREP AC600
1 615-830-120 TUBE PFA .125X .0625 ID 10 FT
1 621-605-665 TOOL INSTALL O-RING VALVE CHECK VESSEL
1 621-605-666 STAND REMOVAL O-RING VALVE CHECK VSL
1 621-605-686 PACKAGE O-RING VESSEL AC600
1 621-605-687 PACKAGE O-RING PREP STATION AC600
5 294-004 NUT HEX PLN 6-32 304 SST
1 601-980 BOTTLE 250 ML RD LDPE WASH*
1 621-605-744 ADAPTER FLUSH VALVE STATION PREP
1 772-738 O-RING 010 .250X .374X.062V

2 633-101-923 ASSY STAND VESSEL COMBUSTION
1 621-605-960 ASSY STATION PREP VESSEL
1 209-050-105 CD ROM AC600 SVC VIDEO INSTALLATION
621-605-418 Accessory Pack Auto Calorimeter - Halogen Res

1 615-830-120 TUBE PFA .125X .0625 ID 10 FT
5 294-004 NUT HEX PLN 6-32 304 SST
1 772-738 O-RING 010 .250X .374X.062V

621-605-271 Dual Accessory Pack
1 615-830-120 TUBE PFA .125X .0625 ID 10 FT
1 621-830 FTG QD T .25T - .25T - .25T
10 294-004 NUT HEX PLN 6-32 304 SST
1 772-738 O-RING 010 .250X .374X.062V

621-605-419 PACK ACCESSORY DUAL HALOGEN RES
1 615-830-120 TUBE PFA .125X .0625 ID 10 FT
10 294-004 NUT HEX PLN 6-32 304 SST
1 772-738 O-RING 010 .250X .374X.062V

621-605-725 AC600 Add-On Accessory Pack
1 615-830-120 TUBE PFA .125X .0625 ID 10 FT
5 294-004 NUT HEX PLN 6-32 304 SST

621-605-726 AC600 Halogen Res Add-On Accessory Pack
1 615-830-120 TUBE PFA .125X .0625 ID 10 FT
5 294-004 NUT HEX PLN 6-32 304 SST

Specifications
Method
Isoperibol
Range
Joules/Charge: ............................14000 to 35000
Calories/Charge: ..........................3300 to 8300
BTU/Charge: ...............................13 to 33 (6000 to 15000 BTU/lb for a 1
gram sample)
Precision
0.10% RSD*
Analysis Time
TruSpeed Mode: ........................5 minutes
Delta T Mode: ..............................9 minutes
Corrections
Nitrogen, sulfur, fuse wire, moisture, spike, and ash
User-Selectable Ignition
String or wire-fuse
Temperature Measuring Resolution

0.0001 C
Gas Requirements
Analytical: ...................................Oxygen 450 psi (31.0 bar) max; 99.5% purity
Pneumatic: ..................................Compressed Air; 12 psi (0.8 bar); 99.5%
purity; source must be oil and water free
Electrical Power Requirements

90 to 127 V~/180 to 260 V~(at max load), 50/60 Hz, single phase, 5 A/2.5 A, 2,000
BTU/hr
Water Requirements
Recirculating Water Chiller
Nominal Temp: ..........................15C (59F)
Cooling Capacity (at 15C): ...........Single AC600: 680 BTU/hr
Dual AC600: 1,400 BTU/hr
Type:..........................................Distilled Water NOTE: Do NOT use deionized
water

pH: ............................................6 to 8
Dissolved Solids: ..........................0.5 to 100 ppm
Resistivity: ..................................0 kcm to 2 Mcm (0.5 s/cm to 20 s/cm)
Pressure: ....................................4 to 15 psi (0.3 to 1.0 bars)
Volume: ......................................Single AC600: 3 gallons (12 liters) for initial
setup
Dual AC600: 9 gallons (35 liters) for initial setup
Required Work Space**

15 in. W x 21 in. D x 18 in. H (38 cm x 53 cm x 46 cm)
Weight (approximate)
Instrument ..................................135 lb. (61 kg)
Shipping Weight ...........................148 lb. (209 kg)
Environmental Conditions
Operating Temp: ..........................15C to 35C (59F to 95F)
Humidity: ....................................20% to 80%, non-condensing
General: .....................................Area should be free of drafts, and shielded from
sunlight
and other radiation sources
*Based on analysis of benzoic acid at 1 gram; n = 7.

**Allow a 6-inch (15 cm) minimum access area around instrument.
Lower values can be measured by spiking samples that are not completely
combusting.
This is the combustion vessel safety limit. Do NOT exceed this limit. Exceeding this
limit
could result in vessel failure causing death, serious personal injury, and/or property
damage.
Chiller must be capable of operating continuously with flow stopped to the AC600.
V~ denotes VAC.

Certificate of Traceability
This section provides the Certificate of Traceability for the following

part numbers:
621-610-010 Jacket Thermistor Probe
621-605-122 Bucket Thermistor Probe

Oxygen Combustion Vessel Safety Notice
All LECO oxygen combustion vessel assemblies are proof tested as prescribed by the American
Society for Testing and Materials (ASTM) E144-94 (2006)e1.
Explosion Potential
The operator must observe safe operating practices when using high pressure oxygen
combustion vessels. Operating personnel must be trained to practice safe operation and
WARNING maintenance of oxygen combustion vessels.
Safety Notice
Prior to use of a calorimeter, all operating personnel should be thoroughly familiar with all
instructions pertaining to the safe operation of oxygen combustion vessels.
After every 500 firings the oxygen combustion vessel should be disassembled for cleaning and
the o-rings should be replaced. Hydrostatic and proof tests shall be repeated if any of the
following have occurred:
Five thousand (5000) firings.
Firing with an excessive charge of either sample (>35000 Joules*) or oxygen (>500 PSI).
Ignition of any internal part of the vessel, including crucible.
Excessive corrosion or surface defects.
A noticeable change in thread play between vessel enclosure and capnut; Thread tolerance should not
be more than 0.010 inch axial and 0.020 inch diametrical.
*This is the combustion vessel safety limit. Do NOT exceed this limit. Exceeding this limit
could result in vessel failure causing death, serious personal injury, and/or property
WARNING damage.
Additional Safety Precautions

The recommendations outlined in the following section are in accordance with ASTM E 144-94
E144-94 (2006)e1, which defines the Standard Practice for Safe Use of Oxygen Combustion
Bombs. Additional safety practices may be necessary to comply with internal laboratory safety
procedures and alternative international standards.
If an unknown sample is suspected of having a higher heat combustion value, a smaller sample shall
be used during the first analysis.
Never fire the oxygen combustion vessel with a sample that might react explosively.
Never combust benzoic acid (or other acids) in powder form except when benzoic acid powder is used
as a spike. Powdered acids must be pelletized for safe combustion.
Use caution when combusting dry samples, which may combust rapidly thereby igniting the elastomer
seals.
Use caution when combusting fluffy or fibrous material that may result in the dispersal of uncombusted
sample or residue on the inner surfaces and seals of the oxygen combustion vessel.
Do not ignite volatile samples without using a sealed sample holder.
Do not fire an oxygen combustion vessel after any event in which the sample may have been spilled
within the vessel.

Do not fire an oxygen combustion vessel that is leaking oxygen. Check the oxygen combustion vessel
for leaks in an external reservoir prior to use.
The pressure regulator is equipped with a pop-off valve set for 500 psi (34.5 bars) and should be
tested periodically. The correct oxygen pressure is 420 psi (29.0 bars).
Always maintain the oxygen combustion vessel in good condition. Any parts that show signs of
deterioration must be replaced immediately.
Always use matched sets of oxygen combustion vessel bodies, oxygen combustion vessel caps, and
capnuts.
Always stand away from the oxygen combustion vessel during ignition and for at least 20 seconds
afterward.
Never fire the oxygen combustion vessel unless it is completely submerged in water.
Never handle the oxygen combustion vessel for
3 minutes after firing.
Never fire an oxygen combustion vessel that has been mechanically modified. Such alterations can
result in vessel failure during operation, which may cause injury and/or death.
Hydrostatic and Proof Testing

For general overhaul and hydrostatic and proof testing of LECO oxygen combustion
vessels, contact your local LECO Representative (for USA users call 1-800-292-6141)
to obtain an RMA number, then complete the combustion vessel hydrostatic and
proof testing return form (203-505-443). Return the form with the cleaned oxygen
combustion vessel to the address below.
LECO Corporation
Attn: RMA _________
1444 Hilltop Road
St. Joseph, Michigan, USA 49085
Phone: 1-800-292-6141
The contact person listed on the combustion vessel hydrostatic and proof testing
return form will be contacted concerning testing, repair costs, or other issues
encountered in the testing of the vessel. The testing process will not be started
without a valid purchase order. Vessels should be assembled with matching serial
numbers. Mismatched vessel parts will be replaced at additional cost.

General overhaul and hydrostatic and proof testing of vessels includes

the following:
- Disassembly, cleaning and visual inspection of all of the vessel

parts
- Confirmation of matching serial numbers for vessel body, cap,
and cap nut
- Polishing inner surfaces of the vessel cap and body
- Re-assembling vessel with new insulator, ceramic washer, o-rings
and electrodes if necessary
- Hydrostatic and proof testing of the vessel as prescribed by the
American National Standards Institute and the American Society for
Testing and Materials (ANSI/ASTM) E144-94 (2006)
The general overhaul and hydrostatic and proof testing service is normally
completed within 3 business days from the receipt of the vessel. If the
vessel cap, cap nut, or body must be replaced, the necessary parts will be
invoiced at current LECO US List prices. If the vessel fails to pass hydrostatic
and proof testing, it will be destroyed. The non-usable vessel will only be
returned to the customer upon request.
For general overhaul and hydrostatic and proof testing of LECO oxygen
combustion vessels, contact your local LECO Representative (for USA users
call 1-800-292-6141) to obtain an RMA number, then complete the
combustion vessel hydrostatic and proof testing return form (203-505-443).
Return the form with the cleaned oxygen combustion vessel to the address
below.
LECO Corporation
Attn: RMA _________
1444 Hilltop Road
Phone: 1-800-292-6141
The contact person listed on the combustion vessel hydrostatic and proof testing
return form will be contacted concerning testing, repair costs, or other issues
encountered in the testing of the vessel. The testing process will not be started
without a valid purchase order. Vessels should be assembled with matching serial
numbers. Mismatched vessel parts will be replaced at additional cost.
Form No. 203-505-418 REV10

Combustion Vessel Hydrostatic and Proof Testing
Return Form
Combustion Vessel Hydrostatic and

Proof Testing Return Form
Contact Name________________________ Company Name_______________________

LECO Acct No.________________________ Phone ______________________________
Fax________________________________ e-mail_______________________________
Ship to Address_______________________ Bill to Address________________________
__________________________________ ___________________________________
__________________________________ ___________________________________
Vessel Part Number___________________ Vessel Serial Number__________________
RMA # ______________________
Method of Payment Purchase Order (Number)_____________________
Shipping (UPS unless otherwise specified)____________________________________
Collect (if UPS or FedEx, your collect account number is required)___________________
Special Instructions / Comments: ____________________________________________
________________________________________________________________________
________________________________________________________________________
________________________________________________________________________
Returned Vessels are required to be cleaned and assembled with matching serial
number vessel body, cap and cap nut.
Return Vessels to:
LECO Corporation
Attn: RMA __________
1444 Hilltop Road
Phone: 1-800-292-6141
Form No. 203-505-443 REV0


2 Installation
During installation and operation of this instrument, the

ON/OFF switch must be easily accessible.
Illustrations .................................................................................. 22
Lifting and Moving the Instrument ................................................... 23
Installing Instrument for First-Time Analysis ..................................... 24
Installing Data Transmit .......................................................... 213
International Installation .............................................................. 214
Installing Dual Instrument Configuration ........................................ 215
Instruments Dialog Box........................................................... 215
Transfer an Existing Database............................................. 216
Installation AC600 21
Illustrations
Figure 2-1 Shipping Strap ...............................................................24

Figure 2-2 Connecting Water Filter ...................................................25
Figure 2-3 Power Cord Connection ....................................................26
Figure 2-4 Pneumatic T-Fitting .........................................................27
Figure 2-7 Vessel Prep Station Rear Connections ................................210
Figure 2-8 Ethernet Switch ..............................................................211
22 AC600 Installation
Lifting and Moving the Instrument
Refer to Specifications, page 141, for the approximate

shipping and instrument weight. To lift or move the
instrument, use equipment capable of safely lifting this
weight.
1. Properly distribute weight prior to lifting.
Front panels and other cosmetic parts of this instrument are

not designed to be weight bearing. DO NOT use such parts
as lifting points or damage may result. ALWAYS lift near the
feet at the sides or the rear of the instrument base.
2. Position instrument in a location convenient to power and gas
supplies, providing a minimum access space of 6 inches around
the instrument.
Installing Instrument for First-Time Analysis
The external chiller, balance, and printer are not supplied with the
calorimeter, and must be purchased separately. Refer to Options, page
133.
1. Refer to the AC600 Pre-installation Guide for a detailed list of site

requirements for floor space, power requirements, gas supplies,
environmental conditions, and additional instructions.
Shipping Strap:
Do not use shipping strap or top cover of calorimeter as a
lifting point.
Do not remove shipping strap until unit has been positioned
on a bench in laboratory.
Figure 2-1
Shipping Strap
2. Prepare a location for the computer system, calorimeter, external
chiller, balance, and printer that has convenient electrical power,
water, oxygen, and air supplies. Refer to the Facility
Requirements, page 102. Provide a minimum space of six inches
around the instrument for airflow.
3. Remove packing materials from instrument.
4. Use a small lift or at least two people to move the instrument
onto the workbench in the location designated in step 2.
5. Remove shipping strap from top cover of calorimeter.
Do not lift top cover manually.
6. Install the 1 Micron water filter into the Water Inlet Filter
Assembly as explained below:
A. Obtain new filter and install in filter housing by aligning the
filter with the flanges in the filter housing top and bottom.
B. Screw the filter housing bottom onto the filter housing top.
7. Mount the water inlet filter assembly on the back of the AC600.
8. Obtain a piece of 1/4 inch tubing and cut it to the length between
the pressure gauge and the Coolant In connection on the back of
the AC600.
9. Firmly insert one end of the tubing to the push-to-connect fitting
on the pressure gauge and then firmly insert the opposite end of
the tubing to the Coolant In fitting on the back of the instrument.
Refer to Figure 2-2, below.
Figure 2-2
Connecting Water Filter
10. Verify the tubing is not kinked. It may be necessary to remove
the tubing from the push-to-connect fittings, recut the tubing,
and replace the tubing in the push-to-connect fittings.
11. Setup the chiller, refer to Sized (7L) and Dual Sized (15L) AC600
Chillers, page 39.
High Voltage Hazard
This equipment operates from a 115/230V~ source. Contact
with this voltage can be fatal. Do NOT connect the
instrument to the facility power source until instructed to do
so.
12. Connect the AC Power Cord supplied with the calorimeter to the
power connector on the back of the calorimeter. Use a
screwdriver to secure the line cord to the instrument using the
attached strain relief assembly, but do NOT plug it into facility
power. Refer to Figure 2-3. For installation outside the U.S.A.,
refer to International Installation, page 214.
If a power cord with the proper plug is not available, use the
wiring diagram to install the proper plug. Refer to Figure 10-3.
Figure 2-3
Power Cord Connection
13. Connect the computer to the AC600 as instructed below;
however, the power cables for the computer, printer, and balance
should be unplugged, and the instrument power should be off.
A. Connect the video cable from the monitor to the monitor
connector on the back of the computer.
B. Connect the cables from the keyboard and mouse to the
computer.
14. If an optional balance was purchased with the instrument,
connect the balance cable to the interface connector on the back
of the balance and connect the other end of the cable to serial
port COM 1 on the computer. Refer to Installing Balance, page
33.
15. If an optional Printer was purchased with the instrument, connect
the printer cable to the printer port on the back of the computer.
Printer software, if required, will be installed at a later step in this
procedure.
16. Use in. flexible tubing to connect the 12 psi (0.8 bar) air supply
line to the push-to-connect fitting labeled Pneumatic In on the
back of the calorimeter. Refer to Figure 2-5.
For a dual instrument configuration,
A. Attach a 1/4 in. T-fitting to the flexible tubing from the
pneumatic supply. Refer to Figure 2-4.
B. Attach a piece of 1/4 in. tubing to each connection on the T-
fitting. Refer to Figure 2-4.
C. Connect each piece of 1/4 in. tubing from the T-fitting to the
Pneumatic In connection on the back panel of each AC600.
Figure 2-4
Pneumatic T-Fitting
Figure 2-5
Pneumatic and Oxygen Connections
Oxygen Combustion Vessel Explosion Potential

The operator must observe safe operating practices when
using high pressure oxygen combustion vessels. Operating
personnel should be trained to practice safe operation and
maintenance of oxygen combustion vessels.
17. Connect the oxygen supply to the back of the calorimeter. The
connectors and hardware for this procedure are included in the
component pack.
A. Remove the cap plug from the O2 IN fitting on the back of
the calorimeter. Refer to Figure 2-5.
B. Using the required connector, connect one end to the
pressure regulator on the oxygen supply and the other end
to the 1/8 in. connector labeled O2 IN on the back of the
calorimeter. Refer to Figure 2-5.
If the pressure regulator is not purchased from LECO, it must have a
500 psi (34 bar) safety pressure relief valve to provide safe venting of
the gas should the regulator fail.
C. The pressure regulator is equipped with a pressure safety
release valve set to 500 psi (34 bar). Check this valve by
adjusting the regulated pressure to, or just above, 500 psi
(34 bar). The safety valve should release. Reset the
regulated pressure to 450 psi (31.0 bar) for normal
operation. For instructions to adjust the pressure relief
valve, refer to Adjusting the Pressure Safety Release Valve,
page 638.
D. The pressure safety valve should be checked periodically for
proper operation. Refer to Adjusting the Pressure Safety
Release Valve, page 638. The valve for the main regulator
tank should be turned off when the calorimeter is not in use.
18. Connect the sample prep station to the back of the calorimeter.
The sample prep station provides the means to fill and vent the
oxygen combustion vessel. The connectors and hardware for this
procedure are included in the component pack.
A. Remove the cap plug from the O2 OUT fitting on the back of
the calorimeter. Refer to Figure 2-5.
B. Using the required connector, connect the oxygen fill line to
the 1/8 in. connector labeled O2 OUT on the back of the
calorimeter. Refer to Figure 2-5.
Figure 2-6
Pneumatic and Oxygen Connections
C. Connect the other end of the oxygen fill line to the sample
prep station as shown below in Figure 2-7.
D. Connect the vent line on the back sample prep station to an
exhaust system. Refer to Figure 2-7.
E. Connect the cable from the sample prep station to the
connection on the calorimeter. Refer to Figure 2-7.
Figure 2-7
Vessel Prep Station Rear Connections
19. Connect the AC power cables from the computer, monitor,
balance, and printer to facility AC power. DO NOT turn the
computer on until instructed to do so.
20. Verify the AC Power Switch on the back of the instrument is in the
OFF position. Plug the calorimeter into the facility AC power
source.
21. Turn on the oxygen supply by using the regulator at the supply
tank.
22. Turn on the pneumatic air supply.
23. Verify distilled water was added to the external chiller during the
installation process. Refer to Specifications, page 141, for
further information about water quality.
24. Set the external chiller to approximately 7-8C below nominal
room temperature (typically 25C) and check for water leaks. For
a dual instrument configuration, refer toSingle Sized (7L) and
Dual Sized (15L) AC600 Chillers, page 39.
25. Turn on the computer but keep the power to the AC600 off.
26. Typically the software is installed by LECO. If the software has
not been installed, refer to Installing LECO Software, page 93.
27. When the Microsoft Windows login screen appears, login to the
Microsoft Windows operating system.
On computers supplied by LECO, the administrator password is LECO.
The password may be changed after logging in.
28. Confirm that the LECO ACWin software has been installed by
checking to see that the ACWIN icon has appeared on the
desktop.
29. For computers not supplied by LECO, refer to Configuring
Ethernet, page 911, and Configuring Firewall Settings, page
920.
30. If installing a dual instrument configuration, install the Ethernet
switch as follows:

A. Attach cable from PC to Ethernet switch. Refer to
Figure 2-8.
B. Attach cable from Ethernet switch to instrument or to each
instrument for dual instrument configurations. Refer to
Figure 10-7.
Figure 2-8
Ethernet Switch
31. For the optional printer, refer to manufacturer's instructions and
install printer software if required.
32. Turn on the power for the AC600.
33. Verify that the copy protection key is installed in one of the USB
ports. Refer to Copy Protection Key, page 931.
34. Double-click the ACWin icon on the desktop to start the ACWin
application.
35. The bucket lid should rise fully and the jacket should begin to fill.
The ACWIN software will automatically attempt to fill the AC600 when
the software is started and the water level sensor indicates a low
level. The system will attempt to fill the jacket for 900 seconds.
36. On the Diagnostics Solenoids/Switches tab,

A. Clear the Heater Control option check box.
B. Select the Jacket Fill check box.
37. While the jacket is filling, add water as necessary to the external
chiller to prevent the reservoir from running dry. If a low water
error message appears on the chiller,
A. Add the specified amount of distilled water. Refer to the
chillers instruction manual for more information.
B. Turn off and then turn on power to the chiller's heater
element.
38. Once the jacket reaches the correct level, the jacket water level
low will indicate that the water level is OK.
To compensate for evaporation, be certain to add distilled

water to the chiller and not the instrument.
39. After filling the instrument with distilled water, use a soft brush to
remove any air bubbles that form on the walls of the bucket,
baffle, and jacket. The bubbles must be removed before analysis.

It may be necessary to remove air bubbles over a course of several
days after changing the water.
40. Adjust the water temperature setpoint as follows:
A. In the ACWIN software, click Configuration and then click
System.
B. For Water Temperature set point, LECO recommends that
this temperature be set approximately 2 to 3 C higher than
nominal room temperature and that the external chiller be
set approximately 8 to 10 C below the temperature set in
System/Configuration in the ACWIN software. The default
temperature is 25 C.
A. Select the heater control active check box.
B. Select the bucket stirrer check box.
42. Verify that the bucket stirrer is stirring.
43. After the temperature reaches equilibrium, adjust the Flow Adjust
knob on the back of the unit until the Duty Cycle reaches a value
that corresponds with the line voltage. The goal Duty Cycle is
25% at 115 VAC and 15% at 230 VAC. Refer to Duty Cycle,
page 941.

Installing Data Transmit
This procedure configures the hardware for Data Transmission.
All character generation is coded in ASCII or UNICODE format. Special

characters (such as expanded print characters) are filtered out. Refer
to Creating Transmission Formats, page 435.
1. Connect the Data Transmit Connector on the computer to either a

serial com port or an Ethernet (Ethernet is the default). The
Ethernet must use a different port than what the instrument uses.
Refer to Configuring the Ethernet, page 911.
2. Configure the instrument's output to match that of the peripheral
device. Refer to Creating Transmission Formats, page 435.

International Installation
For international installation, a HAR approved line cord for use in the
end country must be obtained. This product requires a disconnect
device that may either be the plug of the power cord or a disconnect
device installed at the installation site if the equipment is permanently
wired.
When the plug on the power supply cord is intended to serve as the
disconnect device, the socket/outlet must be installed near the
equipment and shall be easily accessible. When the wiring is
permanently connected, a disconnect device (such as a circuit breaker
or switch) must be lockable, installed near the equipment, and be
easily accessible.

Installing Dual Instrument Configuration
The dual instrument procedure should be used for the AC600DC or

AC600DHC, page 130. For installation outside the U.S.A., refer to
International Installation, page 214, for additional information.
1. Follow the instructions in Installing Instrument for first-time

analysis, page 23, for each unit.
2. Create the database connections. Refer to Managing Databases,
page 450.
3. Set up the system software for dual configuration. Refer to
Instruments Dialog Box, page 215, for additional information.
Instruments Dialog Box

This section explains how to configure the software for dual units. To
transfer an existing database to a dual unit configuration, refer to
Transfer an Existing Database, below.
1. Click on the multiple instruments desktop icon. The Instruments

dialog box will appear.
2. The Select Vessel Type dialog box will appear. Select the vessel
that will be used and click OK.

Dual instruments should be installed separately but launched at the
same time for best results.
3. Obtain the serial number from the back of each unit and enter
this information into the Serial Number column.
4. Click Add to add additional units. Click Remove to delete a unit
from the Instruments dialog box. Several instruments can be
listed in the Instruments dialog box, but no more than two can be
launched at the same time.
5. Click in the Start column for each unit that you would like to run.
The Status column will display whether a unit is available or
running.
6. Click Continue to start each selected instrument. Click Cancel to
close the Instrument dialog box without making any changes.
Transfer an Existing Database

After entering the serial number into the Instruments dialog box, enter
the corresponding Database name. For example if the serial number is
3334, then the Database name would be Database3334. This
information can also be obtained from the CD created by LECO's Test
Department.
It may also be necessary to change the Database properties to remove

the Read-Only attribute. To change the Read-Only attribute,
1. Right-click on the folder and select Properties.

2. Remove the check in the Read-Only check box by clicking on it
once.
3. When the question "Include all Subfolders?" displays, click Yes.
4. Click OK.

3 Option Installation
Illustrations .................................................................................. 32
Installing Balance .......................................................................... 33
Preparing the Balance ............................................................... 33
Setting the Data Characters Parameters...................................... 34
Setting Up Communication with Balance ..................................... 35
Testing the Balance .................................................................. 36
Resetting the Balance ............................................................... 36
Entering Sample Weight from Balance ........................................ 37
From the Sample Login Dialog Box ........................................ 37
Directly into the Sample Grid ................................................ 37
Installing Printer ........................................................................... 38
Single Sized (7L) and Dual Sized (15L) AC600 Chillers ....................... 39
AC600 Chiller Kits: ................................................................... 39
Recirculating Chiller Kit 7L 120V (621-606-160) ...................... 39
Recirculating Chiller Kit 7L 240V (621-606-162) ...................... 39
Recirculating Chiller Kit 15L 120V (621-606-164) .................. 310
Recirculating Chiller Kit 15L 240V (621-606-166) .................. 310
Installing the Chiller and Sterilizer ............................................ 311
Adding Distilled Water ............................................................ 315
Setting Temperature............................................................... 316
Cleaning Chiller Condenser ...................................................... 316
Completing Chiller Warranty Registration .................................. 316
Bar Code Reader ......................................................................... 317
Installation Instructions .......................................................... 317
Scan Bar Code for Vessel Number ............................................ 317
Scan Other Bar Codes ............................................................. 317
Option Installation AC600 31

Illustrations
Figure 3-1 Balance Control Panel .......................................................... 34

Figure 3-2 Chiller Rear Panel ............................................................. 311
Figure 3-3 Chiller Sterilizer Installation ............................................... 312
Figure 3-4 Water Filter ...................................................................... 312
Figure 3-5 External Chiller Cover ........................................................ 313
Figure 3-6 Drain Connection .............................................................. 313
Figure 3-7 Drain Tubing Installed ....................................................... 314
32 AC600 Option Installation

Installing Balance
A Sartorious analytical balance is available as an option. The

following procedures should be performed to install a 4 or 5 place
balance. For further information, refer to the manual supplied with the
balance.
The instrument will only support Sartorious analytical balances.

Other balances may be used; however, LECO is not responsible for
their installation or proper operation.
After the balance is set, do not change any of the configuration
parameters. The configuration parameters can be changed to custom
configure the balance but only after the installation procedure is
completed and the balance is properly operating with the instrument.
To restore the balance to factory defaults, refer to Resetting the

Balance, page 36.
1. Set up the balance in the location where it will be used. Refer to

Preparing the Balance below.
2. Follow the procedure in Data Characters Parameters, page 34.
3. Set up communication between the balance and instrument
software. Refer to Setting Up Communication with Balance, page
35.
4. Test the balance to ensure proper operation. Refer to Testing the
Balance, page 36.
5. Complete and return the Warranty Registration Card that came
with the Balance to the Balance manufacturer.
Preparing the Balance

1. Unpack the Balance and assemble it as shown in the manual
supplied with the balance.
2. Plug the AC adapter, supplied with the balance, into facility
power.
3. Connect the AC adapter cable to the power-input jack on the rear
of the balance.
4. Locate the level bubble on the rear of the balance and adjust the
balance feet to level the balance. The balance is level when the
level bubble is positioned in the center of the circle.
5. Connect the balance interface cable to com 1 on the PC tower and
the balance connector on the rear of the balance.

Figure 3-1
Balance Control Panel
Setting the Data Characters Parameters

Set the data character parameter to 16 code 7_2_1 using this
procedure.
1. Turn the AC power on to the balance by pressing the power

button. As soon as all segments on the display illuminate, push
Tare. The display will be blank briefly and then the menu code
settings will appear.
2. Press CAL to display 7 as the left digit.
3. Press Print to display the center digit.
4. Press CAL to display 2 as the center digit.
5. Press Print to display the right digit.
6. Press CAL to display 1 as the right digit.
7. Press and hold Tare until parameters are set.

Setting Up Communication with Balance
The following section explains how to set up communication between
the computer and the external balance.
1. From the Configuration menu, click System. The System

Configuration window will appear.
2. Click the Balance tab. The Balance Configuration screen will
appear.
3. For Port, click the arrow and select the port location from the list
that matches the port selected on the PC tower. Default is COM1.
4. For Baud Rate, click the arrow and select the baud rate from the
list. Refer to the Sartorius Instruction Manual. Default is 1200
bps.

5. For Data Bits, click the arrow and select the number of data bits
from the list. Refer to the Sartorius Instruction Manual. Default is
7.
6. For Parity, click the arrow and select either odd or even. Refer to
the Sartorius Instruction Manual. Default is Odd.
7. For Stop Bits, click the arrow and select either 1 or 2 from the
list. Refer to the Sartorius Instruction Manual. Default is 1.
8. For Readability, the default is 4.
9. For Balance Mode, select Normal if a balance is connected to the
system. Select Disabled if a balance is not connected to the
system.
10. For Send Command, click the arrow and select the desired
command from the list. The default is <ESC>P<CR><LF>.
11. For Tare Command, click the arrow and select the desired
command from the list. The default is <ESC> T.
12. Click Print to print a copy of the balance parameters, if desired.
13. Use Test Commands when it is necessary to check the operation
of the balance. Click Send to send a weight from the balance.
When operational, the balance reading will display in the
spreadsheet. Click Tare to set the balance display to zero.
Testing the Balance

From the Configuration menu, select System, select the Balance tab,
and then select Send. The weight displayed in the Weight from Balance
box should match the weight displayed on the balance.
Resetting the Balance

The following section explains how to restore the balance to factory
defaults. Consult LECO Service before resetting the balance to factory
defaults.
1. Turn the AC power on to the balance by pushing the power on

button. Refer to Figure 3-1.
2. As soon as all the segments on the display light, push the Tare
button. The display will blank for a few seconds and then the
menu code settings will appear.
3. Press CAL to display 9 in the left digit. Refer to Figure 3-1.
4. Press Print to skip the center digit.
5. Press CAL to display 1 as the right digit. Refer to Figure 3-1.
6. Press TARE and hold it for 2 seconds or more.
7. Set the data characters parameters. Refer to Setting the Data
Characters Parameters, page 34.
8. Continue with testing the balance. Refer to Testing the Balance,
page 36.

Entering Sample Weight from Balance
To receive weights from the balance, the Balance (F4) on the Toolbar
must be selected or Balance must be selected from the sample menu.
From the Sample Login Dialog Box

1. From the Samples menu, click Login.
2. Click Balance to enter a weight from an external balance.
Directly into the Sample Grid

1. Place the crucible on the balance.
2. Press Tare on the balance.
3. Place the sample in the crucible.
4. Press Print on the balance or click the Samples menu and select
Balance (F4). The sample mass will be entered into the first row
of the sample grid without a mass entry.

Installing Printer
Printers are available as purchasable options for the instrument. Refer

to Options, page 133.
If installing the printer at the same time as the instrument for a first-
time analysis, refer to Installing Instrument for First-Time Analysis,
page 23.
If installing the printer after the instrument and computer are

installed, refer to printer manufacturer's instructions for the
installation procedure.

Single Sized (7L) and Dual Sized (15L) AC600 Chillers
A chiller is not supplied with the instrument. It must be purchased

separately. There is a single sized (7L) and dual sized (15L) chiller
available as an option. Refer to Options, page 133. Refer to the
Manufacturers Operating Manual for further information.
AC600 Chiller Kits:
Recirculating Chiller Kit 7L 120V (621-606-160)

1 589-187 TAPE THD SEG TEF .250X 520 IN*
1 803-283 FTG PLUG BR .25NPTF CSK HEX
1 621-606-129 ASSY COVER CHILLER 7L SST
1 621-606-130 CHILLER RECIRCULATING 120V 7L
1 621-606-139 FTG QD ADPTR .25MPT - .250T
1 621-606-161 BULLETIN KIT INSTRUCTIONS FOR 621-606-160

1 621-606-139 FTG QD ADPTR .25MPT - .250T

1 621-807 FTG T HDPE.75HB- .75HB- .75HB
1 621-606-139 FTG QD ADPTR .25MPT - .250T
1 621-606-141 FTG QD Y .250T - .250T - .250T

1 621-807 FTG T HDPE.75HB- .75HB- .75HB
1 621-606-139 FTG QD ADPTR .25MPT - .250T
1 621-606-141 FTG QD Y .250T - .250T - .250T

Installing the Chiller and Sterilizer
1. Unpack the chiller and position it on the floor (or at a lower level)
near the AC600. Refer to Facility Requirements, Figure 10-2 for a
diagram of the proper placement.
Verify the front and back vents are NOT blocked. If these vents are
blocked, the chiller will turn off. Keep at least 8-inches (20 cm) of
open space around the front and back vents.
2. Apply 589-187 thread tape to the threads of the 803-283 plug
fitting if there is not already thread tape on the fitting. Install the
803-283 plug fitting into the Inlet port on the rear panel of the
chiller. Refer to Figure 3-2.
3. Apply 589-187 thread tape to the threads of the 621-606-139
adapter fitting. Install the 621-606-139 fitting into the Outlet port
on the rear panel of the chiller. Refer to Figure 3-2.
Figure 3-2
Chiller Rear Panel
4. If not done already, use a piece of inch tubing supplied with

the AC600 and cut it to length between the IN side of the water
filter housing on the back of the AC600. Firmly insert the inch
tubing into the push-to-connect fitting on the IN side of the water
filter housing and into the 621-606-139 adapter fitting at the
outlet port of the chiller. Refer to Figure 3-2.
5. Install the 621-606-153 7L/15L Chiller Sterilizer to the rear of the
chiller unit as shown in Figure 3-3 by using two 190-278 screws.
Installation of the 621-606-153 7L/15L Chiller Sterilizer will
require removal of two of the existing rear panel screws.

Figure 3-3
Chiller Sterilizer Installation
6. Connect the 619-590-821 tubing between the fitting on the back

of the chiller and the adapter fitting at the bottom of the
sterilizer.
7. For Single Sized Chillers, connect the water line from the filter on
the back of the AC600 to the top fitting on the sterilizer. Refer to
Figure 3-4.
Figure 3-4
Water Filter
8. To set up the 15L chiller for dual AC600s, install the

622-606-141 Y-fitting into the fitting at the top of the sterilizer.
Refer to Figure 3-3.
9. To set up the 15L chiller for dual AC600s, Connect the water lines
from the Y-fitting to the back of each AC600 water filter. Refer to
Figure 3-4.

10. Fill the chiller reservoir using only distilled water. Do not overfill.
11. Locate the chiller cover assembly and use this cover in place of
the original cover. Refer to Figure 3-5.
Figure 3-5
External Chiller Cover
12. Obtain 3/4 inch ID drain tubing. Cut the drain tube to length as
necessary to fit between the AC600 drain connection and the
chiller cover.
13. Connect one end of the 3/4-inch drain tubing to the drain at the
back of the AC600. Refer to Figure 3-6.
Figure 3-6
Drain Connection

14. Install the other end of the 3/4-inch drain tubing through the
grommet on the chiller's cover. Avoid kinks and sharp bends to
ensure that water flows freely from the AC600 to the external
chiller. Allow approximately 3 to 4-inches (7.5 to 10 cm) of tubing
to extend through the grommet far enough into the chiller
reservoir to ensure that the tubing is securely mounted in the
chiller cover.
Figure 3-7
Drain Tubing Installed
15. Connect the controller power cable at the back of the controller to
the main outlet at the back of the chiller base as shown in the
Manufacturers manual. Plug the main power cable into an
appropriate power outlet.
16. Power on the chiller.
17. Plug in the sterilizer to an appropriate power outlet. The sterilizer
will turn on as soon as it is plugged in.
18. Check the push-to-connect fittings to verify that no leaks are
present. If leaks are present, it may be necessary to power off
the chiller and heater element, remove the tubing from the push-
to-connect fittings, re-cut the tubing, and replace the tubing in
the push-to-connect fittings.
19. After setting the chiller in position, wait about one hour before
operating the unit to ensure maximum cooling performance.
Refer to the Manufacturers manual for further information.
20. Set the pump speed to the maximum of 100, the default is 70.
Refer to the Manufacturers manual for further information.
21. Return to Installing Instrument, step 12, page 26, to finish
installing the AC600.

Adding Distilled Water
Check distilled water level daily or according to the instruction manual
for the chiller.
It is important to maintain the correct water level in the

chiller. A low water level may cause the water in the chiller
to freeze. For optimum cooling efficiency, the bath fluid
level should be kept above the cooling coils at all times.
The chloride salts used in most algaecides are a significant cause of

corrosion and should be avoided in the AC600.
1. Lift the chillers cover and add distilled water to the reservoir until
it reaches the recommended fill level shown below, which is
approximately 1-inch (20 mm) below the top of the reservoir. Do
Not fill the chiller to the top of the reservoir or it will overflow.
2. Start the chiller and instrument. Allow the jacket in the
instrument to fill with distilled water. Upon start up, it may be
necessary to add fluid to maintain proper levels or damage to the
heater coil may occur. Refer to the manufacturers manual for
further information.
3. As the jacket fills, lift the chillers cover while still keeping the
drain tube over the water and continue to add distilled water to
the reservoir until the jacket and chiller water levels are filled.

Setting Temperature
The following section explains how to set the temperature for the
single and dual sized chillers. Refer to the manufacturers manual for
more information.
1. Plug in the power cord.

2. Select the language by using the control panel. Refer to the
manufacturers manual for more information.
3. Set the Safety Set Point. Refer to the manufacturers manual for
more information.
4. Turn on the controller. Refer to the manufacturers manual for
more information.
5. Set the Bath Temperature Set Point. Refer to the manufacturers
manual for more information.
Cleaning Chiller Condenser

Clean the condenser as necessary to maintain optimum performance.
Refer to section 6 of the PolyScience Operator Manual.
Completing Chiller Warranty Registration

Complete the Warranty Registration Card sent within the chiller
packaging. Submit completed card to the chiller manufacturer.

Bar Code Reader
An optional bar code reader, also known as a Keyboard Wedge Reader,

is available for the AC600 to provide an automatic means to enter the
correct vessel number for each sample.
A total of 10 bar code labels, numbered 0-9, are provided to help

identify the vessel number. Whenever multiple vessels are used, it is
recommended that these labels be affixed to each combustion vessel
to correlate the correct calibration coefficient with the current vessel.
Installation Instructions
1. Follow the manufacturers instructions to install the bar code
reader.
2. Follow the manufacturers instructions to configure the bar code
reader to recognize the Codabar symbology.
Scan Bar Code for Vessel Number

1. Complete Installation Instructions, above.
2. If multiple vessels are used, affix a bar code label to each vessel.
3. Follow the manufacturers instructions to enable the Start (A) and
Stop (C) characters, which are used by the ACWin software to
recognize the scanned code as a vessel number. The bar code
reader will not function properly with the ACWin software if the
Start and Stop characters are suppressed.
4. Follow the manufacturers instructions to disable recognition of
unnecessary bar code symbologies, which can decrease the speed
and accuracy of the reader.
5. When the ACWin software is open and activated, it will recognize
the Codabar symbology when a vessel bar code is scanned. The
vessel number will be automatically entered for the next sample
to be analyzed.
The vessel bar code scanned will apply to the next sample analyzed and
will overwrite any existing vessel number entered for that sample.
Scan Other Bar Codes

If desired, the bar code reader can also be used to enter other bar
code information into the ACWin software as explained below.
1. Complete Installation Instructions, above.

2. Configure the scanner to recognize the appropriate bar code
symbology (e.g., UPC, Code 128, etc.).
3. In the ACWin spreadsheet, click in the desired field such as
Comment, Description, or Sample Name.
4. Scan a bar code to enter that information into the spreadsheet.


4 System Setup
Selecting Language ....................................................................... 44
ACWIN Software Main Window ........................................................ 45
Menu Bar ................................................................................ 46
Database Menu ................................................................... 46
Edit Menu ........................................................................... 46
View Menu ......................................................................... 47
Samples Menu .................................................................... 48
Configuration Menu ............................................................. 49
Diagnostics Menu ................................................................ 49
Maintenance Menu ............................................................ 410
Help Menu ........................................................................ 410
Dialog Box Buttons ................................................................. 410
Using Toolbars ............................................................................ 412
Toolbar ................................................................................. 412
Small Buttons ........................................................................ 413
Customizing Sample Spreadsheet .................................................. 414
Customizing Font and Columns ................................................ 414
Modifying Font .................................................................. 414
Modifying Columns ............................................................ 415
Navigating Sample Spreadsheet ............................................... 416
Column Scroll Bar Menu ..................................................... 416
Row Scroll Bar Menu .......................................................... 417
Navigating the Spreadsheet using the View Menu .................. 417
Customizing Software Main Window............................................... 418
Adding Dashboard Panes ......................................................... 418
Using the Dashboard Menu ...................................................... 420
Identifying Parts of a Pane ...................................................... 421
Using the Tab Menu ................................................................ 422
Moving a Pane ....................................................................... 422
Resizing Panes ....................................................................... 423
Configuring Main Window for Dual Monitors ............................... 424
Creating a New Frame ....................................................... 424
Detaching a Frame ............................................................ 424
Using Screen Layouts Dialog Box ............................................. 424
Saving Screen Layouts ....................................................... 424
System Setup AC600 41

Selecting a Layout to Appear in the Main Window .................. 425
Deleting a Layout .............................................................. 425
Modifying Position of Screen Name ...................................... 425
Displaying Original Screen .................................................. 425
Determining User Permissions....................................................... 426
Adding User in Windows OS ..................................................... 426
Adding Users to Instrument Software ....................................... 426
Changing Users in Windows OS ................................................ 426
Deleting Users in the Instrument Software ................................ 427
Adding or Changing User Permission for Instrument ................... 428
Configuring System ..................................................................... 430
Wake Up Tab ......................................................................... 431
Importing Sample Data ................................................................ 432
Format Sample Data ............................................................... 432
Importing Sample Data into Spreadsheet .................................. 433
Creating Sample Templates .......................................................... 434
Creating Transmission Formats ..................................................... 435
Creating and Modifying Transmission Formats............................ 435
Properties Dialog Box.............................................................. 435
Fields Tab ........................................................................ 435
Delimiters Tab .................................................................. 436
Automation Tab ................................................................ 437
Communication Settings Tab .............................................. 438
Advanced Tab ................................................................... 438
Preview Tab ...................................................................... 440
Creating Export Format ................................................................ 441
Creating and Modifying Export Formats ..................................... 441
Properties Dialog Box.............................................................. 441
Filename Tab .................................................................... 441
Fields Tab ........................................................................ 442
Delimiters Tab .................................................................. 442
Automation Tab ................................................................ 443
Advanced Tab ................................................................... 443
Preview Tab ...................................................................... 444
Creating and Modifying User Defined Fields .................................... 445
Number Formatting ................................................................ 446
Format Examples .............................................................. 446
Formulas ............................................................................... 447
Comparison Functions ........................................................ 449
Managing Databases .................................................................... 450
Using the Start Dialog Box ...................................................... 451
Creating and Retrieving Database Backups ................................ 452
42 AC600 System Setup

Create Backup .................................................................. 452
Retrieve Backup ................................................................ 453
Selecting a Database Connection.............................................. 453
Adding a Database Connection ................................................. 454
Adding a Connection to an Existing Database ........................ 454
Adding a Connection to a New Database .............................. 455
Deleting a Database Connection ............................................... 457
Validating a Database ............................................................. 457
Reviewing Orphan Objects .................................................. 459
Compacting/Repairing a Legacy Database ................................. 460
Managing Databases for 21 CFR Part 11 Compliance ................... 460
Enabling Logging for an Existing Database ........................... 461
Enabling Logging for a New Database .................................. 462
Database Menu ................................................................. 464
Adding a Connection to a Log Archive Database .................... 469
Removing Results from a Database ..................................... 469
Disabling Logging on an Existing Database ........................... 470

Selecting Language
The Select Languages dialog box displays the different language

choices in the software.
1. From the Configuration menu, click Select language.
2. Select the desired language.

3. Select OK.

ACWIN Software Main Window
The ACWIN software is used to operate the AC600 Calorimeter and

process acquired sample data for precision analytical results.
The main window of the software displays the Title Bar, Menu Bar,
Spreadsheet, and Dashboard. The Status Bar and Toolbar will appear if
selected on the View menu. For further information about enabling the
Status Bar and Toolbar, refer to the View Menu, page 47.
The Title bar identifies the sample filter that is applied to the samples
and provides the buttons to minimize, maximize, and close the
software main window. In the example above, the filter applied is
called TruSpeed Samples. Refer to Using Sample Filters, page 520.
The Menu bar, page 46, provides menus that perform various
operations in the software.
A Toolbar provides quick access to frequently used functions. Refer to

Using Toolbars, page 412, for a description of the two Toolbars that
are available.
The Spreadsheet displays sample data. The fields displayed in the

spreadsheet will vary, depending on the fields designated as visible in
the Sample Display dialog box.
The Dashboard can be configured in many ways, including Bucket

Temperature (C) vs. time (sec); Jacket Temperature (C) vs. time
(sec); Filtered Bucket Temperature (C) vs. time (sec); Filtered Jacket
Temperature (C) vs. time (sec). Refer to Customizing Software Main
Window, page 418.

The Log Bar (not shown) can be selected from the View menu to
appear in the main window; however, the log bar will always appear in
the main window to display communication failures, errors, and
aborted analyses whether or not it has been selected from the View
menu. When the Log Bar is selected on the View menu, however, it
will display when any action is logged. The Log Bar will disappear from
the main window once the View Log File button has been clicked. Refer
to View Menu, page 47.
The Status Bar displays operational prompts and status messages.

Refer to the View Menu, page 47.
Menu Bar
The following section explains the menus available on the menu bar.
Database Menu
Selections on the Database menu are available when logging has been
enabled for a database connection. Refer to Managing Databases, page
450.
Presentation Time - Refer to View Presentation

Time, page 464.
View History - Refer to View History, page 465.
Archive Log - Refer to Archive Log, page 466.
Delete by Date Refer to Delete by Date, page
468.
Exit - Select Exit to close the software program.
Edit Menu
Select the Edit menu to access commands for entering sample data
into the spreadsheet.
Insert - Refer to Inserting a Sample Out of Sequence,

page 515.
Fill - Refer to Repeating Data in Multiple Cells, page
514.
Cut - Select Cut to remove data from an entire row in
the spreadsheet to the clipboard. Data can then be
pasted into another row.
Copy - Select Copy to duplicate data from a row in the
spreadsheet to the clipboard. Data can then be pasted
into another row of the spreadsheet, duplicating the
copied row.
Paste - Select Paste to insert data from the clipboard to
a selected row in the spreadsheet.

View Menu
Select the View menu to enable or disable the Toolbar, Status Bar, and
Log Bar, and to navigate the spreadsheet.
Toolbar - Select Toolbar to display the

Toolbar in the software main window. A
means the Toolbar will appear in the
software main window. To hide the Toolbar,
click the and it will not display.
Status Bar - Select Status Bar to enable or
disable the Status Bar in the software main
window. A means the Status Bar will
appear in the software main window. To
hide the Status Bar, click the and it will
not display.
Log Bar - Select Log Bar to enable or
disable the Log Bar in the software main
window. A means the Log Bar will appear
in the software main window. To hide the
Log Bar, click the and it will not display.
Small Buttons - Select Small Buttons to
display the Small Buttons toolbar in the
software main window. A means the
Small Buttons toolbar will appear in the
software main window. To hide the Small
Buttons Toolbar, click the and it will not
display.
First Row - Select First Row to access the
first row in the spreadsheet.
Analysis Row - Select Analysis Row to
access the row that contains the next
sample to be analyzed in the spreadsheet.
Last Row - Select Last Row to select the
last row in the spreadsheet.
New Dashboard Pane - Refer to Adding
Dashboard Panes, page 418.
Screen Layouts - Refer to Using Screen
Layouts, page 424.

Samples Menu
Select the Samples menu to perform operations for sample data.
Login - Refer to Logging In a Sample, page 514.

Balance - Refer to Preparing the Balance, page 33.
Analyze - Refer to Analyzing a Sample, page 518.
Abort - Stop an analysis in progress.
Recalculate - Refer to Recalculating Results on page 5
26.
Transmit - Refer to Transmitting Results, page 538.
Print - Refer to Printing Analysis Results, page 530.
Print Preview - Refer to Configuring Analysis Report
before Printing, page 530.
Print Setup - Change the paper size, orientation, or the
printer.
Text Import Data - Refer to Importing Sample Data,
page 432.
Text Export Data - Refer to Exporting Data, page
536.
Text Export Buffers - Refer to Exporting Buffers, page
537.
Transfer Export - Refer to Transfer Import and Export,
page 534.
Transfer Import - Refer to Utilizing Transfer Import and
Export, page 535.
Sign - Refer to Applying Sample Signatures, page
528.
View Signatures - Refer to Applying Sample Signatures,
page 528.
Delete - Refer to Deleting a Sample, page 519.
View History - Refer to View History, page 465.

Configuration Menu
Select the Configuration menu to configure instrument parameters for
sample analysis.
Calibration - Set the accuracy of the instrument to

that of known calibration standard samples. Refer to
Calibration, page 524.
Standards - Refer to Calibration, page 524.
Methods - Refer to Creating or Modifying Methods,
page
59.
Counters - Refer to Maintenance Counters, page 6
6.
User Defined Fields - Refer to Creating and
Modifying User Defined Fields, page 445.
Sample Templates - Refer to Creating Sample
Templates, page 434.
System - Refer to Configuring System, page 430.
Users - Refer to Adding or Changing User
Permission, page 426.
Transmission Formats - Refer to Creating
Transmission Formats, page 435.
Text Export Formats - Refer to Creating Export
Format, page 441.
Select Language - Refer to Selecting Language,
page
44.
Auto Widths - Adjust the width of each cell so that
all of the text within each cell appears.
Display - Refer to Customizing Sample Spreadsheet,
page 414.
Sample Filters - Refer to Using Sample Filters, page
520.
Vessel - Refer to Instrument Dialog Box, page
215.
Diagnostics Menu
Select the Diagnostics menu to monitor the instrument and help
maintain proper instrument operation.
Chart - Refer to Monitoring Ambient Chart, page 82.

Offset Thermistors - Refer to Using Offset Thermistors,
page 810.
Solenoids/Switches - Refer to Solenoids and Switches,
page 88.
Lift Mechanism - Refer to Lift Mechanism, page 812.

Network - Refer to Network, page 814.
Maintenance Menu
Select the Maintenance menu to log in periodic maintenance or to view
the instrument log file.
Login - Refer to Log In Periodic Maintenance, page

68.
View Log File - Refer to Viewing Log, page 610.
Dock Wizard - Refer to Using Dock Wizard, page 940.
Flow Adjust - Refer to Adjusting Duty Cycle, page 941.
Help Menu
Select the Help menu to access further information about the
instrument.
Information and Help - Select Information and Help to

access the AC600 instruction manual in a pdf.
About - Select About to access instrument information
such as the version number, serial number, and
copyright information and to register the instrument
using the Edit License dialog box. Refer to Registering
Software, page 925.
Dialog Box Buttons

The following table explains the buttons available on dialog boxes
throughout the ACWIN software.
Button Action
Inserts a row into a table or provides the ability to add a
new item such as a method name.
Select Ascending, and items will appear in alphabetical
and/or numerical order from lowest to highest.
Clone appears on the Methods dialog box.
1. Select the method to be cloned.
2. Click Clone. The new method is inserted above the
cloned method with the same name plus a dash and
the number one (-1).
3. Select the new method, rename the method, and then
enter parameters for the method. Refer to Creating or
Modifying Methods, page 59.
4. Click OK to close the Method dialog box.

Button Action
1. Select the desired item to remove. A dialog box will
display to verify the delete.
2. Click OK.
Methods can be deleted unless referenced by samples.
Moves an item to a lower position, which means it will
display later in a table or list.
Select Descending, and the items will appear in
alphabetical and/or numerical order from highest to
lowest.
Click to access the Export dialog box. Refer to Exporting
Methods, page 512.
Click the Help button to access the AC600 instruction

manual in a pdf.
Click to access the Import dialog box. Refer to Importing

Methods, page 513.
Provides another option for adding a row to a table where
desired. The inserted new row will be placed above the
selected row; therefore, click on the row beneath the
desired location for the new row before clicking Insert.
Click to print an item.
Moves an item to a higher position, which means it will

display earlier in a table or list.
Click Properties to determine the values, settings, or

parameters for a particular area.

Using Toolbars
A toolbar provides buttons that provide the means to quickly perform

main tasks. There are two toolbars available in the ACWin software as
explained in the following section. Refer to Toolbar, below, and Small
Buttons, page 413. Refer to the View menu, page 47, for
instructions to display the toolbars.
Toolbar
Toolbar Button Action
Select F1 to access the electronic version of the instruction

manual.
Select F3 to access the Sample login menu and log in a sample.

Select the arrow to access another menu for login or drift sample
login. Refer to Logging in a Sample, page 514.
Select F4 to display the mass value for a sample in the

spreadsheet.
Refer to Analyzing a Sample, page 518.
Select F6 to stop an analysis.
Select F7 to put the instrument into the Idle state.
Select F8 to close the software.

Small Buttons
Small Buttons displays a smaller toolbar with more buttons available
than the standard toolbar. Refer to the View menu, page 47, for
further information about displaying the toolbars.
To identify a toolbar button, hover the mouse cursor over a toolbar

button to display a tooltip that identifies the purpose of the button.
Toolbar Button Action
Information and Help
Login Sample
Add a Sample Mass from the Balance
Print Spreadsheet Selection
Print Preview Sample Spreadsheet Selection
Analyze Now
Abort the Current Analysis
Idle and Wake up. Use this button to put the instrument into
an idle state. When in idle state, the button appears as ,

which will wake up the instrument when clicked.
Opens and Closes Calorimeter
View Ambient Chart
View and Modify Solenoid States
Network (tab) on Diagnostics Dialog Box
Maintain the Methods
Edit the System Setting
Vessel Calibration

Customizing Sample Spreadsheet
This section explains how to customize the font and columns in the
spreadsheet and how to navigate the spreadsheet.
Customizing the samples that display can be accomplished using

sample filters. Refer to Using Sample Filters, page 520.
Customizing Font and Columns

1. Select Configuration and then select Display or right-click
anywhere in the spreadsheet and then select Properties. The
Fields tab will display automatically.
2. Use the tabs on the Sample Display dialog box to change the
spreadsheet display. Refer to Modifying Columns, page 415, and
Modifying Font, below.
Modifying Font
Use the Font dialog box to change the font, style, and size of text.
The current selections are highlighted and appear in the boxes.
1. Right-click anywhere in the spreadsheet and select Properties or

click the Configuration menu and select Display.
2. Click the Font tab.
3. While making changes, use Sample Text to view the text as it will
display before accepting the changes.
4. Change the Font Name, Style, or Size by single-clicking the
desired selection in the list.
5. Select OK when the text displays as desired.

Modifying Columns
Use the Fields tab to display or hide columns and to change the order
of the columns in a spreadsheet. For definitions of the columns that
display in the spreadsheet, refer to Glossary, page 121. Customized
column headings can also be created with User Defined Fields. Refer to
Creating and Modifying User Defined Fields, page 445.
Locked columns is not available on the Report Settings Fields tab.
To display a column, select the desired column in Invisible Fields and

then select Show or double-click on the name of the desired column in
Invisible Fields.
To remove a column from a display, select the column in Visible Fields
and then select Hide or double-click on the name of the desired
column in Visible Fields.
Select Default to restore the columns that are preset to display.
For Locked Columns, enter a value to lock the leftmost columns so
that these columns are always displayed when scrolling left or right on
the spreadsheet. For example, if 4 is entered in the locked columns
entry box, the first four columns listed in Visible Fields will display
even when the scroll arrows are moved to the end of the spreadsheet.

Navigating Sample Spreadsheet
The spreadsheet can contain numerous rows and columns. Use the
row scroll bar menu and column scroll bar menu to easily navigate the
data in the spreadsheet.
To access these menus, right-click on the column scroll bar to page

through the columns or right-click on the scroll bar the row scroll bar
to page through the rows. The column scroll bar is only available when
there are several columns displayed in the spreadsheet. Refer to
Column Scroll Bar Menu, below, and Row Scroll Bar Menu, page 417.
Column Scroll Bar Menu

Scroll Here displays the data at a certain location in the
spreadsheet. For example, to display columns near the
end of the spreadsheet, right-click on the right most side
of the column scroll bar and then select Scroll Here. The
last columns in the spreadsheet will display.
Left Edge displays the first column of the spreadsheet.
Right Edge displays the last column of the spreadsheet.
Depending on the point selected on the column scroll bar,
Page Left will go to the left most point equivalent to one
page.
Page Right will go to the right most point equivalent to one
page.
Scroll Left moves the spreadsheet to the left by one
column.
Scroll Right moves the spreadsheet to the right by one
column.

Row Scroll Bar Menu
Scroll Here displays the data at a certain location in
the spreadsheet. For example, to display rows near
the middle of the spreadsheet, right-click near the
middle of the row scroll bar and then select Scroll
Here. Rows near the middle of the spreadsheet will
display.
Top displays rows at the top of the spreadsheet.
Bottom displays rows at the bottom of the
spreadsheet.
Depending on the point selected on the column
scroll bar, Page Up will move the rows up
equivalent to one page.
scroll bar, Page Down move the rows down
equivalent to one page.
scroll bar, Scroll Up moves the spreadsheet up by
one row.
scroll bar, Scroll Down moves the spreadsheet
down by one row.
Navigating the Spreadsheet using the View Menu

From the View menu, select First Row to go to the first row in the
spreadsheet.
Select Analysis Row to go to the row of the current sample to be
analyzed.
Select Last Row to go to the last row of the spreadsheet.

Customizing Software Main Window
The ACWIN main window consists of a sample spreadsheet and

dashboard. Refer to AC600 Software Main Window, page 45, for
further information about the areas of the software main window. The
contents of the sample spreadsheet are determined by the sample
filter. Refer to Using Sample Filters, page 520. The dashboard can
consist of one pane or several panes. Refer to Adding Dashboard
Panes, below.
The spreadsheet and dashboard of the software main window can be

arranged in various ways. The sample spreadsheet and dashboard
panes can be moved next to, above, and below each other. After
customizing the layout, the arrangement can be saved and then used
for various samples thus simplifying the review of sample data. Refer
to Using Screen Layouts Dialog Box, page 424.
This section explains the following topics:
Adding Dashboard Panes, below Moving a Pane, page 422

Using the Dashboard menu, page 420 Resizing Panes, page 423
Identifying Parts of a Pane, page 421 Using the Tab Menu, page 422
Using Screen Layouts Dialog Box, page Configuring the Main Window for Dual
424 Monitors, page 424
Adding Dashboard Panes

1. From the View Menu, click New Dashboard Pane.
2. Select either the Show Plot check box or the Show Values check
box. When Show Plot is selected, configure the plot by selecting
the reporting units, plot pattern, plot color, and display of the Y-
Axis.
3. For Plot Options, click the buttons to determine how items appear
in the dashboard.

4. Select the check box to Show Control Chart with Stats, Show
Control Chart, Show Stats, or Overlaid Plots.
5. Select the stats to display.

6. Select the Label Stats Points check box to label points.
7. Enter the value for significant digits.
8. In the Tab Label box, enter a descriptive title for the dashboard
tab.
9. Click OK.

Using the Dashboard Menu
Zoom In - Position the mouse over the desired area.
While holding the left mouse button down, draw a box
with the mouse. The area inside the box will be
magnified. Draw another box to zoom in farther.
Zoom Out - Select Zoom Out to restore the plot to
the original magnification.
Zoom Out One Level - Select Zoom Out One Level
to reduce the magnification by one level.
Label Points - When selected, points on the plot are
labeled to show the order in which they were selected
from the Spreadsheet. To label points on the plot,
select multiple samples from the Spreadsheet, right-
click in the plot, select Label Points from the menu.
Statistics - When Statistics is disabled (no ),
sample names display in the plot, and the color of the
sample name listed to the right of the display
corresponds with the color of the line indicating the
sample displayed in the plot. When enabled with a ,
sample names do not display, and the result curves
change to result points. Points can be labeled, see
Label Points, above. To enable or disable Statistics,
select multiple samples from the Spreadsheet, click in
the desired plot, and click Statistics on the menu.
Auto Independent Scale - Plots of different sized
scales are displayed as the same size in order to
compare the plots more easily using Auto
Independent Scale. To enable or disable Auto
Independent Scale, select multiple samples from the
Spreadsheet, click in the desired plot, and then select
Auto Independent Scale from the menu.
Print - Refer to Printing Reports, page 530.
Print Preview - Refer to Configuring Analysis Report
before Printing, page 530.
Properties - Refer to Adding Dashboard Panes, page
418.

Identifying Parts of a Pane
Button Name Action

Title Bar Click to access the title bar commands in a list
Drop-Down format. Useful when there are several dashboard
Menu panes open.
Move The move handle slides to the left or right to

Handle hide or display title bar commands and tabs.
Each dashboard pane is represented by a tab.

When a tab is selected, that pane becomes
active in the dashboard and the name of the
Tabs pane appears in boldface on the tab. If an active
Tab does not display in the title bar, click the
shaded scroll arrows until the active tab
appears.
Scroll Arrows can be clicked to cycle through the
tabs that display in the title bar. Shaded scroll
Scroll
arrows indicate that there are more tabs to
Arrows
display. Unshaded scroll arrows indicate that
there are no more tabs.

Using the Tab Menu
To display the Tab menu, right-click on a tab.
New Frame - Creates an empty frame that can be

moved to another monitor when using dual monitors.
Refer to Creating a New Frame, page 424.
Close - Use to remove a dashboard pane from the
window
Next - Use to move to the next dashboard pane. You
can also hold CTRL and click Tab to move to the next
pane.
Previous - Use to move to the previous dashboard
pane in the window. You can also hold CTRL and click
Tab to move to the previous pane.
Toggle Views - Use to make the pane and smaller.
Select Toggle Maximize to make a pane fill the
window; select Toggle Minimize to make a pane
smaller.
Detach - When using dual monitors, use Detach to
move a dashboard pane to another monitor. Click on
the dashboard pane that has been detached and then
drag the pane to the second monitor.
Moving a Pane
Dashboard panes can be arranged to display next to, above, or below
each other.
1. If all of the tabs do not display, use the move handle or the scroll
arrows to locate a tab.
2. Click on the tab to move a dashboard pane to another location.
While the dashboard pane is being dragged, a highlight bar and a
guide arrow will display. The highlight bar indicates the location of
the dashboard pane being moved. The length of the highlight bar
corresponds to the length the window will be when it is moved.

While dashboard views are being moved, hatching will appear to
indicate that one pane is overlaying another pane. Once the dashboard
pane being moved is in the final location and the mouse button is
released, hatching will disappear. The tabs that display in the title bar
indicate the number of dashboard panes within a window.
Resizing Panes
1. Move the cursor over the splitter bar of the window to resize until
cursor becomes a double arrow.
2. Once the cursor is a double arrow, click and drag the window in to
minimize or out to maximize.

Configuring Main Window for Dual Monitors
The following section explains how to detach a pane or create a new
frame for dual monitors.
Creating a New Frame

1. Right-click on a tab and select New Frame from the drop-down
menu. An empty frame is displayed.
2. Once an empty frame has been created, views can be dragged
into the empty frame. Click on the tab of the pane to move and
then drag that pane into the empty frame.
Detaching a Frame
1. Right-click on the tab of the pane to detach and select Detach.
2. Click on the detached pane and drag it over to the second
monitor.
Using Screen Layouts Dialog Box

Use the Screen Layouts dialog box to save, delete, and select screen
layouts or restore the software to the default configuration.
Saving Screen Layouts

Saving a screen layout retains dashboard parameters so they can be
used for multiple samples.
1. Configure screen as desired. Refer to Moving a Pane, page 422.

2. From the View menu, select Screen Layouts.
3. Click Save. A new screen layout named layout will appear.

4. Type in a descriptive label for the screen.
5. Click Close to close the dialog box. The new name of the new
screen layout will appear in the Screen Layouts dialog box.

Selecting a Layout to Appear in the Main Window
1. From the View menu, select Screen Layouts.
2. Click on the desired screen name and then click Select.
Deleting a Layout
1. From the Screen Layout dialog box, select the layout, and then
click Delete. A confirmation dialog box is displayed.
2. Click Yes to confirm the screen layout deletion.
3. Click Close to close the dialog box.
Modifying Position of Screen Name

Select the desired screen name, and then click Move Up to move a
screen to a higher position in the Screen Layout dialog box or click
Move Down to move the screen to a lower position. This ability is
useful to keep the names of frequently used screen configurations
visible when there are several names that appear in the dialog box.
Displaying Original Screen

The original screen at the time the instrument was shipped has been
saved as the default. From the View menu, select Screen Layouts and
click Default to display the original configuration.

Determining User Permissions
Users on the Configuration menu helps prevent unauthorized operation

by permitting the system administrator to assign permission for users
to perform selected functions in the instrument software. The following
section explains how to add users to the Windows OS (Operating
System) on the local pc and how to add users to the instrument
through a network/domain login.
Adding User in Windows OS

To add a user, refer to the Windows OS help system as follows:
1. From the desktop, click Start and then click on Help. Help may be
referred to as Help and Support depending on the Windows OS
that is used.
2. In the search box, type Users and Passwords.
3. Make a selection from the Users and Passwords options list, click
Display and follow the instructions provided.
Adding Users to Instrument Software

The following section explains how to add users to the instrument
software. This procedure applies when a user is not assigned in the
Windows OS on the local pc but will be logging onto the instrument
through a network/domain login.
1. On the Configuration menu, click Users. The Users dialog box will
appear.
2. On the Users dialog box, click Add. The word User will appear
under Name.
3. Click on User and type in the network/domain login for the user.
If the user identification entered here does not match the
required network/domain login for the user to log on to the pc
from a network, the user will not have the permissions designated
in the software.
4. Refer to Adding or Changing User Permission, page 428, for
Instrument for instructions to assign permissions to individual
users.
Changing Users in Windows OS

The following section explains how to change users. This procedure
applies both to users assigned in Windows and to users added to the
instrument on a network/domain login.
1. Close the software.

2. On the desktop, click Start and then click Log Off. This step will
vary depending on the Windows OS that is used.

3. Enter the username and password to log on the new user. This
step will vary depending on the Windows OS that is used.
4. Log in to the instrument.
Deleting Users in the Instrument Software

Only users added to the instrument on a network/domain login can be
deleted. Users assigned in the Windows OS cannot be deleted from the
Users dialog box.
1. Click Configuration and select Users. The Users screen will

appear.
2. Click on the name to be deleted and then click Delete. A message

3. Click Yes to delete the username; click No to keep the username.

Adding or Changing User Permission for Instrument
Users names will appear in the Name column of the Users dialog box.
The current user logged into the Windows system will display in blue.
1. Click Configuration and select Users. The Users screen will

appear.
A. To disable all user permissions for a specific user, place a X
in the Guest column. When the user logs on to the system
they will be considered a Guest and will have READ-ONLY
access to the software. For Guest users, the check boxes
listed on the User Properties dialog will be cleared as they
cannot perform any of the tasks listed.
B. Select the Enable User Permissions check box and user
permissions will be checked during the operation of the
instrument. When the Enable User Permissions checkbox is
cleared, user permissions are not checked and all users can
perform any function on the instrument.
2. To assign user permissions, click on the name of a user.
3. If one user requires the exact same permissions as a user that

already has permissions assigned, the Same As column can be
used to save time.
A. Select the name of the user to add or change permission by
clicking in the Row column for that user.
B. Single-click in the Same As column.
C. From the list, select the name of the user that already has
the same permissions assigned.
4. Click Properties. The User Properties dialog box will appear.

5. Select the desired check boxes to assign or remove user
permission for the functions listed in the edit box. When an X
displays, the user has permission to perform that function.
6. Click OK when finished assigning permissions.

Configuring System
System Configuration permits the operator to set the overall

instrument operating settings and parameter values for an application.
The following section explains the System tab and the Wake Up tab.
For the Balance Tab, refer to Setting Up Communication with Balance,
page 35.
1. From the Configuration menu, click System. The System

Configuration dialog box will appear.
2. For Fuse Type, Cotton is recommended.

3. For Fuse Length, enter the length of the fuse consumed during
an analysis. The default value for thread fuse is 10.0 cm. This
value should match the length of thread fuse on the ignitor wire.
Refer to step 5.D, page 55.
4. For Fuse Combustion Heat, enter the amount of heat that is
caused by combustion of the fuse in units as determined by the
selection made in Result Units, below. The default value for
cotton is 6.6 J/cm and for wire is 9.6 J/cm.
5. For Significant Digits, enter the number of digits, other than
zero, displayed in the analysis result. The default value is 5.

6. For Result Units, click the arrow to select the unit value for each
result.
7. For Sleep Timeout, Enter the length of idle time that will lapse
before the system enters sleep mode. The default is 240 Minutes.
8. For Water Temperature, enter a value to set the water
temperature. The default is 25C. Refer to Adjusting the Water
Temperature Set point, step 40, page 212.
9. Enable Auto Increment Sample Name and the sample name is
automatically incremented every time a sample is entered into
the sample spreadsheet. A number will appear after the sample
name and automatically increase by 1 as samples are entered.
10. Select the Alarm check box and an alarm will sound three
seconds before ignition. Clear the check box and there will be no
alarm.
11. Click Print to print the system parameters.
Wake Up Tab
Use the Wake Up tab to automatically power on the instrument.
Select the Monday - Friday check box and/or the Saturday and/or
Sunday check box and enter a time for each check box selected. The
time can be entered using AM or PM (for example 1:00 PM) or it can
be entered using the 24-hour clock format (for example 13:00). If the
time is entered using the 24-hour clock format, the software converts
it to AM or PM, so, for example, 13:00 would convert to 1:00:00 PM.

Importing Sample Data
Text Import Data provides the means to import sample data into the
instrument software. For example, the sample weights could be
obtained from a balance that is not connected to the instrument.
Sample information including the mass weight is then entered into a
text editing or spreadsheet program, and Text Import Data can be
used to import these sample weights into the sample spreadsheet.
Format Sample Data

1. Open a text editor such as Windows Notepad or spreadsheet
program such as Windows Excel.
A text editor such as Notepad is recommended. Some spreadsheet
software will insert quotation marks at the beginning and end of the
data. If quotation marks are inserted behind numerical data such as
the mass value, the numerical data may not display in the
spreadsheet.
2. Enter sample data into the text editor using the guidelines below.
Place the information for each sample on a separate line.
The following list shows the fields that can be entered and the
order in which they should appear: Sample Name, Mass,
Description, Comment, Operator.
An example of the correct format for sample data is shown

below.
If a field is missing from the first line or placed out of order in

any line, the information will not display in the correct
spreadsheet column.
If a field is left blank, the software will fill in the information
for that field from the previous sample. For example if the
first sample has Smith listed for Operator and the second
sample has a blank Operator field, the software will fill in
Smith for the blank field.
The fields can be separated by a comma or a tab.
3. Save the file in a .txt or .csv format.
4. Refer to Importing Sample Data into Spreadsheet, page 433.

Importing Sample Data into Spreadsheet
1. Select Samples on the Menu bar and then select Text Import
Data.
2. Select the file to import and click Open.
3. Verify the Sample Name, Mass, Description, Comment, Operator

columns display in the spreadsheet. If these columns do not
appear, refer to Modifying Columns, page 415.
4. The data from the text file will be imported into the spreadsheet
as shown below.

Creating Sample Templates
Sample templates provide a quick way for the operator to enter
repetitive information.
1. Select the Configuration menu and then select Sample Templates.

The Sample Templates dialog box will display.
For further information about the buttons in the Sample
Templates dialog box, refer to Dialog Box Buttons, page 410.
2. Select Add. A new row will display with Sample- in the Name
column.
3. Double-click in the Name column of the newly added row and
enter a new name for the sample, if desired.
4. Select a method for the sample from the menu. If the desired
method has not been created, refer to Creating or Modifying
Methods, page 59.
5. Enter information in the Comments and Description column, if
desired.
6. Click OK. The sample template can now be selected from the
Name column in the spreadsheet as shown below.
7. After a sample template has been created, samples can be easily

logged in to this template. Refer to Logging In from Sample
Template, page 517.

Creating Transmission Formats
Transmission Formats allows sample data to be sent to another

computer that has been configured to receive the information.
The following section explains how to create and modify transmission

formats. To send sample data using a transmission format, refer to
Transmitting Results, page 538.
Creating and Modifying Transmission Formats

The following section explains how to create and modify transmission
formats.
1. Select Configuration and then select Transmission Formats. The

Transmission Formats dialog will appear. For further information
about the Transmission Formats dialog box buttons, refer to
Dialog Box Buttons, page 410.
2. Select Add to insert a blank row into the table. Transmit- will
appear in the new row, which will be positioned above the
currently selected row.
3. Double-click in the Name column of the newly added row and
enter a new name for the sample.
4. Refer to Properties Dialog Box, below, to configure the
transmission format.
Properties Dialog Box
Fields Tab
Select Fields to determine the Fields that will transmit. Fields are
defined in the Glossary, page 121.
To transmit a field, select the field from the Fields selection box and
then select Add. To remove a field from transmit, select the field from
the Transmit selection box and then select Remove.
To change the order in which the fields will transmit, select the field to
move. Select Promote to move the field to a higher position or select
Demote to move the field to a lower position.

For Average, select the arrow and then select Off to transmit the
individual results for each sample. Select On to calculate and then
transmit an average value for each field selected. Select Group by
Sample Name to calculate an average value for each field and then
transmit the fields grouped by sample name.
Delimiters Tab
Select Delimiters to configure the display of the transmitted data.
1. Select the XML Format checkbox, and the data will export in XML
format. When the XML checkbox is cleared, data will transmit in
normal text.
2. Select the Column Headers check box to have the transmitted
data organized with column headers.
3. Select one delimiter as a means to separate the data. Comma
separates the data by commas; Tab separates the data by a
blank space equivalent to one tab; Other separates the data by a
user-determined punctuation mark or symbol.
4. Select how the Start of Transmission will appear. None displays
nothing before transmitted data; Other allows you to enter the
text or symbol that will appear, or you can click the arrow and
then select an item from the list.

5. Select how the End of Transmission will appear. Carriage Return
displays the data followed by a carriage return. Carriage Return
Followed by a Line Feed (CR/LF) displays the data followed by a
carriage return and line feed. Other allows you to enter the text
or symbol to display, or you can click the arrow and then select
an item from the list.
Automation Tab
On the Automation tab, select the Automatically Transmit Each New
Analysis checkbox, and each new analysis will transmit.

Communication Settings Tab
Select the Communication Settings to select the Encoding and Device.
Refer to Glossary, page 121, for definitions.
1. Select either ASCII or Unicode. Both ASCII and Unicode provide
the means for storing text. ASCII can represent a small number
of characters and is therefore useful only for English or other
Western languages. Unicode can represent a large number of
characters and is therefore useful for non-Western languages.
2. Select Serial Port and then select Configure to enter the serial
port parameters. Or, Select Network and then select Configure to
enter the Host Name and Host Port. Contact your system
administrator for these settings.
Advanced Tab
Select the Advanced tab to enter and modify the fields that are
transmitted. The Advanced tab provides almost the same function as
the Fields and Preview tabs except that in the Advanced tab, transmit
information can be changed or added directly in the Transmission
Format box.

To add a field to the Transmission Format, select the desired field from
the Fields selection box and then select Add Field to Transmit Format.
The field appears in the Export Format selection box.
In the Transmission Format box, information such as nested xml

formulas or formulas with complicated formatting can be typed or cut
and pasted into the box; however, the XML check box on the
Delimiters tab must be cleared. When additional information is entered
directly, it is not necessary to use []. The software uses [] to identify a
field. When transmit information is added or changed in the
Transmission Format box, the appearance of the transmission format
can be viewed using the Preview tab.
Numeric Field Formatting allows you to quickly enter number

formatting for all of the fields selected for transmit. Number Width
specifies the number of characters that will appear in the number
format and Precision specifies the number of places that display after
the decimal point. To change these values, enter a new value in the
box for Precision and/or for Width and then select Set to display the
format in the Transmission Format area. For example if 8 is entered
for Number Width and 3 is entered for Number Precision, 8.3 will
display for each field with numeric value results in the Transmission

Format area as shown below. Select Remove to remove number
formatting from the Transmission Format area.
Preview Tab
Select the Preview tab to display the appearance of the data before it
is transmitted. Any changes can then be made before the data is
actually transmitted. The following example displays the data with the
following parameters selected on the Delimiters tab: Column Headers
checkbox checked, comma checked for Delimiter, and the Carriage
Return checkbox checked for End of Transmission. Refer to Delimiters
Tab, page 436, to change any delimiters.
The way the date and time display can be changed using the Date
and Time Properties dialog box on the Microsoft Windows Control
Panel.

Creating Export Format
The following section explains how to create an export format to

export sample data to another system such as LIMS, to backup data to
a network, to export sample data to another program such as
Windows Excel, or to export sample data to another computer for
processing. For instructions to export data after creating an export
format, refer to Exporting Data, page 536.
Creating and Modifying Export Formats

1. Select Configuration and then select Text Export Data. The Export
Formats dialog box will display. For further information about the
Export Formats dialog box buttons, refer to Dialog Box Buttons,
page 410.
2. Select Add. Export- will display in the new row that has been
added to the Export Formats spreadsheet.
3. Double-click in the new row to change the name of the export, if
desired.
4. Select Properties and determine the properties of the text export
format. Refer to Properties Dialog Box, page 441.
Properties Dialog Box
Filename Tab
Use the Filename tab to configure the file for the export.
1. Enter the name for the file or select Browse and then select the
file from the list.
2. Select one of the following:
Select Append to File to attach the sample analysis data
highlighted in the spreadsheet to the previously saved file.

Select Automatically Increment Filename to automatically
increment the last characters in the filename by one if these
characters contain numbers when the file is saved.
Select Prompt for Filename to display the Export Format dialog box
and prompt the operator to enter a filename.
Fields Tab
Select Fields to determine the Fields that will transmit.
To export a field, select the field from the Fields selection box and then
select Add. To remove a field from export, select the field from the
Export selection box and then select Remove.
To change the order in which the fields will export, select the field to
move in the Export list box and then select Promote to move the field
to a higher position or select Demote to move the field to a lower
position.
For Average, select the arrow and then select Off to export the
individual results for each sample. Select On to calculate and then
export an average value for each field selected. Select Group by
Sample Name to calculate an average value for each field and then
export the fields grouped by sample name.
Delimiters Tab
Select Delimiters to configure the display of the exported data.
1. Select the XML Format checkbox, and the data will export in XML
format. When the XML checkbox is cleared, data will transmit in
normal text.
2. Select the Column Headers check box to have the exported data
organized with column headers.
3. Select one delimiter as a means to separate the data. Comma
separates the data by commas; Tab separates the data by a
blank space equivalent to one tab; Other separates the data by a
user-determined punctuation mark or symbol.
4. Select how the Start of Transmission will appear. None displays
nothing before exported data; Other allows you to enter the text
or symbol that will appear, or you can click the arrow and then
select an item from the list.

5. Select how the End of Line Delimiter will appear. Carriage Return
displays the data followed by a carriage return. Carriage Return
Followed by a Line Feed (CR/LF) displays the data followed by a
carriage return and line feed. Other allows you to enter the text
or symbol to display, or you can click the arrow and then select
an item from the list.
Automation Tab
On the Automation tab, select the Automatically Transmit Each New
Analysis checkbox, and each new analysis will transmit.
Advanced Tab
Select the Advanced tab to enter and modify the fields that are
exported. The Advanced tab provides almost the same function as the
Fields and Preview tabs except that in the Advanced tab, export
information can be changed directly in the Export Format box. When
export information is changed using the Advanced tab, the Fields tab
and Preview tab automatically update.

To add a field to the Export Format, select the desired field from the
Fields selection box and then select Add Field to Transmit Format. The
field appears in the Export Format selection box.
In the Export Format box, information such as nested xml formulas or
formulas with complicated formatting can be typed or cut and pasted
into the box; however, the XML check box on the Delimiters tab must
be cleared. When additional information is entered directly, it is not
necessary to use []. The software uses [] to identify a field. When
export information is added or changed in the Export Format box, the
appearance of the export format can be viewed using the Preview tab.
Numeric Field Formatting allows you to quickly enter number
formatting for all of the fields selected for export. Number Width
specifies the number of characters that will appear in the number
format and Precision specifies the number of places that display after
the decimal point. To change these values, just enter a new value in
the box for Precision and/or for Width and then select Set to display
the format in the Export Format area. For example if 8 is entered for
Number Width and 3 is entered for Number Precision, 8.3 will display
for each field with numeric value results in the Export Format area as
shown below. Select Remove to remove number formatting from the
Export Format area.
Preview Tab
Select the Preview tab to display the appearance of the data before it
is exported. Any changes can then be made before the data is actually
exported. The following example displays the data with the following
parameters selected on the Delimiters tab: Column Headers checkbox
checked, comma checked for Delimiter, and the Carriage Return
checkbox checked for End of Transmission. Refer to Delimiters Tab,
page 442.
The way the date and time display can be changed using the Date
and Time Properties dialog box on the Microsoft Windows Control
Panel.

Creating and Modifying User Defined Fields
User Defined Fields provides the means to create customized fields,

such as column headings, to be added to the spreadsheet. User
defined fields can display results from functions or they can display
notes or comments.
1. From the Configuration menu, select User Defined Fields. For

further information about predefined user defined fields that
display in the user defined fields dialog box, refer to Critical
Calculations, page 73.
2. Create or modify a user field as follows: To create a user field,

select Add. A new row will be inserted into the table; Or, to
modify a user field, select the desired user field in the table.
To delete a user field from the table, select the row of the desired
user field and then select delete.
3. For a new user field, type a name in the Name column.
4. Complete the table for the new or modified user field as follows:
Select the Read Only check box to prevent the user field from
being edited in the spreadsheet.
Select the Numeric check box and only numeric values can
appear in the spreadsheet.
For Format, enter a format to determine how the result of the
user defined field displays in the spreadsheet. Refer to Number
Formatting, page 446.
For Formula, enter a formula to use if the field will be used for a
calculation. Refer to Formulas, page 447.
Select the Login check box and the field will appear in the
Sample dialog box. Refer to Logging In a Sample, page 514.
Select the Stats check box and statistics will appear when
printing the plot. When selected, both Read Only and Numeric
are automatically selected.

Select the Standard check box and the user defined field can be
used with standards, which means the standard can define its
value and range and can be calibrated.
5. After creating a new user defined field, a column labeled with the
name of the new user field will display in the spreadsheet.
6. To apply a user defined field to a previously analyzed sample,
select the sample in the spreadsheet and then select Recalculate
from the Samples menu.
Number Formatting
Use the Format column in the User Defined Fields dialog box to enter a
number format. This format determines how the result of the user
defined field appears in the spreadsheet. The following section
provides examples of formats and how the result will display
depending on which format is utilized.
Format Examples
*Format Value Format for Result Result
Type
A 4.50360 A 4.50360000
Fn.m 0.123456 F4.5 0.1235
0.000789 F3.5 0.00079
0.000789 F3.2 0.00
321.8765 F3.5 322
Sn 0.123456 S4 1.235x10-1
0.000789 S3 7.89x10-4
0.000789 S2 7.9x10-4
In 321.8765 I3 322
321.8765 I2 320
*A = Default format
n = Total number of significant digits to be represented
m = Maximum number of digits after the decimal
I = Integer notation
S = Scientific notation: An exponential format (y.yyy x 10e) in which any number is
expressed as a number between 1 and 10 multiplied by a power of 10 that indicates the
correct position of the decimal in the original number.
F = Fixed point notation: Traditional decimal notation

Formulas
Formulas can be entered into the Formula column of the User Fields
dialog box and are used to calculate the result. The following section
provides some example formulas and the result based on their
calculation. Spacing and other details of the formula must be exact. If
an error message such as "badOpt" or "badOpn" appears in the
spreadsheet, verify the syntax of the formula matches the syntax of an
example formula in the table below.
The values listed in the table below will be used in the function
examples.
Formula Type1 Result
@ABS(exp)
Example: @ABS([Qvad (J/g)]) Absolute value
@ABS([Qvad (BTU/lb)])
@Log10(exp)
Example:
Log base 10
@LOG10([Qvad (J/g)])
@LOG10([Qvad (BTU/lb)])
@ln(exp)
Example:
Natural log
@LN([Qvad (J/g)])
@LN([Qvad (BTU/lb)])
@SQRT(exp)
Example:
Square root
@SQRT([Qvad (J/g)])
@SQRT([Qvad (BTU/lb)])
@Maximum(exp1, exp2)
Finds Maximum
Example: @MAXIMUM([e1], [e2], [e3], [e4])

@Minimum(exp1, exp2)
Example: Finds Minimum
@MINIMUM([e1], [e2], [e3], [e4])
@IF(cond, true, false) If the cond is true, the value will

appear for that field. For
Example: example, if the formula indicates
@IF([Jacket Temperature]<24.95,[Jacket that the jacket temperature is
Temperature], 25.0) less than 24.95 and this is true,
the value of the jacket
temperature will display in the
field; otherwise if the jacket
temperature is greater than
24.95, then 25 will display for
the value of the field.
@AND(cond1, cond2) If cond1 is true and cond2 is

true, the statement is true and a
Example: 1 will appear as the value for
@IF(@AND[Jacket Temperature]<24.95,[Initial that field; otherwise, the
Temperature<24.95], [Jacket Temperature], 25.0) statement is false and zero will
appear for the value of the field.
@OR(cond1, cond2) If cond1 or cond2 is true, then

the formula is true and a 1 will
Example: appear for the value of the field;
@IF(@OR[Jacket Temperature]<24.95,[Initial otherwise, the formula is false
Temperature<24.95], [Jacket Temperature], 25.0) and zero will appear for the
value of the field.
@XOR(cond1, cond2) If cond1 or cond2 is true but not

both, then the formula is true
Example: and a 1 will appear for the value
@IF(@XOR[Jacket Temperature]<24.95,[Jacket of the field; otherwise, the
Temperature>25.05], [Jacket Temperature], 25.0) formula is false and zero will
appear for the value of the field.
The term exp stands for expression. Use exp in a formula to specify
a value or perform a calculation on values. It may represent a single
number or a formula that returns a number.
The term cond stands for condition. Use cond for comparisons based
on single or multiple conditions. It is used with a comparison such as
<, >, =, or with the @AND, @OR, and @XOR formulas.
Refer to Comparison Functions, page 449, for further information.

Comparison Functions
The following table explains the comparisons that can be used in a
formula.
Function Definition
+ Plus
- Minus
* Multiply
/ Divide
^ Raise to the power
= Equal
> Greater than
>= Greater than or equal to
< Less than
<= Less than or equal to

Managing Databases
Over time the instrument database can accumulate a great deal of

information. It is good practice to establish a regular database backup
procedure. Refer to Creating and Retrieving Database Backups, page
452.
LECO software applications use a database to store and maintain all

the information necessary to run the instrument, including methods,
standards, system parameters, and sample results. A file system
database is created automatically the first time the software is started.
In addition, a database connection that contains the name and location
of the database is created. The database connection is used to specify
which database to open.
LECO software provides the means to create and maintain the

instrument database and database connections. A database
management wizard allows you to add database connections, to select
a database connection for use, and to delete database connections.
When you add a connection, it can be to a new database or to an
existing database. The new connection name is added to the list of
available database connections.
For 21 CFR Part 11 compliance, logging can be enabled when a

database connection is created. When logging is enabled, Presentation
Time, View History, and Archive Log appear on the Database menu in
the instrument software.
This section explains the following topics:
Using the Start Dialog Box, page 451

Creating and Retrieving Database Backups, page 452
Selecting a Database Connection, page 453
Adding a Database Connection, page 454
Deleting a Database Connection, page 457
Validating a Database, page 457
Compacting/Repairing a Legacy Database, page 460
Managing Databases for 21 CFR Part 11 Compliance, page 460
Enabling Logging for an Existing Database, page 461
Enabling Logging for a New Database, page 462
Presentation Time, page 464
View History, page 465
Archive Log, page 466
Adding a Connection to an Archive Log Database, page 469
Removing Results from Database, page 469
Disabling Logging on an Existing Database, page 470

Using the Start Dialog Box
The following section explains how to use the Start dialog box in order
to add a new database connection, select and, optionally, validate an
existing connection, or delete a database connection. A compact/repair
selection is available for legacy databases.
1. Exit the instrument software.

2. Click Start on the Windows desktop, select Programs, select
LECO, select the instrument, and then click Database
Management. The Start dialog box will appear.
When database connections are created, they will appear under

Connections. The file path for the selected database connection
appears at the bottom of the Start dialog box. Database connections
that are no longer valid appear with dimmed text in the Connections
list. When the user selects a dimmed connection, the software allows
the user to delete the database connection or to reconnect to the
database.
Click Add to add a database connection. Refer to Adding a Database

Connection, page 454.
Or
Click on an existing database connection and then make one of the

following selections:
Click Select to connect to a database that already exists. Refer to

Selecting a Database Connection, page 453.

Click Validate to validate the database with which the connection
corresponds; however, Select must also be selected to perform
validation. Refer to Validating a Database, page 457.
Click Delete to remove a database connection. Refer to Deleting a
Database Connection, page 457.
Compact/Repair is not necessary for file system databases (and
does not appear on the Start dialog box); however, it is available
for Legacy Databases. Click Compact/Repair to compact an existing
Legacy Database to conserve disk space and to repair a possibly
corrupted Legacy Database. Refer to Compacting/Repairing Legacy
Database, page 460.
Creating and Retrieving Database Backups

It is good practice to routinely back up data to prevent data loss in the
event something such as a hard drive failure should occur. The
procedure below explains how to backup a database and should be
performed on a regular basis. This procedure applies for all databases
whether or not logging is enabled.
Create Backup
1. In the Start dialog box, highlight the database connection of the
database to back up. The file location of the corresponding
database will appear as shown below.
2. Close the instrument software.

3. To locate the files for the database connection, right-click on Start
on the desktop and use the Windows Start Menu to navigate to
the folder location.
4. Select the folder and click Copy.
5. Paste the files to the desired storage media (e.g., CD, USB
external drive, etc.) or network drive location.

Retrieve Backup
Data can be retrieved using either method described below. The
instrument software must be closed to perform either procedure.
If there is a problem with the original database and the backup is to

replace it, copy the backup database folder from where it was stored
and use Windows Explorer to paste the folder into the original folder
location for the database. Be aware that data generated in the original
database between the time the backup was made and the time the
backed up data is restored will be lost.
OR
To access the backup as a separate database, copy the backup

database to the desired location. If prompted, do not overwrite an
existing database in this case. Use the Database Management wizard
to add a database connection to this database. Refer to Adding a
Connection to an Existing Database, page 454.
If restoring from read-only media, after copying the database to its

new location, use Windows Explorer to change the attributes for all
folders and files so that they are not read only. To do this, right-click
on the folder name, select Properties, and then clear the Read Only
check box.
Selecting a Database Connection

3. Under Connections, click on the desired database connection.

4. Click Select.

5. Click Finish to open the selected database.
Adding a Database Connection

The following section explains how to connect to an existing database
or a new database.
Refer to Adding a Connection to an Existing Database, page 454.
Refer to Adding a Connection to a New Database, page 455.
Adding a Connection to an Existing Database

Connecting to an existing database allows you to use an existing file
system database, which could be very important in a situation that
required a software reinstall such as a system crash. This type of
connection provides the means to reconnect to an existing database.

Management.
3. In the Start Dialog Box,
A. Select Add.
B. Click Next.
C. Select File System Database - Use Existing.
D. Click Next.
4. When the Connect File System Database dialog box appears,
enter the information for the desired database as follows:
A. For Connection Name, enter a name for database connection

that will also appear in the Start dialog box in the
Connections list.
B. For Directory Name,
1) Select Browse.
2) Navigate to the folder for the database and click on it as
shown in the screen shot below. Do not click on the Data
folder itself. The names assigned to the databases in the
directory on your system may not match the folder
names in the screen shot.

3) Click OK.
5. If desired, select the Read Only check box. When selected, the
database information can be viewed but not changed. When the
check box is cleared, the database can be modified.
6. Clear the Log Activity check box.
7. Click Next.
8. Click Finish.
9. The Select Vessel Type dialog box will appear. Select the vessel
that will be used and click OK.
Adding a Connection to a New Database

New databases will be file system databases. This database type uses
files and folders as its storage media. The size of the database is only
limited to the free space on the hard drive.
To prevent the database from running slow, it is recommended that

virus checking of the database directory be disabled. It is also
recommended to use NTFS as the hard drive file format.

Management.
A. Select Add.
B. Click Next.
C. Select File System Database - Create New.
D. Click Next.
4. Complete the Create File System Database dialog box as follows:

Connections list.
B. To use the default location and name for the database
folder, proceed to step C. To use another location,
1) Create a folder in the desired location using Windows
Explorer.
2) Select the Advanced check box, and the Directory Name
selection box will appear.
3) For Directory Name, click Browse.
shown in the screen shot below. There will not be a data
folder since it is a new database. The names assigned to
the databases in the directory on your system may not
match the folder names in the screen shot.
5) Click OK.

C. Clear the Log Activity check box.
5. Click Next and the Start dialog box will appear.
6. The Select check box is automatically selected. Click Finish to
access the newly created database.
Deleting a Database Connection

Delete does not remove physical files from the hard drive. Use
Windows Explorer to remove the physical files.
Management.
3. Under Connections, click on database connection to remove.
4. Click Delete.
5. Click Next. The Delete dialog box will appear.
6. Click Next to remove the database connection.
Validating a Database
During database validation, the database files will be reviewed for
corruption. If orphan objects are found, refer to Reviewing Orphan
Objects, page 459.

To validate a database,

3. Under Connections, click on a database to validate, click Select,

and then click the Validate check box.
4. Click Finish. The Database Validation dialog box will display the
status of the database validation.

Reviewing Orphan Objects
When orphaned objects or corrupt database objects are discovered, a
dialog box such as the one shown below will display. It is
recommended to select No and review orphaned objects (such as
samples, methods, and standards) as they display in the Orphaned
Database Object dialog box to ensure they are valid.
If the database is being validated because database objects are

missing, for example samples have disappeared from the spreadsheet,
then recover the orphans by selecting No or No All. Select No to be
prompted for each orphan or select No All to recover all orphans
without being prompted for each one.
If all samples are displayed in the spreadsheet and there are no

apparent problems with the database, then the orphans are likely
objects that weren't completely removed from the database when they
were deleted and these orphans can be deleted. Select Yes to be
prompted before deleting each orphan or select Yes All to delete all
orphans without being prompted for each one.

Compacting/Repairing a Legacy Database
Compact/Repair is available on databases that are not file system
databases. For file system databases, the compact/repair selection
will not appear on the Start dialog box.
Management.
3. Under Connections, click on the database to compact/repair.
4. Click Compact/Repair.
5. Click Next and the following message will display.
6. Click Next to compact/repair the database.
Managing Databases for 21 CFR Part 11 Compliance
The following section provides further information about how to create

and view log archive databases for 21 CFR Part 11 compliance. For
general database topics such as Using the Start Dialog Box or Deleting
a Database Connection, refer to Managing Databases, page 450.
In the software, logging can be enabled to keep a record of all changes

as they are made to the database. Logging provides a history of the
changes made as well as the current database values.
By default, logging is not enabled. Logging can be enabled or disabled

when a database connection is added. Refer to Enabling Logging for an
Existing Database Connection, below and Enabling Logging for a New
Database, page 462.

Enabling Logging for an Existing Database
Connecting to an existing database allows you to use an existing file
system database, which could be very important in a situation that
required a software reinstall such as a system crash. This type of
connection provides the means to reconnect to an existing database.

Management.
A. Select Add.
B. Click Next.
C. Select File System Database - Use Existing.
D. Click Next.
4. When the Connect File System Database dialog box appears,
enter the information for the desired database as follows:

Connections list.
B. For Directory Name,
1) Select Browse.
shown in the screen shot below. Do not click on the Data
folder itself. The names assigned to the databases in the
directory on your system may not match the folder
names in the screen shot.
3) Click OK.

5. If desired, select the Read Only check box. When selected, the
database information can be viewed but not changed. When the
check box is cleared, the database can be modified.
6. Select the Log Activity check box to turn on logging for any future
changes made to the database through the instrument software.
7. Click Next.
8. Click Finish.
Enabling Logging for a New Database

New databases will be file system databases. This database type uses
files and folders as its storage media. The size of the database is only
limited to the free space on the hard drive.
To prevent the database from running slow, it is recommended that

virus checking of the database directory be disabled. It is also
recommended to use NTFS as the hard drive file format.
Management.
A. Select Add.
B. Click Next.
C. Select File System Database - Create New.
D. Click Next.

4. Complete the Create File System Database dialog box as follows:

Connections list.
B. To use the default location and name for the database
folder, proceed to step C. To use another location,
1) Create a folder in the desired location using Windows
Explorer.
2) Select the Advanced check box, and the Directory Name
selection box will appear.
3) For Directory Name, click Browse.
shown in the screen shot below. There will not be a data
folder since it is a new database. The names assigned to
the databases in the directory on your system may not
match the folder names in the screen shot.
5) Click OK.

C. Select the Log Activity check box to turn on logging for
changes made to the database through the instrument
software.
6. The Select check box is automatically selected. Click Finish to
access the newly created database.
Database Menu
Items on the Database menu in the instrument software will only
appear if logging was enabled when the database connection was
created. Refer to Enabling Logging for an Existing Database, page 4
61.
Presentation Time
When logging is enabled for a database connection, the presentation
time can used to view the database as it existed at some previous
point in time. For example, it could be used to view results before a
change in calibration was performed. While a presentation time is set,
and the Live check box is not selected, changes are not allowed to the
database. For example, samples cannot be added and changes cannot
be made to methods.
1. Click the Database menu in the instrument software and select

Presentation Time. The Presentation Time dialog box will appear.
2. Select the time and date for the presentation time as follows:
Select the Live check box to view current information or clear the
Live checkbox in order to select a different date and time.

When the Live check box is cleared, Date and Time are active.
A. For Date, click the arrow to display a calendar.

B. From the calendar, select a date. If desired, select the time
and then select either Local or UT (Universal Time). Local
displays the local time zone. UT displays the universal time
that corresponds with the UTC (Universal Coordinated Time)
as defined by the National Bureau of Standards.
C. Click OK. The results as they were at the selected date and
time will appear in the spreadsheet.
View History
When logging is enabled for a database connection, View History
displays a log of database changes that could be used to identify the
time/date when some particular change took place. It can only be used
to identify who made a change because there is no description of what
each change represents.
1. Click the Database menu in the instrument software and select

View History. The View Log dialog box will appear.
2. The log items that appear in the View Log dialog box are
explained below.
Date/Time displays the date and time that the database change
occurred.
Entry ID displays a unique identifying number for the database
object that was changed. For example, each sample would have a
unique number.

Action displays Created, Modified or Deleted to indicate the type
of action that occurred.
User displays the username of the person who performed the
action.
3. Select the time zone to use for displaying Date/Time. Local
displays the local time zone. UT displays the universal time that
corresponds with the UTC (Universal Coordinated Time) as
defined by the National Bureau of Standards.
Archive Log
When logging is enabled for a database connection, an Archive Log
database can be created to copy log entries to another file and
possibly reduce the amount of data stored in the database.
1. From the Database Menu in the instrument software, select

Archive Log. The Archive File dialog box will appear.
2. In the Archive File dialog box,

A. Select the Delete Entries upon Completion check box to
delete entries from the database after they are copied to the
output file. Clear the check box and entries will not be
deleted from the database. Selecting this check box reduces
the amount of data stored in database files. The file size may
not change as a result of this, but space will be made
available inside the file for more data to be stored. As a
precaution, LECO recommends performing a regular
database backup right before using Delete Entries upon
Completion. Refer to Creating and Retrieving Database
Backups, page 452.
B. For the Stop Date, click the arrow and select a date. Any log
entries generated on or before this date will be placed into
the output file.
C. Enter a filename for the log archive database.

D. Select the location for the log archive database.
E. Click Save.
3. After a log archive database is created, you can create a database
connection to the archive log file and view the information in a
read-only fashion, which means you can view the log archive
database but cannot operate the instrument or analyze samples.
Refer to Adding a Connection to a Log Archive Database, below.

Delete by Date
Used to delete all analyzed samples prior to a certain date.
1. From the Database Menu in the instrument software, select
Delete by Date. The Delete Old Samples dialog box will appear.
2. In the Delete Old Samples dialog box,

A. Enter a date or click the arrow to access the calendar.
B. Select a date that you want all samples prior to that date
deleted.
C. Click Delete to delete samples.
3. Click the box next to Transfer Export Samples to be deleted if you
wish to export and save the selected samples and just remove
them from the database.

Adding a Connection to a Log Archive Database
A. Select Add.
B. Click Next.
C. Select Database Log Archive.
D. Click Next.
4. Complete the Connect Log Archive dialog box as follows:
A. For Connection Name, enter a name for database log archive
connection that will also appear in the Start dialog box in the
Connections list.
B. For File Name, Click Browse and navigate to the log archive
file. The log archive file should have a .GLA file extension.
5. Click Next. The Start dialog box will appear.
6. Click Select and then click Finish.
Removing Results from a Database

When logging is enabled for a database connection, the amount of
data stored in the database can become significantly large, and it may
become necessary to remove results from the database. Deleting
results in the instrument software will only increase the size of the
database because the database keeps track of all changes when
logging is enabled. The following procedure explains how to remove
results from the database for file system databases or for other
databases.
For File System Databases

To remove results from a file system database, it is only necessary to
create an archive log as explained below.
1. Create an archive log by following the steps in Archive Log, page

466.
For Legacy Databases
For databases that are not file system databases, use the following
steps to compact/repair the database and recover the freed up space.
1. Create an archive log that has the Delete Entries Upon
Completion check box selected by following the steps in Archive
Log, page 466.

4. Select the database connection for the database, not the archive
log, click Compact/Repair, and then click Next. The following
message will display.
5. Click Next to compact/repair the database.
Disabling Logging on an Existing Database

Use the following instructions to disable logging on a database in which
logging is enabled.

Management.
3. In the Database Start dialog box, select the existing database
connection in which you prefer to disable logging. Remember the
name of the database and the base file location because you will
need this information in order to reconnect to the database in
step 8.A, page 470.
4. Select Delete, and follow the instructions provided by the
software. Refer to Deleting a Database Connection, page 457,
for further information. The Delete operation will not delete the
actual database; it will only remove the database connection
name from the list.
5. Return to the Database Start dialog box.
6. In the Start dialog box, select Add, and then select Next.
7. Under Database Types, highlight File System Database-Use
Existing, and click Next.
8. Complete the Connect Database dialog box as follows:
A. For the Connection Name, enter the same name as the
database that was just deleted.
B. Enter the Path to the database files.
9. Verify that the checkbox next to Log Activity is blank and click
Next.
11. The Select check box is automatically selected.
12. Click Finish.

5 Operation
During installation and operation of this instrument, the

ON/OFF switch must be easily accessible.
Illustrations .................................................................................. 53
Preparing for Analysis .................................................................... 54
Creating or Modifying Methods ........................................................ 59
Exporting Methods ................................................................. 512
Importing a Method ................................................................ 513
Logging in a Sample .................................................................... 514
Entering and Modifying Data in Spreadsheet .............................. 514
Repeating Data in Multiple Cells .......................................... 514
Inserting a Sample Out-of-Sequence ................................... 515
Using Sample Login Dialog Box ................................................ 516
Logging In Mass Value from Balance .................................... 517
Logging In from Sample Template ....................................... 517
Analyzing a Sample ..................................................................... 518
Deleting a Sample .................................................................. 519
Using Sample Filters .................................................................... 520
Filters Dialog Box Buttons ....................................................... 520
Adding Filters ................................................................... 520
Filter Properties ................................................................ 521
Deleting Filters ................................................................. 522
Predefined Filters ................................................................... 522
Modifying Predefined Filter ................................................. 523
Calibration ................................................................................. 524
Recalculating Results ................................................................... 526
Viewing History of a Sample ......................................................... 527
Applying Sample Signatures ......................................................... 528
Signing ................................................................................. 528
Viewing Signatures ................................................................. 529
Operation AC600 51
Printing Reports .......................................................................... 530
Configuring Report before Printing ............................................ 530
Printing from the Software ...................................................... 532
Transfer Import and Transfer Export .............................................. 534
Transfer Export ...................................................................... 534
Transfer Import ..................................................................... 535
Importing and Exporting Data ....................................................... 536
Exporting Data ....................................................................... 536
Importing Data ...................................................................... 536
Exporting Buffers ........................................................................ 537
Transmitting Results .................................................................... 538
52 AC600 Operation
Illustrations
Figure 5-1 Oxygen Combustion Vessel Assembled ..............................55

Figure 5-2 Vessel Prep Station - Fill Side ...........................................56
Figure 5-3 Oxygen Fill Button ..........................................................57
Figure 5-4 Vessel Installed ..............................................................58
Figure 5-5 Bucket Lid Mating Socket .................................................58
Figure 5-6 Vessel Prep Station - Vent Side ........................................519
Operation AC600 53
Preparing for Analysis
The following procedures must be completed in order to perform a

sample analysis.
1. Complete required maintenance procedures. Refer to Periodic

Maintenance Schedule, page 63.
2. Clean crucible as explained in steps 2 A - 2 C. If the crucible is
new, it should be heated to 500C for 5 hours in a muffle furnace
to remove surface oil and to oxidize the surface of the crucible.
A. Scrub the inside of the crucible with a wire brush.
B. Heat the crucible with a Bunsen burner, or equivalent, to
burn off residual matter.
C. Scrub the inside of the crucible with a wire brush again.
3. Place the crucible in the center of the weigh pan inside of the
balance and press the Tare button.
For samples which are not easily combusting, LECO recommends

the use of paraffin oil as a spiking agent.
Do not touch the sample with your fingers or hands as this

will contaminate the sample.
Oxygen Combustion Vessel Explosion Potential
The operator must observe safe operating practices when

using high pressure oxygen combustion vessels. Operating
personnel should be trained to practice safe operation and
maintenance of oxygen combustion vessels.
4. Refer to Oxygen Combustion Vessel Safety Guidelines, page

144.
Always use matched sets of oxygen combustion vessel cylinders,

oxygen combustion vessel caps, and screw caps.
5. Prepare the oxygen combustion vessel for analysis as follows:

A. Use a clean, lint-free cloth to remove any moisture from the
oxygen combustion vessel cap. This helps prevent misfires
by providing a dry environment for attaching the fuse.
B. If necessary, wake up the instrument and allow to
equilibrate.
C. Position oxygen combustion vessel on sample prep station.
54 AC600 Operation
D. Prepare oxygen combustion vessel for thread fuse or wire
fuse as explained below. A thread fuse is recommended.
Refer to 619.
Thread Fuse (Recommended) Wire Fuse
1. Inspect ignitor wire. Replace if broken or deteriorated. Refer to
Refer to Replacing Ignitor Wire for Thread Fuse, page Replacing
619. Wire Fuse,
2. Tie the 10 cm thread fuse to the wire ignitor so the page 620.
fuse hangs into the crucible.
Keep the ignitor wire from contacting the crucible.
6. Add the sample to the crucible.

7. Attach crucible to crucible holder. If the sample is powder, the
thread fuse should be placed on top of the sample. If the sample
is a pellet, the pellet is placed on top of the thread fuse.
To prevent misfires, avoid letting the crucible holder

contact the side of the oxygen combustion vessel.
8. To assemble oxygen combustion vessel, place vessel lid including

crucible and sample onto oxygen combustion vessel but avoid
pressing the vessel lid down.
9. Secure the vessel lid using the closure ring. Refer to Figure 5-1.
Also refer to the oxygen combustion vessel illustration,
Figure 10-8.
Figure 5-1
Oxygen Combustion Vessel Assembled
10. Remove the oxygen combustion vessel from the vessel holder.
11. Install the oxygen combustion vessel on the fill side of the vessel
prep station as follows:
A. Slide the flange fitting on the vessel lid into position and
continue holding the oxygen combustion vessel with one
hand.
Operation AC600 55
B. Lower the lever. Refer to Figure 5-2.
Figure 5-2
Vessel Prep Station - Fill Side
12. Pressurize the oxygen combustion vessel by pressing the fill
button location behind the fill lever. Refer to Figure 5-2. While
filling, the status bar on the software main window will display
"Filling."
56 AC600 Operation
Figure 5-3
Oxygen Fill Button
13. Once the oxygen combustion vessel is filled, an audible noise will
sound.
14. Raise the lever to release vessel.
15. Remove oxygen combustion vessel from the fill side.
16. Perform a leak check on the oxygen combustion vessel. Refer to
Leak Checking Oxygen Combustion Vessel, page 613.
Operation AC600 57
17. To install the oxygen combustion vessel on the bucket lid, insert
the oxygen combustion vessel cap flange into the mating socket
on the bucket lid. To correctly orient the electrode contacts, the
cap flange should be inserted with the electrode facing to the
rear. Refer to Figure 5-4 and Figure 5-5.
Figure 5-4
Vessel Installed
Figure 5-5
Bucket Lid Mating Socket
18. Refer to Analyzing a Sample, page 518, for steps to analyze a
sample.
58 AC600 Operation
Creating or Modifying Methods
A method is a set of analytical parameters used to control the

instrument during analysis and calculation of the final result. Before
analysis, a method must be created or the default method is used.
1. From the Configuration menu, click Methods. The Methods dialog

box shown below will appear. For further information about the
buttons on the Method Dialog Box, refer to Dialog Box Buttons,
page 410.
2. Create or edit a method.

A. To create a method, click the Add button to add a method
and complete the Add Method dialog box. Refer to
Predefined Methods, above.
B. To edit a method, select the method by clicking on the name
of the method in the Methods dialog box.
3. Click Properties. The Parameters tab will appear.
Operation AC600 59
4. Enter the Parameters for the method.
A. For Standards Mode, click the arrow to select a standard.
Standards are listed below. When a standard is selected, the
method will preload with the correct parameters for the
method. A custom mode for user-determined parameters is
also available as a selection.
ASTM D240-02 Standard Test Method for Heat of
Combustion of Liquid Hydrocarbon Fuels
by Bomb Calorimeter
by Bomb Calorimeter (Precision Method)
ASTM D5468-02 Standard Test Method for Gross Calorific
and Ash Value of Waste Materials
Value of Coal and Coke
Custom User-determined method
ISO Solid Mineral Fuels- Determination of
1928:1995(E) Gross Calorific Value by the Bomb
Calorimetric Method, and Calculation of
the Net Calorific Value
AS 1038.5-1998 Coal and Coke- Analysis and Testing-
Gross Calorific Value
DIN 51900 Determination of the Gross Calorific
Value by the Bomb Calorimeter and
Calculation of the Net Calorific Value
(General Information, Basic Apparatus,
Basic Methods)
BS1016- Methods for Analysis and Testing of Coal
105:1992 and Coke. Determination of Gross
Calorific Value
B. For Spike, enter the calorific value of the accelerator added
to aid in the combustion of the sample. Refer to Configuring
System, page 430, for additional information.
C. For Thermochemical Corrections, enter the parameters as
explained below.
1) For Nitrogen Units, click the arrow to select a reporting
unit from the list.
510 AC600 Operation

2) For Titrant Energy Value, enter the heat of formation
for nitric acid, HNO3, formed during combustion of the
sample.
(Titrantenergysoftware)(conc.user )
Titrantenergyuser =
concfromASTMs tan dard
Where,
Titrantenergyuser: Titrant energy level to be entered in the method

by the user if the acid concentration differs from an ASTM standard
listed in the software. If any titrant concentration other than from an
ASTM standard listed in the software is used, Custom must be selected
in Method Parameters and the titrant energy value entered.
Titrantenergysoftware: The given titrant energy level for a given

ASTM standard listed in the software.
Conc.user: Users titrant acid concentration
Concfrom ASTMstandard: Titrant acid concentration from an ASTM

standard listed in the software
3) For Sulfur Units, click the arrow to select a reporting

unit from the list.
4) For Sulfur Correction, enter the heat of formation for
sulfuric acid, H2SO4, formed during combustion of the
sample.
5. Click the Mode tab and enter parameters.
Operation AC600 511

A. For Mode, Select the Heat Correction mode used to
compensate for the amount of heat transferred between the
bucket and the surrounding environment. Refer to Critical
Calculations, page 73, for further information.
B. Analysis Time displays the total time period for an analysis.
C. For Equilibrate Time, enter a value to specify the first time
period that is used to allow the various components of the
calorimeter to reach thermal equilibrium. At this time, the
rate of heat transfer between the bucket and environment is
assumed constant. The range is 0.1 to 10 minutes.
D. For Pre-Fire Time, enter a value to specify the length of
time referred to as the first rating period. During this time,
the rate of the bucket temperature change is measured.
E. For Main Time, enter a value to specify the main time
period, which begins when the oxygen combustion vessel is
fired. The range is 0.1 to 10 minutes.
Exporting Methods
Export Method exports method parameters to a file. The method can
be saved on the computer hard drive or transferred to another media
for safe storage. The method can then be imported to the same
instrument or transferred to another calorimeter. Refer to Importing a
Method, page 513.
1. Click the Configuration menu and select Methods. The Methods

2. Select the method to export by clicking on it. An asterisk will
appear next to the selected method.
3. Click Export. The Export screen will appear.
4. Select the folder to store the method in. The method name will
appear as the file name. Do not enter an extension. The software
will automatically add the proper file extension.
5. Click Save to copy the method to the selected folder.
512 AC600 Operation

Importing a Method
Import a Method imports a method to same calorimeter it was exported from or
another calorimeter that has the ACWIN software installed.
1. Click the Configuration menu and select Methods. The Methods
2. Select Import .
3. On the Import dialog box, select the file to import.

4. Click Open. The method will be added to the Methods dialog box.
Operation AC600 513

Logging in a Sample
Before a sample is analyzed, sample information is directly entered

into the spreadsheet or entered into the spreadsheet using the Sample
dialog box. Information can be entered manually or it can be entered
automatically using the Samples dialog box. The following section
provides further information about entering sample information into
the spreadsheet.
Entering and Modifying Data in Spreadsheet

Before a sample is analyzed, sample information is directly entered
into the spreadsheet or entered into the spreadsheet using the Sample
dialog box. The following section explains how to manually enter and
modify sample data in the spreadsheet.
To change the column headings that display in the spreadsheet, refer

to Customizing Sample Spreadsheet, page 414. For definitions of
Spreadsheet Column Headings, refer to Glossary, page 121.
1. In the last empty row of the spreadsheet, click in the Name

Column.
2. In the Name column, select the arrow and then click on the
sample name from the list.
3. In the Method column, select the arrow and then click on the
name of the method for that sample from the list.
4. Enter sample data in the remaining columns as required for the
sample.
Repeating Data in Multiple Cells

Quickly fill a group of cells in the spreadsheet with the same data.
1. Select and drag the mouse pointer to select the cells to fill with
the same data.
514 AC600 Operation

2. Select Edit and then select Fill.
3. Enter the data to fill into each selected cell and select OK.
Inserting a Sample Out-of-Sequence

Insert a sample out of sequence between unanalyzed samples. Insert
will place a new row before the selected row.
1. Click in the row immediately below the last analyzed sample.

2. Select Edit and then select Insert. The sample information
displayed in the inserted row will be duplicated from the row
before the inserted row.
Operation AC600 515

Using Sample Login Dialog Box
The following section explains how to log in samples for analysis using
the Sample dialog box. Samples can also be logged in using Balance
Login or logged in using a sample template. Refer to Logging in a Mass
Value from Balance, page 517, or Logging in from a Sample
Template, page 517.
1. Select Samples and then select Login. The Sample dialog box will
appear.
2. Enter sample information as required for the sample. The

Username of the user logged on to the Instrument will display in
the Operator entry box.
A. In the Sample Name entry box, enter the name of the
sample or select the arrow and then select a sample from
the list.
B. For Mass, refer to Entering Sample Weight from Balance,
page 37.
An external balance must be interfaced with the instrument to enter
weights automatically. Prepare the sample for analysis. Refer to
Preparing for Analysis, page 54, for additional information. When a
single computer is used to control multiple instruments, a checkmark,
to the left of Balance on the samples menu, is used to indicate which
instance of the ACWIN software is communicating with the external
balance.
C. Enter the method by selecting the arrow and then selecting a
method from the list.
D. For vessel, enter the identification number of the oxygen
combustion vessel that is being used for analysis. This
number can also be entered by using an optional bar code
reader. Refer to Bar Code Reader, page 317.
E. Enter a comment in the Comments entry box, if desired.
516 AC600 Operation

F. Enter a description in the Description entry box, if desired.
G. Select one of the following options by selecting in the
appropriate check box. In the spreadsheet, the sample
currently scheduled for analysis is designated by a yellow
arrow. The selections that appear depend on the number of
samples logged into the spreadsheet.
Select Add to End of List to add the sample at the end of
the spreadsheet.
Select Add as Next Sample to Run to designate the sample
as the next sample to run after the sample currently
selected with a yellow arrow.
Select Add Before ____ to add the sample to the
spreadsheet before the sample selected with a yellow arrow.
Select Add After _____ to add the sample to the
spreadsheet after the sample selected with a yellow arrow.
Logging In Mass Value from Balance

Before the mass can be automatically transferred to the spreadsheet,
the balance must be able to communicate with the instrument. Refer
to Installing Balance, page 33, for instructions.
1. Select Samples and then select Balance or press F4 on the

Toolbar. A new row will display in the spreadsheet with the mass
from the balance automatically entered. The Sample name and
method will repeat from the previous row.
2. Enter a new sample name and method if necessary by double-
clicking in designated cells.
Logging In from Sample Template

1. If a sample template has not already been created, refer to
Creating Sample Templates, page 434.
2. Select the Samples menu and then select Login. The Login screen
will display.
3. Select the arrow in the Sample Name dialog box and then select
desired sample template from the list.
4. Select OK. Information from Sample Template will display in the
spreadsheet.
Operation AC600 517

Analyzing a Sample
The following instructions assume that all installation steps have been
completed. Refer to Installing Instrument for First-Time Analysis, page
23.
Accurate analysis results are obtained after the instrument has been
calibrated. Calibration should be performed after changing analysis
modes or analysis times. Refer to Calibration, page 524.
HIGH PRESSURE HAZARD

Do not permit your hands and face to remain over the
calorimeter at the end of the oxygen combustion vessel
ignition. Serious personal injury could result. Stay clear for at
least 20 seconds after the oxygen combustion vessel ignites.
1. If the instrument has not been prepared for analysis, refer to

Preparing for Analysis, page 54, and follow instructions.
2. Analyze a conditioning sample if required before the calorimeter
is stable.
3. Create a method for the analysis. Refer to Creating or Modifying
Methods, page 59.
4. Log in Sample. Refer to Logging in a Sample, page 514.
5. Install oxygen combustion vessel on bucket lid and press the
analyze button on the front panel of the instrument or press F5
Analyze Now on the toolbar. The instrument will complete the
analysis sequence. Refer to the Analysis Sequence diagram,
Figure 10-30, page 1031.
6. Review the status bar for instrument messages during the
analysis sequence. During prefire, the current bucket and jacket
temperatures will be displayed in the lower right corner of the
status bar. The timer left before ignition is displayed in the lower
left corner of the status bar. Three seconds before ignition, a
beeper will sound and a message will flash (lower left corner) with
a warning to stay clear of the calorimeter.
7. Once analysis completes, the bucket lid will rise.
8. Slide the oxygen combustion vessel from the bucket lid.
518 AC600 Operation

9. Install the oxygen combustion vessel on the vent side of the
vessel prep station as follows:
A. Slide the flange fitting on the vessel lid into position and
continue holding the oxygen combustion vessel.
B. Lower the level for the vent side. Refer to Figure 5-6.
Figure 5-6
Vessel Prep Station - Vent Side
10. Once the oxygen combustion vessel is vented, raise the lever and
remove vessel.
11. Use the vessel lid removal tool to remove the lid from the oxygen
combustion vessel.
12. Rinse vessel with distilled water and then empty water from
vessel.
Deleting a Sample
A sample that has been logged in or analyzed can be deleted from the
spreadsheet; however, the currently logged in user must have
permission to delete analyzed samples. Refer to Determining User
Permissions, page 426.
1. Select the desired sample or samples in the spreadsheet by

selecting on the number for each sample in the Row column. To
select more than one sample, hold down the CTRL key while
selecting the desired samples.
2. From the Samples menu, select Delete or right-click and then
select delete from the menu. When the dialog box with the
question Are you sure you want to delete the selected samples
displays, select Yes to remove samples from the spreadsheet;
select No to keep samples in the spreadsheet. Once a sample is
deleted, it is not possible to restore the data.
Operation AC600 519

Using Sample Filters
Use the Sample Filters command from the Configuration menu to

create filters that determine how the sample results are grouped in the
spreadsheet of the software main window. For example, sample results
can be grouped by a method name, a date range, or a sample name. A
filter can be created that selects all samples analyzed before a certain
date for deletion, or a filter can be created that selects all of Today's
results to transmit, export, or print. Some filters have been predefined
in the software. For further information, refer to Predefined Filters,
page 522. Filters can be set to automatically update. Refer to step 7,
page 522.
1. From the Configuration menu, click Sample Filters. The Sample

Filters dialog box will display.
2. To select a filter, click on the name of the filter in the Filters
dialog box and then click OK. To add a new filter, refer to Add
Filters, below.
3. Use the buttons on the Filters dialog box to modify or delete

filters if desired.
To modify the properties of filters, refer to Filter Properties, page
521.
To delete a filter, refer to Deleting Filters, page 522.
Filters Dialog Box Buttons
Adding Filters
Use the Add command to create a new filter.
1. To add a new filter, click Add. "New Filter" will display in the
Filters dialog box. Each time Add is clicked "New Filter" will
increment by one and display as "New Filter 1," "New Filter 2,"
etc.
520 AC600 Operation

2. Click Properties to configure the filter. Refer to Filter Properties,
below.
Filter Properties
Use the Properties command to determine the parameters for a filter.
1. To determine or modify the properties for a filter, click on the

name of the filter in the Sample Filter dialog box and then click
Properties. The Sample Filters dialog box will display.
2. Click New Filter and then click Properties. The Sample Filter dialog
box will display.
3. In the Filter Name entry box, type in the name for the filter.
4. For Export Format, click the arrow to select the export format for
this filter.
5. For Transmit Format, click the arrow to select the transmit format
for this filter.
6. Add a parameter, delete a parameter, or modify columns for the
sample filter.
A. To add a parameter,
1) In the Field entry box, click the arrow and select the
desired field.
2) In the Compare entry box, click the arrow and select the
desired comparator. The comparator selections change
depending on the selected field.
Operation AC600 521

3) In the With entry box, enter the desired parameter
depending on the selected field. For example, if Analysis
Date is selected for Field and On is selected for
Compare, in the With column, enter the desired date for
the analysis results.
4) Click Add to insert a new row.
5) In the And/Or entry box, click the arrow and make
desired selection.
6) Repeat steps 1) - step 5), above, until all parameters for
the filter have been determined.
B. To delete a parameter or all parameters, click in the desired
row, or select multiple rows by holding CTRL while selecting
rows.
C. To modify columns, click the Fields button. Refer to
Modifying Columns, page 415.
7. Determine Automatic Updates if desired by selecting the check
box. Filters that are based on time should be automatically
updated in order to ensure the selected sample results are
displayed accurately. When the check box is selected, the Start
Time and Update Frequency will be enabled.
A. For the Start Time, enter a date as MO/DD/YYYY and a time
as 00:00:00. The Start Time indicates the time the update
will first be applied.
B. For Update Frequency, select the check box for hours or
days and then enter a numerical value to indicate how often
the update will be applied.
Deleting Filters
Use the Delete command to remove sample filters from the Filters
dialog box.
1. Click on the desired sample to remove.

2. Click Delete.
Predefined Filters
Filters that may be frequently used have been predefined in the
software. Default filters are All Samples and Today's Samples. The
remaining filters that display are based on created methods. To select
a predefined filter, click on the name of the filter, and then click OK.
522 AC600 Operation

Modifying Predefined Filter
To modify a predefined filter, click on the name of the filter and then
select Properties. The Properties dialog box will display. Only the Fields
and Automatic Update of a predefined filter can be modified.
In the Sample Filter dialog box, the Filter Name displays the name of
the predefined filter. The Description explains the filter and whether or
not the fields or automatic updates can be modified. For example, for
All Samples, only the Fields can be modified. To modify the fields, click
the Fields button. For further information about the fields, refer to
Modifying Columns, page 415.
When the Automatically Reapply Sample Filter check box is checked,

the software will update the sample filter according to the parameters
entered for Start Time and Update Frequency. To determine the
automatic update, refer to step 7, page 522.
Operation AC600 523

Calibration
Calibration is the process that adjusts the instrument to produce an

analysis result to equal that of a known calibration standard. The
following section explains the calibration procedure for the instrument.
Accurate analysis results are obtained after the instrument has been
calibrated. Calibration should be performed after changing analysis
modes or analysis times.
1. Define calibration standards to create a list of calibration

standards and their certified values for use during calibration.
Benzoic Acid is the preferred standard for calibration.
A. From the Configuration menu, click Standards. The

Standards screen will appear.
B. Click Add to list a standard. A row will be added to the

bottom of the sample grid.
Units will be the same as those set in System Configuration.
C. Click the row and enter a standard name, value, lower

control limit (LCL) and upper control limit (UCL).
The lower control limit, or LCL, is the minimum standard
result value. If the standard result is below the lower
control limit, a notice will appear.
The upper control limit, or UCL, is the maximum
standard result value. If the standard result is above the
upper control limit, a notice will appear.
If an LCL or UCL value is not entered analysis will
continue regardless of the result data.
D. If desired, the list of standards can be arranged in the
Standards dialog box as follows: To move a standard to a
higher position, select the standard and then select Promote
until standard reaches desired position. To move a standard
to a lower position, select the standard and then select
Demote until standard reaches desired position. Select
Ascending to sort standards in alphabetical and/or numerical
order from lowest to highest. Select Descending to sort
standards in alphabetical and/or numerical order from
highest to lowest.
524 AC600 Operation

E. Click OK to save any changes and exit.
2. Create method for analyzing standards. Refer to Creating or
Modifying Methods, page 59.
3. Log in standards. Refer to Logging in a Sample, page 514.
4. Analyze standard calibration samples. Refer to Analyzing a
Sample, page 518, and perform the analysis using defined
standard calibration samples.
5. Select Samples to be used for Calibration as explained below.
A. From the Configuration menu, click Calibration. The Calibrate
B. Review the calibration results. If the calibration values

displayed are acceptable, check the Save box. If the values
are not acceptable, click Cancel and perform another
standard analysis.
C. Repeat step 2 for each oxygen combustion vessel.
D. Click Print to print a copy of the new calibration results.
E. Click OK to save the new calibration.
Operation AC600 525

Recalculating Results
Results such as weight, oxygen combustion vessel, or fuse length, are

automatically recalculated when a column in the spreadsheet is edited.
When a calibration is changed, it can be reapplied by following the

procedure below.
1. Select the samples in the sample grid to recalculate.

2. From the Samples menu, click Recalculate. The selected samples
will be recalculated using the new calibration or method
parameter.
526 AC600 Operation

Viewing History of a Sample
View History shows a history log of the actions performed on a

selected sample.
1. In the spreadsheet, select the desired sample.

2. Click the Samples menu and select View History. The View History
Date and Time displays the date and time the action took
place.
Action displays Created, Modified, Or Recalculate to indicate
how the sample was modified.
User displays the username of the person who performed the
action.
3. For Time, click the Local Time check box to display the time in
local 12-hour time or select the UT check box to display the time
in Universal Coordinated Time.
4. Click OK to exit view history.
Operation AC600 527

Applying Sample Signatures
A signature confirms that a user has accepted the sample information

displayed in the spreadsheet. Any change to the sample information
after it is signed will clear the signature. For this reason, a signature
indicates that sample information has not changed and thereby
ensures the validity of the sample information.
Signing
Sign provides the means to apply a signature to samples. Sign is only
available if logging was enabled when the database was created. Refer
to Managing Databases, page 450.
1. Select the desired sample in the spreadsheet.

2. From the Samples menu, click Sign. The Sign dialog box will
display. The system name, user name, date, and time are
obtained from the Windows operating system and cannot be
changed from this dialog box.
In the Sign dialog box, System displays the name assigned to the
computer that identifies the computer on a network.
User displays the name of the user logged onto the Windows
Operating System.
Date and Time display the date and time the signature was
applied to the sample.
Local or UT will be checked depending on the selection made for
the presentation time. Refer to Presentation Time, page 464.
3. For Name, enter the name of the person applying the signature to
the sample.
4. For Description, enter information to help identify the sample, if
desired.
528 AC600 Operation

Viewing Signatures
View Signatures allows sample signatures to be viewed in order to
determine if they are valid. A sample must be signed before the
signature can be viewed. View Signatures is only available if logging
was enabled when the database was created. Refer to Managing
Databases, page 450.
1. Select desired sample in the spreadsheet by clicking in the Name

column.
2. From the Samples menu, click View Signatures. If information
associated with the sample was changed after it was signed, the
signature will be cleared and the view signatures screen will not
appear.
In the View Signature dialog box, Signers displays the signatures
assigned to the sample, and the date these signatures were
applied. Valid will either display Valid or Not Valid. Valid indicates
the result has not been modified, and Not Valid indicates that the
current data encryption code for the result does not match the
data encryption code stored with the result at the time the result
was signed/validated.
System displays the name assigned to the computer that
identifies the computer on a network.
User displays the name of the user logged onto the Windows
Operating System.
Date and Time display the date and time the signature was
applied to the sample. Local or UT will be checked depending on
the selection made for the presentation time. Refer to
Presentation Time, page 464.
Operation AC600 529

Printing Reports
Configuring Report before Printing

A report of analysis results can be generated and printed on the
system printer. The following section explains how to use the Report
Settings dialog box to determine the format of the report.
1. In the spreadsheet, select the samples as follows:

A. Place cursor in the column under row until a black arrow
displays.
B. Hold down right mouse key and drag the mouse over the
desired samples.
C. Unclick the mouse. Selected samples appear highlighted in
blue.
2. Click Samples and select Print Preview. Click Print Preview to
access the Report Settings dialog box in order to preview how
selected samples will print on the system printer. The Report
Settings Screen will appear.
3. Configure the report by clicking the Report tab, Field tab, Font
Tab, and Element tab and entering the desired settings as
explained in the steps below. The Fields tab will only appear when
Define Report Fields is checked on the Report tab.
4. On the Report Tab,

A. Click the arrow next to Report Format to determine the
format of the report.
Click Report with Plots to display a report with data
plotted.
Click Tabular Report to display data in a table.
Click Simple Print to display a report based on the
columns that appear in the spreadsheet. This report can
then be printed.
530 AC600 Operation

Click Group Report to display the average, the standard
deviation, and the relative standard deviation when
multiple samples are selected.
Click Ambients to display ambients.
Click Hardware Calibration to display the hardware
calibration.
B. Click the arrow next to Statistics to select how statistics will
display.
Select None, and statistics will not display.
Select Report with Plot, and statistics will display as a
line plot.
Select Tabular Report, and statistics will display in a
table.
C. For Heading Text, enter a title for the report, if desired.
D. Select the Define Report Fields check box and the Fields tab
will display. Use the Fields tab to select the columns from
the spreadsheet that will display in the report.
E. For Line Printing, select the Automatically Print after Each
Analysis check box. Enable line printing when printing with a
dot matrix printer.
F. When Line Printing is enabled, the Automatically Print After
Each Analysis checkbox is enabled. When selected, a report
will automatically print after each analysis.
5. Complete the Fields tab as follows to determine the fields that
display in the report. The Fields tab will only display when Define
Report Fields is checked on the Report tab. Fields that appear
vary, depending on the instrument.
Operation AC600 531

To display a Field that does not appear in the report, select the field
from Invisible Fields, and then click Show. The Field will automatically
move to the Visible Fields column.
To remove a Field so that it does not display in the report, select the
field from Visible Fields and then click Hide. The Field will automatically
move to the Invisible Fields column.
To display the default fields, click Default.
To move a field so that it displays earlier in the report, select the Field
from the Visible Fields column and click Promote until the field displays
in the desired position.
To move a field so that it displays later in the report, select the Field
from the Visible Fields column and click Demote until the field appears
in the desired position.
6. Use the Font tab to configure the text in the report to improve the
readability of the report. Refer to Modifying Font on page 414.
7. Use the Elements tab to determine the elements that display in
the report. Refer to Adding Dashboard Panes on page 418.
Printing from the Software

1. From the spreadsheet, select the desired samples that have been
analyzed to print. When several samples are selected, the
software will group the samples by sample name.
2. Click Samples and click Print. Clicking Print or Print Preview will
open the Report Settings dialog box.
3. Refer to Printing Reports, page 530, to format the report as

desired.
4. From the Samples menu, click Print Setup. The Page Setup dialog
box will display.
532 AC600 Operation

5. Use the Page Setup dialog box to change the size, orientation,
and margins of the paper before printing.
When multiple columns are selected to appear in the report, the font
and page orientation can be adjusted to improve the readability of
the report. The font size can be changed using the font tab as
described in Printing Reports, page 530.
6. Click OK. The Print dialog box will appear.
7. Click OK to print.
Operation AC600 533

Transfer Import and Transfer Export
The transfer export and import commands provide the means to

transfer sample results so they can be saved to a file for storage or
viewed on another computer that also has the ACWIN software
installed. The transfer commands offer an advantage because
everything associated with the sample results such as buffers,
calibrations, and data will be transferred.
Transfer Export
Transfer files created with newer versions of the ACWIN software
cannot be imported into older versions of the software.
1. In the spreadsheet, select the samples for export. If no sample is
selected, only the last sample in the sample grid will be exported
and saved.
2. From the Samples menu, click Transfer Export.
3. In the Export dialog box, enter a File Name for the sample
transfer and then click Save to save the sample transfer in the
current location or select a new location by clicking the arrow for
Save in, select a new location, and click Save.
534 AC600 Operation

Transfer Import
The transfer export and import commands provide the means to
transfer sample results so they can be saved to a file for storage or
viewed on another computer that also has the ACWIN software
installed. The transfer commands offer an advantage because
everything associated with the sample results such as buffers,
calibrations, and data will be transferred.
Transfer files created with newer versions of the ACWIN software

cannot be imported into older versions of the software.
1. From the Samples menu, click Transfer Import.
2. In the Import dialog box, select the sample to import by clicking
on it and then click Open.
Operation AC600 535

Importing and Exporting Data
Exporting Data
Text Export Data exports selected sample data and to a file. Sample
data can be imported into Microsoft Excel. Refer to Importing Data,
page 536.
1. Create an Export Format. Refer to Creating Export Formats, page

441.
2. In the spreadsheet, select the samples for export. If no sample is
selected, only the last sample in the sample grid will be exported
and saved.
3. Select Samples on the Menu bar and then select Text Export
Data.
4. In the Select Export dialog box, select the desired text export
format.
5. In the Save As dialog box, the filename and location associated

with the export format selected is automatically entered as the
File name. Comma Delimited (*.csv) is automatically selected as
the Save as Type.
Importing Data
Text Import Data permits the operator to import sample data back into
the ACWIN software after it had been exported to another location.
1. Click the Sample menu and select Text Import Data. The Open
2. Select the file to import.

3. Click Open to import the file.
536 AC600 Operation

Exporting Buffers
Text Export Buffers exports selected sample data buffers to a file.

Sample data buffers contain bucket and jacket temperature data along
with the time each was collected. Sample data can then be imported
into Microsoft Excel.
1. In the spreadsheet, select the samples for export.

2. Select Samples on the Menu bar and then select Text Export
Buffers.
3. In the Save As dialog box, select or enter a filename and
extension. File extensions (.txt) or (.csv) are good choices to
insert the saved file into an Excel spreadsheet.
Operation AC600 537

Transmitting Results
Results can be transmitted or transferred to a computer at another

location for storage and/or possible processing. To automatically
transmit analysis results after an analysis, refer to the Automation tab,
page 437.
A sample can be transmitted using more than one Transmission

Format.
1. If a transmission format has not already been defined, define

transmission format. Refer to Creating and Modifying
Transmission Formats, page 435.
2. Select the desired sample or samples in the spreadsheet by
selecting in the Row column to highlight the entire row. Select
multiple samples by holding down the CTRL key while clicking on
the samples.
3. On the Menu bar, select Samples and then select Transmit.
4. In the Select Transmit dialog box, select the Transmit format for
sending the data by selecting on the name of the transmit format
and then select OK.
5. Select OK in the Transmit Done dialog box.
538 AC600 Operation

6 Maintenance
Illustrations .................................................................................. 62
Periodic Maintenance Schedule ....................................................... 63
Modifying Maintenance Counters ..................................................... 66
Logging In Periodic Maintenance ................................................ 68
Viewing Log ................................................................................ 610
Performing Prep Station Maintenance............................................. 611
Leak Checking Oxygen Combustion Vessel ..................................... 613
Replacing Oxygen Combustion Vessel O-Rings ................................ 614
Replacing Oxygen Charger O-Rings ............................................... 616
Rinsing Prep Station .................................................................... 617
Replacing Ignitor Wire Assembly for Thread Fuse ............................ 619
Replacing Optional Wire Fuse ........................................................ 620
Draining and Replacing Distilled Water ........................................... 622
Replacing Water Filter .................................................................. 624
Removing and Cleaning Fan Filter ................................................. 625
Polishing Bucket and Baffle ........................................................... 626
Lubricating Screw for Lift-Arm Mechanism ...................................... 632
Adjusting the Pressure Safety Release Valve ................................... 638
Replacing Ceramic Washer ........................................................... 639
Maintenance AC600 61
Illustrations
Figure 6-1 Orientation of Lock Vessel ................................................612

Figure 6-2 Vessel Lid ......................................................................614
Figure 6-3 O-Ring Removal Tools .....................................................615
Figure 6-4 Prep Station with Rinse Bottle Attached .............................617
Figure 6-5 Drainage Port .................................................................618
Figure 6-6 Electrode Sleeve and Slots ...............................................620
Figure 6-7 Wire Fuse in Electrode Slots .............................................621
Figure 6-8 Wire Fuse with Crucible ...................................................621
Figure 6-9 Front Panel ....................................................................622
Figure 6-10 Fan Filter .....................................................................625
Figure 6-14 Bolts for Front Panel ......................................................627
Figure 6-16 Stirring Motor Gear Box .................................................628
Figure 6-17 Upper Setscrew ............................................................629
Figure 6-18 Thermistor Leads ..........................................................629
Figure 6-20 Power Switch ................................................................632
Figure 6-24 Front Panel Bolts ...........................................................634
Figure 6-26 Lift-Arm Plate and Molding .............................................635
Figure 6-27 Side Casing for Lift Arm .................................................636
Figure 6-29 Top Casting Cover Screw Tabs ........................................637
Figure 6-30 Pressure Safety Valve ....................................................638
62 AC600 Maintenance
Periodic Maintenance Schedule
Perform the following maintenance procedures on a regular basis.

Periodic maintenance of the instrument will result in improved
instrument performance, which can extend the life of the instrument.
Only qualified personnel should perform inspection, cleaning,

maintenance, or repair. Only original manufacturer consumable and
spare parts should be used.
Frequency Item Procedure

Refer to Oxygen Combustion Vessel Safety
Notice, page 144. The check-valve o-ring and
Oxygen Combustion closure o-ring on the oxygen combustion vessel
500 Firings
Vessel should be replaced after every 500 firings. Refer
to Replacing Oxygen Combustion Vessel O-Rings,
page 614.
Send oxygen combustion vessel to be
Oxygen Combustion hydrostatically and proof tested by LECO at 5000
5000 Firings
Vessel firings. Refer to Oxygen Combustion Vessel
Safety Notice, page 144.
Inspect ignitor wire prior to each analysis.
Ignitor Wire for Thread Replace ignitor wire when it breaks. Refer to
Fuse Replacing Ignitor Wire for Thread Fuse, page 6
Prior to Each 19.
Analysis
Leak check the oxygen combustion vessel prior
Oxygen Combustion
to each analysis. Refer to Leak Checking Oxygen
Vessel
Combustion Vessel, page 613.
Check distilled water level daily. Add distilled
Chiller water when the level falls below indication line.
Refer to Adding Distilled Water, page 315.
Daily If many halogenated compounds are being
analyzed, use the prep station rinse tool to rinse
Prep Station
the prep station. Refer to Rinsing Prep Station,
page 617.
Inspect weekly at a minimum. Inspect more

often depending on operating conditions. Clean
Fan Filter
when visibly dirty. Refer to Removing and
Cleaning Fan Filter, page 625.
Check-Valve O-Ring and Inspect check-valve o-ring on oxygen

Closure O-Ring on combustion vessel weekly. Replace when it
Weekly Oxygen Combustion shows signs of wear. Refer to Replacing
Vessel Combustion Vessel O-Rings, page 614.
Use the vessel prep station rinse tool to

rinse the prep station. Refer to Rinsing Prep
Station, page 617.
Vessel Prep Station
The vessel prep station handles should be
removed, washed with soap and water,
dried, and then greased with silicone grease.
Drain and replace distilled water. Refer to
Distilled Water Draining and Replacing Distilled Water, page
622.
Drain and replace distilled water every two
months or as recommended in the Chiller
Distilled Water in Chiller Instruction Manual. Refer to Adding Distilled
Water, page
Two Months 315.
Clean condenser. Refer to Cleaning Chiller
Chiller Condenser
Condenser, page 316.
Water filter should be replaced every two months
at a minimum. Replace more often depending on
Water Filter
operating conditions. Refer to Replacing Water
Filter, page 624.
Grease screw every six months or as needed due
Screw for Lift-Arm
Six Months to excessive noise. Refer to Lubricating Screw on
Mechanism
Lift-Arm Mechanism, page 632.
Polish annually at a minimum or when
Bucket and Baffle discoloration occurs. Refer to Polishing Bucket
and Baffle, page 626.
Inspect the bucket anodes and replace if
damaged or severely corroded and no longer
Bucket Anodes
secure tightly to the support rod. Refer to step
21, page 629.
The oxygen combustion vessel should be
inspected and the following parts should be
replaced on a yearly basis at minimum: All O-
Oxygen Combustion
Rings, Ceramic Insulator, Insulator Electrode,
Vessel
Ground Electrode. This maintenance could be
required more often depending on operating
conditions.
Annually Pressure Regulator on
Oxygen Combustion Refer to Adjusting the Pressure Safety Release
Vessel Charger Valve, page 638.
Assembly
Change every 365 days when the counter on the
sterilizer reaches 0. Refer to the manufacturers
UV Sterilizer Bulb
manual provided with the sterilizer for bulb
(located on sterilizer)
replacement instructions. The replacement UV
sterilizer bulb part number is 621-605-866.
Inspect when changing the UV sterilizer bulb and
clean according to the manufacturers manual
Quartz Sleeve provided with the sterilizer. Replace the quartz
(located on sterilizer) sleeve if cleaning did not remove mineral
deposits. The replacement quartz sleeve part
number is 621-605-867.
Modifying Maintenance Counters
The Counters dialog box tracks the periodic maintenance performed on

selected instrument components and alerts the operator when periodic
maintenance is due. Until the required maintenance is logged in, the
Maintenance is Required Soon dialog box will continue to display each
time an analysis is initiated. Refer to Logging In Periodic Maintenance,
page 68.
Only users with permission can edit the Counters dialog box. Refer to
Adding or Changing User Permission for Instrument, page 428.
1. Select Configuration and then select Counters. The Counters

dialog box will display.
2. Add or modify a counter.
To add a counter, select Add. A row will be added above the
currently selected row.
To modify a counter, select the counter by selecting on the row
column that corresponds with the counter.
3. Select in each column and enter information as required for
maintenance.
A. In the Name column, enter a name or description of the

component or assembly that requires periodic maintenance.
B. In the Type column, select the arrow and then select the
method used to track periodic maintenance.
C. The Count column tracks the number of items selected in the
Type column.
D. In the Warning column, enter a value to indicate the number
of items from the Type column that can occur before periodic
maintenance is necessary. Analysis will not stop when this
counter limit is reached, but a warning prompt will display
until the maintenance is performed. To turn this function off,
enter zero.
E. In the Stop column, enter a value to indicate the number of
items from the Type column that can occur before the
instrument will stop and no longer analyze samples until
periodic maintenance is performed. To turn this function off,
enter zero.
F. The Resets column displays the total number of times that
periodic maintenance has been performed.
G. The Reset column displays the date and time periodic
maintenance was last performed.
H. In the Comments column, enter any notes regarding
maintenance.
4. Modify the Counters dialog box, if desired, as follows:
To delete a counter, select the desired counter and then select
Delete.
To return the counters in the list to the original settings and/or
return system counters that have been deleted, select Restore.
To sort the Counters, select Ascending, and the Counters will
automatically display in alphabetical and/or numerical order from
lowest to highest. Select Descending, and the Counters will
automatically display in alphabetical and/or numerical order from
highest to lowest.
To change the order of the Counters, select desired counter to
move. Select Promote to move a counter to a higher position in
the table. Select Demote to move a counter to a lower position in
the table.
Logging In Periodic Maintenance
Use the Maintenance dialog box to log in periodic maintenance after it
has been performed. The maintenance counter will be reset when
periodic maintenance is logged in.
1. Select Maintenance and then select Login. The Maintenance dialog

box will appear.
2. Select the check box for the item that received periodic
maintenance. If an item is already checked, periodic maintenance
is necessary based on the parameters set for that item in the
Counters dialog box. Refer to Maintenance Counters, page 66.
3. Enter information in the Comments dialog box if desired.
4. When maintenance is logged in for a vessel, a dialog box for the
Safety Notice will appear.
A. In the dialog box, click View Combustion Vessel Safety
Notice and read the Safety Notice that displays.
B. Close the Combustion Vessel Safety Notice.
C. Select the check box for I agree to the terms of the Safety
Notice.
5. Click OK. A dialog box, such as the following example, will display
for each item checked.
6. Select Yes if maintenance has been performed; select No if

maintenance has not been performed. Selecting Yes will reset the
periodic maintenance counter for that item to zero, and create a
log entry. Refer to Viewing Log File, page 610.
Viewing Log
The Log File displays a history of past events. This information can
help to troubleshoot problems that may occur during operation. Every
time one of the following procedures is performed, it will be recorded
in the log file.
Change of Mass by Operator Network Sign-on Errors
Data Out of Range (Ambient Monitor Sample Aborted

parameter values)
Date of last calibration Sample Deleted
Date scheduled maintenance is Standard check out-of-range
performed
Network Errors
1. Select Maintenance and then select View Log File. The log will
appear.
2. To copy, select desired entry by selecting in the Time column for
each entry. To select more than one entry, hold CTRL while
selecting in the Time column. Once desired entries are selected,
select Copy. The information can then be pasted into another
software application such as Microsoft Word or Excel.
3. To print, select desired entries by selecting in the Time column for
each entry. To select all entries in the log, select in the Time
column of the first entry and then hold Shift, CTRL, and End. Click
Print and then click OK.

Performing Prep Station Maintenance
The following procedure explains how to replace the prep station o-

rings and how to clean the prep station.
1. Although not necessary, it may be helpful to remove the stainless

steel tubing (p/n 621-605-887 and/or 621-605-888) from the
cover lock (p/n 621-605-782). This can be done using a 7/16
open-ended wrench.
2. Remove (3) screws (p/n 621-605-821). Once the screws are
removed, the Base Vessel Lock (p/n 621-605-783) will detach
from the Base Lever (p/n 621-605-808), thus exposing the
internal parts of the prep station. Carefully remove all loose parts
and set aside for reinstallation.
3. For the fill side of the prep station, remove (2) o-rings (p/n 772-
738) and (1) o-ring (p/n 611-543) from Insert Valve Charge (p/n
621-605-923). Use caution when removing o-rings in order to
avoid marring the stainless steel surfaces. A small jewelers flat
head screwdriver or xacto blade works well. Lubricate and install
new replacement o-rings.
4. Liberally lubricate and install new replacement o-rings on the fill
side. Once o-rings are installed, lubricate entire insert valve
charge.
5. For the vent side of the prep station, remove (2) o-rings (p/n
772-738) and (2) o-rings (p/n 611-543) from the Insert Valve
Exhaust (p/n 621-605-924). Use caution when removing o-rings
in order to avoid marring the stainless steel surfaces. A small
jewelers flat head screwdriver or xacto blade works well.
6. Liberally lubricate and install new replacement o-rings on the
vent side. Once o-rings are installed, lubricate entire insert valve
exhaust.
7. Using Figure 10-32 as a guide, reposition all loose parts and
tighten (3) screws (p/n 621-605-821).
Follow Figure 6-1 to position the (2) Lock Vessel (p/n 621-
605-784) in the correct orientation before tightening the
screws. This orientation is the same for both the fill and
vents side of the prep station.
Once all loose parts are in position, hold Base Lever (p/n
621-605-787) and Base Vessel Lock (p/n 621-605-783)
together while inserting and tightening the screws.

Figure 6-1
Orientation of Lock Vessel

Leak Checking Oxygen Combustion Vessel
The oxygen combustion vessel should be leak checked before each

analysis, paying close attention to the closure o-ring and check-valve
o-ring. The o-rings should be replaced at every 500 firings. A 2000 ml
beaker is included in the component pack for this purpose.
1. Fully submerge the oxygen combustion vessel in distilled water

for no less than 30 seconds.
2. Monitor the oxygen combustion vessel for air bubbles.
3. If there are no air bubbles, a leak is likely not present. If air
bubbles appear, determine if the air bubbles are escaping from
the closure o-ring or the check valve by inspecting the o-rings for
wear and then replacing the o-rings if necessary.

Replacing Oxygen Combustion Vessel O-Rings
The check-valve o-ring and closure o-ring on the oxygen combustion

vessel should be inspected weekly at a minimum. The following section
provides instructions to replace the oxygen combustion vessel check-
valve o-ring and closure o-ring.
1. Remove the oxygen combustion vessel lid using the oxygen

combustion vessel lid removal tool.
2. Remove the check valve and check valve retaining screw. Refer to
Figure 6-2. Refer to Figure 10-8 for part numbers.
1 Check Valve and Check
Valve Check Valve O-
Ring
2 Electrode Post
3 Oxygen Combustion
Vessel Lid
4 Closure O-Ring
Location
5 Check Valve Retaining
Screw (not shown)
Figure 6-2
Vessel Lid
3. Place the check valve into the o-ring removal block. Refer to
Figure 6-3.
4. Cut the check valve o-ring in the o-ring removal block using the
straight edge knife. Refer to Figure 6-3.

Figure 6-3
O-Ring Removal Tools
5. Wipe the grooves in the check valve and check valve retaining
screw with a clean cloth.
6. Obtain a new o-ring.
7. Wipe a minimal amount of silicone lubricant onto the o-rings and
wipe off any excess lubricant.
Greasing the o-ring on the outer lid is not necessary; however, a
small amount of silicone grease may be used. All excess grease
should be removed from the o-ring by gently wiping it with a lint-free
cloth.
8. Affix cone onto the metal block. Refer to Figure 6-3.
9. Place o-ring onto cone.
10. Remove cone from metal block and invert onto check valve
retaining screw.

Replacing Oxygen Charger O-Rings
The oxygen charger assembly o-rings should be replaced if the oxygen

charger assembly leaks when the combustion vessel is charged.
Leakage will be noticed around the nozzle where it mates with the
combustion vessel.
1. Using the o-ring removal tool, pry out the two o-rings and
discard.
Do not use a metal blade in place of the plastic o-ring

removal tool.
2. Use a minimum amount of silicone grease on the o-rings and

insert them into the nozzle. The o-ring removal tool may also be
used to insert the o-rings.
3. Inspect o-rings for wear.
4. If o-rings are worn, remove the o-rings using the o-ring removal
tool and discard.
Do not use a metal blade in place of the plastic o-ring

removal tool.
5. Use a minimum amount of silicone grease on the o-rings.

6. Reattach new o-rings. The o-ring removal tool may also be used
to insert the o-rings.

Rinsing Prep Station
The prep station should be rinsed weekly to prevent residue build up.
If many halogenated compounds are analyzed, the prep station should
be rinsed daily. The following section explains the procedure for rinsing
the prep station.
1. Attach the rinse knob to the prep station.

2. Insert the nozzle of the water bottle into the port on the rinse
knob.
Figure 6-4
Prep Station with Rinse Bottle Attached

3. Place a container at the drainage port on the rear of the sample
prep station.
Figure 6-5
Drainage Port
4. Gently squeeze the water bottle and allow water to pass through
the prep station until the water in the drainage container is clear.

Replacing Ignitor Wire Assembly for Thread Fuse
The ignitor wire that holds the thread fuse should be inspected prior to
each analysis. It can be reused until it breaks. The following section
explains the procedure to replace the ignitor wire. Refer to
Figure 10-8.
1. Loosen the nut for the crucible holder using the 5/16 wrench.
2. Loosen the screw beneath the shorter electrode.
3. Remove the lower half of the long electrode by turning it beneath
the ignitor wire assembly.
4. Position new fixed wire on the electrodes.
5. Using the 3/16" wrench, reattach and secure the lower half of the
long electrode.
Use extreme caution while tightening the electrode. A snug

fit is sufficient. Do not overtighten.
6. While securing the short electrode in place with the 3/16" wrench,
reattach and tighten the screw beneath the short electrode. The
short electrode must remain stationary while tightening the
screw. Failure to do so can result in shearing off the electrode
threads. A snug fit is sufficient. Do not overtighten.
7. Reattach and tighten the nut for the crucible holder using the
5/16" wrench. You will need to secure the crucible holder in place
with your hand while tightening the nut. A snug fit is sufficient.
Do not overtighten. Refer to Figure 10-8.
8. Perform an ignitor test by following the procedure in Performing
Ignitor Test, page 89.

Replacing Optional Wire Fuse
A new wire fuse should be obtained for each analysis. Refer to

Figure 10-11 for part numbers.
1. Twist and then slide the electrode sleeve to reveal the electrode
slot. Refer to Figure 6-6.
1 Electrode Sleeve
2 Electrode Slot (2)
3 Crucible Holder
Figure 6-6
Electrode Sleeve and Slots
2. Remove the wire fuse from the slots and discard.
3. Obtain new wire fuse.

4. Bend the wire and position it in the electrode slots as shown in
Figure 6-7. Verify that one end of the wire fuse extends
approximately one inch out of the electrode slot.
Figure 6-7
Wire Fuse in Electrode Slots
5. Slide the electrode sleeves over the wire fuse in the slot and then
twist the electrode sleeve to secure it.
6. Place the crucible and sample onto the crucible holder. Verify the
wire fuse just touches the sample but does not touch the crucible.
Avoid having the wire fuse touch the crucible because if this
happens, a misfire may occur.
Figure 6-8
Wire Fuse with Crucible

Draining and Replacing Distilled Water
The distilled water should be drained and replaced every two months.
The chloride salts used in most algaecides are a significant cause of

corrosion and should be avoided in the AC600.
1. Exit ACWIN software.
2. Use Power Switch on back panel to turn off power to instrument.
3. Remove the front panel by using a 7/16 wrench to loosen the 2
bolts that secure the front panel in place. (The bolts are located
underneath and to the sides of the panel.) Refer to Figure 6-9.
4. Obtain the quick disconnect drain hose assembly and place the
open end of drain hose into an empty five-gallon container.
5. Attach the quick-disconnect end of the drain hose to the fitting
and allow water to drain. Refer to Figure 6-9.
Figure 6-9
Front Panel
6. Remove quick-disconnect hose.
7. Drain the external chiller.
8. Clean the external chiller. Refer to the manufacturers manual for
further information.
9. Refill the external chiller. Refer to Adding Distilled Water, page
314.
10. Siphon water from bucket.
11. Power on the instrument.
12. Double-click the ACWin icon on the desktop to start the ACWin
application.
13. The bucket lid should rise fully and the jacket should begin to fill.
The ACWIN software will automatically attempt to fill the AC600 when
the software is started and the water level sensor indicates a low
level. The system will attempt to fill the jacket for 900 seconds.

B. Select the Jacket Fill check box.
15. While the jacket is filling, add water as necessary to the external
chiller to prevent the reservoir from running dry. Once the jacket
reaches the correct level, the jacket water level low will indicate
that the water level is OK.

16. After filling the instrument with water, use a soft brush to remove
any air bubbles that form on the walls of the bucket and jacket.
The bubbles must be removed before analysis.
17. Adjust the water temperature set point as follows:
A. In the ACWIN software, click Configuration and then click
System.
B. For Water Temperature set point, LECO recommends that
this temperature be set approximately 2 to 3C higher than
nominal room temperature and that the external chiller be
set approximately 8-10C below room temperature. The
default temperature is 25C.

Replacing Water Filter
The water filter should be replaced a minimum of every two months or

more often, depending on operating conditions. Replace the filter when
it shows excessive residue. The filter may also need to be replaced
when the instrument displays poor jacket control.
For part numbers, refer to Figure 10-25.
1. Exit the ACWIN software.

2. Turn off power to the instrument and the chiller.
3. Unscrew the filter housing bottom.
4. Remove filter from filter housing bottom and discard.
5. Empty the distilled water from the filter housing bottom.
6. Clean filter housing bottom with water and, if necessary, mild
detergent.
7. Rinse filter housing bottom with distilled water.
8. Dry the outside of the filter housing bottom by using a clean, lint-
free cloth.
9. Obtain new filter and install in filter housing by aligning the filter
with the two flanges in the filter housing top and bottom.
10. Turn on power to the instrument and chiller.
11. Screw the filter housing bottom onto the filter housing top.
12. Check push-to-connect fittings for water leaks. Refer to
Figure 2-2. If leaks are present, verify the tubing is not kinked. It
may be necessary to remove the tubing from the push-to-connect
fittings, recut the tubing, and replace the tubing in the push-to-
connect fittings.
13. Start ACWIN software by double clicking the ACWIN desktop icon.

Removing and Cleaning Fan Filter
The fan filter should be inspected weekly at a minimum. Inspect more

often depending on operating conditions. The following section
provides instructions to remove and clean the fan filter.

3. Remove the filter housing cover from the fan filter housing by
pulling it straight out. Refer to Figure 6-10.
Figure 6-10
Fan Filter
4. Remove fan filter.
5. Wash fan filter with warm soapy water and allow to air dry.
6. When dry, replace the fan filter in the fan filter housing.
7. To replace the filter housing cover, position the flat side of the
cover against the fan filter and then push it back into place.
8. Turn on power to the instrument.
9. Start ACWIN software by double clicking the ACWIN desktop icon.

Polishing Bucket and Baffle
The bucket and baffle should be polished when discoloration occurs or

annually at a minimum.
1. From Diagnostics and select the Lift Mechanism tab.

2. Click the arrow for "Go To Position," select Vessel Raised, and
then click Go.
5. To remove the top casting cover, first loosen and remove the 4
screws. Refer to Figure 6-11.
Figure 6-11
Top Casting Cover Screws
6. Pull the top casting cover forward and then remove from the lift
arm.
7. Disconnect white c-flex tubing for the pneumatic lead, leaving the
barb fitting on the lift-arm side of the tubing. Refer to Figure
6-12.
Figure 6-12
Pneumatic Lead

8. Use a small screwdriver to remove the 2 back electrode leads on
the lift arm. Refer to Figure 6-13.
Figure 6-13
Back Electrode Leads
9. Use a torx wrench to loosen the 3 lift-arm screws and remove the
lift arm panel. Refer to Figure 6-13.
bolts that secure the front panel in place. Refer to Figure 6-14.
11. Once the bolts are loosened, pull the panel toward the front of the
instrument.
Figure 6-14
Bolts for Front Panel
All instrument panels are heavy. Use caution when removing

them to avoid injury.

12. Remove side panels by using a Phillips screwdriver to loosen the
screws that secure the panels in place and then by pulling the
panels from the bottom of the AC600. Each side panel has one
screw in the front and one screw in the rear that secure it. Refer
to Figure 6-15.
13. Remove top panel by using a Phillips screwdriver to loosen the
screw that secures the panel in place and then lift the panel from
the AC600. Refer to Figure 6-15.
Figure 6-15
Screw Locations for Side and Top Panels
14. Obtain a quick-disconnect drain hose.
15. Place the open end of the quick-disconnect hose into an empty
five-gallon container and attach the quick-disconnect end to the
drain hose fitting. The drain hose will remove the water from the
outside of the bucket.
16. Loosen the upper setscrew on the stirring motor gearbox. Refer
to Figure 6-17, page 629.
Figure 6-16
Stirring Motor Gear Box

Figure 6-17
Upper Setscrew
17. Remove 2 screws on the stirring motor gear box and remove gear
box.
18. Disconnect the thermistor leads for the bucket. Refer to Figure
6-18.
Figure 6-18
Thermistor Leads
19. Siphon the water from inside the bucket.
20. Remove the bucket by rotating in a counterclockwise direction
less than 1/8 of a turn.
21. Check the three bucket anodes for corrosion as explained in the
Periodic Maintenance Schedule. When the bucket anodes require
replacement, they simply unscrew from the support rod. If they
are severely corroded, it might be necessary to use pliers to
unscrew them.

22. Use steel wool to polish the entire surface of the bucket and baffle
until all debris and smudges have been removed.
23. While placing bucket into jacket, align the bucket with the 3
alignment points in the jacket and then rotate clockwise 1/8 turn
to secure.
24. Replace the lift arm panel and place the 3 lift-arm screws in
position but do not tighten them. Refer to Figure 6-19.
Figure 6-19
Lift-Arm Screws
25. In order to properly align the bucket, replace it as follows:
A. Turn on power to the instrument.
B. Start the ACWIN software by double clicking the ACWIN
desktop icon.
C. Add water to the external chiller to fill AC600.
D. In the software, click Diagnostics and then select the Lift
Mechanism tab.
E. On the Lift Mechanism tab, select Analyze Position and then
click Go.
F. As the bucket lid is descending, guide bucket lid onto bucket.
G. In the software, click Diagnostics and then select the
Solenoids/Switches tab.
H. On the Solenoids/Switches tab, select the Inflate Bucket Seal
check box.
I. Tighten the three lift-arm screws on the panel. Refer to
Figure 6-19.
J. On the Solenoids/Switches tab, clear the Inflate Bucket Seal
check box.
26. Reconnect the thermistor leads for the bucket. Refer to Figure
6-18, page 629.
27. Replace gear box and then secure by tightening the 2 screws.
28. Tighten setscrew on the upper motor stirring shaft coupling. Refer
to Figure 6-17, page 629.
29. Replace side and front panels.
30. Replace 2 small back electrode leads on the lift arm and tighten
with a small screwdriver. Refer to Figure 6-19.
31. Reattach c-flex tubing to the pneumatic lead. Refer to Figure
6-12.

32. Replace top casting cover by aligning the boss fittings on the top
casting cover with the corresponding top casting cover screw tabs
on the lift arm. Refer to Figure 6-29.
33. Replace the 4 screws in the top casting cover and carefully
tighten, stopping at the first sign of resistance. The top casting
cover screw tabs should stay in a parallel position to the lift arm.
Do not overtighten the 4 screws in the top casting cover.
34. Keep the bucket lid raised as the system is filled.

35. Wait for the bucket lid to raise fully.
B. Select the Jacket Fill check box. The jacket will passively fill
to the correct level. This will take a few minutes.
37. Refill the system with distilled water by adding water as
necessary to the external chiller to prevent the reservoir from
running dry. Once the jacket reaches the correct level, the jacket
water level low will indicate that the water level is OK.

38. After filling the instrument with water, use a soft brush to remove
any air bubbles that form on the walls of the bucket and jacket.
The bubbles must be removed before analysis in order to prevent
any variation in the volume of water trapped in the bucket during
analysis.
39. To begin analyzing samples, refer to Preparing for Analysis, page

54.

Lubricating Screw for Lift-Arm Mechanism
The screw on the lift-arm mechanism should be lubricated every six

months.
1. Remove the oxygen combustion vessel if installed.

2. Use power switch on back panel to turn off power to instrument.
Figure 6-20
Power Switch
3. To remove the top casting cover, first loosen and remove the 4
screws. Refer to Figure 6-21.
Figure 6-21
Top Casting Cover Screws

4. Pull the top casting cover forward and then remove from the lift
arm.
5. Disconnect white c-flex tubing for the pneumatic lead. Refer to
Figure 6-22.
Figure 6-22
Pneumatic Lead
6. Use a small screwdriver to remove the 2 back electrode leads.
Figure 6-23
Back Electrode Leads
7. Loosen and remove the 3 screws on the lift arm panel. Refer to
Figure 6-23.
8. Remove the lift arm.
bolts that secure the front panel in place, and then by pulling the
panel toward the front of the instrument. (The bolts are located
underneath and to the sides of the panel.) Refer to Figure 6-24,
page 634.

Figure 6-24
Front Panel Bolts
All instrument panels are heavy. Use caution when removing

them to avoid injury.
10. Remove side panels by using a Phillips screwdriver to loosen the

screws that secure the panels in place and then by pulling the
panels from the bottom of the AC600. Each side panel has one
screw in the front and one screw in the rear that secure it. Refer
to Figure 6-25.
11. Remove top panel by using a Phillips screwdriver to loosen the
screw that secures the panel in place and then by lifting the panel
from the AC600. Refer to Figure 6-25.
Figure 6-25
Screw Locations for Side and Top Panels

12. Use a torx wrench to loosen 3 screws that attach the plate and
molding to the lift-arm mechanism. Refer to Figure 6-26.
Figure 6-26
Lift-Arm Plate and Molding
13. Remove the screws, plate, and molding from the lift arm
mechanism.
14. Remove the side casing from around the lift-arm mechanism.

Figure 6-27
Side Casing for Lift Arm
15. Rub lubricant 2-3 times along the length of the screw until it is
thoroughly coated with a thin layer. Refer to Figure 10-12.
16. Replace side casing on lift-arm mechanism. Refer to Figure 6-27.
17. Replace the plate and molding and tighten the screws removed in
step 13, page 635.
18. Replace the lift arm.
19. Place the 3 screws in position on the lift arm panel but do not
tighten them. Refer to Figure 6-28.
Figure 6-28
Lift-Arm Screws
20. From the Maintenance menu, click Dock Wizard, and follow the
instructions that display in the Loader Dock Wizard dialog box to
correctly engage the lift-arm mechanism and loader motor.
21. In the software, click Diagnostics and then select the Lift
Mechanism tab.
22. On the Lift Mechanism tab, select Analyze Position and then click
Go.

23. As the bucket lid is descending, guide bucket lid onto bucket.
24. In the software, click Diagnostics and then select the
25. On the Solenoids/Switches tab, select the Inflate Bucket Seal
check box.
26. Tighten the 3 screws on the lift arm panel. Refer to Figure 6-28.
27. On the Solenoids/Switches tab, clear the Inflate Bucket Seal
check box.
28. Use small screwdriver to reattach the 2 back electrode leads.
29. Reconnect c-flex pneumatic lead. Refer to Figure 6-22.
30. Replace top casting cover by aligning the boss fittings on the top
casting cover with the corresponding top casting cover screw tabs
fittings on the lift arm. Refer to Figure 6-29.
Figure 6-29
Top Casting Cover Screw Tabs
31. Replace the 4 screws in the top casting cover and carefully
tighten, stopping at the first sign of resistance. The top casting
cover screw tabs should stay in a parallel position to the lift arm.
Do not overtighten the 4 screws in the top casting cover.
32. Replace side and front panels.

33. To begin analyzing samples, refer to Preparing for Analysis, page
54.

Adjusting the Pressure Safety Release Valve
The following procedure explains how to adjust the pressure safety

release valve. For maintenance requirements, check the accuracy of
the pressure regulator on the oxygen tank regulator annually by
following the adjustment procedure explained below.
1. Verify the oxygen tank regulator valve is open. If the tank

pressure is above approximately 500 psi (34.47 bar) when
opening the tank regulator knob, a hissing noise will emit from
the pressure safety release valve.
2. Insert a 1/8" Allen wrench into the valve locking nut.
3. Use an open-ended wrench to just loosen the valve locking nut.
Do not completely loosen or remove the valve locking nut.
Figure 6-30
Pressure Safety Valve
4. Use the 1/8" Allen wrench to adjust the set screw inside the valve
locking nut until the pressure gauge reads approximately 500 psi
(34.47 bar).
5. When the target pressure of 500 psi (34.47 bar) is reached, with
the Allen wrench still in the hole of the valve locking nut, use the
open-ended wrench to tighten the valve locking nut.
6. Use the adjusting screw to set the pressure regulator to 450 psi
(31.03 bar).

Replacing Ceramic Washer
Refer to Figure 10-8 for an illustration of the ceramic washer.
Care should be taken to avoid overtightening the electrode.

Overtightening the electrode may damage the ceramic
washer.


7 Theory of Operation
Theory of Operation....................................................................... 72
Critical Calculations ....................................................................... 73
Energy and Temperature Calculations ......................................... 73
TruSpeed Equation for Energy .............................................. 73
Delta T Equation for Temperature Change .............................. 73
Calibration .............................................................................. 74
TruSpeed Equation for Calibration ......................................... 74
Delta T Equation for Calibration............................................. 74
Gross Calorific Value Calculation, Qvad ......................................... 75
TruSpeed Calculation ........................................................... 75
DeltaT Calculation ............................................................... 75
Calculations and Corrections ...................................................... 76
e1 Nitrogen Correction ......................................................... 77
e2 Fuse Correction .............................................................. 78
e3 Sulfur Correction ............................................................ 79
e4 Spike or Tape Correction ............................................... 710
e5 Uncombusted Carbon Correction ..................................... 710
Calculation to other Bases ....................................................... 711
ASTM D3180-07 ................................................................ 711
Theory of Operation AC600 71

Theory of Operation
The LECO AC600 semi-automatic calorimeter is a Windows based

instrument, developed to measure the calorific content of various
organic materials such as coal, coke and fuel oil.
The calorific value of a sample is determined by the combustion of the

sample in a controlled environment. The heat released is proportional
to the calorific value of the substance.
In the AC600, the sample is placed in a high-pressure oxygenated

environment called an oxygen combustion vessel. The oxygen
combustion vessel is surrounded by water, and the sample is ignited.
The temperature of the water is measured by an electrical
thermometer with a resolution of 0.0001 of a degree. During analysis,
the oxygen combustion vessel is lowered into a water bath known as a
bucket. The bucket is sealed using an inflatable bladder. Surrounding
the bucket is the region known as the jacket. The water temperature
in the jacket is controlled very accurately at a set temperature.
In this Isoperibolic system, there may be some energy exchange

between the outside environment, jacket, and the water inside the
bucket. The design of the AC600 minimizes the heat transfer between
the bucket and jacket. Two options for analyzing data are available. A
simple temperature difference may be chosen by the user, in which
calorific values will be determined by simple maximum temperature
rise of the bucket. No corrections for energy transfer into or out of the
bucket by environmental forces are taken into account. Secondly, a
user may choose a thermodynamic model that has been developed to
model heat exchange between the bucket and jacket. The model
takes into account heat capacities of system components, and heat
exchange rates. The thermodynamic model will be discussed in
following sections.
The microprocessor measures the temperature of the water inside the

bucket and jacket every second. The analog to digital converter
converts this output into a binary number that is stored in memory.
The temperature data is compiled by the computer, and results
generated based on the choice of data analysis, and corrected for
spiking if necessary. Corrections can also be made for nitrogen,
sulfur, hydrogen, moisture, and ash content of the sample. A titration
of the contents of the oxygen combustion vessel may then be made
and the results recalculated if the sulfur or nitrogen values were
entered incorrectly.
72 AC600 Theory of Operation

Critical Calculations
Energy and Temperature Calculations

The calculation modes available on the AC600 for determination of
gross calorific values are identified as TruSpeed and Delta T.
TruSpeed is a calculation mode used to improve analysis speed and

precision.
TruSpeed Equation for Energy
MainTime
ETS = K vb * [Tv (n) Tb (n)] + C v * [Tv (n + 1) Tv (n)]
n =0
Where:
ETS: Calculated energy of sample based on thermodynamic model of
the calorimeter (J)
Tv(n): Calculated temperature of the combustion vessel at time interval
n (C)
Tb(n): Measured temperature of the bucket at time interval n (C)
Kvb(n): Thermal conductance of the combustion vessel to the bucket
(J/C)
Cv(n): Heat capacity of the vessel (J/C)
Delta T Equation for Temperature Change
Tmax = Tmax Tmin (C )
Where:
Tmax: The maximum temperature recorded during the main time
period (C)
Tmin: The minimum temperature recorded during the main time
period (C)

Calibration
The results for the selected standard(s) are averaged to determine the
calibration factor.
Calibration factors are stored independently by method and by vessel

number.
TruSpeed Equation for Calibration

n
( mi H STD ) + e1i + e2 i + e4 i + e5i

i =1 ETS ( i )
K=
n
Delta T Equation for Calibration

n
( mi H STD ) + e1i + e2 i + e4 i + e5i

i =1 Tmax(i )
E=
n
Where:
K: Average TruSpeed calibration factor (unitless)
E Average heat capacity of the calorimeter (J/C, MJ/C, cal/C, or
Btu/C). This is the displayed calibration value for the Delta T
calculation mode.
HSTD: Heat of combustion for the selected standard (J/g, MJ/kg, Btu/lb, or
cal/g)
m i: Mass of sample for analysis i (g)
e1i: Nitrogen correction for analysis i (J, MJ, Btu, or cal)
e2i: Fuse correction for analysis i (J, MJ, Btu, or cal)
e4i: Spike Correction for analysis i (J, MJ, Btu, or cal)
e5i: Uncombusted carbon correction for analysis i (J, MJ, Btu, cal)
ETS(i): Calculated energy of sample i based on the thermodynamic model of
the calorimeter (J, MJ, Btu, or cal)
Tmax(i): Maximum change in temperature recorded during the main time
period (C)
n: Number of standard analyses included to determine average
calibration factor

Gross Calorific Value Calculation, Qvad
The Gross Calorific value is calculated and reported at constant volume
on an as-determined basis.
TruSpeed Calculation
( K ETS ) e1 e2 e3 e4 e5
Qvad =
m
DeltaT Calculation
( E * Tmax ) e1 e2 e3 e4 e5
Qvad =
m
Where:
Qgross: Gross calorific value (J/g, MJ/kg, Btu/lb, or cal/g)

e1: Correction for the energy of formation of nitric acid (J, MJ, Btu, or
cal)
e2: Correction for the energy of fuse wire (J, MJ, Btu, or cal)
e3: Correction for the energy of formation of sulfuric acid (J, MJ, Btu, or
cal)
e4: Correction for the heat of combustion for the spike material (J, MJ,
Btu, or cal)
e5: Uncombusted carbon correction (J, MJ, Btu, cal)
m: Sample weight (g)
E: Calculated energy of sample based on the thermodynamic model of
the calorimeter (J/C, MJ/C, cal/C, or Btu/C)
Tmax: Maximum change in temperature recorded during the main time
period (C)
ETS(i): Calculated energy of sample i based on the thermodynamic model of
the calorimeter (J, MJ, Btu, or cal)
K: Average TruSpeed calibration factor (unitless)
The ACWIN software always displays sample mass in grams
regardless of which units are selected from the Configuration
menu/System Tab. Internal corrections are used to correct the
sample mass for the result units of MJ/kg or Btu/lb.

Calculations and Corrections
Correction factors for the following calculations and corrections have
been included in the AC600 for the formation of nitric acid, sulfuric
acid, combustion of the fuse, combustion of the spike, and
uncombusted carbon.

by Bomb Calorimeter
by Bomb Calorimeter (Precision Method)
and Ash Value of Waste Materials
Value of Coal and Coke
ISO 1928:1995(E) Solid Mineral Fuels- Determination of
Gross Calorific Value by the Bomb
Calorimetric Method, and Calculation of
the Net Calorific Value
AS 1038.5-1998 Coal and Coke- Analysis and Testing-
Gross Calorific Value
DIN 51900 Determination of the Gross Calorific
Value by the Bomb Calorimeter and
Calculation of the Net Calorific Value
(General Information, Basic Apparatus,
Basic Methods)
BS1016-105:1992 Methods for Analysis and Testing of Coal
and Coke. Determination of Gross
Calorific Value

e1 Nitrogen Correction
HN (J/ml) HN (MJ/ml) HN HN e1
(cal/ml) (Btu/ml)
ASTM D240-02 5.0 5.0x10-6 1.19 0.004739 HN*v
ASTM D4809-06 5.0 5.0x10-6 1.19 0.004739 HN*v
-6
ASTM D5468-02 4.1868 4.1868x10 1.00 0.003968 HN*v
-6
ASTM D5865-07 4.1868 4.1868x10 1.00 0.003968 HN*v
ISO 1928:1995(E) 6.0 6.0X10-6 1.43 0.005687 HN*(20-10*V1c1)
-6
AS1038.5-1998 6.0 6.0X10 1.43 0.005687 HN*(20-10*V1c1)
-6
DIN 51900 6.0 6.0X10 1.43 0.005687 HN*(20-10*V1c1)
BS1016-105:1992 6.0 6.0X10-6 1.43 0.005687 HN*(20-10*V1c1)
Thermochemical correction for the formation of nitric acid (J, MJ, Btu,
or cal)
Where,
v: Volume of titrant used (ml). Software refers to this as "nitrogen."

HN: Heat of formation of nitric acid (J/ml, MJ/ml, cal/ml, or Btu/ml). Software refers
to this as "titrant energy value." Refer to Titrant Energy Value, page 511.
V1 Volume of hydrochloric acid solution (ml)
c1 Concentration of hydrochloric acid solution (M)
The values for HN are for nitric acid formed from liquid water and
gaseous nitrogen and oxygen. See specific standards for details.

e2 Fuse Correction
Thermochemical correction for the combustion of the fuse wire or
cotton string (J, MJ, cal, Btu)
e2 = H F L
Where:
L: Length of combusted fuse (cm)

HF: Heat of combustion of the fuse wire or cotton string (J/cm, MJ/cm, cal/cm,
cal/cm, or Btu/cm)
HF (J/cm) HF (MJ/ cm) HF (cal/ cm) HF (Btu/

cm)
Wire Fuse 9.60 9.60x10-6 2.29 0.00910
String Fuse 6.60 6.60x10-6 1.58 0.00626

e3 Sulfur Correction
Thermochemical correction for the formation of sulfuric acid (J, MJ, cal,
or Btu)
For %S,
e3 = m H S S (%)
Where:
m: Mass of sample (g)

S%: Sulfur concentration in weight percent (%)
HS: Heat of formation of sulfuric acid (J/g, MJ/g, cal/g, or Btu/g)
HS (J/g) HS (MJ/g) HS (cal/g) Hs (Btu/lb)

ASTM D240-02 58.0 0.0580 13.85 24.94
ASTM D4809-06 58.6 0.0586 14.00 25.19
ASTM D5468-02 55.2 0.0552 13.18 23.73
ASTM D5865-07 55.18 0.05518 13.18 23.72
ISO 1928:1995(E) 94.1 0.0941 22.48 40.46
AS1038.5-1998 95 0.0950 22.69 40.84
DIN 51900 94.1 0.0941 22.48 40.46
For titrations according to ISO 1928:1995(E), BS1016-105:1992, DIN

51900, and AS1038.5-1998,
e3 = H s (10 *V1 * c1 + 20 *V2 c2 20)

Where:
V1: Volume of hydrochloric acid solution used

(ml)
V2: Volume of barium hydroxide solution
used (ml)
c1: Concentration of hydrochloric acid (M)
c2: Concentration of barium hydroxide (M)
Hs (J/ml) Hs (MJ/ml) Hs (cal/ml) Hs (Btu/ml)

All Standards 15.1 .0151 3.61 6.49
e4 Spike or Tape Correction

Thermochemical correction for the combustion of spike or tape (J, MJ,
cal, or Btu)
e4 = H SP m SP
Where:
HSP: Heat of combustion of spike or tape as specified by operator (J/g, MJ/g,

cal/g, or Btu/lb)
mSP: Mass of spike or tape (g)
e5 Uncombusted Carbon Correction

Thermochemical correction for uncombusted carbon as determined by
loss of mass on ignition of the sample residue from the crucible
e5 = H c mc
Hc(J/g) Hc(MJ/g) Hc(cal/g) Hc(Btu/lb)

AS1038.5-1998 33.5 0.0335 8.001 14.40
BS1016-105:1992 33.5 0.0335 8.001 14.40
Where:
Hc: Heat of combustion of uncombusted carbon (J/g, MJ/kg, cal/g, or Btu/g)

mc: Mass of uncombusted carbon (g)

Calculation to other Bases
For convenience, a set of default User Defined Fields have been
defined to convert the result from an As-Determined basis.
Additional User Defined Fields can be created as necessary to

accommodate other corrections or basis conversions. Refer to User
Defined Fields on page 445 for more information.
ASTM D3180-07
As-Received Basis
100 M ar
Qvar = Qvad *
100 M ad
Dry Basis
100
Qvd = Qvad *
100 M ad
Dry Ash-free Basis
100
Qvdaf = Qvad *
100 M ad Aad
Where:
Qvad: Gross calorific value as determined (J, MJ, cal, or Btu)

Mar: Moisture as-received basis (%)
Mad: Moisture as-determined basis (%)
Aad: Percent ash


8 Diagnostics
Monitoring Ambient Chart............................................................... 82
Ambient Nominal Values ........................................................... 83
Ambient Graph Menu ................................................................ 84
Customize Graph Lines ............................................................. 85
Customize Ambient Column Display ............................................ 87
Solenoids and Switches .................................................................. 88
Performing an Igniter Test ......................................................... 89
Using Offset Thermistors .............................................................. 810
Backup Offset Thermistors ...................................................... 811
Restore Offset Thermistors ...................................................... 811
Lift Mechanism ............................................................................ 812
Network ..................................................................................... 814
Diagnostics AC600 81
Monitoring Ambient Chart
Use the Ambient Chart to monitor instrument parameters during

operation or service of the instrument.
1. Click on the Small Buttons Toolbar or click Diagnostics on the

menu bar and then click Chart to display the Ambient Monitor
Chart. Refer to Small Buttons, page 413, for further information.
2. To display the parameter value in the graph, select the check box
to the left of the desired parameter. More than one parameter
can be displayed by holding down Ctrl on the keyboard and then
selecting check boxes. The software will mark any values that are
out of range with a yellow exclamation icon ( ) in the Ambient
screen and ( ) on the status bar.
The parameter value is displayed on the vertical axis and the time
[minutes] is displayed on the horizontal axis. The box in the lower
left corner of the graph displays the number of hours since the
instrument was turned on or the graph reset. The hours
automatically reset to zero after 24 hours.
To reset, restore, zoom in, zoom out, and set the graph
range, right-click inside the graph to access the menu. Refer
to Ambient Graph Menu, page 84.
To reset the maximum and minimum parameter values in the
chart and time axis on the graph, click Reset Chart.
To print the parameter values, click Print.
82 AC600 Diagnostics
Ambient Nominal Values
Parameter Definition Nominal Value
Temperature as
Bucket Temperature As defined in the ACWIN
measured through the
(C) software.
thermistor.
Temperature as
Jacket Temperature As defined in the ACWIN
measured through the
(C) software.
thermistor
.1+.02v without vessel; 0 with
The voltage applied to vessel attached.
Ignitor (volts)
the ignition current. When fired: Cotton 1.8 +.1
Wire 12 + .5
The measured AC
voltage of the 90-127
Line Voltage (volts)
incoming power 180-260
source.
The internal
Cabinet
temperature of the 15-40C
Temperature (C)
instrument.
The frequency of the 50 hz + 2
Line Frequency (Hz) incoming power
source. 60 hz + 2
15% or 25% + 3% with flow

The percentage of time knob properly adjusted and
Duty Cycle that the heater is stable bucket temperature.
operating. Refer to Duty Cycle, page 9
41.
Ambient Graph Menu
Use the commands on the plot dialog box to reset, restore, zoom in,
zoom out, and set the plot range. The parameter value is displayed on
the vertical axis and the time is displayed on the horizontal axis.
To access the graph menu, right click in the ambient graph. The
ambient graph menu will display.
Reset - Click Reset, and then select either Time or Graph.

Select Time to move the zero point on the x-axis. Select
Graph to begin plotting at zero.
Zoom In - Click Zoom In to increase the magnification of
the ambient graph. Each time Zoom In is clicked, the
magnification of the ambient graph is increased by one
level. Zoom will display in the upper corner of the plot, and
the area being magnified is indicated by a red square as
illustrated below. The mouse can also be used to zoom in
on an area of the ambient plot. Place the mouse cursor on
the area to magnify. Click and drag the mouse around the
location to zoom. A dotted rectangle displays the section
selected. When the mouse is released, the selected
section magnifies.
Zoom Out - Once the magnification of the ambient plot has
been increased, click Zoom Out to reduce the
magnification by one level. Zoom Out can be clicked until
Zoom no longer displays in the graph. Each click decreases
the magnification by one level.
Restore - After zooming in several times, click Restore to
return the plot to the original starting zoom level.
Range - Click Range to determine the boundaries of the
ambient plot. Click the Automatic checkbox, and the
software will determine the range. To enter the range
manually, unclick the Automatic checkbox, and enter a
value in the lower bound and the upper bound.
Customize Graph Lines
The precision, line width, and line color for each ambient that displays
in the Ambient Chart can be customized.
1. Double-click on the name desired ambient. The Properties dialog

box will display.
2. Determine the precision by clicking the arrows until desired

precision is achieved. Click to decrease precision. Click
to increase precision.
3. Use the pen width to determine the thickness of the line that
displays in the chart. Click to decrease line thickness. Click
to increase line thickness.
4. Determine the color of the line by clicking the button next to the
pen width arrows. The Color dialog box will display.
5. Select the desired color for the background by selecting a basic

color or by adding a custom color.
6. To select a basic color, click the desired color and then click OK.
7. To select a custom color:
A. Click in one of the empty custom color selection boxes.
B. Click Define Custom Color. The Color Dialog Box expands to
display the Custom Color Graph.
C. Select the desired color range from the custom color graph.
The range that falls under the selector ( ) will appear in
the custom color selection grid.
D. Select the specific color from the custom color selection grid.
E. Click Add to Custom Colors.
F. Click OK. The color will appear in the custom color selection
box as a new color choice.
8. To customize another ambient, click the arrow under Ambient in
the Properties dialog box, and select the desired ambient from
the list. Repeat steps 2-7.
9. Click OK. The selected precision, pen width, and color choice will
display in the chart for all selected ambients. The checkbox for
each ambient will also display the selected color choice.
Customize Ambient Column Display
The following steps explain how to determine the columns that display
in the ambient monitor.
1. Click on a column heading in the ambient monitor
2. In the dialog box that displays, click in the desired checkboxes.

Click the Log Ambients checkbox to save the ambient data to a
file.
Click the Scale Factor checkbox to show the scale factor.
Click the Min/Max checkbox to display the minimum value read
and maximum value read.
Click View Min/Max to display the minimum current view and
maximum current view.
Solenoids and Switches
Use the Solenoids and Switches tab when adjusting or servicing the
instrument to activate and deactivate the solenoid valves and to
monitor the status of the solenoid valves and switches. Refer to the
Cabinet Schematics, page 111.
1. Click on the Small Buttons Toolbar or click Diagnostics on the

menu bar and then click Solenoids and Switches. If the small
buttons toolbar is not displayed, refer to Small Buttons, page
413, for further information.
2. For the solenoid valves, select the check box of a solenoid valve
to open a valve; clear the check box of a solenoid valve to close
it. The switch states display for diagnostic information; these
states cannot be changed in the software.
For Heater Control Active, select the check box to start the
Jacket Fill (if low), coolant, water, and pump as a means to
regulate the water temperature.
For Instrument Button Disabled, select the check box to
disable the analysis button on the front panel. When this check
box is selected, an analysis can only be initiated through the
software.
For Stir, select the check box to turn on the stirrer to its
analyzing speed, which is 850 + 10 rpm as measured on the
stirring shaft.
For Stir Slow, select the check box to turn on the stirrer to its
slow speed, which is 500 + 10 rpm as measured on the stirring
shaft. The software automatically selects this speed when
lowering the vessel to the equilibrate position during an analysis
to prevent oxygen from being trapped by the vessel.
Click Print to print the solenoid and switch states.
Performing an Igniter Test

An igniter test provides the means to verify that the fixed wire fuse
was correctly installed. This test should be performed after installation
of a new cotton fuse wire.
Do not perform an igniter test under the following

conditions:
When the oxygen combustion vessel is charged, loaded with
a sample, and in the up position.
When the oxygen combustion vessel is not present, and the
instrument is in the down position (i.e., when the igniter
would potentially be underwater).
1. From Diagnostics and select the Lift Mechanism tab.

2. Click the arrow for "Go To Position," select Vessel Raised, and
then click Go.
3. Install vessel lid without the body.
4. From Diagnostics on the Menu bar, click Solenoids/Switches. The
Igniter Test parameters will appear on the Solenoids/Switches
tab.
5. For Cycles, enter 3 (recommended) to indicate the number of
igniter test cycles for the igniter fuse.
6. Click Start Igniter Test.
While the igniter test is running, you can click Stop Igniter
Test to stop the test.
A counter tracks the number of igniter test cycles that have
been performed. Click Reset Counter to set the counter back
to zero.
7. If the wire is correctly installed, the wire will glow bright orange
while firing.
Using Offset Thermistors
Use the Offset Thermistor tab to normalize the response of the bucket
and jacket thermistors to each other. If the offset values are lost due
to a system problem or the thermistors or circuit cards are replaced,
this procedure should be performed before samples are analyzed.
Contact LECO Service before performing offset thermistors.
The previous slope and offset values can be restored by clicking Reset
to Previous. The original offset values can be restored by clicking Reset
to Factory Defaults.
1. From the Diagnostics menu, click Offset Thermistors.
2. To normalize both thermistors, click Calculate Offsets. The dialog

box displays the Calculating Offsets message along with an
Abort button.
The software will start at the system configuration temperature
setting, stabilize, collect thermistor information and go to that
temperature + 3 degrees, stabilize, collect thermistor
information, and then calculate the slopes and offsets.
Once the offset thermistor procedure is started, clicking Abort is the
only way to stop it.
3. When the procedure is finished, a message will appear.
4. To print a copy of the offset thermistors, click Print.
5. The procedure should be saved in a backup file and then restored
if necessary. Refer to Backup Offset Thermistors, below, and
Restore Thermistor Offset, page 811.

Backup Offset Thermistors
Backup Offset Thermistors permits the operator to save offset
thermistor parameter values in a designated file. This file can be
accessed at a later time to restore offset thermistor values that may
have been lost or changed. It is not necessary to backup the offset
thermistor values to save them; the instrument will automatically save
them in a system file.
1. From the Diagnostics menu, click the Offset Thermistor tab. The
Offset Thermistor dialog box will appear.
2. Click Backup to create a backup file of the offset thermistor
parameter values.
3. In the Save As dialog box, select the folder location.
4. Enter a file name and click Save.
Restore Offset Thermistors

1. From the Diagnostics menu, click the Offset Thermistor tab.
2. Click Restore to load the offset thermistor values that have been
saved in a backup file. The Open dialog box will appear.
3. Select the folder location and backup file to restore.
4. Click Open to load the offset thermistor values from the selected
backup file.

Lift Mechanism
The Lift Mechanism tab is typically only used by LECO Service for
operation and service of the lift mechanism motor.
Position indicates the current physical location of the vessel.
For Go to Position, click the arrow, select a position from the list, and
then click Go. Refer to
Figure 10-28 for an illustration of the lift motor positions.

For Move, enter a value in mm to check the operation of the lift
motor.
For Command, enter motor-specific commands and then click Send to

transmit the command to the lift motor. Command is used by LECO
Service to check the operation of the lift motor controller.
The Send with Check Sum check box should always be selected.
For Auto Find Home, always leave the check box selected. Upon
startup, the ACWin software automatically finds the home position.
The Download button is used when running software with a new lift
mechanism motor. Clicking Download will download the required
software program to operate the motor.
The DL Export button exports the default motor program to a text

file.
The DL Custom button downloads a program from a text file. This

button is useful when changes to motor positions and parameters are
required.
Read Properties displays information about the motor properties as

shown below.

Network
The Network dialog box identifies the version of firmware and the
operational status of the peripheral devices. Also, the network can be
reset, the network power can be turned off, and the firmware can be
upgraded.
Information on the Network dialog box should only be used for

reference purposes such as to view the versions of the boards and of
the firmware. Nothing on the Network dialog box should be changed
except by LECO Service.

9 Service
Illustrations .................................................................................. 92
Installing LECO Software ................................................................ 93
Required Settings for LECO Software .......................................... 93
Operating System (OS) Requirements ................................... 93
OS User Permission Requirements ......................................... 93
Data File Permissions ........................................................... 94
Antivirus Software ............................................................... 94
Control Panel Settings ......................................................... 94
Software Installation Procedure ................................................. 95
Configuring the Ethernet Adapter .................................................. 911
Windows 7 ............................................................................ 911
Windows Vista ....................................................................... 915
Windows XP........................................................................... 917
Configuring Firewall Settings ........................................................ 920
Configuring DHCPLite ................................................................... 921
Connecting Instrument to a Network That Uses 10.10.10.x
Addresses ........................................................................ 921
Changing the IP Address for LECO Instruments in Windows .... 923
Registering Software ................................................................... 925
Troubleshooting Software Registration ...................................... 927
Submitting Registration Information to LECO ............................. 927
Adding an Option or Changing Customer Name .......................... 929
Troubleshooting Copy Protection Key ............................................. 931
Copy Protection Key Error Messages ......................................... 931
General Troubleshooting .............................................................. 932
Jacket Temperature Troubleshooting ............................................. 934
Fault Conditions .......................................................................... 936
Software Error Codes ................................................................... 938
Aligning Bucket Lid ...................................................................... 939
Using the Dock Wizard ................................................................. 940
Adjusting Duty Cycle ................................................................... 941
Service AC600 91
Illustrations
Figure 9-1 Jacket Temperature for Single Analysis ..............................934

Figure 9-2 Jacket Temperature for Series of Analyses .........................935
Figure 9-3 Lift-Arm Screws ..............................................................939
Figure 9-4 Duty Cycle Adjustment Knob ............................................941
92 AC600 Service
Installing LECO Software
The following section explains the required settings, below, and the
installation procedure, page 95, for LECO software. Additional
information can be found in Configuring the Ethernet Adaptor, page 9
11, Configuring Firewall Settings, page 920, Configuring DHCPLite,
page 921, and Registering the Software, page 925.
Required Settings for LECO Software
Operating System (OS) Requirements

The following table explains the minimum settings required for LECO
software. LECO recommends that the system always be updated to
correspond with the latest service packs available at
www.microsoft.com.
Windows OS Minimum Requirements

7 (32-bit or 64-bit,
None
64-bit preferred)
Vista (32-bit) None
XP (32-bit) SP2
*SP=Service Pack; **URP=Update Rollup; ***IE=Internet Explorer
OS User Permission Requirements

The following table shows the minimum permissions that a user must
have in the Microsoft Windows OS in order to perform certain tasks in
the software. Refer to User Permissions.
Task Minimum Permission

Using Software Standard User
Installing Software Administrator
Upgrading Software Administrator
Setting up Users Administrator
LECO Service Administrator
Service AC600 93
Data File Permissions
To use LECO software, read-write access is required for all the data
files. The proper permissions are automatically set up during the
software installation; however, if these permissions are ever changed,
file access errors can occur. The following table shows the data folders
that require read-write permissions.
Data Folder (including all

Windows OS subfolders/files) (Use the appropriate
drive letter, typically C.)
7, 64-bit ProgramData\LECO (hidden OS folder)
Vista ProgramData\LECO (hidden OS folder)
XP C:\Documents and Settings\All
Users\Application Data\LECO
Antivirus Software
LECO recommends that antivirus checking be turned off
for the files listed below to avoid interference with data
collection or storage.
Data Folder (including all

Windows OS subfolders/files) (Use the appropriate
drive letter, typically C.)
Vista ProgramData\LECO (hidden OS folder)
XP C:\Documents and Settings\All
Users\Application Data\LECO
Control Panel Settings

Control Panel Item Required Setting
Power Power Schemes Always On

Options Turn off Hard Disks Never
If Fast User Switching is
active (off by default on PCs
from LECO), close the LECO
User
Use Fast User Switching software in one account
Accounts
before switching to a
different account and trying
to run it there.
94 AC600 Service
Software Installation Procedure
The software must be started at least once on the administrative
level since the software must be able to access and modify the
registry.
Do not install the Copy Protection Key until after the software
has been installed.
1. Verify the instrument is turned off.

2. Turn on the computer tower.
3. Install the communications cable (typically Ethernet or USB) as
appropriate for the instrument.
4. For an Ethernet connection, configure the Ethernet adapter. Refer
to Configuring Ethernet Adapter, page 911.
5. Log in to the operating system as administrator.
6. Insert the software installation CD-ROM into the CD-ROM disk
drive (typically D).
7. Install the LECO DHCPlite software by clicking OK when the
following message appears. (If the LECO DHCPlite software is
already installed or not applicable, this message will not appear.)
8. If a version of Adobe Reader is already installed, refer to step 14.

If Adobe Reader is not installed, the following dialog box will
appear.
9. Select Yes. The following message box will appear to indicate

Adobe Reader is preparing for installation.
Service AC600 95
10. Determine the folder location for Adobe Reader. Select Next for
the default location, or select Browse, select a different location,
and then select Next.
96 AC600 Service
11. When the "Ready to Install Program" dialog box appears, click
Install.
12. When the "Setup Completed" dialog box appears, click Finish.
Service AC600 97
13. If the instrument software Welcome dialog box does not appear
A. Select the Start button in the lower left-hand corner.
B. Select Run. The Run dialog box is displayed.
C. Enter D:\Setup.exe and then select OK. (The letter D
indicates the location of the CD Rom drive. Typically this
drive is D, but the letter that is entered should correspond
with the CD-ROM drive on the computer's hard drive.)
14. At the instrument software Welcome dialog box, click Next.
15. Determine the folder location for the software. Select Next for the
default location, or select Browse, select a different location, and
then select Next.
98 AC600 Service
16. Select Next to install the software.
17. Once the software has installed successfully, select Finish. The
icon for the instrument software will appear on the desktop.
Service AC600 99
18. After installing the software, it may be necessary to restart the
system. If the following dialog box displays, select Yes to
immediately restart the system.
19. Turn on the instrument.

20. Turn on the gas supplies.
21. Double-click the desktop icon for the instrument software to start
the software.
If the Edit Registration dialog box appears, refer to Registering
the Software, page 925.
910 AC600 Service

Configuring the Ethernet Adapter
The following procedure is necessary for the proper operation of the

software with a Copy Protection Key and applies for computer systems
that are not supplied by LECO. For computers supplied by LECO, this
configuration has already been completed.
It is required that PCs used for running LECO applications be

configured with a separate Ethernet adapter dedicated for
communications with LECO instrumentation. (Connection to a
network would require a second Ethernet port.)
Windows 7
The following steps apply when using the Windows 7 operating
system.
1. Click on the Windows desktop and then click Control Panel.

2. Click Network and Sharing.
Service AC600 911

3. Click Change Adapter Settings.
4. Right-click on the name of the connection for the instrument and

rename it to LECO Hardware.
5. Right-click and select Properties.
912 AC600 Service

6. Clear all of the check boxes except Internet Protocol Version 4
(TCP/IPv4).
Service AC600 913

7. Highlight Internet Protocol Version 4 (TCP/IPv4) by clicking on it
and then select Properties.
914 AC600 Service

8. For IP address, enter 10 10 10 2, and for Subnet mask, enter 255
255 255 0. The remaining fields should be empty as shown
below.
9. Click OK.
Windows Vista
The following steps apply when using the Windows Vista operating
system.
1. Click on the Windows desktop.

2. From the Start Menu, select Control Panel.
3. From the Control Panel, select Network and Internet, click
Network and Sharing, and then select Manage Network
Connections.
4. On the Manage Network Connections tab, click on the connection
that will be used for the instrument.
Service AC600 915

5. Click on the name of the connection and rename it to LECO
Hardware.
6. Right-click and select Properties.

7. Clear all of the check boxes except Internet Protocol Version 4
(TCP/IPv4) as shown below.
8. Highlight Internet Protocol Version 4 (TCP/IPv4) by clicking on it

and then select Properties.
916 AC600 Service

9. For IP address, enter 10 10 10 2, and for Subnet mask, enter 255
255 255 0. The remaining fields should be empty as shown
below.
10. Click OK.
Windows XP
1. Determine if a network connection is installed as follows: click

Start on the Windows desktop, select Settings, Control Panel, and
then double-click on Network Connections. If a network
connection exists, it will appear in the Network Connections dialog
box. An example is displayed below.
2. If a network connection is not installed, install an Ethernet

adapter. Refer to the instructions supplied with the Ethernet
adapter for installation procedures.
3. Once the Ethernet adapter is installed and with the computer on,
select Start, Settings, Control Panel, and then double-click on
Network Connections.
4. Click on the name of the connection for the instrument and then
rename it to LECO Hardware.
Service AC600 917

5. Right-click on LECO Hardware and select Properties. The
Properties dialog box will appear.
6. Select the Internet Protocol (TCP/IP) check box. The other check
boxes should be cleared.
7. Click on Internet Protocol (TCP/IP) and select Properties. The
TCP/IP Properties dialog box will appear.
8. Enter the IP address as 10 10 10 2.
918 AC600 Service

9. Enter the Subnet Mask as 255 255 255 0.
10. Default Gateway, Preferred DNS Server and Alternate DNS Server
should be left blank.
11. Click OK.
12. Click OK again to save the settings.
Service AC600 919

Configuring Firewall Settings
When the LECO software is installed, it automatically configures the

Microsoft Windows firewall settings for the instrument software. (If the
Microsoft Windows firewall settings are ever changed, the easiest fix is
to reinstall the LECO software.)
The following steps apply only when a firewall program other than
Microsoft Windows is used.
1. If another firewall program is installed, search all folders and

subfolders in C:\Program Files\LECO and C:\Program
Files\Common Files\LECO folders and note the .exe files that are
found. For Windows 7, 64-bit OS systems, check C:\Program Files
(x86)\LECO.
These are the default locations; however, the default location may
vary if it was changed during the software installation.
2. Follow the instructions for the firewall program to grant these
.exe files permission in order to run the LECO software.
920 AC600 Service

Configuring DHCPLite
The following section explains the process for connecting an instrument

controlling PC to a corporate network.
When operating instrument with user permissions enabled and using
domain names for logging in instead of local PC accounts, you must
manually add each of the domain users to the list and assign them
the appropriate permissions.
Connecting Instrument to a Network That Uses

10.10.10.x Addresses
The PC that controls the LECO instrument(s) has a network board dedicated
to communicating with the LECO instrument(s). A unique IP address is
assigned to that board. Unique IP addresses are also assigned to each LECO
instrument connected to the PC. (One IP for the PC board and a different IP
for each of the LECO instruments the PC controls.) This is in addition to any
network connection to the corporate network which will have its own unique
IP address.
Make sure any non-LECO network traffic does NOT hinder data
collection from the LECO instrument.
If the corporate network uses 10.10.10.x values there could be a
conflict with the PC and/or LECO instrument(s) IP addresses.
To prevent conflict:
1. Close the LECO instrument software.
2. Stop the LECO DHCPLite Service in Task Manager.
3. Delete any existing .dhcpx files in C:\ProgramData\LECO\DHCPLite folder

(or equivalent on older operating systems).
4. Open the C:\ProgramData\LECO\DHCPLite\Config.xml file (or equivalent

on older operating systems).
Service AC600 921

ProgramData is a hidden folder.
5. The ServerAddress is the IP address that will be used for the network
card in the LECO instrument PC that is used for communicating with the
LECO instrument(s).
Change the ServerAddress to an IP value that doesnt conflict with

anything on the corporate network. The default value is 10.10.10.2.
The value 10.10.10.1 is reserved.
The IP of the board in the PC that connects to the LECO
instrument(s) must also be changed in Windows to match. Refer
to Changing the IP Address for LECO Instruments in Windows,
page 923.
The customer is responsible for ensuring that the IP addresses
used for the LECO instrument(s) and PC are never assigned to
anything else.
6. The AddressMin and AddressMax are the ending numbers for the IP
address that will be generated for the LECO instrument itself. One unique
IP will be created for each instrument, from within the #.#.#.min through
#.#.#.max range, where #.#.# is from the first three sections of the
ServerAddress.
Change the AddressMin and AddressMax values so that none of the

values from #.#.#.min to #.#.#.max conflict with any existing
#.#.#.x values being used on the corporate network. The default
value is 3 for min and 254 for max. Make sure the range is large
enough to ensure that every LECO instrument connected to the PC will
have its own unique address.
The customer is responsible for ensuring that the IP addresses used
for the LECO instrument(s) and PC are never assigned to anything
else.
Example
In the following, the PC that controls the LECO instrument(s) uses a
network card for instrument communication that has an IP address of
10.10.10.2 and the IP address that will be generated for the LECO
instrument(s) will be any address from 10.10.10.3 through
10.10.10.254. In this case, all addresses from 10.10.10.1 through
10.10.10.254 should NOT be used by the corporate network because
they are reserved for communication with the LECO instrument(s).
<configuration>
<add key="AddressMin" value="3"/>
<add key="AddressMax" value="254"/>
<add key="ServerAddress" value="10.10.10.2"/>
<add key="SubnetMask" value="255.255.255.0"/>
</configuration>
7. Save changes made to config.xml.
8. Start the LECO DHCPLite Service in Task Manager.
922 AC600 Service

9. Start the LECO instrument software.
Changing the IP Address for LECO Instruments in Windows
1. Click on the Windows desktop and then click Control Panel.

2. Click on Network and Sharing Center.
3. Click on the LECO Hardware connection to open it.
Make sure any virus scanning and security measures are turned off
for the LECO Hardware network connection.
4. A status window will come up. Click on the Properties button.
5. In the Properties window, highlight the Internet Protocol Version 4
(TCP/IPv4) line and click on Properties button.
Service AC600 923

6. Change the IP address to match the ServerAddress setting in config.xml.
924 AC600 Service

Registering Software
To register software for a new instrument and PC from LECO, insert

the copy protection key into a USB port. Refer to Troubleshooting Copy
Protection Key, page 931, for further information.
The following procedure applies when the license is being upgraded
due to the addition of new hardware or a new software version. The
software must be registered before it can be used. If a PC is not
purchased from LECO, refer to Submitting Registration Information to
LECO, page 927, and contact LECO Service for further information
about registering the instrument.
Do not insert the copy protection key into the USB port until
the LECO software is installed and the PC has been
rebooted.
1. Install Copy Protection Key into a USB port on the computer.

2. Double-click the software's desktop icon.
3. In the softwares main window, click Help and then click About.
The following dialog box appears:
Service AC600 925

4. Click Change. The Edit License dialog box will appear.
5. Registration information can be entered in two ways as explained

below. It is preferable to copy and paste the information to help
avoid errors.
Type in the registration information exactly as it appears.
If the upgrade information is received in an email from LECO,
copy and paste the registration information as explained in the
following steps.
A. In the email, highlight the information beginning with
<base64> ........ </base64> as shown below.
B. Copy the information by pressing at the same time Ctrl and

C on the keyboard.
C. On the Edit License dialog box, click Paste. (Do not press
CTRL and V on the keyboard.)
D. Click Save.
E. Click OK when the following dialog box appears:
926 AC600 Service

Troubleshooting Software Registration
Error Message Checks and Solutions
Verify all entries in the Edit License

dialog box exactly match the registration
information.
Check capitalization.
Invalid Registration Error Message Check that the product version is correct.
For example, the Product Version in the
Edit License dialog box will appear as 400
(no period) but on the Help/About dialog
box, the product version will appear as
4.00 (with a period).
Check that the registration number is
correct.
Check that the spacing between words is
accurate.
Submitting Registration Information to LECO

If the PC is not purchased from LECO, it may be necessary to submit
the registration information to LECO Service. Contact LECO Service to
assist you in the registration process. LECO Service will require your
company name, serial number, model number, and any options
purchased. The following section explains this procedure.
1. In the software, click Help and then select About.
2. On the About dialog box, click Change.
Service AC600 927

3. The Edit License dialog box will appear. Enter your Customer
(company), Instrument Serial Number, and Options.
4. Click Copy.
5. Open a blank email message and press Ctrl and V on the
keyboard to paste the license information into the email message.
6. Send the email or just the Key number to the LECO designee.
928 AC600 Service

Adding an Option or Changing Customer Name
1. Request/purchase option from LECO. LECO will provide a new key
number and registration information.
2. In the software, click Help on the Menu bar and then select
About.
3. On the About dialog box, click Change.
4. The Edit License dialog box will appear.
Service AC600 929

5. Registration information can be entered in two ways as explained
below. It is preferable to copy and paste the information to help
avoid errors.
Type in the registration information exactly as it appears.
If the upgrade information is received in an email from LECO,
paste the registration information as explained in the
following steps.
A. Select all of the text in the email from LECO.
B. On the Edit License dialog box, click Paste. The information
from the email, including customer name and any options
will appear in the Edit License dialog box.
C. Click Save.
930 AC600 Service

Troubleshooting Copy Protection Key
A Copy Protection Key is required to use the software.

Do not insert the copy protection key into the USB port until the
LECO software is installed and the PC has been rebooted.
The Copy Protection Key should remain installed in one of the
USB ports while using the software.
Copy Protection Key Error Messages
The Copy Protection Key Not Found or License Not Valid dialog box
may appear if the copy protection key is not installed, the software is
not registered, or the software is already running. Follow the steps
below.
Verify the copy protection key is installed. If not,
1. Click OK, and then insert the copy protection key.
2. On the Licenses dialog box, click Close. The software login will
appear.
If the copy protection key is installed, the software may not be
registered.
1. Click OK.
2. Insert the copy protection key. The Licenses dialog box will
appear.
3. Click on the old version and then click Change. Follow the
instructions in Registering Software, beginning with step 5.
If the copy protection key is installed, the software may already be

running on the computer. Click Close.
Service AC600 931

General Troubleshooting
Area Condition Solution
Corrosion on bucket lid - Clean lid contact.

Misfires
Crucible holder touching side of oxygen
combustion vessel - Realign crucible holder.
Intermittent high results can be caused by
a leaking oxygen combustion vessel.
Bubbles that form on interior surfaces are
Analysis an indication of a leaking oxygen
Results combustion vessel.
Intermittent high results Inspect enclosure o-ring. Replace if worn.
Inspect check-valve o-ring. Replace if
worn.
Refer to Replacing Oxygen Combustion
Vessel O-Rings, page 614.
Leaking Bucket Lid Seal - Remove lid, check
Downward trend
for water, and then replace o-ring.
Refer to Replacing Ignitor Wire for Thread
Ignitor Wire Failing prematurely
Fuse, page 619.
Check the operation of the spring in the
spring-loaded lever.
No movement Check the setscrew in the lift-arm
carriage. The set screw should not be too
tight or wobble, which indicates it is too
Lift-Arm loose.
Mechanism
Check that nut is positioned correctly on
lift mechanism and is not too tight or too
Excessive vibration or loose.
erratic positioning
Check that the carriage and rail were
aligned properly using the alignment tool.
The duty cycle drops to zero and does not
Needle Valve Loss of control of jacket move. Open the needle valve completely by
(Duty Cycle) temperature turning counterclockwise. Leave open for 5
minutes to flush the valve.
Oxygen charger assembly Replace the oxygen combustion vessel
Oxygen leaks when the charger assembly o-rings. Refer to
Charger combustion vessel is Replacing Oxygen Charger O-Rings, page
charged. 616.
Check Ethernet connection between PC
Communications cannot tower and instrument.
Power System
be established. Check the log for error messages. Refer
to Viewing Log, page 610.
932 AC600 Service

Area Condition Solution
Delayed with minimal rise
Check stirrer motor and belts.
in temperature
Slower than normal Stirrer moving too slowly - check stirrer
temperature rise motor.
Bucket lid may not be sealing.
Check compressed air. Target range
Temperature profile is 12 psi (0.827 bars) +3.
trends downward quickly Check lid alignment. Refer to Aligning
after maximum, and Bucket, page 939.
jacket temperature Check for pinched air line. The c-flex
increases dramatically pneumatic line may become pinched,
Temperature especially after maintenance or
replacement.
Adjust needle valve (Duty Cycle). Refer to
Adjusting Duty Cycle, page 941.
Check needle valve operation. Refer to
Needle Valve, page 932.
Check chiller for proper operation. Refer to
Poor jacket control
the manufacturers manual.
Check water filter. Refer to Replacing Water
Filter, page 624.
Check pump to verify that water is flowing
from the nozzle in the jacket.
Verify the check-valve o-ring is properly
positioned and in good condition. Refer to
Won't pressurize
Replacing Oxygen Combustion Vessel O-
Vessel Rings, page 614.
Check and replace o-rings. Refer to
Leak indicated by air
Replacing Oxygen Combustion Vessel O-
bubbles
Rings, page 614.
Service AC600 933

Jacket Temperature Troubleshooting
1. Fluctuations after lowering the vessel should be similar to those

shown below in Figure 9-1, with no positive-going peak as the
temperature stabilizes. Positive peaks are indicative of a poorly
aligned water nozzle or an inappropriate jacket set point for
ambient conditions. Inspect cool water inlet within the Jacket for
proper positioning. Verify the jacket set point within software is
25C or 2 to 3C higher than nominal room temperature for the
lab.
Figure 9-1
Jacket Temperature for Single Analysis
934 AC600 Service

2. Jacket temperature at 60 seconds should be stable within
0.002C during a series of sequential analyses, refer to
Figure 9-2. Inspect chiller and associated plumbing if not
Figure 9-2
Jacket Temperature for Series of Analyses
3. Jacket fill errors are indicative of low water pressure, which is

most likely caused by a clogged water filter. Change inline water
filter for the AC600 system. Refer to Water Filter, page 624.
4. Verify the instrument duty cycle.
5. Inspect the water level float switch and ensure smooth
travel/movement with no evidence of water penetration into float
assembly.
Service AC600 935

Fault Conditions
The following fault conditions are intended to assist LECO Service in

diagnosing instrument conditions.
Observed Condition Possible Root Cause Checks and Solutions

Check that the water is
Consistently bad results The stirrer motor,
stirring. Check electrical
with a slow increase in controller or
connections from Motion
bucket temperature after mechanical coupling
Control Card to controller to
ignition. may have failed.
stirrer motor.
Try to reset the network from
the Diagnostics Network tab
as follows: Click Diagnostics,
Network, and then select
All parameters in the Communications to the Reset Network. If this doesn't
software Ambient Chart instrument may be work, exit software, cycle
are flat-lining. lost. power to the instrument and
then restart the software. If
this doesn't work, check
electrical connections between
PC & instrument.
There is a problem
with the sensor that is
Some but not all
flat-lining. If the flat
parameters in the software Check electrical connections to
line is at the limit of
Ambient Chart are flat- sensors.
the range of that
lining.
sensor, the sensor
may be disconnected.
Software reports that the
oxygen combustion vessel
is not in analyze position
and can therefore not There is a problem Check electrical connections to
ignite the sample when in with the Analyze and mechanical alignment of
fact the oxygen Position Switch. the Analyze Position Switch.
combustion vessel appears
to be in the proper
position.
Check the software for errors
related to motion control and
check the log. Refer to
There is a problem Software Error Codes, page
The vessel cannot be
with the vertical motor 938, and refer to Viewing
moved up or down.
or its controller. Log, page 610. Check
electrical connections from
Motion Control Card to
controller to vertical motor.
936 AC600 Service

Observed Condition Possible Root Cause Checks and Solutions
Check pneumatic pressure.
Low pneumatic
Bucket will not seal. Check that the bucket seal
pressure.
valve is working properly.
Jacket temperature is too Jacket fill valve may Check the wiring and
low, duty cycle (in be stuck open, or the operation of the jacket fill
software ambient chart) is heater or pump may valve, heater, thermostat, and
high. not be working. pump.
Check the error log.
Jacket temperature is too Firmware may have Reset the network from the
low, duty cycle (in turned off heater Diagnostics Network tab as
software ambient chart) is control because of follows: Click Diagnostics,
low. error condition. Network, and then select
Reset Network.
Jacket temperature is too
low, duty cycle (in Check the wiring and
The Coolant valve may
software ambient chart) is operation of the Coolant
be stuck off.
low. Jacket fill valve Valve.
occasionally turns on.
Check the wiring and
Elevated jacket The Jacket fill valve
operation of the Jacket Fill
temperature. may be stuck closed.
Valve.
Elevated jacket The heater may be on Check the voltage across the
temperature and because of a part heater and compare to the
temperature continues to failure on the AC duty cycle on the Ambient
increase. Control Card. Chart in Diagnostics.
Service AC600 937

Software Error Codes
The following fault conditions are intended to assist LECO Service in

diagnosing ACWIN software error codes observed in the Log or on the
Status Bar. Refer to Viewing Log, page 610.
Error Name Probable Root Cause

The A-to-D converters on the AC Control Card are not
A/D Converter Fault
communicating properly with FPGA.
On the AC Control Card, either 1) The FPGA failed to
communicate with the on-card digital thermometer; 2) the
On Board FPGA
firmware failed to refresh the watchdog in the allowed time; or
Error
3) the firmware failed to set Interrupt Acknowledge bit high &
low after interrupt.
FPGA Load Error The FPGA on the AC Control Card has failed to load properly.
The FPGA on the AC Control Card did not start up within 50 ms
FPGA POR Error
of the firmware performing a power-on reset.
1) There is no line voltage to the AC Control Card or 2) very
Card Loop Error
poor line voltage conditions exist.
The Windows software failed to extract data from the A/D
ADC Queue Error Converters on the AC Control Card in a timely way and the 5-
second ADC data buffer has overflowed.
1) The line frequency appears too high because of either poor
line voltage conditions or because there is a problem with
Half Period Error zero-cross measurement circuit on the AC Control card or 2)
The Windows software has set the blank-out time too short,
less than one quarter of the period of the line voltage.
1) The Windows software has set the igniter ontime for >3
Igniter Timing Error seconds or 2) the Windows software attempted to fire the
igniter when it was already on.
The Jacket does not seem to be filling in a timely manner
because 1) There is a blockage in the water supply, 2) there is
Jacket Fill Error
a water leak, 3) The Jacket Water Level switch stuck in the
unfilled position, or 4) The Jacket Fill Valve is stuck closed.
There has been an over-run condition in the period counter in
the AC Control Card firmware because either 1) there is no
Zero Cross Error
line voltage to AC Control Card or 2) there is a problem with
the zero-cross detection circuit on the AC Control card.
938 AC600 Service

Aligning Bucket Lid
The following procedure explains how to properly align the bucket. The
bucket will require alignment whenever the lift-arm mechanism has
been removed.
The following procedure assumes the oxygen combustion vessel is in

the raised position. Refer to Figure 10-28.
1. Replace the 3 screws that hold the lift arm in place but do not
tighten them. Refer to Figure 9-1.
Figure 9-3
Lift-Arm Screws
2. From Diagnostics, select the Lift Mechanism tab, For Go To, select
Analyze, and then click Go.
3. While the shelf is lowering, verify the bucket lid descends freely
into the bucket. Manually guide the bucket lid into place if
necessary.
4. In the software, click Diagnostics and then select the
5. On the Solenoids/Switches tab, select the Inflate Bucket Seal
check box.
6. Tighten the three lift-arm screws on the panel. Refer to Figure
9-1.
7. On the Solenoids/Switches tab, clear the Inflate Bucket Seal
check box.
8. Test the position of the bucket lid as follows:
A. From Diagnostics, select the Lift Mechanism tab, for Go To,
select Vessel Raised, and then click Go. Allow the vessel to
raise fully.
B. From Diagnostics, select the Lift Mechanism tab, for Go To,
select Analyze, and then click Go. Monitor the bucket lid to
verify it descends freely into the bucket.
C. After the vessel is in the analyze position, repeat steps A-B
at least once more.
Service AC600 939

Using the Dock Wizard
The dock wizard is used to correctly engage the lift-arm mechanism

and loader motor whenever the lift arm has to be removed for service
or maintenance.
1. To access the dock wizard, click Dock Wizard on the Maintenance

menu.
2. Follow the software instructions that display on the Loader Dock
Wizard dialog box.
940 AC600 Service

Adjusting Duty Cycle
It may be necessary to adjust the duty cycle when the instrument

displays poor temperature control.
1. Click Maintenance on the Menu Bar, and then select Flow Adjust.
2. Verify the conditions that display in the message are met and
then click Next.
3. Locate the Flow Adjust Knob on the back of the instrument. Refer
to Figure 9-2.
Figure 9-4
Duty Cycle Adjustment Knob
4. Turn the Flow Adjust Knob counterclockwise while monitoring the
Duty Cycle value.
Service AC600 941

942 AC600 Service

10 Illustrations
Figure 10-1 Reference Card .............................................................102

Figure 10-2 Facility Requirements ....................................................103
Figure 10-3 Wiring Diagram.............................................................104
Figure 10-4 Instrument Overview .....................................................105
Figure 10-5 Instrument Overview - Panels Removed...........................105
Figure 10-6 Left Side View ..............................................................106
Figure 10-7 Rear View ....................................................................107
Figure 10-8 Oxygen Combustion Vessel Assembly ..............................108
Figure 10-9 Halogen-Resistant Combustion Vessel .............................109
Figure 10-10 Jacket Thermistor ........................................................1010
Figure 10-11 Wire Fuse Assembly ....................................................1011
Figure 10-12 Lift-Arm Screw ............................................................1012
Figure 10-13 Locking Mechanism .....................................................1013
Figure 10-17 Oxygen Manifold Assembly ...........................................1017
Figure 10-18 Pneumatic Manifold Assembly .......................................1018
Figure 10-19 Card Control Assembly .................................................1019
Figure 10-20 Motor Stirrer Gearbox ..................................................1020
Figure 10-21 Jacket Assembly..........................................................1021
Figure 10-22 Switch for Bucket Water Level ......................................1022
Figure 10-23 Water Heater Assembly and Pump .................................1023
Figure 10-24 Bucket Sealing Cover Assembly ....................................1024
Figure 10-25 Water Inlet Assembly...................................................1025
Figure 10-26 Bucket .......................................................................1027
Figure 10-27 Lift Arm Assembly .......................................................1028
Figure 10-28 Lift-Arm Positions ........................................................1029
Figure 10-29 Flow Diagram .............................................................1030
Figure 10-30 Semi-automated Analysis Sequence ..............................1031
Figure 10-31 Top-Level Exploded View ..............................................1032
Figure 10-32 Vessel Prep Station......................................................1033
Illustrations AC600 101

AC600
Delivering the Right Results
Consumables & Spare Parts Reference Card
Note: Part numbers and standards' values may change. Consult LECO for the latest information.
191-064
SCREW 621-605-744
VESSEL
4 REQ'D FLUSH CAPNUT
621-823G ADAPTER
LATE MTG
772-738
O-RING
621-605-952
ALIGNMENT 621-605-938/
TOOL 621-605-980*
621-781
762-363 FTG POST ELECTRODE
FTG
621-779 621-605-182
VALVE INSULATOR
767-866 773-913 LID
FTG TEE O-RING
621-604 PART OF 621-656

FTG HOUSING 621-605-886 VESSEL CAP
TUBING
621-656-001 O-RING
FOR 621-656 HOUSING 621-605-665
O-RING INSTALL
778-113 TOOL 621-605-560
GAUGE O-RING
621-657
FILTER CARTRIDGE 621-605-664
O-RING 621-605-657/
621-605-918*
CHECK VALVE
776-562
WASHER 621-605-422/
621-605-917*
621-605-873 RETAINER VALVE
621-605-919*
ELECTRODE 621-605-874/
UPPER BAR 621-605-920*
774-204 621-605-777
WIRE FUSE ELECTRODE
CRUCIBLE 621-656 KIT
BAR
HOUSING 621-605-875
502-460
621-605-921*
IGNITER WIRE
ELECTRODE
LOWER BAR 621-605-314
BRACKET
191-173
SCREW
(2 REQD) *DENOTES PART
NUMBER FOR
HALOGEN-
RESISTANT
VESSEL
VESSEL BODY
625-602-297
633-101-923 O-RING 603-493
601-980 (2 REQD) O-RING
WASH BOTTLE VESSEL STAND
780-831 621-605-949
O-RING INSULATION
621-605-928 772-738
621-605-987 O-RING
HANGER
621-605-809 LEVER BASE
LEVER (2 TOTAL) 191-184 191-180
(2 TOTAL) SCREW SCREW
621-605-823 (2 REQD) 191-180
621-605-820 PIN
SCREW
KNOB (2 TOTAL) 621-605-948 190-715 SCREW
(2 TOTAL) 190-364 PLUG (2 REQD)
SCREW
(2 TOTAL)
621-605-824
SPRING (2 REQD) 621-605-822
621-605-828 INSERT CAP
621-605-104 RETAINING RING 191-066 (2 REQD)
LEVER ROLLER MOUNT 2 REQD SET SCREW
(2 TOTAL) (4 TOTAL) 621-605-924
621-605-661
621-605-997 HOLDER EXHAUST
BEARING PIN VALVE
(2 TOTAL) 621-605-923
621-605-974 INSERTS
CHARGE VALVE INSERT
BEARING
2 REQD (4 TOTAL) 772-738
621-605-956
O-RING
LOCK COVER
(4 REQD)
621-605-784
VESSEL LOCK 621-605-973
(4 REQD) INSERT SEAL
621-605-783
LOCK VESSEL 633-101-524
BASE (4 REQD) BALL PLUNGER
(4 REQD)
621-605-821
SCREW 703-226
(6 REQD) DOWEL PIN
(4 REQD)
621-605-561
STRAINER
621-605-944
BASIN
621-605-439
AC600 BASIN
775-031
FOOT (4 REQD)
See reverse side for contact information

Form No. 203-104-052 Rev. 12 LECO is a registered trademark of LECO Corporation 4/5/13
Figure 10-2
Facility Requirements

NEMA 5-15P PLUG
BROWN
POWER
BROWN BLUE
115 V~ BLUE
NEUTRAL
0 V~ GREEN/YELLOW
GROUND
IEC 60320 C-13 GREEN/YELLOW

WALL OUTLET CONNECTOR AC600
115V~ WIRING DIAGRAM (U.S.A.)
NEMA L14-30P PLUG
BROWN X
POWER Y
115 V~ GREEN/YELLOW
GROUND G
230 V~ 115 V~ G W
BLUE
POWER X
NEUTRAL W Y
(OPTIONAL)
IEC 60320 C-13
CONNECTOR
WALL OUTLET AC600
230V~ WIRING DIAGRAM (U.S.A.)
PLUGSPECIFIED BY
LOCAL WIRING STANDARDS
BROWN
POWER
100/200/220240 V~ BLUE
NEUTRAL
0 V~ GREEN/YELLOW
GROUND
IEC 60320 C-13

WALL OUTLET CONNECTOR AC600
100/200/220/240V~ INTERNATIONAL WIRING DIAGRAM

Figure 10-3
Wiring Diagram
104 AC600 Illustrations

Figure 10-4
Instrument Overview
Figure 10-5
Instrument Overview - Panels Removed

Figure 10-6
Left Side View

Figure 10-7
Rear View

Figure 10-8
Oxygen Combustion Vessel Assembly

Figure 10-9
Halogen-Resistant Combustion Vessel

Figure 10-10
Jacket Thermistor

Figure 10-11
Wire Fuse Assembly

Figure 10-12
Lift-Arm Screw

Figure 10-13
Locking Mechanism

Figure 10-14
Water Manifold Assembly View 1

Figure 10-15

Figure 10-16

Figure 10-17
Oxygen Manifold Assembly

Figure 10-18
Pneumatic Manifold Assembly

Figure 10-19
Card Control Assembly

Figure 10-20
Motor Stirrer Gearbox

Figure 10-21
Jacket Assembly

Figure 10-22
Switch for Bucket Water Level

Figure 10-23
Water Heater Assembly and Pump

Figure 10-24
Bucket Sealing Cover Assembly

Figure 10-25
Water Inlet Assembly


Figure 10-26
Bucket

Figure 10-27
Lift Arm Assembly

Raised Position Equilibrate Position Analyze Position
Figure 10-28
Lift-Arm Positions

Analyze Position Switch
Raised Vertical Motor

Control
Vertical
Equilibrate
Motor
Cotton
Wire
Analyze Bucket Stirrer
O2 Fill Switch Front Panel
Lighted Switch Igniter Circuit
Bucket Lid Top (Coated Al)

Vessel
Manifold Bucket Seal Insulation Stirrer
Motor
Bucket Lid Bottom (SST)
To
Vessel
Igniter Contact
Vessel Mount
Low Water Level Switch

Vent O2 Vent
Thermal Switch
Manual Overide Max Water Level
F O2 Fill 60 C
450 psig Jacket Thermistor
Restirctor
115/230 v~
1 L/min
Oxygen Manifold
O2
99.99%
2000 W Heater Cartridge

Bucket Seal
15 psig Valve
Over Flow
To Recirculating Chiller
Through Rear Panel
Air
Bucket Thermistor
Jacket Fill Valve

Over Flow
N S
Pump
Check
Insulated Stainless Steel Bucket Assy
Valve
15C F
Needle Coolant Valve
Valve S N
Water Circulation System
Water Manifold Assy
External
Chiller Insulated Stainless Steel Bucket Assy
Figure 10-29
Flow Diagram

Thermodynamic Corrections
Prefire Time
Cancel (Method Parameter) Collect and Measure
User Enters Sample Info and User Confirms
Remaining Fuse
Selects Method Leak Check Passed
Fire Vessel
Prepare Sample Crucible (Cotton or Wire)
1) Clean crucible
2) Place on balance & tare Edit Fuse Length
3) Add sample to crucible Lift Open Main Time
Position Abort
(Method Parameter)
Misfire Sample Titration
Not Open Rinse vessel, vessel lid, and crucible
Record Sample Weight in with distilled water
Postfire Period
Software
Move to the (Method Parameter) Collect rinsings
Abort
Open Position Titrate Rinsings
No
Spike Sample? Position
Yes Error Stop Pump and Slow
Abort
Attach Combustion Vessel Stirrer
Add spike material to crucible To Bucket Lid Position
Error Edit Nitrogen Correction
Move to Open Position
Record Spike Weight in Press Green Button to Begin

Cancel
Software Analyze Sequence Enter Additional
Enable Water Level/
Temperature Control Corrections
Prepare Vessel
(Sulfur, Hydrogen, Total
Decrease Stirrer Rate H2O, Moisture, and Ash)
Place sample crucible in sample holder Move to Equilibrate
Attach fuse
Place vessel lid on vessel and lock in place Prepare Vessel
Detach Vessel
Vent Vessel
Equilibrate Vessel Clean Vessel
Abort
Attach Oxygen Manifold to Vessel (Method Parameter) Drain Vessel
(Collect Rinsings as Necessary)
Equilibration
Error
Increase Stirrer Rate

Press Oxygen Fill Button Yes
Analyze More
Repeat Procedure Samples?
No
Wake Up (If Necessary) No Jacket Control
Enable Water
Abort Wait Timeout?
Level/Temperature Abort Move to Analyze
Control & Bucket Stirrer Yes
Jacket Temp Error
Move to the
Jacket Fill Error Position Abort
Standby Mode Open Position
Error
Disable Pump
Disable Stirrer Position
Abort Fill Vessel with Oxygen Seal Bucket Disable Jacket Control Error
Lower Bucket Lid Wake Up (If Necessary)
Oxygen Fill Error Enable Water
Abort
Level/Temperature
Control & Bucket Stirrer
Detach Oxygen Manifold from Vessel Jacket Temp Error
Jacket Fill Error
Press Green Button toWake Up

User Leak Checks Vessel
Figure 10-30
Semi-automated Analysis Sequence

Figure 10-31
Top-Level Exploded View

Figure 10-32
Vessel Prep Station


11 Schematics
This section only includes pages of the schematic drawing that are
applicable for service of the instrument.
Figure 11-1 Temperature Control and Measurement ...........................113

Figure 11-2 Motion Control ..............................................................114
Schematics AC600 111

112 AC600 Schematics

1 2 3 4 5 6 7 8 9 10 11
Name: 150996
Location: TOP- Module Sheet 2 OF 3
TEMPERATURE CONTROL
A & MEASUREMENT A
ETHERNET CARD
NOTE: USE 619-610 CABLE TO
ETHERNET_CARD CONNECT TO HUB, P/N 633-101-920
A2 J573B
ETHERNET 620-677
CROSS-OVER_CABLE
ETHERNET TO PC A1A
666-573X
J573C J569A
ECLIPSE ECLIPSE ECLIPSE
666-310X120
HOST-IN
B ECLIPSE_DAUGHTER
B
A2A
666-310X210
MT1 T
TB1
1+ THERM1+
621-605-122
JACKET_THERMISTOR 5k THERM1- J569
ECLIPSE_ETHERNET 1-
THERMISTORS
MT2 T
TB2
2+ THERM2+ J569X
621-610-010
5k ECLIPSE ECLIPSE_586
BUCKET_THERMISTOR 2- THERM2- ECLIPSE 3-A3
J573A J569Y
A1 ECLIPSE COMBUSTION VESSEL
WIRING HARNESSES 666-731X
AC600_CONTROL_CARD J569D J569D
TB101
TERMINAL_BLOCK
A6 A7
IGNITER OUT 1 1 WHITE 1 1
WHITE HTR2
J569MA BLACK 502-460
C A8 A12 1 24GND
24GND 2 2 2 2
BLACK IGNITER
C
2 SW0 776-682
J569KA 621-605-953 621-605-954 VESSEL
3 24V(LIMITED) BUCKET_COVER COMBUSTION_VESSEL
SOL0 1
J569MB 24GND 2 (621-605-975 HALOGEN RESISTANR)
1 24GND
J569KB J569KB 621-822
HTR2A
2 SW1 502-462
621-605-410 621-605-379 3 24V(LIMITED)
SOL1 1 1 + + RED CABINET_FAN FUSE_IGNITER
WIRING_HARNESS CABLE_ASSEMBLY 24GND 2 2 - - BLACK FAN1
AC600_CABINET JP2-J586J J569MC
J569KC J569KC J110 J110
1 24GND
SOL2 1 1 1 1 + RED PUMP1
621-605-361 SW5 2 SW2
24GND 2 2 2 2 WATER_PUMP
LOW_WATER_LEVEL_SWITCH 3 24V(LIMITED) - BLACK 621-617
A9 A13 J569MD
J569KD
SOL3 1
1 24GND
24GND 2
2 SW3
BACK 3 24V(LIMITED) J569G J569KE
D
PANEL
J569ME
1 24GND
24GND 1
STRING_EN 2
SOL4 1
24GND 2
VALVES D
621-605-340 621-605-441 2 SW4 J569KF J569KF
WIRING_HARNESS CABLE_ASSEMBLY YELLOW_DOT_ON_+
AC600_POWER IGNITER_VESSEL WASH STATION 9

8
9
8
9
8
9
8
J569MF
3 24V(LIMITED)
J569MF
SOL5 1
24GND 2
1
2
+
-
+
- SV5
OXYGEN_FILL_VALVE
608-722
7 7 7 7
6 6 6 6
1 1 24GND J569KG J59KG YELLOW_DOT_ON_+
5 5 5 5
2 2 SW5 SOL6 1 1 + + SV6
OXYGEN_VENT_VALVE
A10 A14 4 4 4 4
3 3 24V(LIMITED) 24GND 2 2 - - 608-722
SW6 NC B 3 3 3 3 J569MG J569MG J569KH

NO A 2 2 2 2 2 2 1 1 24GND SOL7 1
621-605-673 1 1 1 1 1 1 2 2 SW6 24GND 2
COM C
OXYGEN_FILL_SWITCH J226 J226 J225 J225 J224 J224 3 3 24V(LIMITED)
J569KJ
JSW7 J569MH J569MH SOL8 1
621-605-289 621-605-675
CABLE_ASSEMBLY ASSY_BULKHEAD SW7 603-065 C 1 1 1 24GND 24GND 2
E VERTICAL_MOTOR WASH_STATION
OXYGEN_PRESSURE_SWITCH NO 2 2
3
2 SW7
3 24V(LIMITED)
J569KK J569KK JSV9 JSV9 E
24VDC POWER SUPPLY J569B
SOL9 1
24GND 2
1
2
1
2
1
2
+
- SV9
621-606-122
JACKET_FILL_VALVE
+V 1 +24VDC_IN J569KL J569KL JSV10 JSV10

A11 A15 + +V 2 586_24V 3-G4 J569C DC POWER IN SOL10 1 1 1 1 + 621-606-122
SV10 COOLANT_VALVE
-V 3 +24VDC_RET 24GND 2 2 2 2 -
PS1 - -V 4 586_GND 3-G4
625-601-923 G 5 J569Z J569Z
N 6 1 1 HOT1 J569R
AC L 7 2 2 N/C AC POWER HOT1 1 1 MOV1 HEATER & THERMOSTAT
621-605-290 621-605-557 24V_POWER_SUPPLY 3 3 HOT2 AC POWER N/C 2 2 619-001
CABLE_ASSEMBLY ASSY_CABLE_CONNECT HOT2 3 3 MOV
J569P J569P
RS485 STATION_PREP
GND
1 1 HOT1 J569S J569S J109 J109 T F1
621-619
THERMOSTAT
2 2 N/C AC POWER HOT2 1 1 1 1
3 3 HOT2
HEATER HOT1 2 2 2 2
F
666-731X
HTR1 F
A16 621-605-431
HEATER
INPUT POWER
LINE_FILTER
CB1 5A
621-605-526 LINE_CORD LOAD LINE LOAD R
LECO St. Joseph,

CABLE_ASSEMBLY 776-997
MOTOR_POWER 7.5A LOAD LINE LOAD
LC115 115V
GND
MAIN_BREAKER 614-314 Michigan USA
FL1 621-825
Description
Schematic AC600
G CABINET G
GND
Part Number Rev
150-996 R
Date: 16-08-2012_15:40 Type M
Schematic Sheet 2 OF 3
1 2 3 4 5 6 7 8 9 10 11
1 2 3 4 5 6 7 8 9 10 11
Name: 150996
MOTION CONTROL Location: TOP- Module Sheet 3 OF 3
J586 J586S J586S

ECLIPSE_586 ECLIPSE
2-C9 ECLIPSE SOL0_+24 1 1
A
J586CH
GND
SOL1_+24
2
3
2
3
LIGHT, VALVE A
3 +24V A3 GND
SOL2_+24
4
5
4
5
2 SW15
GND 6 6
1 GND 666-586X120 LAMP+
J586CG
SOL3_+24
GND
7
8
7
8 LAMP-
SW2 621-605-381
BUTTON/LIGHT
3 +24V AUTOLOADER_CONTROL GND 9 9
2 SW14
1 GND
J586T J586T
SOL4_+24 1 1 + + SV4
621-605-515
J586CGF
A3A GND 2 2 - - BUCKET_SEAL_VALVE
3 +24V SOL5_+24 3 3
2 SW13 GND 4 4
1 GND 666-310X120 SOL6_+24 5 5
ECLIPSE_DAUGHTER GND 6 6
J586CE
SOL7_+24 7 7
B 3 +24V
GND 8 8 B
2 SW12
GND 9 9
1 GND
J586CD J586AE
J586U J586U
SOL8_+24 1 1
3 +24V
GND 2 2
2 SW11
1
J586CC
GND
SOL9_+24
GND
SOL10_+5SIG
3
4
5
3
4
5
VERTICAL MOTION
3 +24V GND 6 6
2 SW10 SOL11_+5PWR 7 7 WHITE/GREEN
GREEN/WHITE
1 GND JTAG GND 8 8
J586AG GND 9 9
J586CB
NC 1 2 GND
LS1
3 +24V J586V J586V 621-605-284
TDO 3 4 GND 1 +
2 SW9 SOL12_+24 1 1 TCH-86-530-Q(M)
TDI 5 6 GND 2 -
1 GND GND 2 2 ALARM_BUZZER
C J586CA
TMS
TCK
7 8
9 10
GND
GND
SOL13_+24 3 3 C
GND 4 4
3 +24V
SOL14_+5SIG 5 5
2 SW8
1 GND J586AH GND 6 6 P1 JP1
3V3D 1 2 GND SOL15_+5PWR 7 7 I/O POWER 1 1
J586BH GND 8 8 I/O GND 2 2
3 +24V GND 9 9 I/O 1 3 3
2 SW7 A4 I/O 2 4 4
1 GND 625-505-802 I/O 3 5 5
J586W
BLACK VERTICAL_CNTRL I/O 4 6 6
J586BG MOTOR1 GND 3 3
CH A+ 7 7 BLUE/WHITE
MFORCE
3 +24V POWER NC 2 2
CH A- 8 8 WHITE/BLUE
RED
2 SW6 PORT5 MOT1_+24V 1 1
CH B+ 9 9 BROWN/WHITE
1 GND J586H J586W WHITE/BROWN
CH B- 10 10
NC 2 1 GND
J586BF CAP/TRIP 11 11
TXA_TX 4
3 +24V
RXA_RX 6 5 TXB_RTS
J586J J586J JP2 P2 ANALOG IN 12 12
D 2 SW5
+24V 8 7 RXB_CTS
RXB_CTS 1 1 BROWN
GREEN
1 1 TX+ INDEX+ 13 13 ORANGE/WHITE
WHITE/ORANGE
D
1 GND GND 2 2 2 2 COM-GND INDEX- 14 14
GND 10 9 GND BLACK
TXA_TX 3 3 3 3 RX- +V 15 15
J586BE RED
RXA_RX 4 4 4 4 TX- PWR GND 16 16
JM1
3 +24V
1
2
3
4
5
6
7
8
9
10
PORT1 NC 5 5 5 5 AUX-LOGIC
STIRRER MOTOR SWITCHES 2

1
SW4
GND PORT4
J586G
TXB_RTS
NC
6
7
6
7
WHITE 6
7
6
7
RX+
RX+ PHASE /A
P3
1
JP3
1 RED/WHITE
RED
1 2 3 4 5 6 7 8 9 10
& CONTROLLER SW3 COM WHITE 1

J114
1
3
2
J586BD
3
2
+24V
SW3
NC
TXA_TX
RXA_RX
2 1
4
6 5
GND
TXB_RTS
NC
GND
NC
8
9
10
8
9
10
DRAIN
8
9
10
8
9
10
RX-
TX+
TX-
PHASE A
PHASE /B
PHASE B
2
3
4
2
3
4
GREEN
GREEN/WHITE
M1
G G I- I+ A- A+ 5V 5V B-
621-605-241
B+
621-605-409 NO RED 2 2 1 1 GND +24V 8 7 RXB_CTS VERTICAL_MOTOR

E57H4A-3.25-052
ANALYZE_POSITION NC BLUE 3 3 J586BD GND 10 9 GND
SWITCH J586BC
3 3 +24V
A
SERIAL IN
621-605-381 SW2 B
2 2 SW2 J586Z
BUTTON/LIGHT 1 1 GND MOTOR3 GND 3
J586BC POWER NC 2
E 1 1 1
J586BB
3 +24V
MOT3_+24V 1 E
2
2 SW1
POWER ENCODER MOTOR 1 GND
INPUT PHASES J586L
J586BA
RXB_CTS 1
3 +24V
GND 2
STIRRER_CONTROL 2 SW0
TXA_TX 3
1 GND
JENC ENCODER STEP/DIR RXA_RX 4
ORANGE 1 1 +5V +24V 1 PORT3 NC 5
GREEN 2 2 S3 +5V 2 TXB_RTS 6
GREY 3 3 S2 STEP 3 J586X NC 7
YELLOW 4 4 S1 DIR 4 3 3 GND MOTOR2 NC 8
M2 BLACK 5 5 GND
POWER INPUT
2 2 NC POWER GND 9
BROWN 6 6 CH A 1 1 MOT2_+24V NC 10
WHITE GND 2 2
7 7 +5V J586X
BLUE +V 1 1
F DA23BBB-M200
8
9
8
9
CH B
INDEX
JPOWIN F
621-605-237 10 10 GND
SERIAL IN JSERIN J586K J586K
24V 1 1 1 1 RXB_CTS J586Y
STIRRER_MOTOR GREEN MOTOR0
JMOTPH MOTOR PHASES GND 2 2 2 2 GND GND 3
1 1 PHASE C RS485B 3 3 3 3 TXA_TX POWER NC 2
2 2 PHASE B RS485A 4 4 RED 4 4 RXA_RX MOT0_+24V 1
3 3 PHASE A N/C 5 5 5 5 NC PORT2
N/C 6 6 WHITE 6 6 TXB_RTS
OPTO SENSORS R
N/C 7 7 7 7 NC
LECO St. Joseph,

1 GND J586M
N/C 8 8 8 8 NC
2 AN IN 1 DRAIN RXB_CTS 1
9 9 GND
3 AN OUT 1
4 GND
SERIAL OUT
24V 1
10 10 NC
GND
TXA_TX
2
3
Michigan USA
5 AN IN 2 GND 2 RXA_RX 4
Description
6 AN OUT 2
7 DIG IN 1
8 DIG IN 2
RS485B 3
RS485A 4
N/C 5 2-E5 586_24V
J586A
1
J586A
1 +24V
PORT0 NC
TXB_RTS
NC
5
6
7
Schematic AC600
G
DSV-405
N/C 6 2-E5 586_GND 2 2 GND POWER IN NC 8 CABINET G
N/C 7 3 3 GND GND 9
621-605-283
A5 N/C 8 4 4 +24V NC 10 Part Number Rev
150-996 R
Date: 16-08-2012_15:40 Type M
Schematic Sheet 3 OF 3
1 2 3 4 5 6 7 8 9 10 11
12 Glossary
1/Certified Weighting: A weighting As-Received Basis: Analytical data
that can be applied to the calibration calculated to the moisture condition of
data points that will counteract a bias the sample as it arrived at the
for higher concentrations that comes laboratory and before any processing
naturally out of the curve fitting or conditioning. If the sample has been
routines. maintained in a sealed state so that
there has been no gain or loss, the as-
received basis is equivalent to the
A moisture basis as sampled.
Abort: Stops an analysis in progress.
Accuracy: Closeness of a measured
B
value to the true value.
Baseline: Electronic line determined
Ambient Temperature: The ambient
as the zero or reference line that is
temperature inside the instrument as
used to differentiate the actual analyte
measured by a temperature
concentration.
transducer. This value is in degrees
centigrade. Baud Rate: The data transmission
speed between the computer and
Analysis Date: The date and time
balance.
the analysis completed.
Bias: Deviation of a measurement
Analysis Time: The integration time.
process from the true or accepted
Analyte: The specific component value.
measured in a chemical analysis.
Blank: The signal obtained during an
As-Determined Basis: Analytical analysis that cannot be attributed to
data obtained from the sample after the sample and should be deducted
conditioning and preparation. As- from a measured value to give the net
determined data represents the value due solely to the analyte of
numerical values obtained at the interest in the sample.
particular moisture level in the sample
at the time of analysis. These values
are normally converted to conventional C
reporting bases. Calculated: Displays the
Ash-Free Basis: Data calculated to a concentration of the standard as
theoretical base of no ash associated calculated by the instrument using the
with the sample. measured areas and concentration
curve.
Glossary AC600 121

Calibration: A comparison of a D
measurement standard or instrument
Data Bits: The number of transmitted
with another standard or instrument to
data bits per byte.
report or eliminate, by adjustment,
any variation or deviation in the Delimiter: A character that separates
accuracy of the item being compared. fields of transmitted data.
(Taylor, John K. "Standard Reference Detector: A device that produces a
Materials Handbook for SRM Users." voltage change in response to a
NIST Special Publication, 260-100, change in the composition of the
1993.) material in its flow cell.
Calibration Curve: A series of Device: A list of the various
standard samples containing known electronic assemblies in the instrument
concentrations of the analyte are that are connected to the network and
analyzed. These standards should monitored by the program.
cover the range of interest and have a Dosing: Injecting known volumes of
matrix composition as similar to the gas into an instrument.
samples as possible. A blank sample
Drift: Compensates standard
must be analyzed and subtracted from
calibration and accounts for variances
each of the standard samples. The
or drift in the instrument hardware
Adjusted Area Aadj is plotted along the
that can slightly change the
X-axis versus the known concentration
calibration.
along the Y-axis for each of the
analyzed standard samples. The curve Drift Correction: The process of
that best fits the plotted points is the determining the drift factor.
calibration curve. Drift Factor: A factor that is applied
Calibration Factor: The slope of the to the signal of an analyzed defined
obtained calibration curve. standard to adjust it to the expected
signal; based on information
Calibration Plot: Displays the
extrapolated from the calibration
certified concentration versus the
curve. It is then used to adjust analyte
measured concentration of the sample.
signals to correct for instrument drift.
Certified: Concentrations for a
Drift Repetition: The number of drift
standard.
standards used to adjust the
CFR: Code of Federal Regulations calibration curve to the instruments
Checksum: A four digit number current conditions.
unique to the application software and Dry, Ash-Free Basis: Data
used to verify proper installation. This calculated to a theoretical base of no
number will vary between electronic moisture or ash associated with the
assemblies but is constant between sample.
instruments for a given electronic
Dry Basis: Data calculated to a
assembly. This number changes with
theoretical base of no moisture
each software update.
associated with the sample.
Class: A two digit listing of all
Duty Cycle: The percentage of time
different groups of circuit boards that
that the heater is operating.
are signed on to the network. Each
group will have a distinct class
assigned.
Counters: Tracks and then indicates
when periodic maintenance is
necessary.
122 AC600 Glossary

E Minimum Analysis Time: The
minimum amount of time allotted for
Encoding: Customizes the
analysis. This is also called integration
appearance of the data. Select either
time. During this time the cell output
Unicode or ASCII. Both ASCII and
is being integrated to determine the
Unicode are codes used to represent
result.
text making it possible to transfer data
from one computer to another. Unlike Moisture: Denotes the moisture as
ASCII, which uses 7 bits for each determined.
character, Unicode uses 16 bits for
each character, which means that it
N
can represent more unique characters;
therefore, Unicode is more useful for NI Version: The version number of
languages such as Chinese, Greek, the software currently being used. This
and Japanese, but not as useful for number may vary between circuit
English or Western European boards, but is constant between
languages. instruments for a given circuit board.
F O
Field Delimiter: Determines how the Origin: The intersection of the X and
transmitted data will be separated. Y axes. On the calibration curve this is
zero concentration and zero signal.
Flow Control: Selects the means to
control the data flow from one device Orphan: The database keeps track of
to another to ensure the receiving data objects such as samples,
device can handle all of the incoming calibrations, standards, methods, etc.
data. that are associated with each other.
Orphan database objects are created
when the connection between data
I objects is broken due to a rare
Instance: A unique number assigned occasion such as when a sample is
to an electronic assembly that shows deleted and the software does not
how many variations of each electronic perform the save correctly.
assembly are present in the
instrument.
P
Parity: The quality of being odd or
L even. Parity is used to ensure the
LCL: Lower Control Limit validity of the data.
Pause: Select to stop or delay an
analysis and then resume the analysis
M manually or at a predetermined time.
MAC- ID: The network ID number pdf: portable document format
assigned to the electronic assembly
connected to the network. This Pneumatic Pressure: The pressure
number is assigned at power up and of the pneumatic gas (compressed
can vary. air). The value is in psi (pounds per
square inch).
Method: A set of analysis parameter
values specified for an analysis. Poll Devices: Determines which
electronic assemblies are signed on to
the network.
Glossary AC600 123

Port: The serial port of the computer S
used to connect and communicate with
Sample: A determined mass of a
the balance. Default COM 2.
substance of unknown analyte
ppm: parts per million concentration. The analyte
Precision: Variability of the individual concentration will be determined by
results of replicate measurements. performing the analysis.
Preload Depressurization: The Sample Prep Power: The set
length of time the system will furnace power during sample
depressurize before the loading head preparation time.
opens. Sample Prep Time: The time period
before analysis that surface oxides are
removed. This setting should always
Q
be just below the melting point.
Qvad: Gross Calorific Value at Sample Preparation Time is not
constant volume, as-determined basis. included or added to the Integration
Qvar: Gross Calorific Value at Time Period.
constant volume, as-received basis. Send: Select to send a weight from
Qvd: Gross Calorific Value at constant the balance. When operational, the
volume, dry basis. balance reading will display in the
Qvdaf: Gross Calorific Value at spreadsheet.
constant volume, dry ash-free basis. Send Command: The command sent
Qvad Max (J/g): Gross Calorific from the instrument that will allow the
Value at constant volume, as- balance results to be sent and
determined basis. automatically entered into the
spreadsheet for the sample.
Sensitivity Factor: A multiplicative
R factor applied to the adjusted area
Readability: The smallest increment (Aadj) for the purpose of adjusting the
of weight displayed. Determines the units and to give a calibration factor
number of digits that will display from near 1.0.
the balance results. Serial Number: The hardware ID
Recalculate: After an analysis is number assigned to the electronic
complete, Recalculate Results can be assembly. This number is assigned
used to recalculate the result if the during manufacturing and is unique to
extraction data or calibration has each electronic assembly. The serial
changed. number is stored on the circuit board
Recalculated Date: The date when in a PROM.
an analysis is recalculated. Until an Significant Digits: The digits
analysis is recalculated, this column required to represent the accuracy of
will display the same data as the an approximate number beginning
Analysis Date column. with the leftmost non zero digit and
Reporting Units: Determines the ending with the rightmost non zero
elements that will display in a plot or digit (or a zero considered to be the
report. exact value). For example 0.132 has
Residual Error: Plots the residual three significant digits and 3.142 has
error versus the certified concentration four significant digits.
of the sample. Residual Standards: Determination of analyte
Error=Calculated-Certified. concentration by several laboratories
utilizing more than one technique
when applicable.
124 AC600 Glossary

Stop Bits: The number of data bits W
that are used to signal the end of
Weighting: Displays a factor
transmitted data.
manually entered by the user to
weight a particular calibration point.
T When one calibration point is assigned
a higher value than other calibration
Tare: Set the balance display to zero.
points, that point is considered more
Text Export Buffers: Select to important and is therefore favored by
export raw data buffers to another the calibration curve.
software application.
Total Moisture (H2O): Denotes the
total moisture as received.
Transmission Formats: Transmit
data to a network computer for
storage and/or processing.
TruSpeed: A calculation mode used
to improve analysis speed and
precision.
U
UCL: Upper Control Limit
Uncertainty: The range of values
within which the true value is
estimated to be. It is the best estimate
of the possible inaccuracy due to both
random and systematic error. (Taylor,
John Keenan. Statistical Techniques
for Data Analysis. Lewis Publishers,
Inc.: Chelsea, Michigan. 1990).
V
VDC: Volts Direct Current. Current
flows in a single direction.
Version: The version number of the
application software located on the
electronic assembly. This software can
be upgraded from the network
procedure.
Glossary AC600 125

126 AC600 Glossary

13 Index
A
Accessories List ..............................................................................135
Ambient Chart, Monitoring...............................................................82
Analysis
of Samples ...............................................................................518
Preparing for ............................................................................54
Sequence (Diagram) ..................................................................1031
Archive Log ...................................................................................466
B
Balance
Check Balance Parameters .........................................................34
Communication, Establishing ......................................................35
Control Panel (Photograph) ........................................................34
Installation ...............................................................................33
Setup ......................................................................................36
Test Procedure ..........................................................................36
Bar Code Reader (Optional) .............................................................317
Bucket
Lid (Illustration) ........................................................................1024
Lid Alignment Procedure ............................................................939
Polishing Bucket and Baffle Procedure ..........................................626
Water Level Switch (Illustration) .................................................1022
Index AC600 131

Buffers, Export Text .......................................................................537
C
Calculations, Critical .......................................................................73
Calibration ....................................................................................524
Standards, Define .....................................................................524
Change User Permission ..................................................................428
Chiller, External (Optional)
Add Water ................................................................................315
Installation ...............................................................................311
Set Temperature .......................................................................316
Clone Button .................................................................................410
Combustion Vessel, Oxygen
O-ring Replacement ...................................................................614
Preparation for Analysis .............................................................54
Compact/Repair, Database ..............................................................460
Components and Accessories List .....................................................135
Configuring System ........................................................................430
Configure Maintenance Counters ......................................................66
Copy Protection Key .......................................................................931
Creating a Sample Template ............................................................434
Crucible Preparation .......................................................................54
D
Data Transmit Installation ...............................................................213
Data
Export .....................................................................................536
Import .....................................................................................536
Transmit ..................................................................................538
132 AC600 Index

Databases, Managing .....................................................................450
Connection, Add ........................................................................454
Delete a Sample.............................................................................519
Detach a Frame .............................................................................424
Display Original Screen Layout .........................................................425
Dock Wizard ..................................................................................940
Duty Cycle Procedure .....................................................................941
E
Edit a Method ................................................................................59
Equipment packages .......................................................................130
Error/Fault Conditions .....................................................................934
Ethernet Adapter, Configuring..........................................................911
Export Button ................................................................................410
Export Data ...................................................................................536
F
Facility Requirements (Illustration) ...................................................102
Fault Conditions .............................................................................934
Fields, Configure ............................................................................415
Fields, User-Defined .......................................................................445
Fill Cells with Same Data .................................................................514
Filter, Fan
Housing (Photo) ........................................................................625
Removal and Cleaning ...............................................................625
Filters, Sample ...............................................................................520
Filter, Water
Housing (Photo) ........................................................................25;312
Replacement ............................................................................624
Index AC600 133

Firewall, Configuring Settings ..........................................................920
Flow Diagram ................................................................................1030
Fonts, Configure ............................................................................414
Formating, Number ........................................................................446
Formulas, User-Defined Fields..........................................................447
G
Gearbox, Motor Stirrer (Illustration) .................................................1020
H
Hydrostatic Testing.........................................................................146
I
Ignitor Wire, Replacing ...................................................................619
Import Data ..................................................................................534
Instrument
Installation ...............................................................................23
Rear View (Illustrations) ............................................................107
Overview (Illustrations) .............................................................105
Interference to Other Devices ..........................................................125
International Installation .................................................................214
J
Jacket
Assembly (Illustration)...............................................................1021
Thermistor (Photo) ....................................................................630
134 AC600 Index

L
Lanquage, Select............................................................................44
Layout, Customize ..........................................................................418
Layout, Display Original ..................................................................425
Layout, Save .................................................................................424
Leak Check of Oxygen Combustion Vessel .........................................613
Lift-Arm
Assembly (Illustration)...............................................................1028
Lubricating Screw Procedure .......................................................632
Positions (Illustration)................................................................1029
Screw (Illustration) ...................................................................1012
Screw Lubricating ......................................................................632
Log Archive, Database ....................................................................466
Log File, View ................................................................................610
Login Periodic Maintenance ..............................................................68
Login Sample .................................................................................514
M
Maintenance Counters, Configure .....................................................66
Periodic Schedule ......................................................................63
Messages, Error .............................................................................934
Method .........................................................................................59
Create .....................................................................................59
Import a Method .......................................................................513
Monitor, Ambient ......................................................................82
Move a Pane ..................................................................................422
N
Needle Valve (Troubleshooting) .......................................................93
Index AC600 135

O
Options .........................................................................................133
Oxygen Charger O-Rings, Replacement .............................................616
Oxygen Combustion Vessel Safety Notice ..........................................144
P
Parts List .......................................................................................130-135
Periodic Maintenance Schedule ........................................................63
Permission, Add or Change User ......................................................428
Pneumatic Manifold Assembly (Illustration) .......................................1018
Prep Station, Vessel - Refer to Vessel Prep Station
Preparation for Analysis ..................................................................54
Print Results ..................................................................................530
Proof Testing Oxygen Combustion Vessel ..........................................146
R
Recalculate Results.........................................................................526
Resizing a Pane ..............................................................................423
Results, Printing .............................................................................530
S
Sample
Analysis ...................................................................................518
Filters ......................................................................................520
Login .......................................................................................514
Preparation ..............................................................................54
Signature, Applying ...................................................................528
Template, Create ...................................................................... 434
Screen Layout, Dialog Box ...............................................................424
Select Language.............................................................................44
136 AC600 Index

Setup, Balance...............................................................................36
Software
Error Codes ..............................................................................938
Installing..................................................................................93
Solenoids and Switches ...................................................................88
Specifications ................................................................................141
Standard Calibration .......................................................................524
System, Configuring .......................................................................430
T
Tab Menu ......................................................................................422
Thermistor, Offset ..........................................................................810
Thread Fuse ..................................................................................55
Toolbars ........................................................................................412
Transmit Results ............................................................................538
Troubleshooting, General ................................................................93
U
User-Defined Fields ........................................................................445
User Permission, Add or Change ......................................................426
Index AC600 137

V
Vessel, Oxygen Combustion
O-Ring Replacement ..................................................................614
Preparation for Analysis .............................................................54
Thread Fuse .............................................................................55
Vessel Prep Station
Fill Button ................................................................................57
Fill Side....................................................................................56
Rear Connections ......................................................................210
Vent Side .................................................................................519
W
Warranty.......................................................................................116
Water
Adding to Chiller .......................................................................315
Draining and Replacing ..............................................................622
Filter, Replacing ........................................................................624
Heater and Pump Assembly (Illustration) .....................................1023
Manifold Assembly (Illustration) ..................................................1014
System, Filling ..........................................................................622
Wiring Diagram ..............................................................................104
138 AC600 Index

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4 System Setup ............................................................................. 41

7 Theory of Operation ................................................................... 71

10 Illustrations ............................................................................. 101

11 Schematics ............................................................................... 111

12 Glossary ................................................................................... 121

13 Index ....................................................................................... 131

Figure 1-1 Declaration of Conformity ................................................126

110 AC600 Introduction

Introduction AC600 111

By installing the Licensed Software, the Licensee acknowledges that

This is an agreement between the Licensee and LECO Corporation

"Instruction Manual" shall mean a guide describing the use and

II. License Grant

a. the right to use a copy of the Licensed Software in executable form

c. the right to make one backup copy of the Licensed Software.

112 AC600 Introduction

1. transfer or allow transfer of copies of the Licensed Software to any

3. cause or permit unauthorized copying, reproduction, or disclosure of

4. attempt to disassemble modify, or reverse engineer the Licensed

5. attempt to defeat or defeat the copy-protection mechanism;

6. attempt to or access features not purchased.

III. Enhancements And Support

IV. Termination Of Software License

V. Copyright And Proprietary Information

Introduction AC600 113

114 AC600 Introduction

b) All notices hereunder shall be in writing and shall be sent by

c) No delay on the part of LECO in exercising any right, power or

d) No amendment, modification or waiver of, or any consent with

e) This Software License shall be construed in accordance with and

f) Licensee agrees that it is responsible for obtaining proper

Introduction AC600 115

Equipment manufactured by LECO Corporation, St. Joseph, Michigan is

116 AC600 Introduction

LECO Corporation is not responsible for damage to any associated

Introduction AC600 117

Disposal of WEEE and the Wheeled Bin Symbol

Furthermore, WEEE is a vast source of raw materials. With the ever

If equipment is collected separately, the equipment can be recycled

Electrical and Electronic Equipment is labeled with the following

End users should contact their dealer/distributor or our company on

118 AC600 Introduction

Dell ProSupport provides expert assistance when you need rapid

24 x 7 Access to advanced-level North American-based phone

Live Chat tech support

DellConnect remote diagnosis and resolution

Next Business Day On-Site Service after Remote Diagnostics

For more information, call 1-800-WWW-DELL (1-800-999-3355) or

Introduction AC600 123

An internet connection is required to complete the transfer. If an

For Domestic Customers:

For International Customers:

2. Do not enter information into the fields. Instead, click

124 AC600 Introduction

Reorient or relocate the radio or television receiving antenna.

Introduction AC600 125

126 AC600 Introduction

This instruction manual provides information about the AC600 as

Chapter 1, Introduction, page 15, describes general information

Chapter 2, Installation, page 21, describes hardware setup and

Chapter 3, Option Installation, page 31, describes the purchasable

Chapter 4, System Setup, page 41, describes starting and

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