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brochure

In-line Oil in Water Analyser - Model OIW-EX100P and OIW-EX1000P

Advanced Sensors Ltd Oil in Water Analyser System known as the OIW-EX100P
or OIW-EX 1000P. The system is designed to monitor the residual hydrocarbon
content of pipelines carrying produced water at oil production facilities and
refineries etc. The OIW-EX100P uses laser radiation to energise the contents of
the process pipe with an incident optical wavelength. A sensitive tuned detector
at a different wavelength is then used to measure the stimulated fluorescence
value. This fluorescence value is used to determine the proportion of
hydrocarbons within the chamber.

Measuring technique:
The measurement technique incorporated in the Advanced Sensor’s monitors is laser-
induced fluorescence. The inline probe is a patented combined Optical and Ultrasonic
component.
The measurement probes combine two distinct technologies:
• Laser induced fluorescence for the oil in water measurement.
The laser emission is transmitted via optical fibre from the analyzer enclosure to and
through the probe. The light is then transmitted via the sapphire optical window
embedded at the front of the probe into the water in the process pipe. The
fluorescence from the water sample travels back through the sapphire window, along
In-line Oil In Water analyser model EX
the optical fibre to the analyzer enclosure to the optical detection system. OIW 100-P and OIW EX 1000-P
• Ultrasonic transduction which provides the automatic cleaning of the probe.
The sapphire window is kept clean by the ultrasonic cavitations created by the probe.
It is this feature that enables the analyzer to operate without the need of routine
maintenance.

Probe, umbilical cable and analyser enclosure:


The In-Line type analyser (The EX100-P and EX1000-P)has a measurement probe
attached to the analyser enclosure via an umbilical cable. The Probe can withstand
pressures in excess of 100 Bar. The analyser’s probe should be inserted into the water
line via a 2” flange interface. The analyser should be wired for mains and
communications and then powered up. The analyser will immediately perform
measurements.

Dual-stream / dual-probe:
Even two measurement probes can be connected to a single analyser. The EX100P is
designed for ease of installation. The EX100P unit is delivered complete, mounted on a
stand (316L stainless) and ready to go. Take the unit out of the delivery packaging, wire
the mains power, insert the probe and turn on.

Ex d/ATEX: Oil In Water (OIW) monitor schematic


The EX100P EX1000-P are EX d rated and do not require purged air.

Probes and installation location:


The lengths of the probes are not arbitrary; they must be calculated and manufactured
at specific lengths. The probes can be provided at lengths suitable for any specific
application, allowing the probes to be inserted into pipelines as small as 2” requiring
probe lengths of 0.75m and into tanks requiring probe lengths greater than 3m. The
probes must be positioned for optimum measurement detection whilst taking into
consideration the wavelength of the ultrasonic frequency so that the cleaning
performance is also optimised.

Clear full color screen in Ex d housing


In-line Oil in Water Analyser - Model OIW-EX100P and OIW-EX1000P

Models:
• OIW EX100-P: Fluorescence is measured via an optical filter and photo
multiplier tube (PMT), the optical filter selected depends on the wavelength
properties in the water;
• OIW EX1000P: Fluorescence is measured via an optical UV spectrometer. The
spectrometer takes the optical fingerprint of the oil, should the oiltype change,
the analyser will automatically detect the change and select the appropriate
calibration file to provide consistently accurate measurement. This feature is
unique to Advanced Sensors analysers.

Spectrometer
The in-built UV spectrometer (EX1000 only) scans the water every 10 minutes and
files the results for 10 years for future investigation. The spectrometer is of great
value when detailed analysis of water content is required. An installed unit was
periodically reporting higher OIW concentration results than the field laboratory
that used solvent extraction and IR detection. The spectrometer logs were
examined during this event, and the spectra indicated the presence in the water of
an interferent other than oil. Further tests were performed, and the substance
causing the anomaly was identified. This led to the selection of a new wavelength
range and an optical filter that was fitted to the PMT, thereby eliminating the
interference.

Whilst chemicals can be evaluated in the Advanced Sensors Laboratory and


isolated before the monitors are delivered, the in-built spectrometer facilitates the
evaluation and analysis of new chemicals or additives being introduced to the
process.

Operating dynamic range


The dynamic range of most OIW monitors is limited to 500 ppm or a maximum of
1000 ppm TPH. The standard EX100/1000 can operate up to 3000 ppm TPH
(Total Petroleum Hydrocarbons). The “EX1000Advance” has a direct fluorescent
dynamic range of 20000 ppm OIW without any extrapolation. In the figure (right),
the direct fluorescent curve for 0 to 30000 ppm OIW without any extrapolation.
After 20000 ppm, the instrument flat-lines. The flat-lining in itself is a new
development, traditionally as oil levels increase the fluorescence
flat-lines and then falls, this can confuse an instrument in believing the oil content
is falling when it is actually rising. The extended range monitor EX1000 Advance”
facilitates the monitoring the efficiency of separators and hydro-cyclones, providing
a greater insight to process dynamics.

Fluoresence scan / range

Screens, parameter Settings and Configuration and remote Access


In-line Oil in Water Analyser - Model OIW-EX100P and OIW-EX1000P

Sample flows continuously through the process Oil built up. Ultrasonics activated.
pipe in front of the probe Oil will contaminate the sapphire window The sapphire window starts to vibrate

Oil contamination and particles are removed Oil in water being measured by measuring the Analysed Oil concentration is presented on
from the sapphire window intensity of the fluorescence screen and outputs and stored

Features
The Advanced Sensors’ OIW monitors are continuous, on-line, self-cleaning UV fluorescence detection systems.

Advantages of this laser fluorescence system for monitoring OIW are many:
• Instead of the laser or light source having to pass across a pipe to a detector, the requirement to completely flow photons
through moving water is eliminated.
• With the Advanced Sensors probe design the light source and detector with the specially coated sapphire window detects all
Total Petroleum Hydrocarbons (TPH) or Oil and Grease (O&G) in process pipe.
• The range of the analysers are oil from 10ppb (parts per billion) to 20000 ppm (parts per million).
• The ultrasonic beam cleans the sapphire window. In the presence of “sticky” precipitates or from soapy emulsions,
ultrasonics maintains a clean window.
• The Advanced Sensors’ technology is able to cope with system upsets, well flow variations, and solids. The
homogenization mode is especially applicable to sour systems where oil coated iron sulphide solids may be present in
suspension or in emulsions.
• For each application of this technology, UV fluorescence signatures may be obtained so that the bandwidth is specific only
to dispersed oil. When chemical additives are present that overlap with the oil bandwidth, Advanced Sensors professionals
are able to remotely squeeze the bandwidth tighter to ensure that the output signal is focused on oil alone.
• The standard communication interfaces are 4-20mA, Ethernet and ADSL (2 wire Ethernet), wireless is available as an
option. The 4-20 mA is for connection to the Control room (DCS) and the Ethernet and ADSL is for connection to the
company’s intranet. The intranet/internet connection facilitates the connectivity to the instrument form other company
locations or the advanced sensors laboratory for further diagnostic and analysis support.
• Data logs. PPM measurements are stored every second in daily logs as excel files, the daily logs are stored for 10 year on
the instrument. The spectrometer’s scans are run every 10 minutes and excel logs are also stored for 10years on the
instrument. Software is provided to interrogate both data logs (LogView) and Spectrometer Logs (Span). Both LogView and
Span can be utilized remotely, the software will reach down to the Monitor and extract the selected filed for investigation.
• Alarm levels may be set for trending or operator attention to the water treatment and processing system.
• The unit can also manage dual probes / dual streams to the instrument.
• Water Composition: Our analyzer’s spectrometer monitors water composition and will generate alarms should the
composition change.
• Proof of Performance: Operationally our analyzers provide 100% customer satisfaction year on year with no cleaning or
maintenance.
In-line Oil in Water Analyser - Model OIW-EX100P and OIW-EX1000P

Analyser OIW EX 100-P / EX 1000-P


Analytical principle UV Fluorescence Class 3 industrial Laser; selective optical filter and photo multiplier de-
tector. Model EX 1000-P with real time spectrometer
Range 3000 ppm Standard ( 20000 ppm enhanced)
Accuracy +/- 1%
Repeatability 1%
Operating ambient temperature -15 ºC. to 80 ºC.
Operating conditions for sample No flow control or pressure regulation required
Sample flow (minimum / norm / maximum) 5 / 20 / 100 ltr/min
Sample temperature (minimum / maximum) 0 - 100 ºC.
Sample pressure (mini / maxi) 0 - 12 bar (0 -174 psi); Extended pressure range 0 - 200 bar ( 0 - 2900 psi)
Response time < 1 second
Cycle time Continuous
Weight Approx 79 Kg (enclosure plus measurement chamber & stand)
Footprint (W x D) 600 x 640 mm
It is recommended 500 mm be maintained at the front and rear of the unit for user access.
Type and Qty of signal 4-20 mA Galvanic isolation (free from earth) / 1
Interface 4-20 mA / Ethernet / RS232 & 2-wire ADSL (HART optional)
Power supply and consumption 110 or 230 VAC, 50 or 60 Hz / < 300W at maximum draw. ~ 60W in normal conditions.
Distance between probe and monitor Maximum 3 meter
Internal Data Logging >10 years
Tropicalized Yes
Electrical area classification certificate / N° ATEX Ex d II 2 G Ex d IIB T4
Standards EN61010-1:2001 Safety requirements for electrical equipment for measurement, control
and laboratory use
UL Class 1 Div 1
IMO Approval to MEPC 107(49)
US Coast Guard Type Approval
CRN’s for Canadian provinces
Enclosure rating Ingress Protection IP65
CALIBRATION Annual Inspection
Required Instrument Air Not required
Sample Conditioning System Integrated Ultrasonic Transducer
Process pipe connection 2" 316L 150lb RF ANSI Standard. / see drawings
Wetted parts Our analyzers wetted parts are 316l as standard and optionally 22CR and 25CR (Chrome
Duplex).
Fitted with a sample take off for lab. / location. No
Operational Notes Self cleaning
In-line
Independent of turbidity or bubbles
Viewing window integrated in probe
Network multiple units to Control Centre
Model EX 1000-P; Spectrometer Specifications Integration time: 1 ms -10 seconds
Measuring range: 475 - 1025 nm
Dynamic range: 2 x 108
Sensitivity: 3 x 10-17 watts / 1-second integration
Signal/noise / Dark noise 250:1 (at full signal) / 50 (RMS)
Resolution: 1,5 nm
Stray light: < 0,05% at 600 nm
In-line Oil in Water Analyser - Model OIW-EX100P and OIW-EX1000P

Specifications are subject to change by manufacturer or ODS without notice due to modifications or improvements revision: 2011-04

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