10

10-1)
a)
The regression equation is

C2 = 29.5 - 0.304 C1

Predictor Coef SE Coef T P

Constant 29.476 3.175 9.28 0.000

C1 -0.30400 0.03432 -8.86 0.000

S = 0.149063 R-Sq = 85.8% R-Sq(adj) = 84.7%

(b
Analysis of Variance

Source DF SS MS F P

Regression 1 1.7438 1.7438 78.48 0.000

Residual Error 13 0.2889 0.0222

Total 14 2.0326

. significant

1
10-5)

The regression equation is

C2 = - 73.6 + 0.517 C1

Predictor Coef SE Coef T P

Constant -73.588 6.964 -10.57 0.000

C1 0.51663 0.03805 13.58 0.000

S = 1.36336 R-Sq = 95.8% R-Sq(adj) = 95.3%

Analysis of Variance

Source DF SS MS F P

Regression 1 342.73 342.73 184.39 0.000

Residual Error 8 14.87 1.86

Total 9 357.60

No evidence of lack of fit (P >= 0.1).

Residual Plots for C2

Normal Probability Plot Versus Fits
99
2
90
1
Residual
Percent

50
0

10 -1

1 -2
-3.0 -1.5 0.0 1.5 3.0 10 15 20 25 30
Residual Fitted Value

Histogram Versus Order

4
2
3
Frequency

1
Residual

2 0

1 -1

0 -2
-2 -1 0 1 2 1 2 3 4 5 6 7 8 9 10
Residual Observation Order

2
10-7)

10-9)

Analysis of Variance for C7, using Adjusted SS for Tests

Source DF Seq SS Adj SS Adj MS F P

Concentration 1 18.000 18.000 18.000 14.40 0.019

Temp 1 112.500 112.500 112.500 90.00 0.001

Concentration*Temp 1 0.500 0.500 0.500 0.40 0.561

Error 4 5.000 5.000 1.250

Total 7 136.000

3
 Residual Plots for C7
Normal Probability Plot Versus Fits
99
1.0
90
0.5

Residual
Percent
50 0.0

-0.5
10
-1.0
1
-2 -1 0 1 2 80.0 82.5 85.0 87.5 90.0
Residual Fitted Value

Histogram Versus Order

2.0 1.0

1.5 0.5
Frequency

Residual
1.0 0.0

0.5 -0.5

-1.0
0.0
-1.0 -0.5 0.0 0.5 1.0 1 2 3 4 5 6 7 8
Residual Observation Order

Analysis of Variance for C7 (coded units)

Source DF Seq SS Adj SS Adj MS F P

Main Effects 2 130.500 130.500 65.2500 59.32 0.000

Residual Error 5 5.500 5.500 1.1000

Lack of Fit 1 0.500 0.500 0.5000 0.40 0.561

Pure Error 4 5.000 5.000 1.2500

Total 7 136.000

Half Normal Plot of the Standardized Effects

(response is C7, Alpha = .05)
1.0E+02 Effect Ty pe
Not Significant
Significant

99.98
Percent

98
95

85
80
temp

50
concentration
20
0
0 2 4 6 8 10
Absolute Standardized Effect

4
 Residual Plots for C7
Normal Probability Plot Versus Fits
99
1.0
90
0.5

Residual
Percent

50 0.0
-0.5
10
-1.0
1
-2 -1 0 1 2 80.0 82.5 85.0 87.5 90.0
Residual Fitted Value

Histogram Versus Order

2.0
1.0
1.5 0.5
Frequency

Residual
1.0 0.0

-0.5
0.5
-1.0
0.0
-1.0 -0.5 0.0 0.5 1.0 1.5 1 2 3 4 5 6 7 8
Residual Observation Order

10-11)

Factors: 4 Base Design: 4, 16

Runs: 16 Replicates: 1

Blocks: 1 Center pts (total): 0

All terms are free from aliasing.

* NOTE * This design is not orthogonal.

The following terms cannot be estimated and were removed:

A*B*C*D

* NOTE * Some of the terms requested in MEANS were removed from the analysis.

Estimated Effects and Coefficients for C9 (coded units)

Term Effect Coef

Constant 69.375

A 20.250 10.125

B 1.750 0.875

5
C 8.500 4.250

D 13.250 6.625

A*B -1.250 -0.625

A*C -19.500 -9.750

A*D 15.250 7.625

B*C 1.000 0.500

B*D -1.750 -0.875

C*D -2.500 -1.250

A*B*C 0.500 0.250

A*B*D 2.750 1.375

A*C*D -3.000 -1.500

B*C*D -4.000 -2.000

Half Normal Plot of the Effects

(response is C9, Alpha = .05)

Effect Ty pe
98 Not Significant
Significant

95 A F actor N ame
A A
B B
90 C C
AC
D D
Percent

85
80 AD
D
70 C
60
50
40
30
20
10
0
0 5 10 15 20
Absolute Effect
Lenth's PSE = 3.1875

Estimated Effects and Coefficients for C9 (coded units)

Term Effect Coef SE Coef T P

Constant 69.700 1.153 60.44 0.000

A 20.900 10.450 1.153 9.06 0.000

C 9.150 4.575 1.153 3.97 0.003

D 13.900 6.950 1.153 6.03 0.000

A*C -18.850 -9.425 1.153 -8.17 0.000

A*D 15.900 7.950 1.153 6.89 0.000

6
S = 4.39823 PRESS = 524.934

R-Sq = 96.53% R-Sq(pred) = 89.53% R-Sq(adj) = 94.60%

Analysis of Variance for C9 (coded units)

Source DF Seq SS Adj SS Adj MS F P

Main Effects 3 2409.60 2260.63 753.54 38.95 0.000

2-Way Interactions 2 2429.63 2429.63 1214.81 62.80 0.000

Residual Error 9 174.10 174.10 19.34

Lack of Fit 2 44.60 44.60 22.30 1.21 0.355

Pure Error 7 129.50 129.50 18.50

Total 14 5013.33

Residual Plots for C9

Normal Probability Plot Versus Fits
99
5.0
90
2.5
Residual
Percent

50 0.0

-2.5
10
-5.0
1
-10 -5 0 5 10 40 60 80 100
Residual Fitted Value

Histogram Versus Order

4
5.0

3 2.5
Frequency

Residual

0.0
2
-2.5
1
-5.0
0
-6 -4 -2 0 2 4 6 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Residual Observation Order