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  • Identification of Aliphatic & Aromatic Carboxylic Acid

    Încărcat de

    Mona Nasr
    130 vizualizări3 pagini
    This document provides methods to identify different types of acid amides, imides, and ammonium salts. 1) Physical properties like state, color, odor, solubility and reaction to litmus paper can be used to differentiate between compounds like phthalimide, benzamide, and urea. 2) Chemical tests like reaction with sodium carbonate, 30% sodium hydroxide, and biuret test can identify these compounds. 3) Confirmatory tests like phthalimide test, fluorescein test, reaction with concentrated sulfuric acid and ferric chloride can be done to distinguish between phthalimide, ammonium oxalate, and ammonium ben

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    This document provides methods to identify different types of acid amides, imides, and ammonium salts. 1) Physical properties like state, color, odor, solubility and reaction to litmus paper can be used to differentiate between compounds like phthalimide, benzamide, and urea. 2) Chemical tests like reaction with sodium carbonate, 30% sodium hydroxide, and biuret test can identify these compounds. 3) Confirmatory tests like phthalimide test, fluorescein test, reaction with concentrated sulfuric acid and ferric chloride can be done to distinguish between phthalimide, ammonium oxalate, and ammonium ben

    Drepturi de autor:

    © All Rights Reserved
    Descărcați ca DOCX, PDF, TXT sau citiți online pe Scribd
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    130 vizualizări3 pagini

    Identification of Aliphatic & Aromatic Carboxylic Acid

    Încărcat de

    Mona Nasr
    This document provides methods to identify different types of acid amides, imides, and ammonium salts. 1) Physical properties like state, color, odor, solubility and reaction to litmus paper can be used to differentiate between compounds like phthalimide, benzamide, and urea. 2) Chemical tests like reaction with sodium carbonate, 30% sodium hydroxide, and biuret test can identify these compounds. 3) Confirmatory tests like phthalimide test, fluorescein test, reaction with concentrated sulfuric acid and ferric chloride can be done to distinguish between phthalimide, ammonium oxalate, and ammonium ben

    Drepturi de autor:

    © All Rights Reserved
    Descărcați ca DOCX, PDF, TXT sau citiți online pe Scribd
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    din 3

    Identification of Acid Amides and Imides

    Phthalimide Soluble in Cold Water 2) 30% NaOH test:


    (1/2 spunk. +2ml H2O) 1 Sp Unk. + 2ml of 30% NaOH Heat
    Give Ammonia odur on hot
    Urea
    Phthalimide or Benzamide
    Benzamide Soluble in Hot Water
    (1/2 spunk. +2ml H2O)+heat III) Confirmatory Test:
    Phthalimide or benzamide
    5) Action to litmus paper: 1 ( For Benzamide) : No Confirmatory
    Test
    Urea Neutral: urea or Benzamide
    Slightly Acidic: phthalimide
    2 ( For Urea):
    1- Biuret Test
    II) Chemical Properties: Few crystal of urea in TT
    I) Physical Properties: 1) Na2CO3: Heat until melt and white residue

    1) State:Solid 2ml test solution (1/2 spunk. +2ml H2O) Add 1ml 10% NaOH and dissolve
    dissolve + 1 Sp. Na2CO3
    2) Color: Colorless Crystals or White Add few drops of CuSO4
    Powder Slight Eff. : Phthalimide
    Purple colour
    No Eff : urea or Benzamide
    3) Adour: odourless
    4) Solubility:

    1
    Identification of aliphatic and aromatic Ammonium salts
    ( NH4 oxalate ) ( NH4 Benzoate )

    2) C.H2SO4 :
    3 ( For phthalimide ) : I) Physical Properties: In D.T.T
    1) State :Solid 1 sp unknown + 1 ml conc H2 SO4 &Heat
    1- phthalimide test :
    In D.T.T 2) Color: Colorless crystal or White Eff + no Black ( NH4 oxalate )
    1/2 Sp. Phthalimide + 1/2 Sp. salicylic Powder -ve ( NH4 Benzoate )
    acid + 2-3 dps C.H2SO4
    Heat on direct flame till red (1 min.) 3) Adour: odourless
    cool under tap H2O 4) Solubility: Soluble in cold Water 3) Ferric Chloride test:
    add 1 ml then triturate by glass rod
    add excess NaOH 10% gives pink (1/2 spunk. +2ml H2O) 2ml unknown solution (1/2 Sp. Of unknown
    colour . +2 ml H2O )
    5) Action to litmus paper: Neutral add few dps 2-3 drop of FeCl3
    A) yellow solution ( NH4 oxalate )
    II) Chemical Properties: B) Buff ppt ( NH4 Benzoate )
    2- Fluorescein test :
    In D.T.T
    1/2 Sp. Phthalimide + 1/2 sp resorcinol 1) Na2CO3: (4) 30% NaOH test:
    + 2-3 dps C.H2SO4
    Heat on direct flame till red (1 min.) 2ml test solution (1/2 spunk. +2ml H2O) 1 Sp Unk. + 2ml of 30% NaOH
    cool under tap H2O dissolve + 1 Sp. Na2CO3 Gives Give Ammonia odur on cold
    add 1ml then triturate by glass rod add no Eff. It's not Acidic compound
    excess NaOH 10% gives Red color with ( NH4 Benzoate ) or (NH4 oxalate )
    green Fluorescence (Green Ring)

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