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Experiment 6 observed that adding acetone or isopropyl alcohol to sodium hydroxide and iodine produced a yellow precipitate with an odor like betadine. This indicates that acetone and isopropyl alcohol can undergo the haloform reaction to produce haloforms.
Experiment 7 observed that mixing acetaldehyde and sodium hydroxide produced a yellow solution with an acetaldehyde odor. Boiling the mixture produced an orange solution with a stronger crotonaldehyde odor, indicating that acetaldehyde underwent aldol condensation to form crotonaldehyde.
The experiments demonstrated the haloform reaction and aldol condensation reactions through observation of color changes and distinctive odors produced.
Experiment 6 observed that adding acetone or isopropyl alcohol to sodium hydroxide and iodine produced a yellow precipitate with an odor like betadine. This indicates that acetone and isopropyl alcohol can undergo the haloform reaction to produce haloforms.
Experiment 7 observed that mixing acetaldehyde and sodium hydroxide produced a yellow solution with an acetaldehyde odor. Boiling the mixture produced an orange solution with a stronger crotonaldehyde odor, indicating that acetaldehyde underwent aldol condensation to form crotonaldehyde.
The experiments demonstrated the haloform reaction and aldol condensation reactions through observation of color changes and distinctive odors produced.
Experiment 6 observed that adding acetone or isopropyl alcohol to sodium hydroxide and iodine produced a yellow precipitate with an odor like betadine. This indicates that acetone and isopropyl alcohol can undergo the haloform reaction to produce haloforms.
Experiment 7 observed that mixing acetaldehyde and sodium hydroxide produced a yellow solution with an acetaldehyde odor. Boiling the mixture produced an orange solution with a stronger crotonaldehyde odor, indicating that acetaldehyde underwent aldol condensation to form crotonaldehyde.
The experiments demonstrated the haloform reaction and aldol condensation reactions through observation of color changes and distinctive odors produced.
Procedure experiment Observation result Reaction Conclusion
1.
6. Haloform Reaction Before Acetone and isopropyl
- Sodium hydroxide : alcohol can produce a 3 mL of 5% Sodium colorless haloform and has an odor Hydroxide solution - Iodium : brownish red like betadine (medicine) - Acetone : colorless - Pouring into test tube 1 and test - Isopropyl alcohol : tube 2 colorless - Adding 5 drops of acetone into test tube 1 and test tube 2 After - Adding 10 mL iodium solution - Sodium hydroxide + into test tube 1 and test tube 2 acetone : colorless - Shaking until the colour of - Sodium hydroxide + iodium isnt lost acetone + iodium : - Observing yellow precipitate, has - Smelling it an odor like betadine (medicine) Yellow sediment & - Sodium hydroxide + has an odor isopropyl alcohol : colorless - Sodium hydroxide + isopropyl alcohol + iodium : yellow precipitate, has an odor like betadine (medicine)
7. Condensation of Aldol Before An aldehyde (acetaldehyde)
- NaOH : Colorless can produce an aldol with - Acetaldehyde : yellow crotonaldehyde odor After 4 mL of 1% Sodium Hydroxide - NaOH + acetaldehyde : solution yellow , has an odor - NaOH + acetaldehyde + - Pouring into test tube boling : orange , has a - Adding 0,5 mL acetaldehyde stronger odor solution (crotonaldehyde) - Shaking - Smelling it (acetaldehyde) - Boiling until 3 minutes - Observing - Smelling it again