Documente Academic
Documente Profesional
Documente Cultură
Version 2.0
Run
4010
Instrument
2910 MDSC
V4.3B
Module DSC Calibration
Sample LBMNC1v
Size
1.50000 mg
Method
Operator
Fede
Comment CLOSED
Version 2.0
Run
4010
Instrument
2910 MDSC
V4.3B
Module DSC Calibration
Sample LBMNC1v
Size
1.50000 mg
Method
Operator
Fede
Comment
Xcomment
Pan: Aluminum
Gas1: Argon
122
Text
LBMNC1 volumetrico
Exotherm
Down
Kcell 1.09000
Cpconst 1.0000
Calib 11.80
TempCal 2
pts
155.80 156.60, 417.60 419.73
BaselineCal
-0.4086 50121.30
IsoTrackTime
0.50
Thresholds
0.010 0.0010
Controls
Gas 1 Event Off Sampling 0.2 sec/pt
Nsig
6
Sig1
Time (min)
Sig2
Temperature (°C)
Sig3
Heat Flow (mW)
Sig4
Delta Q (Hz)
Sig5
Uncorrected Temperature (°C)
Sig6
Uncorrected Heat Flow (mW)
Date
19-Feb-13
Time
10:25
File
D:\TA\USER\FEDERICO\LBMNC1v.000
OrgFile D:\DSC\LBMNC1v.000
Gas2: None
0.0000000 21.68182 -0.8436684 50226.52 20.88182 -0.7740076
0.2395000 21.68124 -0.8393366 50226.10 20.88184 -0.7711453CLOSED
Version 2.0
Run
4010
Instrument
2910 MDSC
V4.3B
Module DSC Calibration
Sample LBMNC1v
Size
1.50000 mg
Method
Operator
Fede
Comment
Xcomment
Pan: Aluminum
Gas1: Argon
122
Text
LBMNC1 volumetrico
Exotherm
Down
Kcell 1.09000
Cpconst 1.0000
Calib 11.80
TempCal 2
pts
155.80 156.60, 417.60 419.73
BaselineCal
-0.4086 50121.30
IsoTrackTime
0.50
Thresholds
0.010 0.0010
Controls
Gas 1 Event Off Sampling 0.2 sec/pt
Nsig
6
Sig1
Time (min)
Sig2
Temperature (°C)
Sig3
Heat Flow (mW)
Sig4
Delta Q (Hz)
Sig5
Uncorrected Temperature (°C)
Sig6
Uncorrected Heat Flow (mW)
Date
19-Feb-13
Time
10:25
File
D:\TA\USER\FEDERICO\LBMNC1v.000
OrgFile D:\DSC\LBMNC1v.000
Gas2: None
0.0000000 21.68182 -0.8436684 50226.52 20.88182 -0.7740076
0.2395000 21.68124 -0.8393366 50226.10 20.88184 -0.7711453CLOSED
Version 2.0
Run
4010
Instrument
2910 MDSC
V4.3B
Module DSC Calibration
Sample LBMNC1v
Size
1.50000 mg
Method
Operator
Fede
Comment
Xcomment
Pan: Aluminum
Gas1: Argon
122
Text
LBMNC1 volumetrico
Exotherm
Down
Kcell 1.09000
Cpconst 1.0000
Calib 11.80
TempCal 2
pts
155.80 156.60, 417.60 419.73
BaselineCal
-0.4086 50121.30
IsoTrackTime
0.50
Thresholds
0.010 0.0010
Controls
Gas 1 Event Off Sampling 0.2 sec/pt
Nsig
6
Sig1
Time (min)
Sig2
Temperature (°C)
Sig3
Heat Flow (mW)
Sig4
Delta Q (Hz)
Sig5
Uncorrected Temperature (°C)
Sig6
Uncorrected Heat Flow (mW)
Date
19-Feb-13
Time
10:25
File
D:\TA\USER\FEDERICO\LBMNC1v.000
OrgFile D:\DSC\LBMNC1v.000
Gas2: None
0.0000000 21.68182 -0.8436684 50226.52 20.88182 -0.7740076
0.2395000 21.68124 -0.8393366 50226.10 20.88184 -0.7711453
Xcomment
Pan: Aluminum
Gas1: Argon
122
Text
LBMNC1 volumetrico
Exotherm
Down
Kcell 1.09000
Cpconst 1.0000
Calib 11.80
TempCal 2
pts
155.80 156.60, 417.60 419.73
BaselineCal
-0.4086 50121.30
IsoTrackTime
0.50
Thresholds
0.010 0.0010
Controls
Gas 1 Event Off Sampling 0.2 sec/pt
Nsig
6
Sig1
Time (min)
Sig2
Temperature (°C)
Sig3
Heat Flow (mW)
Sig4
Delta Q (Hz)
Sig5
Uncorrected Temperature (°C)
Sig6
Uncorrected Heat Flow (mW)
Date
19-Feb-13
Time
10:25
File
D:\TA\USER\FEDERICO\LBMNC1v.000
OrgFile D:\DSC\LBMNC1v.000
Gas2: None
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0.8503332 21.67706 -0.8327340 50225.06 20.87768 -0.7640686
1.184334 21.67456 -0.8283672 50224.36 20.87462 -0.7592976
1.518000 21.67274 -0.8217407 50223.64 20.87274 -0.7544474
1.851666 21.67157 -0.8166944 50222.86 20.87197 -0.7490938
2.185333 21.67180 -0.8096585 50222.03 20.87160 -0.7434751
2.318833 21.67113 -0.8090306 50221.66 20.87172 -0.7410105
2.652334 21.67345 -0.8019810 50220.89 20.87383 -0.7357632
2.985666 21.67554 -0.7969425 50220.22 20.87562 -0.7312050
3.319333 21.67992 -0.7916611 50219.56 20.87970 -0.7267798
3.652833 21.68396 -0.7865914 50218.82 20.88387 -0.7217182
3.986167 21.68816 -0.7818098 50218.17 20.88797 -0.7173461
4.319500 21.69428 -0.7767444 50217.47 20.89408 -0.7126030
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9.326500 21.79567 -0.7201950 50209.79 20.99548 -0.6608032
9.660168 21.80177 -0.7172522 50209.40 21.00195 -0.6581540
9.993834 21.80820 -0.7145163 50209.03 21.00862 -0.6556634
10.32767 21.81597 -0.7116252 50208.66 21.01548 -0.6531996
10.66117 21.82187 -0.7095918 50208.32 21.02147 -0.6509210
10.99450 21.82796 -0.7069936 50208.00 21.02812 -0.6488018
11.16133 21.83090 -0.7052806 50207.56 21.03304 -0.6458340
11.20800 21.84524 -0.6970239 50206.33 21.04766 -0.6374872
11.24133 21.86660 -0.6796484 50203.85 21.07015 -0.6207132
11.27150 21.89717 -0.6536759 50200.17 21.10222 -0.5958301
11.30150 21.94062 -0.6179516 50195.17 21.14756 -0.5620430
11.33816 22.01420 -0.5623360 50187.41 21.22316 -0.5096257
11.39816 22.17390 -0.4495241 50171.98 21.39082 -0.4053710
11.47484 22.45674 -0.2921225 50150.86 21.67627 -0.2628672
11.52500 22.68132 -0.1984377 50138.18 21.89672 -0.1774702
11.56834 22.88677 -0.1264071 50128.47 22.10430 -0.1121064
11.60834 23.08844 -.07078904 50121.00 22.30568 -.06195390
11.65500 23.33037 -.01823159 50113.92 22.54845 -.01463423
11.70500 23.59702 0.02375925 50108.27 22.81478 0.02301300
11.75850 23.88370 0.05383034 50104.20 23.10217 0.04987316
11.82516 24.24436 0.07512915 50101.28 23.46152 0.06865004
11.89184 24.60012 0.08334012 50100.10 23.81783 0.07565558
11.97533 25.03977 0.08414486 50099.86 24.25694 0.07611299
12.20883 26.24605 0.07140020 50100.78 25.45915 0.06655493
12.46566 27.54138 0.06850468 50100.59 26.75915 0.06423705
12.79950 29.22528 0.07644613 50099.12 28.44338 0.06956676
12.89284 29.69917 0.07642118 50098.67 28.91524 0.07129861
13.22617 31.39380 0.08491297 50097.03 30.61264 0.07777489
13.55967 33.10332 0.08829441 50095.97 32.31836 0.08027129
13.76300 34.14136 0.08759892 50095.36 33.35995 0.08158955
13.97316 35.22085 0.08935450 50095.02 34.43706 0.08088932
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