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After synthesis of graphite into graphite oxide and then reduction of graphite oxide to graphene

oxide. The next mechanism is a mechanism of incorporation (polymerization) Polyaniline produced


from the aniline with graphene oxide produced from the synthesis of graphite oxide.

Polyaniline is a polymer material which is active or conductive and are categorized as the building
blocks Pseudokapasitor whereas graphene supercapacitor type is the type of constituent material
EDLC supercapacitor type. Both properties are combined and will produce Hybrid Capacitors are
made of different combinations pseudocapacitor supercapacitor or EDLC made.

The mechanism of the reaction of the respective starting materials were combined into one, namely
Polyaniline, Graphene Oxide, and compound agent. Compounds agent whose role is to
Methylbisakrilamide Ammonium peroxydisulfate. In this reaction will occur hydrogen bonds and
covalent bonds between the graphene oxide with polyaniline facilitated by ammonium
peroxydisulfate (initiator substances).

The results of the reaction can be seen in floc-floc formed after the stirring and ice bath, the floc
greenish-black. The color indicates the aniline bound by graphene oxide to graphene oxide
polyaniline transplantation process is successful.

Reaction Mechanism Composite PANi / GO / Cellulose / La


After the merger PANi with graphene oxide, the study adds cellulose as a reinforcement of the
network to form a double-network hydrogels and Lanthanum metal as the metal element will
didopan to increase the conductivity properties of the materials to be formed. The following
reaction scheme:

As a composite material PANi / GO / Cellulose / La it can be said that the conductivity contained in
PANi will be enhanced in the presence of metallic lanthanum as a metal pendoping and cellulose
present as reinforcing network which will facilitate material supercapacitors to perform redox
reactions and expanding the area of conductive material ,

Material characterization
2.2.2.1. FTIR (Fourier Transform Infra Red)
The principle instrument Fourier Transform Infra Red (FT-IR) is when infrared radiation is passed
through a trailer, then the molecules can absorb (absorb) the energy and pass transitions between
vibrational levels (ground state) and the level of vibration excited (exited stated).

XRD

X-ray diffraction or XRD (X-Ray Diffraction) is the analytical technique of X-ray sources to determine
the lattice parameters and structure of the crystal in a solid material. The principle of X-ray
diffraction X-rays are experiencing diffraction (scaterring) after the collision with the atoms of the
crystal. Diffraction pattern showing the crystal structure.

capacitance
The composite material can be used as a supercapacitor when the material has a capacitance is very
large. Capacitance is a parameter that describes the ability of a material to store an electric charge in
a while.

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