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(Submitted April 13, 2017; in revised form August 20, 2017; published online September 27, 2017)
Distortion control during industrial carburizing and quenching operation of precision transmission com-
ponents is of utmost importance due to their direct impact on performance, such as efficiency, noise and
vibrations. The importance of controlling various heat treatment process parameters for mitigating dis-
tortion is well accepted, but their specific influence on mechanisms is less understood. In the present work,
an integrated finite element-based model is used to simulate gas carburizing and quenching operation on a
typical transmission shaft. Investigation is carried out on the effect of raw materials, carburizing and
quenching process parameters to predict, analyze and minimize distortion. The effect of phase transfor-
mation and generation of thermal strain during heating and cooling stage of heat treatment is investigated,
and the mechanisms of bending, diameter and length distortion of a shaft are analyzed. The displacive
nature of transformation of bainite at higher temperature with its inherent large shear component of
deformation was identified to be responsible for bending distortion in a shaft. Bainitic transformation,
martensitic transformation and thermal strains developed during quenching cause volume expansion which
leads to diameter expansion and lesser length shrinkage. Finally, bending distortion of a shaft and bore
distortion of a gear are contrasted, both in terms of mechanisms and distortion control strategies.
Fig. 1 (a) Top figure shows an undistorted shaft (before carburizing). Bottom figure shows a distorted one (after the shaft cools down from
quenching cycle). The shaft bends, diameter expands, and length shrinks. l and d are the initial length and diameter; l¢ and d¢ are the final
dimensions after distortion. (b) Schematic representation of how bending distortion of a shaft is calculated. B¢P is the amount of bending distor-
tion; d¢ d is the amount of diameter distortion/expansion (will be positive); l¢ l is the amount of length distortion/shrinkage (will be negative)
High—H
Chemistry/hardenability—H
Table 1 (a) Alloy chemistry specification range for 20MnCr5 grade steel, (b) two levels of alloy chemistry specification of 20MnCr5 grade steel, (c) two levels of car-
90
105
ideal critical diameter indicating hardenability of the material.
The ideal critical diameter was calculated from its chemical
composition and prior austenitic grain size, which was taken as
0.22
82.83
per ASTM 7 (Ref 37). In the integrated FEM model, the effect
1.3
1.4
0.17-0.22
of composition change was incorporated by changing the
1.0-1.3
1.1-1.4
relevant kinetics. Additionally, equalization time was chosen
from the carburizing stage and quench oil bath temperature
from the quenching stage. The model considered the heat
transfer coefficient of the quench oil to model the heat
extraction from the component. The heat transfer coefficient
of the quench oil was assumed to be constant in this work.
Table 1c shows the two levels (low ÔLÕ and high ÔHÕ) of the
carburizing and quenching parameters.
The shaft distorts in three distinct ways. It has a tendency to
bend; the diameter changes; and length changes as well.
Figure 1(a) shows the exaggerated figure of bending, expansion
of diameter and shrinkage in length of a shaft. Figure 1(b)
demonstrates, schematically, how bending distortion was
calculated. The line shows the central axis of the shaft. A, B
and C represent the original position of the central axis of the
shaft before heat treatment. Locations A and C are at the two
extremes of the shaft. Location B was chosen where the
diameter is maximum. The central axis of the shaft moves to A¢,
B¢ and C¢, respectively, after heat treatment and quenching
operation. This happens because the shaft bends and its
diameter and length change after heating and cooling cycle.
Low—L
41.10
1.0
1.1
Alloying element
axis of the shaft (refer Fig. 3a and b). As the shaft dips
vertically into the quench oil bath, node D (toward the lower
Mn
Mn
Cr
Cr
C
Table 2 Summary of the results of the effect of hardenability, equalization time and quench oil bath temperature on bending, diameter and length distortion of a
node D relative to node E was calculated, and this is a metric of
the bending of the central axis of the shaft. The net
displacement was calculated by square root of the displacement
Reason
in the x- and y- direction. We will consider this metric to
Length distortion
understand the mechanism of bending. Figure 4 shows the
Thermal strain
overall displacement of node D relative to node E (in the x- and
y-direction) during carburizing and quenching cycle. The inset
figure shows the displacement during the duration of the
quench.
Not significant …
Before the quenching begins, the relative movement of node
Amount, mm
ÔLÕ represents lower level and ÔHÕ represents higher level of respective process parameters value. The table summarizes the reason for various types of distortion
hardenability material (Fig. 4) and this is due to the difference
in prior microstructure of the samples before carburizing
Bainite + Martensite phase fraction 0.991
0.818
0.991
0.852
begins. During and after quenching, relative movement of node
D in ÔLÕ hardenability material catches up and passes that of ÔHÕ
hardenability material. This is prominent during the time period
53587-53620 s. Beyond 53620 s, the slope of two lines is
almost parallel.
The relative movement of node D is similar irrespective of
the quench oil bath temperature, till the carburizing cycle
Reason
how nodes near the central axis of the shaft (nodes D and E)
and near the surface (for example, nodes D1 and E1) move
independently during and after the quenching period (for
Not significant …
H (105 C)
H (90 min)
L (65 C)
Fig. 3 (a) A transmission shaft. Quenching direction is with thicker section going first into the quench bath. Node D and node E are chosen
arbitrarily near the axis of the shaft; node B is near the axis of the shaft and at maximum diameter; node Bx+ is on the surface and on the +x-
axis; node B2 is 20 mm from the axis of the shaft; nodes A and C are at the edge and near the axis of the shaft. (b) Cross section of the shaft,
showing nodes D, E, D1 and E1
Region III: positive less steep slope (beyond 53620 s). In how nodes are displaced closer to the center of the shaft. At
addition, slope of lines ÔLÕ and ÔHÕ is almost parallel. node D1 (Fig. 5d), at about 53585 s austenite starts transform-
ing to bainite. The amount of bainitic transformation is more in
To understand the displacement graphs in these three regions, ÔLÕ hardenability material compared to ÔHÕ hardenability mate-
phase transformation near the surface was considered, as rial. Also note that austenite transformed to bainite between
surface gets influenced most by the carburizing operation. 750 and 550 K. Austenite transformed to martensite at
Figure 5(c) and (d) shows the temperature, displacement and 53630 s and between 500 and 450 K. The amount of
phase fraction of node D1 in ÔLÕ and ÔHÕ hardenability material. martensite phase fraction is more in ÔLÕ hardenability material.
Node D1 is situated about 0.67 mm from the surface (Fig. 3), This is linked with the greater amount of bainite formation in
whereas the case depth in ÔLÕ and ÔHÕ hardenability ranges from lower hardenability material. The formation of bainite creates
1.0 to 1.7 mm. When quenching begins, the displacement of ferrite subunits (sheaves)–austenite interphases and resulted in
node D1 increases (displaces away from the axis of the shaft) concentration gradient which accelerates martensite transfor-
for few seconds and then falls continuously. The lines (Fig. 5c) mation kinetics. In addition, one can see the shape of the
show the temperature at node D1 during and after quenching martensite transformation kinetics is changed, becoming less
for ÔLÕ and ÔHÕ hardenability material. The temperature lines for sharp in comparison with high hardenability grade. This present
both hardenability materials coincide. As quenching begins, the simulation outcome is consistent with the similar previous
surface temperature falls drastically and this contracts the observation (Ref 38).
surface (the surface moves closer to the axis of the shaft). The It is well established in the literature that phase transforma-
initial rise in the displacement lines is being seen to depend on tion occurs in two main ways: the reconstructive mechanism
the amount of mass present below the nodes D–D1 (Fig. 3a). It and the displacive mechanism. The reconstructive transforma-
had been seen that this rise is more for node E1 (not illustrated tion involves uncoordinated diffusion of all of the atoms which
here). leads to substantial volumetric strains which are mostly
Figure 5(c) and (d) shows that the displacement of node D1 isotropic. The displacive transformations involve a combination
is not influenced by any phase transformation at that particular of a shear on the habit plane and a dilatational strain which is
node. In fact, phase transformation near the surface dictates directed normal to the habit plane. This transformation leads to
an invariant plane strain (IPS) as it leaves the habit plane The steeper slope in region II, in Fig. 5(a), is responsible for
undistorted and unrotated. The invariant plane strain has a large higher amount of bending in ÔLÕ hardenability material. The
shear component, and the transformed product forms plates steeper slope is due to bainite formation (near the surface) at
which minimize the elastic strain in the austenite phase higher temperature and its inherent large shear component of
(Table 3). deformation (Fig. 5d). There is a very small window at the start
Bainitic and martensitic transformation occurs by displacive of the quenching stage (stage II) that requires precise control to
mechanism. This causes a large deformation because of its minimize distortion. On the contrary, bore distortion in a gear
inherent large shear component. In addition, bainitic transfor- can be reduced by lowering the hardenability of the material
mation occurs at higher temperature compared to martensitic (Ref 8).
transformation. Because of the higher transformation temper- 3.1.2 Effect of Quench Oil Bath Temperature. To
ature of bainite, the deformation of the shaft is significantly understand the effect of quench oil bath temperature on
large (Ref 39). In ÔLÕ hardenability material, since the bending distortion of a shaft, two similar hardenability
transformation starts at higher temperature along with consid- materials (ÔLÕ hardenability material with DI of 41.10 mm)
erable higher amount of bainite (21% for ÔLÕ and 3% for ÔHÕ were quenched at two different quench oil bath temperature
hardenability material), slope is higher in region II (of Fig. 5a) (ÔL,Õ 65 C, and ÔH,Õ 105 C). All other process parameters were
compared to ÔHÕ hardenability material. kept similar (equalization time of 33 min). Bending distortion
In Fig. 5(a), the displacement of node D decreases for few measurements were made after the samples were cooled down
second (7 s). The possibility of this negative slope might be to room temperature. The shafts bend more when the quenching
due to the fall in temperature near the surface which gets was carried out at higher temperature (ÔHÕ) (Table 2).
influenced near the center, as there is no phase transformation During the early stage of quenching, in Fig. 4, the slope of
during this time. The rise in displacement lines in region II does ÔH quench-tempÕ curve is greater than ÔL quench-tempÕ curve.
not start immediately when bainite starts to form near the To understand this behavior, similar nodes were chosen near
surface (node D1 in Fig. 5d). There is few seconds lag in the the central axis of the shaft (nodes D and E) and near the
rise of displacement lines, which is around 3 s. The displace- surface (nodes D1 and E1). Similar analysis of temperature,
ment lines of ÔLÕ and ÔHÕ hardenability materials are almost displacement and phase fraction was carried out. Displacement
parallel in region III. Formation of martensite near the surface lines of node D have steeper slope in region II for higher
at relatively low temperature (compared to bainitic transforma- quench oil bath temperature (Fig. 6a). This steeper slope is
tion) (node D1 in Fig. 5d) gives a continuously increasing responsible for higher bending. The steeper slope is due to the
curve in region III. However, this does not cause any slope higher amount of bainite formation near the surface (D1) for
change in region III between ÔLÕ and ÔHÕ hardenability materials. higher quench oil bath temperature (Fig. 6b).
Similar analysis for temperature, displacement and phase 3.1.3 Effect of Equalization Time. To understand the
fraction distribution at nodes E and E1 showed similar graphs effect of equalization time on bending distortion of a shaft, two
as that of Fig. 5 (not illustrated here). similar hardenability materials (ÔLÕ hardenability material with
Table 3 Shear strain (s) and dilatational strain (d) component of various phases
Transformation Mechanism Shape change s d Morphology
DI of 41.10 mm) were carburized under similar conditions, carried out. The phase fraction, temperature and displacement
except at two different equalization time (ÔL,Õ 33 min, and ÔH,Õ with time were calculated at these nodes. No difference in the
90 min). Quench oil bath temperature (65 C) was kept similar phase fraction distribution was found irrespective of the
for the two samples. Bending distortion measurements were equalization time (not illustrated here).
made after the samples were cooled down to room temperature.
Equalization time does not have significant effect on bending 3.2 Diameter Distortion
distortion of a shaft (Table 2).
Diameter distortion of a shaft was calculated according to
To understand the mechanism, similar nodes were consid-
Fig. 1(a). The diameter of a shaft expands during carburizing
ered near the axis of the shaft—node D and node E—and near
and quenching operation. To understand the mechanism of
the surface—node D1 and node E1. Similar analysis was
Fig. 7 Effect of hardenability on diameter distortion of a shaft. Phase fraction distribution along the diameter of the shaft (node B to node Bx+)
in low (ÔLÕ) and high (ÔHÕ) hardenability materials. The inset figure shows the phase distribution near the surface. The amount of bainite and
martensite phase fraction in ÔHÕ is greater than in ÔLÕ
diameter distortion, the formation of the final phase fraction 3.2.2 Effect of Quench Oil Bath Temperature. The
along the diameter of the shaft was considered. Two diameter of a shaft expands more when it is quenched in higher
nodes—node B (near the central axis of the shaft) and node quench oil bath temperature (Table 2). To understand the
Bx+ (on the surface)—were chosen for investigation (Fig. 3). mechanism, the formation of the final phase fraction along the
3.2.1 Effect of Hardenability. The expansion of diame- diameter of the shaft was again considered.
ter of a shaft is greater in ÔHÕ hardenability material compared to Figure 8 shows the phase fraction and displacement/distor-
ÔLÕ hardenability material (Table 2). Figure 7 shows the tion distribution along the diameter of the shaft, when it is cooled
distribution of phase fraction—when the samples were cooled down to room temperature after quenching cycle. The inset
down to room temperature after quenching cycle—along the figure shows the distribution near the surface of the shaft. Till
diameter of the shaft. Note the amount of bainite and martensite 50 mm from the central axis of the shaft, bainite phase fraction
phase fraction in ÔLÕ and ÔHÕ hardenability material. The higher is higher with higher quench oil bath temperature. Overall (till
amount of bainite and martensite in ÔHÕ hardenability material 55 mm), bainite phase fraction was measured to be similar
leads to larger diameter expansion. irrespective of the quench oil bath temperature. Martensite phase
Fig. 9 (a) Temperature and displacement (in x-direction) of node Bx+ in low (ÔLÕ) and high (ÔHÕ) quench oil bath temperature (QT) during and
post-quenching. (b) Temperature and displacement (in x-direction) of node B2 in low (ÔLÕ) and high (ÔHÕ) quench oil bath temperature during and
post-quenching
fraction is higher when the quench oil bath temperature is lower. Figure 9(a) shows the displacement of the node Bx+ with time
However, diameter expansion is higher with higher quench oil when quenching begins. As soon as the quenching begins, the
bath temperature. This anomaly cannot be explained with the displacement of this node is higher when the quench oil bath
phase fraction distribution along the diameter of the shaft. temperature is high. This is so because of the temperature
The displacement curves in Fig. 8 show that till 30 mm difference of the quench oil bath. As soon as the quenching
from the axis of the shaft the displacement is approximately begins, the surface temperature falls so does its surface
same irrespective of the quench oil bath temperature. Beyond contracts (Bx+ will move closer to the axis of the shaft). This
30 mm, the displacement is high when the shaft is quenched contraction is relatively less when the quench oil bath
in higher quench oil bath temperature. To understand this, two temperature is high. At the final stage, when the component
nodes were considered—node Bx+ on the surface of the shaft is at ambient temperature, the displacement of node Bx+ is
(on the +x-axis) and node B2 which is approximately 20 mm greater for higher quench oil bath temperature. This is
from the axis of the shaft. At these nodes, displacement was equivalent to the fact that diameter expands more when the
calculated during and post-quenching (also refer Fig. 3a). quench oil bath temperature is higher. Figure 9(b) shows the
displacement of node B2 with time when quenching begins. 3.3.1 Effect of Hardenability. The shrinkage in length is
Similar phenomena happen when it is compared with the plot at lower in ÔHÕ hardenability material (Table 2). Figure 10 shows
node Bx+ (Fig. 9a). However, when the component reaches the distribution of phase fraction—when the samples were
room temperature, there is no difference in the displacement cooled down to room temperature after quenching cycle—a-
irrespective of the quench oil bath temperature. This is long the length of the shaft. Note the amount of bainite and
consistent with Fig. 8 of the displacement curves. martensite phase fraction in ÔLÕ and ÔHÕ hardenability material.
Because of the different quench oil bath temperature, nodes The higher phase fractions expand the length a bit. In addition,
B2 and Bx+ behave differently. Displacement of the node B2 is lower amount of bending in higher hardenability material also
same irrespective of the quench oil bath temperature, whereas helps in lesser shrinkage in length.
displacement of node Bx+ is greater when the quench oil bath 3.3.2 Effect of Quench Oil Bath Temperature. The
temperature is high. This is equivalent to saying that displace- length of a shaft shrinks less when the quenching is performed
ment of surface and subsurface (30 to 55 mm) is greater when in higher quench oil bath temperature (Table 2). To understand
the quenchant temperature is high. However, displacement of the mechanism, the formation of the final phase fraction and
the region near the core (till 30 mm) is same irrespective of development of thermal strains along the length of the shaft
the quenchant temperature. Because of the higher quenchant were again considered.
temperature, the surface and subsurface did not get back to the Thermal strains developed during carburizing and quench-
state where it should go. However, quenchant temperature does ing operation are responsible for lesser length shrinkage when
not have any effect near the core region. Some thermal strains quenching was performed at higher quenchant temperature.
have developed in the surface and subsurface regions, and these Higher amount of bending with higher quenchant temperature
regions did not get back to the state where it should be. Hence, does not compensate totally the shrinkage in length.
development of higher thermal strain is responsible for higher Bending distortion in a shaft and bore distortion in a gear are
diameter expansion when quenching is performed at higher significant manufacturing issues, and to maintain its correct
quench oil bath temperature. dimension after heat treatment is of utmost importance for an
automobile and off-highway industry. A shaft undergoes
3.3 Length Distortion straightening operation after carburizing, which is an additional
step in the manufacturing process chain. Often during straight-
Length distortion of a shaft was calculated according to
ening, the shaft cracks and this is again an additional issue to a
Fig. 1(a). The length of a shaft shrinks during carburizing and
heat treat engineer. A gear undergoes hard broaching to rectify
quenching operation. This happens because of mass conserva-
bore expansion or contraction and/or ovality. Transmission
tion, as diameter expands during the process. To understand the
shaft and gear are often made of same grade steel. One of the
mechanism of length distortion, the formation of the final phase
ways to mitigate distortion in a gear is to manufacture gear
fraction along the length of the shaft was considered. Two
from the ingot which has relatively lower hardenability in the
nodes—node B (near the central axis of the shaft and at
specification range, and manufacture shaft from the ingot which
maximum diameter) and node A (near the central axis and at
has relatively higher hardenability.
one edge)—were considered for investigation (Fig. 3).