Documente Academic
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2016
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Combustible
Dust Standards
Facts at Your
Fingertips:
Insulating Heat-
Transfer Piping
Developments
in Petroleum
Mixing: Refining
Protecting Industrial
Control Systems
Innovative Designs Monitoring Flame
and Agitator Seals
page 42
Hazards
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Cover Story
42 Part 1 Mixers: Four Innovations Worth a Closer Look
Many factors can impact the success of mixing in chemical process
operations. The design breakthroughs profiled here address some of the most
commonly encountered issues
50 Part 2 Reliable Operation and Sealing of
Agitators Mechanical seals, as required by most vessel
agitators, are systems sufficiently complex to warrant a good
understanding by engineers and good training for operators
In the News
7 Chementator
Making complex silicone parts by 3-D printing; Syngas-to-lipids
process demonstrated; A joint effort to enable the production of
sulfur-enhanced urea at large scale; Microbes make a meal of
PET; Extremophilic algae selectively recover precious metals from
solution; and more
14 Business News
TCV begins construction of new liquid polybutadiene plant in France; Vertellus 42
completes expansion for DEET insect repellent; Linde to build air-separation
unit in Malaysia; Startup of new purified terephthalic acid line in China; Praxair
signs contracts with glassmaker; and more
T
Bernd Reichert o ensure safe and reliable agitator
on the components of
EKATO operation, the sealing of the rotating an agitator including
shaft is of fundamental importance. the seal result mainly
Depending on the operating condi- from the hydraulic loads
IN BRIEF tions such as pressure, temperature and on the impellers
(1)
pB
With the assumption of a linear pres-
sure drop across the sealing interface cooling and sealing. It must also meet
(Figure 4), the closing and opening certain secondary conditions, such as
forces will balance when K = 0.5. In compatibility with the product and, if
practice, optimum performance is ob- necessary, conformity with the specifi-
tained when the value of K lies between cations of the U.S. Food and Drug Ad-
0.6 and 0.9. ministration (FDA).
The hydraulic balance ratio K is also Figure 6 compares barrier fluids used
used to characterize mechanical seals in mixing applications with respect
as unbalanced or balanced. Unbalanced to their suitability for various tasks. It
mechanical seals have K > 1, whereas is clear that the demands of lubrica-
balanced seals have K < 1. Unbalanced tion and cooling may conflict. Water
seals are expedient for simple operating cools efficiently, but lubricates poorly,
conditions, such as low pressures and whereas the reverse is true for min-
low agitator speeds. Here, the high hy- eral oils and pure glycerin. A mixture of
draulic balance ratio, with closing forces glycerin and water can be a success-
dominant, provides good sealing effi- ful compromise: the glycerin lubricates,
ciency without thermally overloading the while the water phase cools. For this
mechanical seal. In more-difficult oper- reason, glycerin/water mixtures should
ating conditions, such as high pressures always be used if possible. Unfortu-
and high agitator speeds, only balanced nately, not all products tolerate a glyc-
mechanical seals can be used. erin in-leakage of several milliliters per
So far we have ignored the closing day, though it is technically possible to
force contributed by the springs that collect the leaked barrier fluid and keep
form part of every mechanical seal. This it away from the product. FIGURE 6. For many applications, a
mixture of glycerin and water yields the
force is generally equivalent to a pres- Especially when water or organic sol- preferred balance of properties for the
sure of 12 bars. This is important at vents are used as barrier fluids, special barrier fluid
low operating pressures, but can confi-
dently be neglected at vessel pressures Barrier fluid Lubrication Cooling Circulation Product FDA compliance
above 10 bars. Nevertheless, even compatibility
high-pressure mechanical seals require Water
springs to keep them closed while they
Mineral oil 20 cSt
are unpressurized.
Glycerin 100%
VALUE CREATION
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Challenging Column Designs
Large diameter and tall towers present performance and installation
challenges. To help maximize eficiency and capacity and simplify
installation for these towers, Koch-Glitsch has developed innovative
mechanical support technologies that are engineered to:
Maintain levelness and mitigate delection
Enable cross low of liquid and froth on every tray deck
Minimize interference with vapor and liquid trafic between trays
Allow introduction through vessel manway openings
Eliminate or signiicantly reduce welding inside the vessel
Support multiple devices on one set of beams
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Circle 17 on p. 94 or go to adlinks.chemengonline.com/61495-17
(2)
20 Summary
Vessel In most mixing systems, reliable agitator
10
sealing requires a complete mechanical
0 sealing system. As well as the mechanical
2 4 6 8 10 12 14 16 18 20 seal itself, auxiliary equipment is needed to
maintain an adequate flow of fluid at the
Operating time, h
correct temperature and pressure to cool
56 CHEMICAL ENGINEERING WWW.CHEMENGONLINE.COM MAY 2016
design of the mechanical seal itself. The
sealing function of the vessel can only be
guaranteed and maintained if the complete
system is correctly selected, installed and
maintained.
When a mixing system is being commis-
sioned, support and training for the equip-
ment operators are very important to allow
work to proceed rapidly and without prob-
lems. Once the plant is up and running, train-
ing and support are often the cornerstones
needed to ensure high availability of the
complete mixing system.
Edited by Charles Butcher
References
EKATO the Book (2012): Handbook of Mixing Technology, 3rd edi-
tion, EKATO GmbH, ISBN 9783-000386602.
Author
Bernd Reichert is a Senior Mechanical Engi-
FIGURE 12. This automatic refill system serves 24 mechanical neer at EKATO Rhr- und Mischtechnik GmbH
seals (Hohe-Flum-Strasse 37, 79650 Schopfheim,
Germany; E-mail: bernd.reichert@ekato.com).
He is head of the Sealing Technology group
and lubricate the seal faces. Careful selec- within EKATOs R&D department. Reichert
holds a bachelors degree in mechanical engi-
tion of hydraulic and other components neering from the University of Applied Sci-
is thus just as important as the reliable ences Konstanz (Germany).